#------------------------------------------------------------------------------ #$Date: 2013-08-28 13:42:33 +0300 (Wed, 28 Aug 2013) $ #$Revision: 88054 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/90/2019027.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2019027_Fobs loop_ _publ_author_name 'Kaupang, \%Asmund' 'G\"orbitz, Carl Henrik' 'Bonge-Hansen, Tore' _publ_section_title ; A solid-state oxidation of 1,1,3,3-tetramethylguanidinium 4-methylbenzenesulfinate to 1,1,3,3-tetramethylguanidinium 4-methylbenzenesulfonate ; _journal_coeditor_code EG3125 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 778 _journal_page_last 780 _journal_volume 69 _journal_year 2013 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.115 _cell_angle_gamma 90.000 _cell_length_a 11.0959 _cell_length_b 7.4038 _cell_length_c 17.1944 _exptl_crystal_F_000 584.00 _reflns_d_resolution_high 0.7508 _[local]_cod_data_source_file eg3125Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' AAK220MeCN-X in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 156.12 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 444.21 451.47 4.46 o 2 0 0 3238.53 3340.89 41.20 o 3 0 0 2717.53 2966.96 27.56 o 4 0 0 447.49 515.94 5.62 o 5 0 0 16.42 15.53 2.72 o 6 0 0 181.61 202.35 3.11 o 7 0 0 464.84 446.69 5.61 o 8 0 0 1.12 -0.89 0.91 o 9 0 0 1556.46 1461.11 15.42 o 10 0 0 516.40 502.92 6.81 o 11 0 0 153.37 153.69 3.59 o 12 0 0 286.81 275.08 5.09 o 13 0 0 740.72 776.13 8.87 o 14 0 0 231.47 261.96 5.36 o 1 1 0 488.61 541.48 4.77 o 2 1 0 202.35 232.50 1.75 o 3 1 0 1000.88 1054.50 7.30 o 4 1 0 9.72 13.99 0.57 o 5 1 0 2806.12 2976.85 19.90 o 6 1 0 5.35 7.77 0.63 o 7 1 0 13.65 13.31 0.79 o 8 1 0 897.71 849.80 9.47 o 9 1 0 662.08 636.07 5.58 o 10 1 0 9.13 9.18 0.95 o 11 1 0 81.41 81.91 1.95 o 12 1 0 1.23 1.55 1.02 o 13 1 0 1.09 -0.92 0.98 o 14 1 0 45.98 53.76 1.78 o 0 2 0 6704.79 6987.12 78.93 o 1 2 0 314.58 308.41 2.74 o 2 2 0 4906.57 5010.81 43.98 o 3 2 0 1317.98 1303.10 13.54 o 4 2 0 3160.03 3182.60 21.10 o 5 2 0 7724.02 7773.05 54.97 o 6 2 0 0.41 2.07 0.55 o 7 2 0 605.08 591.84 5.04 o 8 2 0 1047.93 1024.23 7.94 o 9 2 0 802.77 714.56 6.11 o 10 2 0 2.65 3.81 0.82 o 11 2 0 35.55 40.90 1.53 o 12 2 0 250.27 250.44 3.74 o 13 2 0 157.51 159.92 3.16 o 14 2 0 