#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:23:45 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180859 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/90/2019035.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2019035_Fobs loop_ _publ_author_name 'Dawe, Louise Nicole' 'Penney, Lisa' 'Black, Daniel A.' 'Miller, David O.' 'Lucas, C. Robert' _publ_section_title ; cis-Dichlorido(3,6,9-trithiabicyclo[9.3.1]pentadecane-\k^2^S^3^,S^6^)palladium(II) acetonitrile 0.8-solvate ; _journal_coeditor_code FN3138 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 727 _journal_page_last 729 _journal_volume 69 _journal_year 2013 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 24.9056 _cell_length_b 18.1436 _cell_length_c 8.3284 _exptl_crystal_F_000 1916.80 _reflns_d_resolution_high 0.7965 _cod_data_source_file fn3138Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C12H22Cl2PdS3/DATE 03-07-13,11:52:37' _shelx_refln_list_code 4 _shelx_f_calc_maximum 806.01 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, z' 'x, -y+1/2, z+1/2' '-x+1/2, -y, z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, -z' '-x, y-1/2, -z-1/2' 'x-1/2, y, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 440.20 591.04 52.13 o 6 0 0 649648.88 540832.25 5658.55 o 8 0 0 268503.62 264515.91 2974.04 o 10 0 0 32006.68 33101.32 652.47 o 12 0 0 143445.77 149990.08 1975.51 o 14 0 0 63408.20 65168.88 1139.00 o 16 0 0 50596.85 51779.60 1043.80 o 18 0 0 12578.61 12977.14 550.41 o 20 0 0 16670.01 16710.84 635.82 o 22 0 0 20301.38 19867.21 748.40 o 24 0 0 54.10 78.56 255.26 o 26 0 0 4841.75 4842.11 468.91 o 28 0 0 5764.85 6047.68 551.88 o 30 0 0 79.86 -78.81 330.15 o 4 1 0 6083.90 5759.14 173.27 o 6 1 0 8572.95 8899.83 261.87 o 8 1 0 599.75 653.45 62.16 o 10 1 0 16928.14 17971.72 461.82 o 12 1 0 3655.96 3587.83 249.88 o 14 1 0 9343.15 9666.84 400.14 o 16 1 0 541.58 649.77 67.79 o 18 1 0 1868.98 2015.16 162.75 o 20 1 0 3923.97 3555.53 350.46 o 22 1 0 2897.62 2832.33 274.35 o 24 1 0 502.11 496.57 89.08 o 26 1 0 76.08 129.71 281.45 o 28 1 0 1262.82 1309.34 124.57 o 30 1 0 1.63 159.32 363.68 o 2 2 0 54028.22 53102.15 645.61 o 4 2 0 3488.49 3591.02 158.34 o 6 2 0 217879.78 214837.86 2396.21 o 8 2 0 101312.27 99469.17 1299.31 o 10 2 0 16674.36 17722.82 459.37 o 12 2 0 85967.12 85265.89 1290.01 o 14 2 0 59245.46 57803.29 1046.49 o 16 2 0 13433.28 13781.59 497.06 o 18 2 0 13332.64 12905.68 542.34 o 20 2 0 18783.92 19141.56 