#------------------------------------------------------------------------------ #$Date: 2013-08-28 13:42:33 +0300 (Wed, 28 Aug 2013) $ #$Revision: 88054 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/90/2019047.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2019047_Fobs loop_ _publ_author_name 'Bojarska, Joanna' 'Maniukiewicz, Waldemar' 'Siero\'n, Les\/law' _publ_section_title ; Three new olanzapine structures: the acetic acid monosolvate, and the propan-2-ol and propan-2-one hemisolvate monohydrates ; _journal_coeditor_code OV3029 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 781 _journal_page_last 786 _journal_volume 69 _journal_year 2013 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.924 _cell_angle_gamma 90.000 _cell_length_a 10.1474 _cell_length_b 12.8562 _cell_length_c 14.5494 _exptl_crystal_F_000 792.00 _reflns_d_resolution_high 0.8416 _[local]_cod_data_source_file ov3029Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Olan-acetic-acid in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 186.78 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 15842.13 16354.65 205.03 o 2 0 0 1902.55 1934.87 17.19 o 3 0 0 5274.45 5112.05 44.83 o 4 0 0 1899.48 1941.72 23.29 o 5 0 0 85.46 82.25 2.26 o 6 0 0 902.33 881.94 25.57 o 7 0 0 5.43 3.20 0.71 o 8 0 0 286.25 289.24 5.68 o 9 0 0 964.07 955.87 39.78 o 10 0 0 578.48 570.06 5.92 o 11 0 0 128.45 121.71 3.96 o 12 0 0 42.20 39.86 1.07 o 1 1 0 26.59 16.80 0.26 o 2 1 0 9.09 9.24 0.16 o 3 1 0 217.92 230.33 1.53 o 4 1 0 530.45 541.92 5.74 o 5 1 0 214.20 313.82 4.92 o 6 1 0 0.47 1.54 0.41 o 7 1 0 0.30 1.07 0.50 o 8 1 0 369.98 343.53 4.57 o 9 1 0 519.74 500.92 4.72 o 10 1 0 31.05 30.76 0.65 o 11 1 0 64.78 66.92 1.19 o 12 1 0 23.59 26.49 0.89 o 0 2 0 8050.76 8650.17 92.78 o 1 2 0 534.83 526.85 3.12 o 2 2 0 3019.28 3377.95 21.96 o 3 2 0 183.14 197.56 1.52 o 4 2 0 1.46 1.97 0.27 o 5 2 0 34.99 42.90 1.01 o 6 2 0 980.50 978.35 11.33 o 7 2 0 22.82 16.94 0.60 o 8 2 0 35.65 38.10 0.75 o 9 2 0 298.96 282.04 3.35 o 10 2 0 56.04 53.85 0.80 o 11 2 0 118.50 119.63 1.42 o 1 3 0 34886.13 33938.93 222.04 o 2 3 0 2550.56 2693.17 18.77 o 3 3 0 1966.06 1944.16 18.97 o 4 3 0 1047.89 1073.98 9.68 o 5 3 0 780.51 803.70 10.22 o 6 3 0 462.01 386.56 4.24 o 7 3 0 71.20 66.73 1.20 o 8 3 