8.16 8.00 1.50 o 1 3 0 155.14 162.09 1.85 o 2 3 0 85.89 114.38 2.33 o 3 3 0 42.89 43.27 0.90 o 4 3 0 479.50 572.61 4.52 o 5 3 0 83.63 87.21 1.44 o 6 3 0 392.46 392.73 3.65 o 7 3 0 71.28 65.59 1.49 o 8 3 0 616.67 595.40 5.81 o 9 3 0 323.83 320.27 3.96 o 10 3 0 7.02 14.72 1.20 o 11 3 0 5.68 7.58 1.16 o 12 3 0 137.99 144.54 2.92 o 13 3 0 1.39 -0.27 1.25 o 0 4 0 7587.24 7898.48 138.98 o 1 4 0 1294.67 1319.80 10.20 o 2 4 0 493.85 510.59 5.94 o 3 4 0 2898.79 2921.99 19.81 o 4 4 0 1423.94 1494.98 11.74 o 5 4 0 551.92 518.30 4.94 o 6 4 0 11.18 13.45 0.99 o 7 4 0 407.44 385.19 4.69 o 8 4 0 62.05 59.16 1.72 o 9 4 0 95.44 86.66 2.07 o 10 4 0 648.75 637.89 7.40 o 11 4 0 27.61 27.82 2.71 o 12 4 0 361.87 370.39 8.62 o 13 4 0 9.59 6.26 3.00 o 1 5 0 147.75 153.17 2.52 o 2 5 0 96.53 88.55 1.68 o 3 5 0 69.04 86.01 1.75 o 4 5 0 158.44 146.92 2.31 o 5 5 0 101.64 110.06 2.10 o 6 5 0 107.51 105.54 3.13 o 7 5 0 1.95 1.51 0.88 o 8 5 0 555.81 529.82 5.59 o 9 5 0 452.93 463.68 5.90 o 10 5 0 13.05 13.87 1.48 o 11 5 0 140.75 141.17 5.36 o 12 5 0 60.35 60.76 2.64 o 0 6 0 876.09 857.13 12.00 o 1 6 0 178.16 182.00 2.96 o 2 6 0 520.80 498.05 5.68 o 3 6 0 328.21 324.98 4.30 o 4 6 0 284.01 270.43 3.86 o 5 6 0 1624.96 1604.20 17.41 o 6 6 0 1.48 2.85 0.94 o 7 6 0 98.71 103.63 2.25 o 8 6 0 74.85 76.61 2.38 o 9 6 0 5.35 3.31 1.61 o 10 6 0 187.96 182.46 4.50 o 11 6 0 42.47 44.22 2.74 o 1 7 0 16.06 19.82 1.60 o 2 7 0 75.66 78.93 2.18 o 3 7 0 93.75 84.33 2.30 o 4 7 0 501.86 490.44 9.91 o 5 7 0 4.01 3.44 1.31 o 6 7 0 113.90 114.38 3.19 o 7 7 0 39.68 35.71 2.77 o 8 7 0 66.74 73.66 3.84 o 9 7 0 36.55 40.54 5.25 o 0 8 0 5.58 6.64 2.13 o 1 8 0 42.05 42.88 2.36 o 2 8 0 155.59 147.96 3.60 o 3 8 0 42.83 45.80 2.23 o 4 8 0 477.29 480.83 7.08 o 5 8 0 328.72 335.30 11.01 o 6 8 0 134.62 142.45 4.92 o 7 8 0 320.88 318.62 8.88 o 8 8 0 100.35 101.59 7.26 o 1 9 0 134.73 135.04 4.25 o 2 9 0 56.54 61.85 2.70 o 3 9 0 19.07 23.66 2.58 o 4 9 0 178.00 184.05 7.01 o 5 9 0 276.20 274.94 6.87 o -14 1 1 64.97 67.56 2.09 o -13 1 1 340.89 357.94 4.04 o -12 1 1 176.76 167.12 2.57 o -11 1 1 730.44 714.49 6.44 o -10 1 1 717.08 688.73 5.63 o -9 1 1 397.66 360.06 3.71 o -8 1 1 4131.85 4005.68 26.95 o -7 1 1 63.84 60.13 1.52 o -6 1 1 1701.43 1783.45 12.42 o -5 1 1 2676.78 2565.63 18.68 o -4 1 1 0.91 