703.13 o 22 2 0 5172.82 5675.92 474.05 o 24 2 0 347.97 119.92 224.67 o 26 2 0 5599.52 6303.92 520.80 o 28 2 0 4417.02 4651.46 349.48 o 30 2 0 17.69 -225.65 225.65 o 2 3 0 8513.06 9770.61 222.95 o 4 3 0 84444.09 90608.48 1103.27 o 6 3 0 30782.93 33164.95 556.29 o 8 3 0 38.30 25.45 141.21 o 10 3 0 2368.43 2372.23 196.03 o 12 3 0 34690.92 35614.27 732.50 o 14 3 0 5759.31 6106.66 336.76 o 16 3 0 1797.35 1834.30 142.68 o 18 3 0 18917.80 19806.02 655.16 o 20 3 0 4993.11 4865.11 420.46 o 22 3 0 2598.27 2550.15 208.03 o 24 3 0 3469.65 3272.37 277.29 o 26 3 0 717.87 632.89 108.91 o 28 3 0 2939.74 3354.11 333.33 o 30 3 0 574.71 435.88 119.19 o 0 4 0 16308.41 18078.92 338.23 o 2 4 0 9747.97 10138.20 258.20 o 4 4 0 2447.03 2591.51 167.15 o 6 4 0 26946.01 29545.30 536.71 o 8 4 0 174.80 202.15 46.26 o 10 4 0 8346.50 8616.67 341.16 o 12 4 0 8341.50 8791.17 364.66 o 14 4 0 10269.93 9826.16 424.37 o 16 4 0 771.05 604.01 72.20 o 18 4 0 7404.24 6713.61 443.46 o 20 4 0 11881.55 11970.79 575.62 o 22 4 0 1549.44 1479.43 148.07 o 24 4 0 917.41 891.33 103.77 o 26 4 0 6649.74 6262.31 534.75 o 28 4 0 1985.15 1837.72 174.74 o 30 4 0 481.06 435.88 120.17 o 2 5 0 17065.77 19291.34 386.68 o 4 5 0 3309.23 4199.19 201.66 o 6 5 0 3159.03 3039.87 197.99 o 8 5 0 3555.16 3699.43 222.71 o 10 5 0 11.56 -167.64 167.64 o 12 5 0 3627.69 3694.78 271.66 o 14 5 0 586.32 535.48 66.08 o 16 5 0 2708.42 2744.96 203.13 o 18 5 0 6586.09 6640.68 420.46 o 20 5 0 689.64 770.43 87.86 o 22 5 0 221.21 342.88 84.92 o 24 5 0 5927.64 5468.63 511.01 o 26 5 0 1627.67 1500.72 150.76 o 28 5 0 353.96 121.14 336.76 o 30 5 0 2796.75 2454.46 223.69 o 0 6 0 46642.39 50571.58 756.97 o 2 6 0 9995.53 10033.46 300.05 o 4 6 0 4591.47 4711.42 231.77 o 6 6 0 7637.82 8773.06 302.00 o 8 6 0 2388.57 2377.61 212.68 o 10 6 0 1572.44 1785.35 151.98 o 12 6 0 3870.70 3635.80 294.17 o 14 6 0 6866.45 6464.47 346.55 o 16 6 0 4314.13 4114.26 324.77 o 18 6 0 10639.88 11253.22 536.22 o 20 6 0 5266.74 4978.18 401.61 o 22 6 0 14.00 -101.81 272.88 o 24 6 0 701.39 544.05 106.95 o 26 6 0 385.56 -46.01 336.27 o 28 6 0 144.79 297.84 112.58 o 30 6 0 1382.23 1305.67 147.09 o 2 7 0 4548.69 4144.36 232.74 o 4 7 0 12771.58 13387.81 370.78 o 6 7 0 9937.64 10989.88 358.54 o 8 7 0 1430.61 1370.28 117.47 o 10 7 0 10352.64 9785.54 405.53 o 12 7 0 1022.46 1234.45 115.52 o 14 7 0 4759.45 4680.34 322.32 o 16 7 0 7609.40 8231.95 437.10 o 18 7 0 8339.80 8456.86 510.52 o 20 7 0 772.42 770.67 90.80 o 22 7 0 