0 514.34 500.89 6.19 o 9 3 0 898.24 885.53 6.71 o 10 3 0 45.07 44.83 0.64 o 11 3 0 1.24 0.89 0.22 o 0 4 0 5698.51 5656.85 50.26 o 1 4 0 9.63 13.60 0.52 o 2 4 0 14.82 11.73 0.28 o 3 4 0 111.40 129.86 1.50 o 4 4 0 369.42 394.00 3.87 o 5 4 0 33.48 27.64 0.48 o 6 4 0 33.87 29.18 0.67 o 7 4 0 17.74 20.93 0.65 o 8 4 0 0.87 1.27 0.40 o 9 4 0 113.57 98.04 1.03 o 10 4 0 265.15 271.83 2.51 o 11 4 0 1.53 1.70 0.44 o 1 5 0 1196.48 1224.27 13.17 o 2 5 0 1058.93 1136.83 11.48 o 3 5 0 998.70 977.62 10.52 o 4 5 0 6.40 18.65 0.39 o 5 5 0 543.80 540.52 4.52 o 6 5 0 50.34 49.50 0.69 o 7 5 0 14.67 12.71 0.49 o 8 5 0 88.96 89.01 1.11 o 9 5 0 1.10 1.82 0.31 o 10 5 0 203.53 205.45 2.50 o 11 5 0 0.88 1.89 0.41 o 0 6 0 1688.37 1517.68 19.33 o 1 6 0 496.87 513.47 5.39 o 2 6 0 451.88 483.47 5.63 o 3 6 0 534.81 464.13 4.19 o 4 6 0 8.60 11.18 0.39 o 5 6 0 13.47 16.89 0.41 o 6 6 0 8.01 12.95 0.41 o 7 6 0 47.42 49.90 0.72 o 8 6 0 31.95 35.45 0.70 o 9 6 0 12.93 9.93 0.47 o 10 6 0 147.12 154.71 2.14 o 11 6 0 4.33 5.45 0.41 o 1 7 0 2.13 2.06 0.23 o 2 7 0 123.25 116.06 1.19 o 3 7 0 1.15 2.85 0.32 o 4 7 0 73.72 68.93 0.87 o 5 7 0 9.51 9.12 0.34 o 6 7 0 175.06 187.98 1.80 o 7 7 0 36.86 33.61 0.65 o 8 7 0 22.74 27.21 0.60 o 9 7 0 100.35 99.80 1.43 o 10 7 0 12.06 9.61 0.34 o 0 8 0 382.11 364.12 4.57 o 1 8 0 478.31 445.29 4.28 o 2 8 0 552.80 512.05 4.60 o 3 8 0 20.89 21.21 0.48 o 4 8 0 173.21 165.25 1.53 o 5 8 0 51.75 60.70 0.82 o 6 8 0 16.59 15.77 0.45 o 7 8 0 28.61 27.40 0.58 o 8 8 0 164.65 158.46 1.57 o 9 8 0 363.00 360.11 3.59 o 10 8 0 62.86 64.94 1.01 o 1 9 0 149.58 136.46 1.79 o 2 9 0 108.07 106.53 1.22 o 3 9 0 0.72 2.68 0.49 o 4 9 0 9.98 15.08 0.45 o 5 9 0 5.52 6.44 0.33 o 6 9 0 6.15 3.80 0.30 o 7 9 0 6.35 8.35 0.36 o 8 9 0 0.15 0.23 0.26 o 9 9 0 34.14 39.47 0.85 o 0 10 0 261.00 274.77 6.04 o 1 10 0 68.07 63.39 1.02 o 2 10 0 683.17 633.23 6.21 o 3 10 0 301.50 309.87 3.32 o 4 10 0 49.75 52.30 0.77 o 5 10 0 4.27 4.43 0.31 o 6 10 0 126.60 125.27 1.31 o 7 10 0 2.74 2.81 0.30 o 8 10 0 33.39 39.05 0.72 o 9 10 0 20.08 23.65 0.87 o 1 11 0 41.17 42.05 1.01 o 2 11 0 419.71 398.27 3.99 o 3 11 0 1.39 1.84 0.32 o 4 11 0 0.69 1.07 0.22 o 5 11 0 143.66 136.86 1.38 o 6 11 0 18.03 18.07 0.71 o 7 11 0 94.07 104.33 1.49 o 8 11 0 70.36 71.49 1.07 o 1 12 0 287.94 259.84 4.16 o 2 12 