1.51 0.42 o -3 1 1 1770.12 1703.79 10.62 o -2 1 1 2072.93 1991.61 13.15 o -1 1 1 604.84 620.29 4.70 o 0 1 1 456.52 553.95 4.30 o 1 1 1 12672.59 12286.87 92.50 o 2 1 1 2065.60 2097.37 13.89 o 3 1 1 5291.33 5413.46 38.37 o 4 1 1 83.50 60.15 1.04 o 5 1 1 6859.14 7048.47 45.97 o 6 1 1 114.48 90.16 2.09 o 7 1 1 1704.14 1603.54 14.65 o 8 1 1 244.28 283.61 3.09 o 9 1 1 157.77 146.25 2.24 o 10 1 1 301.90 321.04 3.61 o 11 1 1 98.01 97.33 2.06 o 12 1 1 1612.05 1576.72 12.24 o 13 1 1 131.62 129.78 2.62 o 14 1 1 300.36 307.62 4.16 o -14 2 1 68.90 75.60 3.30 o -13 2 1 18.32 17.67 1.35 o -12 2 1 22.66 21.67 1.37 o -11 2 1 8.94 10.67 1.23 o -10 2 1 96.35 97.75 2.01 o -9 2 1 2.54 4.01 0.90 o -8 2 1 0.00 -0.42 0.69 o -7 2 1 3.40 4.89 0.67 o -6 2 1 7.68 7.80 0.73 o -5 2 1 88.13 89.67 1.40 o -4 2 1 597.91 713.89 5.32 o -3 2 1 72.08 83.27 1.32 o -2 2 1 2535.14 2447.81 21.30 o -1 2 1 4218.46 4375.10 38.66 o 0 2 1 9302.43 9661.64 123.09 o 1 2 1 410.81 464.06 4.30 o 2 2 1 781.78 826.83 6.43 o 3 2 1 33.66 44.72 0.89 o 4 2 1 602.49 590.56 4.51 o 5 2 1 72.69 69.17 1.26 o 6 2 1 52.93 57.74 1.26 o 7 2 1 15.63 19.78 0.92 o 8 2 1 5.24 4.82 0.98 o 9 2 1 269.82 280.34 3.23 o 10 2 1 43.90 47.06 1.52 o 11 2 1 113.21 117.05 2.25 o 12 2 1 0.43 -0.97 0.97 o 13 2 1 336.12 368.15 4.90 o 14 2 1 16.58 20.83 1.98 o -13 3 1 71.87 75.97 2.48 o -12 3 1 2.69 4.31 1.05 o -11 3 1 715.34 706.08 7.14 o -10 3 1 1082.26 1093.24 9.69 o -9 3 1 41.61 43.14 1.84 o -8 3 1 1406.01 1346.21 11.12 o -7 3 1 536.29 510.66 4.53 o -6 3 1 708.52 682.66 5.50 o -5 3 1 3214.99 3138.05 21.06 o -4 3 1 219.01 224.57 3.10 o -3 3 1 1292.79 1213.04 8.52 o -2 3 1 5.43 4.73 0.69 o -1 3 1 364.04 346.86 4.98 o 0 3 1 285.85 233.18 2.30 o 1 3 1 1378.10 1439.87 12.16 o 2 3 1 810.70 751.70 8.46 o 3 3 1 10.93 11.60 0.69 o 4 3 1 1869.36 1848.76 14.21 o 5 3 1 59.99 41.21 0.99 o 6 3 1 18.06 16.51 0.81 o 7 3 1 2900.62 2915.20 20.00 o 8 3 1 2546.01 2535.10 19.48 o 9 3 1 1348.29 1361.87 12.95 o 10 3 1 233.35 241.37 3.45 o 11 3 1 10.29 10.00 1.78 o 12 3 1 476.62 465.73 6.22 o 13 3 1 64.74 60.12 2.43 o 14 3 1 103.83 108.10 5.50 o -13 4 1 2.02 2.75 2.75 o -12 4 1 15.69 15.27 1.71 o -11 4 1 168.59 167.36 3.53 o -10 4 1 34.69 36.86 1.64 o -9 4 1 209.78 190.35 4.81 o -8 4 1 817.79 787.72 7.38 o -7 4 1 1129.20 1070.69 9.13 