6192.10 5641.66 511.99 o 24 7 0 11077.59 11787.48 653.20 o 26 7 0 2546.75 2467.92 233.97 o 28 7 0 39.12 -388.89 388.89 o 0 8 0 6421.17 7218.74 285.12 o 2 8 0 6259.66 6786.29 278.27 o 4 8 0 1482.43 1698.23 133.87 o 6 8 0 10469.71 10954.89 372.98 o 8 8 0 12489.04 12905.44 421.44 o 10 8 0 927.33 797.84 76.36 o 12 8 0 25157.87 25849.54 670.58 o 14 8 0 640.52 665.19 72.44 o 16 8 0 2643.50 2802.97 223.69 o 18 8 0 10348.86 10815.88 521.04 o 20 8 0 517.79 69.51 299.07 o 22 8 0 47.55 143.42 83.94 o 24 8 0 3610.74 3405.26 267.74 o 26 8 0 847.86 643.17 119.19 o 28 8 0 692.76 784.14 120.41 o 2 9 0 37608.06 35585.89 698.97 o 4 9 0 52854.03 51724.04 893.29 o 6 9 0 9035.52 8720.69 367.59 o 8 9 0 4568.65 4059.44 270.68 o 10 9 0 69009.46 68286.33 1177.18 o 12 9 0 15745.13 16422.79 543.07 o 14 9 0 206.04 140.48 68.28 o 16 9 0 30690.16 30609.41 828.68 o 18 9 0 13383.33 13226.77 615.02 o 20 9 0 1452.98 1565.09 143.66 o 22 9 0 4297.42 4234.18 307.88 o 24 9 0 6958.54 6575.58 592.75 o 26 9 0 3317.95 3168.85 273.86 o 28 9 0 465.94 299.56 126.04 o 0 10 0 29842.63 31794.19 680.61 o 2 10 0 2925.36 3307.37 228.58 o 4 10 0 4003.98 3916.03 276.31 o 6 10 0 19613.78 20524.32 558.49 o 8 10 0 7329.56 7656.82 359.76 o 10 10 0 1267.49 1248.64 117.23 o 12 10 0 14301.32 14192.50 531.81 o 14 10 0 11936.89 12442.88 520.31 o 16 10 0 459.75 458.39 81.50 o 18 10 0 4443.61 5256.45 411.40 o 20 10 0 7308.09 7276.26 504.89 o 22 10 0 1098.83 1313.50 125.79 o 24 10 0 1384.22 1594.21 144.39 o 26 10 0 1976.52 2212.91 200.19 o 28 10 0 810.15 581.49 130.20 o 2 11 0 60026.89 61916.08 1084.67 o 4 11 0 82018.99 80309.98 1292.70 o 6 11 0 8136.24 8582.90 387.91 o 8 11 0 11980.46 12267.65 463.53 o 10 11 0 55249.83 54733.07 1093.97 o 12 11 0 13001.94 12241.71 524.23 o 14 11 0 445.11 500.24 77.58 o 16 11 0 23756.97 24115.09 782.42 o 18 11 0 7945.67 7530.54 498.28 o 20 11 0 1343.89 1412.86 135.83 o 22 11 0 3933.14 4283.38 336.51 o 24 11 0 2063.03 2074.87 187.96 o 26 11 0 3035.78 2752.30 233.48 o 0 12 0 17220.35 18739.95 562.89 o 2 12 0 36635.66 37255.72 824.27 o 4 12 0 3980.41 4279.70 311.55 o 6 12 0 24763.59 25094.53 689.91 o 8 12 0 30227.94 30322.10 769.45 o 10 12 0 320.91 348.26 67.55 o 12 12 0 2841.41 3129.69 235.93 o 14 12 0 20309.33 19898.29 690.40 o 16 12 0 2593.72 2463.03 194.57 o 18 12 0 21.54 19.09 101.57 o 20 12 0 6322.12 5348.96 474.54 o 22 12 0 1363.71 1266.51 121.63 o 24 12 0 694.37 982.37 114.29 o 26 12 0 1007.38 1149.04 122.86 o 2 13 0 15405.77 