#------------------------------------------------------------------------------ #$Date: 2013-08-28 13:42:33 +0300 (Wed, 28 Aug 2013) $ #$Revision: 88054 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/90/2019020.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2019020_Fobs loop_ _publ_author_name 'Zhang, Qian' 'Liu, Jie' 'Lu, Jing' 'Gong, Shu-Wen' _publ_section_title ; Two polyoxometallate-based supramolecular compounds influenced by the ratio between the polyoxometallate anion and organic cation ; _journal_coeditor_code YF3031 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 588 _journal_page_last 593 _journal_volume 69 _journal_year 2013 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 102.194 _cell_angle_beta 98.184 _cell_angle_gamma 115.998 _cell_length_a 11.2350 _cell_length_b 11.7211 _cell_length_c 11.8459 _exptl_crystal_F_000 1065.00 _reflns_d_resolution_high 0.8403 _[local]_cod_data_source_file yf3031IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' 100405c in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 412.49 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 38967.22 38575.48 321.25 o 2 0 0 7776.16 8080.10 97.88 o 3 0 0 616.92 531.52 50.13 o 4 0 0 933.54 1146.01 44.53 o 5 0 0 1192.43 1054.06 48.95 o 6 0 0 63.85 54.81 33.95 o 7 0 0 1648.17 1487.92 106.89 o 8 0 0 6754.89 6780.17 243.26 o 9 0 0 1542.17 1770.60 137.53 o 10 0 0 1695.51 1485.77 135.80 o 11 0 0 3.41 -11.08 62.29 o -12 1 0 138.48 221.97 91.64 o -11 1 0 211.96 131.49 74.23 o -10 1 0 1122.79 983.85 109.76 o -9 1 0 94.25 74.09 51.07 o -8 1 0 652.32 491.42 86.03 o -7 1 0 1535.26 1306.66 97.82 o 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