o -6 4 1 350.94 354.41 4.82 o -5 4 1 6.84 4.51 0.77 o -4 4 1 431.01 450.43 4.34 o -3 4 1 702.42 763.79 6.79 o -2 4 1 298.80 362.88 3.55 o -1 4 1 129.70 166.83 2.06 o 0 4 1 2.81 5.12 0.48 o 1 4 1 177.37 195.14 3.54 o 2 4 1 256.60 308.86 3.58 o 3 4 1 1535.12 1619.24 12.47 o 4 4 1 187.48 183.64 3.10 o 5 4 1 14.96 12.67 0.94 o 6 4 1 7.71 3.75 0.93 o 7 4 1 4.56 4.08 0.90 o 8 4 1 22.68 20.30 1.21 o 9 4 1 388.73 364.19 4.36 o 10 4 1 22.31 20.73 2.24 o 11 4 1 217.10 218.67 4.00 o 12 4 1 24.54 29.11 2.08 o -12 5 1 226.87 238.88 5.42 o -11 5 1 155.43 148.66 3.51 o -10 5 1 307.81 322.37 5.81 o -9 5 1 71.20 75.23 3.43 o -8 5 1 393.61 378.11 4.44 o -7 5 1 0.32 -0.50 0.85 o -6 5 1 812.37 795.07 7.26 o -5 5 1 659.13 677.06 6.26 o -4 5 1 582.87 588.53 5.52 o -3 5 1 507.41 475.51 4.60 o -2 5 1 32.63 26.09 1.00 o -1 5 1 286.02 265.82 3.46 o 0 5 1 933.21 874.87 8.29 o 1 5 1 184.36 173.17 2.68 o 2 5 1 1768.42 1752.69 13.53 o 3 5 1 791.33 788.52 6.83 o 4 5 1 514.99 532.17 5.15 o 5 5 1 156.79 130.34 2.25 o 6 5 1 5.84 5.29 0.93 o 7 5 1 326.07 318.18 4.38 o 8 5 1 48.80 51.25 2.31 o 9 5 1 22.21 28.41 1.69 o 10 5 1 208.49 200.45 3.75 o 11 5 1 173.25 166.74 3.59 o 12 5 1 486.32 501.35 10.22 o -11 6 1 8.12 7.21 1.83 o -10 6 1 89.93 89.69 2.89 o -9 6 1 0.64 -1.16 1.16 o -8 6 1 0.46 -1.07 1.07 o -7 6 1 138.65 131.80 2.31 o -6 6 1 0.24 -0.64 0.69 o -5 6 1 60.92 50.22 1.86 o -4 6 1 135.80 150.99 2.82 o -3 6 1 270.12 248.60 3.60 o -2 6 1 374.25 369.01 4.58 o -1 6 1 1091.57 1151.09 11.52 o 0 6 1 641.50 644.56 6.80 o 1 6 1 194.82 197.41 3.12 o 2 6 1 42.58 49.30 1.77 o 3 6 1 59.30 60.30 1.93 o 4 6 1 0.18 -0.35 0.88 o 5 6 1 27.62 23.12 1.65 o 6 6 1 8.19 9.68 1.26 o 7 6 1 23.77 22.60 1.32 o 8 6 1 61.87 60.23 2.17 o 9 6 1 6.84 6.39 1.37 o 10 6 1 50.87 60.18 2.92 o 11 6 1 67.51 60.59 3.04 o -9 7 1 44.53 48.97 3.42 o -8 7 1 9.39 12.24 2.34 o -7 7 1 1.70 2.87 1.92 o -6 7 1 6.69 7.71 3.75 o -5 7 1 276.80 286.69 4.32 o -4 7 1 39.72 35.14 2.46 o -3 7 1 928.52 886.04 11.81 o -2 7 1 73.06 69.29 2.10 o -1 7 1 451.70 443.19 5.43 o 0 7 1 199.11 174.70 3.12 o 1 7 1 25.94 21.41 1.88 o 2 7 1 186.06 189.89 3.28 o 3 7 1 6.44 5.40 1.62 o 4 7 1 85.39 85.88 2.78 o 5 7 1 15.04 16.39 2.27 o 6 7 1 87.96 87.77 2.92 o 7 7 1 414.59 430.68 6.67 o 8 7 1 216.25 232.35 4.80 o 9 7 1 76.27 