0 29.31 37.19 1.00 o 3 12 0 179.52 166.35 2.04 o 4 12 0 62.33 56.78 0.87 o 5 12 0 14.94 15.90 0.51 o 6 12 0 40.49 39.72 0.79 o 7 12 0 48.34 51.68 0.89 o 1 13 0 136.81 119.34 3.55 o 2 13 0 2.83 1.78 0.41 o 3 13 0 70.20 70.67 1.56 o 4 13 0 73.20 64.69 2.08 o 5 13 0 62.83 61.69 1.38 o 6 13 0 25.98 31.09 1.00 o 2 14 0 13.34 16.69 1.42 o 3 14 0 34.55 32.51 1.00 o 4 14 0 14.28 12.26 0.75 o -12 1 1 2.48 2.45 0.26 o -11 1 1 17.87 17.38 0.48 o -10 1 1 151.22 149.58 1.68 o -9 1 1 6.12 9.18 0.38 o -8 1 1 103.78 115.96 2.63 o -7 1 1 224.05 198.39 3.21 o -6 1 1 190.53 174.53 3.24 o -5 1 1 291.44 241.02 3.72 o -4 1 1 1250.29 1228.86 11.88 o -3 1 1 3260.31 3216.85 20.20 o -2 1 1 259.32 209.73 1.24 o -1 1 1 1469.78 1572.88 9.84 o 0 1 1 343.74 341.87 2.56 o 1 1 1 80.50 68.55 0.60 o 2 1 1 8465.13 8653.42 59.44 o 3 1 1 159.55 123.35 0.92 o 4 1 1 2162.76 2078.56 18.87 o 5 1 1 227.50 221.24 3.22 o 6 1 1 105.46 104.69 1.50 o 7 1 1 905.52 857.90 12.95 o 8 1 1 747.84 791.69 9.95 o 9 1 1 251.78 255.54 3.01 o 10 1 1 57.48 58.44 0.67 o 11 1 1 27.49 31.92 0.59 o -11 2 1 27.53 28.93 0.59 o -10 2 1 9.66 11.32 0.45 o -9 2 1 135.07 133.15 1.76 o -8 2 1 368.96 375.82 3.95 o -7 2 1 187.35 183.09 2.57 o -6 2 1 315.34 305.30 5.87 o -5 2 1 292.64 347.93 5.23 o -4 2 1 609.40 698.32 6.66 o -3 2 1 8.74 7.30 0.16 o -2 2 1 137.29 149.58 0.96 o -1 2 1 1805.11 2004.89 12.78 o 0 2 1 3337.77 3484.27 21.71 o 1 2 1 129.80 86.83 0.60 o 2 2 1 22.66 25.96 0.29 o 3 2 1 610.04 607.72 4.31 o 4 2 1 285.87 267.65 2.53 o 5 2 1 83.44 89.90 1.55 o 6 2 1 32.77 28.14 0.70 o 7 2 1 1.62 1.86 0.30 o 8 2 1 656.75 655.20 8.05 o 9 2 1 417.73 433.01 4.90 o 10 2 1 20.96 18.96 0.46 o 11 2 1 3.34 3.99 0.36 o -11 3 1 0.70 0.59 0.31 o -10 3 1 84.18 84.61 0.92 o -9 3 1 116.88 109.02 1.35 o -8 3 1 42.07 37.98 0.92 o -7 3 1 71.31 52.04 1.10 o -6 3 1 89.51 82.65 1.14 o -5 3 1 227.10 256.37 3.33 o -4 3 1 299.95 200.19 2.23 o -3 3 1 891.56 906.57 8.10 o -2 3 1 953.04 767.92 4.68 o -1 3 1 228.12 220.51 1.48 o 0 3 1 10441.59 10211.00 61.95 o 1 3 1 2403.12 2785.08 17.52 o 2 3 1 6728.02 6849.39 44.59 o 3 3 1 82.20 114.08 1.11 o 4 3 1 4.72 5.16 0.26 o 5 3 1 270.90 314.97 3.88 o 6 3 1 48.51 48.81 0.85 o 7 3 1 62.81 63.54 1.14 o 8 3 1 606.46 604.43 6.71 o 9 3 1 132.92 126.17 1.18 o 10 3 1 110.39 104.74 1.03 o 11 3 