16283.53 545.03 o 4 13 0 11379.88 11246.37 473.32 o 6 13 0 156.87 151.49 64.86 o 8 13 0 4329.59 4731.73 370.78 o 10 13 0 17619.12 16080.15 615.76 o 12 13 0 262.75 188.94 79.78 o 14 13 0 1597.55 1588.09 158.10 o 16 13 0 8898.05 7916.73 542.34 o 18 13 0 1035.00 1021.53 103.28 o 20 13 0 83.17 -236.17 307.63 o 22 13 0 2719.34 3172.76 313.26 o 24 13 0 1962.01 2317.65 208.27 o 0 14 0 7766.03 7440.96 410.42 o 2 14 0 13581.60 13868.96 540.62 o 4 14 0 3925.12 3141.68 240.33 o 6 14 0 2637.63 2831.35 227.12 o 8 14 0 21451.57 21228.92 686.73 o 10 14 0 129.14 -256.24 256.24 o 12 14 0 11.81 66.32 245.23 o 14 14 0 8381.87 8963.71 523.00 o 16 14 0 1345.10 1272.38 125.30 o 18 14 0 1219.47 1129.46 112.33 o 20 14 0 2779.31 3029.84 300.54 o 22 14 0 966.81 1096.17 108.91 o 24 14 0 1043.33 1025.20 125.79 o 2 15 0 65.31 93.49 68.77 o 4 15 0 992.04 1203.61 115.03 o 6 15 0 1805.48 1674.98 167.89 o 8 15 0 1054.84 1031.56 97.65 o 10 15 0 1432.04 1509.53 151.00 o 12 15 0 103.92 -7.10 267.01 o 14 15 0 2778.28 3136.30 263.09 o 16 15 0 2931.45 2999.73 269.21 o 18 15 0 23.23 81.01 93.98 o 20 15 0 514.89 537.20 100.34 o 22 15 0 2423.07 2532.29 222.22 o 0 16 0 607.91 683.79 74.16 o 2 16 0 78.55 83.46 210.47 o 4 16 0 65.43 -248.90 248.90 o 6 16 0 129.50 79.78 244.74 o 8 16 0 1791.28 2051.14 164.22 o 10 16 0 52.13 44.05 92.02 o 12 16 0 187.09 191.14 79.78 o 14 16 0 1965.28 2053.83 177.43 o 16 16 0 307.13 262.85 92.51 o 18 16 0 2.06 -8.08 293.68 o 20 16 0 2121.22 1911.64 171.07 o 22 16 0 625.38 534.50 120.41 o 2 17 0 230.98 127.75 264.07 o 4 17 0 22.01 11.99 241.31 o 6 17 0 81.04 -281.20 281.20 o 8 17 0 832.18 767.74 89.33 o 10 17 0 823.82 796.13 96.92 o 12 17 0 4.32 -247.43 291.73 o 14 17 0 369.28 -219.77 310.82 o 16 17 0 63.38 58.25 156.14 o 18 17 0 8.83 106.95 251.34 o 20 17 0 62.89 -343.12 343.12 o 0 18 0 821.13 1089.32 107.93 o 2 18 0 215.95 172.29 83.21 o 4 18 0 18.89 63.39 169.11 o 6 18 0 1549.93 1684.28 167.89 o 8 18 0 464.66 467.20 90.31 o 10 18 0 30.86 262.85 86.39 o 12 18 0 552.43 455.21 103.77 o 14 18 0 1259.62 1107.92 116.98 o 16 18 0 1146.02 1289.52 118.45 o 18 18 0 337.22 423.15 106.71 o 2 19 0 1002.20 1040.62 102.79 o 4 19 0 2059.62 1922.16 186.00 o 6 19 0 13.88 81.99 204.60 o 8 19 0 836.83 814.48 106.71 o 10 19 0 1335.95 1597.64 145.62 o 12 19 0 216.50 -64.61 318.89 o 14 19 0 182.56 324.77 98.38 o 16 19 0 2086.50 1919.47 183.55 o 0 20 0 8223.58 7744.68 550.17 o 2 20 0 211.99 -341.41 341.41 o 4 20 0 44.08 -135.34 300.29 