73.86 3.91 o -8 8 1 83.40 98.84 7.26 o -7 8 1 254.19 271.21 11.51 o -6 8 1 119.15 130.19 4.74 o -5 8 1 130.55 132.16 4.56 o -4 8 1 118.65 138.03 4.56 o -3 8 1 45.91 38.09 2.09 o -2 8 1 79.09 72.09 2.32 o -1 8 1 13.09 11.13 1.29 o 0 8 1 11.50 15.57 1.52 o 1 8 1 155.52 172.49 3.83 o 2 8 1 4.63 6.98 1.49 o 3 8 1 177.88 194.05 4.10 o 4 8 1 273.20 292.88 5.21 o 5 8 1 127.29 121.20 3.46 o 6 8 1 65.04 61.40 2.70 o 7 8 1 80.69 84.43 4.20 o 8 8 1 48.48 53.80 5.50 o -5 9 1 75.26 87.43 4.13 o -4 9 1 65.45 61.96 3.60 o -3 9 1 204.43 224.20 8.01 o -2 9 1 215.95 219.70 7.76 o -1 9 1 142.97 134.55 4.16 o 0 9 1 58.45 59.56 3.01 o 1 9 1 25.38 25.96 1.99 o 2 9 1 8.62 8.59 1.55 o 3 9 1 72.79 75.02 2.90 o 4 9 1 112.73 114.45 3.49 o 5 9 1 39.34 32.17 3.00 o -14 0 2 588.56 594.72 8.83 o -13 0 2 600.71 606.54 8.66 o -12 0 2 65.84 70.52 2.76 o -11 0 2 459.34 441.71 6.56 o -10 0 2 383.24 374.37 4.92 o -9 0 2 809.61 779.32 8.00 o -8 0 2 838.32 724.36 12.42 o -7 0 2 180.56 191.56 3.20 o -6 0 2 385.82 404.33 4.98 o -5 0 2 17.74 23.80 1.10 o -4 0 2 4643.49 4590.63 36.92 o -3 0 2 17864.64 17458.35 191.30 o -2 0 2 11229.72 10781.77 137.55 o -1 0 2 4835.33 5148.12 60.29 o 0 0 2 2119.22 2213.99 36.03 o 1 0 2 670.93 584.86 8.06 o 2 0 2 5489.01 5825.44 203.93 o 3 0 2 974.07 875.98 8.69 o 4 0 2 3831.96 3706.76 34.48 o 5 0 2 1450.13 1582.82 15.51 o 6 0 2 3497.61 3631.67 34.25 o 7 0 2 2910.71 2939.44 28.34 o 8 0 2 54.29 49.01 2.38 o 9 0 2 940.23 942.37 12.79 o 10 0 2 40.36 61.71 2.35 o 11 0 2 396.13 379.98 5.91 o 12 0 2 18.41 22.69 1.91 o 13 0 2 982.43 1042.66 12.73 o 14 0 2 510.23 485.62 7.65 o -14 1 2 251.48 262.62 4.28 o -13 1 2 0.25 -0.88 0.88 o -12 1 2 69.78 66.91 1.87 o -11 1 2 0.20 0.61 0.77 o -10 1 2 216.04 218.53 2.69 o -9 1 2 70.70 62.97 1.60 o -8 1 2 182.90 170.34 2.34 o -7 1 2 21.69 22.37 0.92 o -6 1 2 6.01 2.51 0.71 o -5 1 2 35.69 38.89 1.01 o -4 1 2 257.80 277.39 2.45 o -3 1 2 238.92 209.08 1.89 o -2 1 2 1346.30 1317.86 10.05 o -1 1 2 616.00 641.92 6.80 o 0 1 2 3488.44 3684.20 29.17 o 1 1 2 306.80 306.23 2.50 o 2 1 2 290.12 259.57 2.12 o 3 1 2 1624.65 1640.37 11.66 o 4 1 2 307.97 341.94 2.90 o 5 1 2 293.25 311.70 2.83 o 6 1 2 23.48 25.57 0.85 o 7 1 2 241.79 268.34 2.83 o 8 1 2 386.73 380.37 3.77 o 9 1 2 140.43 139.52 2.56 o 10 1 2 64.81 52.65 1.61 o 11 