1 12.20 17.01 0.44 o -11 4 1 39.30 43.05 0.87 o -10 4 1 277.07 267.51 2.47 o -9 4 1 225.23 203.85 1.93 o -8 4 1 1855.66 1862.07 18.85 o -7 4 1 39.95 43.35 0.88 o -6 4 1 82.02 76.94 1.09 o -5 4 1 11.32 12.33 0.33 o -4 4 1 45.31 67.69 0.89 o -3 4 1 124.63 168.46 1.69 o -2 4 1 11.16 7.56 0.21 o -1 4 1 11496.38 11389.09 89.51 o 0 4 1 1901.54 1951.37 13.67 o 1 4 1 1087.67 1141.99 7.64 o 2 4 1 2829.22 2749.68 22.83 o 3 4 1 1.98 7.54 0.25 o 4 4 1 547.05 651.19 5.86 o 5 4 1 398.97 354.53 2.99 o 6 4 1 29.32 31.04 0.96 o 7 4 1 65.95 59.08 1.08 o 8 4 1 200.63 203.22 1.99 o 9 4 1 23.88 18.79 0.46 o 10 4 1 0.41 0.62 0.26 o 11 4 1 75.28 74.83 1.29 o -11 5 1 5.55 8.03 0.45 o -10 5 1 0.11 0.00 0.32 o -9 5 1 33.03 33.89 0.75 o -8 5 1 74.19 78.50 0.99 o -7 5 1 459.17 445.65 3.85 o -6 5 1 413.10 407.33 3.68 o -5 5 1 178.54 181.97 1.57 o -4 5 1 56.78 64.12 0.74 o -3 5 1 806.42 829.94 8.01 o -2 5 1 615.01 731.27 7.11 o -1 5 1 117.66 133.45 1.28 o 0 5 1 1.70 5.56 0.33 o 1 5 1 2125.25 2229.64 18.24 o 2 5 1 210.60 240.50 2.79 o 3 5 1 1500.42 1676.58 16.75 o 4 5 1 777.18 762.15 6.34 o 5 5 1 278.72 267.87 2.26 o 6 5 1 326.96 327.52 2.98 o 7 5 1 621.59 611.13 5.36 o 8 5 1 267.98 267.62 2.55 o 9 5 1 0.41 0.00 0.23 o 10 5 1 0.25 0.56 0.30 o 11 5 1 62.72 77.02 1.83 o -11 6 1 29.63 35.88 1.00 o -10 6 1 3.17 3.79 0.34 o -9 6 1 12.66 13.59 0.64 o -8 6 1 464.00 446.04 4.90 o -7 6 1 5.44 8.00 0.38 o -6 6 1 458.13 479.38 3.96 o -5 6 1 252.94 279.56 2.66 o -4 6 1 169.46 201.33 1.72 o -3 6 1 20.65 23.68 0.46 o -2 6 1 814.54 909.72 10.04 o -1 6 1 348.15 349.30 3.93 o 0 6 1 1096.71 1225.99 10.17 o 1 6 1 1053.99 991.51 11.86 o 2 6 1 125.64 128.81 2.04 o 3 6 1 27.08 22.81 0.42 o 4 6 1 0.94 1.28 0.22 o 5 6 1 353.24 345.91 3.06 o 6 6 1 6.57 4.60 0.60 o 7 6 1 134.82 139.87 1.32 o 8 6 1 89.35 81.89 1.31 o 9 6 1 3.58 5.31 0.35 o 10 6 1 114.64 129.89 1.62 o 11 6 1 12.21 18.88 0.68 o -10 7 1 30.91 31.67 1.00 o -9 7 1 35.01 35.98 0.69 o -8 7 1 259.61 254.60 2.75 o -7 7 1 1109.29 1105.23 8.44 o -6 7 1 920.70 939.48 8.07 o -5 7 1 494.06 466.08 3.80 o -4 7 1 319.41 299.41 2.67 o -3 7 1 853.34 906.51 7.24 o -2 7 1 1544.21 1636.91 17.05 o -1 7 1 806.56 792.03 9.07 o 0 7 1 119.16 138.26 1.70 o 1 7 1 367.78 380.50 4.80 o 2 7 1 0.60 2.63 0.24 o 3 7 1 434.79 504.66 4.67 o 4 7 1 619.03 653.30 