o 6 20 0 4399.49 5050.87 463.53 o 8 20 0 803.73 837.49 109.89 o 10 20 0 1391.13 1499.99 150.51 o 12 20 0 2209.98 2509.28 231.03 o 14 20 0 989.28 927.31 122.37 o 2 21 0 3239.95 3336.98 326.72 o 4 21 0 6144.93 5789.48 556.04 o 6 21 0 131.30 112.82 332.84 o 8 21 0 2054.03 1935.37 192.61 o 10 21 0 3582.38 3433.41 325.74 o 12 21 0 1441.86 1645.61 162.26 o 0 22 0 3068.02 3185.98 269.70 o 2 22 0 108.27 313.51 99.12 o 4 22 0 15.34 -125.30 330.64 o 6 22 0 1319.63 1317.66 129.95 o 8 22 0 884.86 915.07 116.01 o 1 1 1 150354.06 137810.53 1529.60 o 2 1 1 1121.71 722.22 58.49 o 3 1 1 329.36 327.95 32.31 o 4 1 1 6121.97 6312.24 219.53 o 5 1 1 57201.94 56533.60 799.31 o 6 1 1 99.52 38.42 145.13 o 7 1 1 86007.30 84527.03 1139.49 o 8 1 1 27182.01 27498.08 552.61 o 9 1 1 64605.64 66074.88 1005.38 o 10 1 1 895.22 796.86 72.69 o 11 1 1 25438.26 26992.70 611.84 o 12 1 1 374.96 322.07 58.25 o 13 1 1 27247.67 26171.86 650.26 o 14 1 1 6342.21 6344.54 348.02 o 15 1 1 43827.80 43960.27 933.91 o 16 1 1 3168.48 2995.33 291.97 o 17 1 1 0.33 -225.40 225.40 o 18 1 1 2137.31 2200.42 205.82 o 19 1 1 10442.89 9779.91 500.00 o 20 1 1 1129.89 1219.77 120.41 o 21 1 1 16421.93 17860.37 672.05 o 22 1 1 1754.92 1554.08 148.07 o 23 1 1 2012.10 1793.92 161.04 o 24 1 1 1037.48 896.96 104.01 o 25 1 1 869.27 916.78 104.75 o 26 1 1 0.14 -317.18 317.18 o 27 1 1 7746.06 7468.13 589.08 o 28 1 1 6.03 -104.01 319.87 o 29 1 1 1348.01 1353.88 124.82 o 30 1 1 371.78 77.09 144.64 o 31 1 1 2.91 73.42 323.30 o 0 2 1 2734.01 2504.63 120.66 o 1 2 1 5705.05 6193.79 174.01 o 2 2 1 3242.41 3237.62 145.37 o 3 2 1 21957.45 21975.61 397.94 o 4 2 1 151.63 186.98 36.22 o 5 2 1 11716.25 12064.77 306.90 o 6 2 1 1422.59 1327.21 121.14 o 7 2 1 3900.89 4242.50 224.18 o 8 2 1 19.79 -37.44 153.45 o 9 2 1 7968.44 7578.75 309.35 o 10 2 1 2401.04 2579.52 219.77 o 11 2 1 1327.47 1435.13 119.92 o 12 2 1 2156.44 1982.12 155.90 o 13 2 1 9074.50 9447.31 389.62 o 14 2 1 3976.15 4276.28 285.61 o 15 2 1 196.74 233.23 62.65 o 16 2 1 1651.56 1359.02 131.91 o 17 2 1 22.57 -119.92 218.79 o 18 2 1 2547.62 2490.44 208.52 o 19 2 1 4676.43 3776.28 371.26 o 20 2 1 1108.37 1048.70 99.85 o 21 2 1 256.60 62.90 184.53 o 22 2 1 1647.16 1551.63 139.99 o 23 2 1 29.04 7.34 296.13 o 24 2 1 2.24 -294.42 294.42 o 25 2 1 845.49 856.09 106.22 o 26 2 1 768.46 727.85 113.07 o 27 2 1 105.10 -172.29 232.01 o 28 2 1 1522.19 1263.33 127.26 o 29 2 1 75.13 65.83 237.15 o 30 2 1 68.84 156.39 265.78 o 31 2 1 122.71 -403.08 416.30 o 1 3 1 33850.25 34509.53 507.58 o 2 3 1 6255.03 6628.68 203.38 o 3 3 1 4315.62 4410.64 188.94 o 4 3 1 8.28 41.12 37.20 o 5 3 1 26731.78 27386.24 496.33 o 6 3 1 3146.15 3180.84 192.36 o 7 3 1 36401.24 36083.43 636.56 o 8 3 1 1532.02 1318.39 131.91 o 9 3 1 9176.69 9366.79 334.07 o 10 3 1 2190.27 2402.58 216.35 o 11 3 1 7176.32 6879.54 318.16 o 12 3 1 1118.76 1535.97 152.47 o 13 3 1 28031.02 27872.78 678.90 o 14 3 1 1345.98 1379.33 130.69 o 15 3 1 16925.94 17594.09 551.15 o 16 3 1 2.06 -153.45 222.47 o 17 3 1 1260.71 1406.01 128.00 o 18 3 1 1.94 79.78 205.33 o 19 3 1 9559.26 8824.21 490.45 o 20 3 1 74.00 54.09 146.11 o 21 3 1 14296.30 15359.41 637.78 o 22 3 1 60.48 -273.62 290.99 o 23 3 1 370.62 373.22 89.33 o 24 3 1 142.22 82.97 146.84 o 25 3 1 1549.83 1805.66 173.03 o 26 3 1 145.43 197.01 99.85 o 27 3 1 5796.34 5404.51 387.66 o 28 3 1 0.10 17.13 188.94 o 29 3 1 1861.52 2326.95 206.31 o 30 3 1 10.97 -345.57 376.65 o 0 4 1 24921.89 25211.27 438.08 o 1 4 1 3844.93 4018.33 180.13 o 2 4 1 9495.43 10239.28 268.72 o 3 4 1 22473.71 22559.06 426.82 o 4 4 1 622.63 634.60 62.90 o 5 4 1 6604.75 6234.66 244.74 o 6 4 1 30.47 24.72 43.56 o 7 4 1 3182.29 3467.42 208.03 o 8 4 1 1436.31 1716.83 164.46 o 9 4 1 12140.28 11869.96 381.79 o 10 4 1 4305.38 4373.68 275.08 o 11 4 1 8110.25 7942.43 340.67 o 12 4 1 2176.49 2610.36 239.84 o 13 4 1 9536.85 9171.74 396.23 o 14 4 1 29.30 -188.20 188.20 o 15 4 1 2605.86 3254.50 286.10 o 16 4 1 532.61 46.99 220.51 o 17 4 1 2965.24 2892.29 219.04 o 18 4 1 158.68 297.60 68.77 o 19 4 1 5947.37 6346.75 430.25 o 20 4 1 113.08 -294.91 294.91 o 21 4 1 64.75 -64.37 286.10 o 22 4 1 2555.15 2338.21 195.54 o 23 4 1 417.46 460.59 96.92 o 24 4 1 18.55 39.89 284.38 o 25 4 1 2521.69 2121.62 185.27 o 26 4 1 361.62 340.67 104.01 o 27 4 1 78.50 196.77 99.61 o 28 4 1 1297.81 1348.74 125.79 o 29 4 1 3.08 78.81 254.28 o 30 4 1 27.37 116.74 250.12 o 1 5 1 559.93 457.41 45.52 o 2 5 1 1134.08 1134.60 103.03 o 3 5 1 1741.20 1879.33 162.50 o 4 5 1 110.28 20.07 61.67 o 5 5 1 20664.91 21141.79 453.25 o 6 5 1 4030.34 4115.49 241.07 o 7 5 1 2757.83 2457.89 191.14 o 8 5 1 49.52 -170.09 170.09 o 9 5 1 134.79 49.44 91.53 o 10 5 1 967.86 982.37 90.55 o 11 5 1 1840.04 1880.80 155.41 o 12 5 1 2808.59 3022.00 261.13 o 13 5 1 9497.27 9777.46 396.72 o 14 5 1 179.52 250.12 59.47 o 15 5 1 1978.39 2118.19 174.50 o 16 5 1 330.61 302.25 68.04 o 17 5 1 209.31 420.46 70.48 o 18 5 1 608.75 428.78 80.27 o 19 5 1 2137.30 