1 2 43.64 44.40 1.52 o 12 1 2 34.25 35.28 1.52 o 13 1 2 32.72 34.52 1.59 o 14 1 2 47.21 59.83 2.21 o -14 2 2 13.73 12.66 3.13 o -13 2 2 81.54 90.28 2.92 o -12 2 2 69.93 78.16 2.23 o -11 2 2 128.77 133.65 2.30 o -10 2 2 56.61 52.99 1.46 o -9 2 2 1695.82 1681.84 12.40 o -8 2 2 508.89 502.16 4.57 o -7 2 2 98.81 93.16 1.66 o -6 2 2 584.47 541.39 4.52 o -5 2 2 1187.62 1194.40 8.54 o -4 2 2 99.02 131.07 1.53 o -3 2 2 4837.67 4934.53 32.23 o -2 2 2 3474.51 3826.27 25.07 o -1 2 2 83.29 118.17 1.24 o 0 2 2 10443.93 11012.62 87.00 o 1 2 2 11088.87 10872.48 70.83 o 2 2 2 5643.39 5575.32 45.69 o 3 2 2 82.60 91.79 1.79 o 4 2 2 4265.19 4345.91 28.56 o 5 2 2 3.79 2.82 0.55 o 6 2 2 1184.50 1141.00 8.37 o 7 2 2 932.24 875.72 6.84 o 8 2 2 831.73 842.61 6.81 o 9 2 2 1417.81 1397.02 10.54 o 10 2 2 254.89 256.71 3.26 o 11 2 2 463.50 444.78 5.15 o 12 2 2 731.12 727.14 10.53 o 13 2 2 22.14 19.16 1.70 o 14 2 2 556.41 606.05 10.90 o -14 3 2 46.81 51.05 5.00 o -13 3 2 193.68 213.40 4.27 o -12 3 2 35.95 37.81 2.05 o -11 3 2 1.22 -0.56 1.03 o -10 3 2 27.00 24.22 1.27 o -9 3 2 94.41 92.27 2.35 o -8 3 2 3.35 4.27 0.94 o -7 3 2 48.09 40.84 1.22 o -6 3 2 0.49 1.88 0.62 o -5 3 2 685.94 646.12 5.11 o -4 3 2 1.53 -0.48 0.48 o -3 3 2 897.25 830.59 6.05 o -2 3 2 89.70 94.78 1.21 o -1 3 2 134.16 155.45 1.98 o 0 3 2 225.51 228.11 2.06 o 1 3 2 415.92 509.96 4.86 o 2 3 2 13.87 19.92 1.24 o 3 3 2 25.53 41.79 1.13 o 4 3 2 17.25 16.16 0.69 o 5 3 2 769.86 767.21 5.44 o 6 3 2 277.38 273.86 2.83 o 7 3 2 36.88 47.44 1.35 o 8 3 2 937.26 882.10 9.64 o 9 3 2 91.96 77.78 1.98 o 10 3 2 25.00 20.92 1.31 o 11 3 2 31.79 32.79 1.82 o 12 3 2 51.66 49.99 2.17 o 13 3 2 2.17 1.83 1.52 o -13 4 2 78.99 82.32 5.50 o -12 4 2 0.02 0.05 1.26 o -11 4 2 55.84 53.08 3.18 o -10 4 2 0.81 -0.65 1.03 o -9 4 2 175.38 170.48 2.63 o -8 4 2 191.55 187.30 3.32 o -7 4 2 239.06 229.70 3.08 o -6 4 2 0.37 0.95 0.78 o -5 4 2 972.26 1064.05 8.80 o -4 4 2 1539.81 1589.52 14.48 o -3 4 2 2033.28 2097.58 14.45 o -2 4 2 1627.48 1736.18 13.18 o -1 4 2 882.60 844.29 6.85 o 0 4 2 674.66 686.92 5.69 o 1 4 2 120.82 103.82 1.84 o 2 4 2 695.97 644.71 5.53 o 3 4 2 17.57 19.91 0.90 o 4 4 2 2055.47 2047.97 17.21 o 5 4 2 334.34 335.09 3.67 o 6 4 2 1635.24 1562.56 11.28 o 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