5.47 o 5 7 1 529.75 505.86 4.27 o 6 7 1 1070.50 1014.87 7.67 o 7 7 1 307.95 308.15 2.65 o 8 7 1 6.78 6.98 0.42 o 9 7 1 0.60 1.12 0.31 o 10 7 1 186.02 201.34 2.25 o -10 8 1 13.10 12.45 0.46 o -9 8 1 15.01 13.39 0.45 o -8 8 1 56.63 55.18 0.82 o -7 8 1 358.20 385.85 3.20 o -6 8 1 434.11 424.58 3.40 o -5 8 1 231.00 229.16 2.17 o -4 8 1 7.37 6.71 0.31 o -3 8 1 7.85 7.18 0.56 o -2 8 1 558.19 588.97 5.92 o -1 8 1 4.46 9.42 0.44 o 0 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o -1 10 1 148.30 147.18 2.26 o 0 10 1 797.26 772.21 11.46 o 1 10 1 176.88 168.65 1.90 o 2 10 1 1012.54 1026.39 9.86 o 3 10 1 675.19 690.74 6.39 o 4 10 1 653.70 618.36 4.77 o 5 10 1 391.46 371.08 3.01 o 6 10 1 27.76 23.77 0.57 o 7 10 1 84.26 80.63 0.93 o 8 10 1 15.56 13.33 0.44 o 9 10 1 22.11 24.51 0.62 o -8 11 1 0.01 0.14 0.31 o -7 11 1 18.70 19.54 0.66 o -6 11 1 40.94 41.86 0.77 o -5 11 1 61.98 63.04 0.90 o -4 11 1 47.10 54.92 0.83 o -3 11 1 1.65 1.40 0.31 o -2 11 1 271.56 265.15 2.62 o -1 11 1 2.95 6.09 0.47 o 0 11 1 149.32 131.77 2.04 o 1 11 1 54.71 52.31 1.62 o 2 11 1 15.43 14.27 0.49 o 3 11 1 353.16 328.98 3.09 o 4 11 1 29.39 30.37 0.56 o 5 11 1 13.90 11.90 0.42 o 6 11 1 7.88 8.79 0.36 o 7 11 1 0.79 0.76 0.24 o 8 11 1 22.34 24.16 0.50 o -6 12 1 19.31 19.26 0.71 o -5 12 1 57.86 63.05 0.91 o -4 12 1 52.91 50.04 0.87 o -3 12 1 80.79 72.88 1.11 o -2 12 1 154.68 145.00 1.83 o -1 12 1 44.80 39.80 0.91 o 0 12 1 23.66 20.90 1.60 o 2 12 1 226.82 212.19 2.48 o 3 12 1 210.66 207.47 2.66 o 4 12 1 14.20 16.00 0.52 o 5 12 1 12.06 13.18 0.43 o 6 12 1 2.14 2.73 0.32 o 7 12 1 118.43 116.81 1.85 o -6 13 1 6.04 6.19 0.41 o -5 13 1 143.99 144.58 1.99 o -4 13 1 386.96 388.99 5.53 o -3 13 1 96.78 92.14 1.55 o -2 13 1 24.99 23.24 0.89 o -1 13 1 108.92 108.96 2.03 o 2 13 1 0.33 2.84 1.07 o 3 13 1 14.42 14.25 0.85 o 4 13 1 21.87 21.01 0.82 o 5 13 1 95.84 107.79 1.85 o 6 13 1 258.39 253.25 6.04 o -4 14 1 0.07 0.00 0.50 o -3 14 1 0.05 0.00 0.71 o -2 14 1 28.76 27.58 1.24 o 2 14 1 21.90 25.22 1.42 o 3 14 1 3.96 5.33 0.71 o 4 14 1 0.10 0.12 0.32 o -2 15 1 3.87 4.62 0.71 o -12 0 2 1.49 0.53 0.25 o -11 0 2 129.23 139.24 2.51 o -10 0 2 357.46 333.13 5.18 o -9 0 2 1172.02 1151.48 31.08 o -8 0 2 162.42 176.53 5.33 o -7 0 2 6.96 1.78 0.71 o -6 0 2 2.53 2.84 0.71 o -5 0 2 784.85 889.75 