1906.99 181.59 o 20 5 1 83.21 57.76 121.14 o 21 5 1 5089.66 5036.43 438.81 o 22 5 1 52.34 -290.50 290.50 o 23 5 1 639.13 580.76 97.16 o 24 5 1 4.26 -53.84 305.68 o 25 5 1 1399.83 1311.05 130.69 o 26 5 1 68.41 35.24 313.26 o 27 5 1 1123.02 1035.23 122.37 o 28 5 1 101.28 115.27 263.09 o 29 5 1 2241.38 2800.52 266.27 o 30 5 1 15.51 -28.14 166.42 o 0 6 1 87.18 -56.78 139.50 o 1 6 1 3480.34 3283.87 199.22 o 2 6 1 14.72 -103.03 141.70 o 3 6 1 40488.66 41974.73 692.36 o 4 6 1 1045.10 1083.69 99.36 o 5 6 1 11677.18 11994.77 351.20 o 6 6 1 851.28 1032.30 97.16 o 7 6 1 572.72 528.63 52.62 o 8 6 1 1283.49 1369.54 107.93 o 9 6 1 16811.85 16653.08 470.63 o 10 6 1 4450.06 4846.27 271.41 o 11 6 1 9181.73 9488.18 389.13 o 12 6 1 252.67 -67.55 194.32 o 13 6 1 1488.92 1760.14 155.90 o 14 6 1 252.47 34.51 211.70 o 15 6 1 8926.40 9314.66 437.10 o 16 6 1 2120.10 2209.72 199.95 o 17 6 1 7041.49 6761.57 438.57 o 18 6 1 321.34 -11.75 258.20 o 19 6 1 6031.59 5795.85 421.68 o 20 6 1 5.26 -4.41 197.01 o 21 6 1 921.14 976.74 94.71 o 22 6 1 266.72 143.66 292.70 o 23 6 1 4716.73 5637.01 451.29 o 24 6 1 84.01 106.46 296.13 o 25 6 1 5006.59 5195.51 482.86 o 26 6 1 0.50 57.02 161.53 o 27 6 1 134.46 163.24 341.16 o 28 6 1 98.67 118.45 346.55 o 29 6 1 809.17 988.49 121.63 o 30 6 1 35.25 109.15 212.43 o 1 7 1 1388.69 1217.56 120.41 o 2 7 1 8591.68 9081.43 320.60 o 3 7 1 3809.07 4129.68 237.88 o 4 7 1 2869.78 2504.39 209.74 o 5 7 1 2010.29 2047.22 202.64 o 6 7 1 779.17 887.90 75.38 o 7 7 1 609.62 563.63 55.07 o 8 7 1 1014.13 1107.68 97.16 o 9 7 1 746.96 710.47 68.04 o 10 7 1 3383.69 3141.68 265.54 o 11 7 1 368.01 416.05 57.02 o 12 7 1 1721.04 1563.13 138.52 o 13 7 1 860.66 814.97 73.91 o 14 7 1 1206.99 1261.86 114.05 o 15 7 1 85.63 -57.27 231.52 o 16 7 1 3790.71 3619.90 232.01 o 17 7 1 798.40 589.81 83.21 o 18 7 1 552.25 556.04 80.52 o 19 7 1 226.82 427.55 79.78 o 20 7 1 1343.23 1494.12 141.95 o 21 7 1 76.84 23.49 103.28 o 22 7 1 354.33 94.96 201.42 o 23 7 1 799.66 779.24 106.95 o 24 7 1 368.61 190.16 335.78 o 25 7 1 162.69 111.60 101.81 o 26 7 1 1826.45 1679.63 156.14 o 27 7 1 124.34 157.37 106.71 o 28 7 1 322.99 264.07 112.82 o 29 7 1 613.24 364.90 128.00 o 0 8 1 5667.43 6033.97 281.69 o 1 8 1 18088.98 18225.27 455.70 o 2 8 1 5705.97 5557.47 265.78 o 3 8 1 24840.61 24557.58 550.90 o 4 8 1 2151.82 2514.91 213.41 o 5 8 1 26566.37 26578.36 584.92 o 6 8 1 6488.39 7026.87 314.98 o 7 8 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