#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:23:45 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180859 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/90/2019011.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2019011_Fobs loop_ _publ_author_name 'Scholz, Stefan' 'Vitze, Hannes' 'Bolte, Michael' 'Lerner, Hans-Wolfram' _publ_section_title ; An approach to creating novel anions: silylated triel compounds with --CH~2~-- and --O-- linkers, [InCl~2~{O(HO)Si(t-Bu)~2~}]~2~ and Li[B(CH~2~SiMe~3~)~4~] ; _journal_coeditor_code WQ3030 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 569 _journal_page_last 572 _journal_volume 69 _journal_year 2013 _space_group_IT_number 7 _symmetry_space_group_name_Hall 'P -2yac' _symmetry_space_group_name_H-M 'P 1 n 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.153 _cell_angle_gamma 90.000 _cell_length_a 10.5661 _cell_length_b 11.7334 _cell_length_c 18.1342 _exptl_crystal_F_000 728.00 _reflns_d_resolution_high 0.8203 _cod_data_source_file wq3030IIsup3.hkl _cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' wa626 in Pn' _shelx_refln_list_code 4 _shelx_f_calc_maximum 204.60 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 -22 11.03 45.79 60.40 o -3 0 -21 20.32 -6.05 43.61 o -1 0 -21 3.84 28.28 37.31 o 1 0 -21 125.39 109.65 49.49 o 3 0 -21 132.49 80.80 60.62 o -3 1 -21 2.14 6.60 28.24 o -2 1 -21 0.85 -4.11 26.93 o -1 1 -21 1.11 -5.32 26.35 o 0 1 -21 28.69 64.06 29.36 o 1 1 -21 5.53 -28.89 32.54 o 2 1 -21 7.11 17.26 28.01 o 3 1 -21 34.87 -32.38 32.38 o 4 1 -21 8.16 -3.83 53.84 o -2 2 -21 9.16 37.39 27.02 o -1 2 -21 3.63 30.57 26.88 o 0 2 -21 119.42 123.49 28.87 o 1 2 -21 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