25.57 o -4 0 2 3987.43 3736.07 57.88 o -3 0 2 1108.33 1026.54 9.59 o -2 0 2 18852.37 18414.85 154.28 o -1 0 2 2682.55 2703.44 27.07 o 0 0 2 88.60 82.32 0.88 o 1 0 2 8632.80 8679.22 88.73 o 2 0 2 57.10 50.56 0.60 o 3 0 2 67.00 63.50 1.10 o 4 0 2 5451.79 5213.17 82.43 o 5 0 2 212.50 246.95 5.65 o 6 0 2 68.40 71.77 1.96 o 7 0 2 11.42 14.29 0.77 o 8 0 2 158.23 175.11 5.33 o 9 0 2 7.98 9.92 2.13 o 10 0 2 396.26 383.28 4.72 o 11 0 2 187.56 222.70 4.97 o -12 1 2 19.63 19.18 0.71 o -11 1 2 5.58 5.51 0.32 o -10 1 2 52.24 47.16 0.83 o -9 1 2 69.47 61.29 1.22 o -8 1 2 65.05 68.05 1.41 o -7 1 2 26.58 23.46 1.00 o -6 1 2 516.64 540.99 8.67 o -5 1 2 5549.52 5805.73 91.76 o -4 1 2 904.59 953.72 8.77 o -3 1 2 493.31 480.83 2.91 o -2 1 2 10527.95 10710.54 62.50 o -1 1 2 7482.54 7837.27 50.16 o 0 1 2 0.49 0.00 0.10 o 1 1 2 2256.55 2325.22 15.09 o 2 1 2 134.65 122.92 0.88 o 3 1 2 0.70 1.67 0.12 o 4 1 2 28.64 29.48 1.14 o 5 1 2 316.84 336.15 5.24 o 6 1 2 0.41 0.71 0.32 o 7 1 2 227.56 205.25 2.71 o 8 1 2 504.63 481.02 7.01 o 9 1 2 221.07 221.11 2.50 o 10 1 2 1.17 2.13 0.24 o 11 1 2 8.85 8.82 0.32 o -11 2 2 42.51 49.98 1.00 o -10 2 2 9.65 4.98 0.31 o -9 2 2 79.61 92.08 1.36 o -8 2 2 151.32 169.22 2.11 o -7 2 2 292.58 297.07 3.90 o -6 2 2 249.12 260.10 5.11 o -5 2 2 159.03 177.42 2.87 o -4 2 2 30.50 51.91 1.00 o -3 2 2 819.07 866.77 6.31 o -2 2 2 19459.65 19287.46 121.76 o -1 2 2 13992.87 14451.11 93.15 o 0 2 2 14654.54 15067.43 98.51 o 1 2 2 1625.28 1507.52 9.52 o 2 2 2 1936.78 1879.49 11.90 o 3 2 2 5.63 2.06 0.19 o 4 2 2 1623.38 1645.74 15.36 o 5 2 2 1138.39 1204.23 15.32 o 6 2 2 246.85 262.14 3.05 o 7 2 2 201.94 202.34 2.38 o 8 2 2 0.40 0.28 0.36 o 9 2 2 709.85 678.88 4.91 o 10 2 2 368.64 357.90 2.98 o 11 2 2 57.79 64.88 1.08 o -11 3 2 109.82 115.50 1.75 o -10 3 2 34.70 30.44 0.56 o -9 3 2 35.63 34.19 0.59 o -8 3 2 888.93 864.33 10.39 o -7 3 2 13.84 14.16 0.99 o -6 3 2 160.73 203.11 3.19 o -5 3 2 2.13 1.82 0.35 o -4 3 2 4012.64 4212.26 44.51 o -3 3 2 4984.57 5316.97 40.27 o -2 3 2 5236.19 5365.24 37.19 o -1 3 2 2275.23 2299.79 15.94 o 0 3 2 13718.24 14029.01 91.83 o 1 3 2 367.65 400.13 2.63 o 2 3 2 12.83 7.42 0.15 o 3 3 2 179.04 233.06 2.10 o 4 3 2 1057.69 1260.32 11.24 o 5 3 2 72.44 65.31 1.02 o 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