#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:23:45 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180859 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/90/2019049.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2019049_Fobs loop_ _publ_author_name 'Bojarska, Joanna' 'Maniukiewicz, Waldemar' 'Siero\'n, Les\/law' _publ_section_title ; Three new olanzapine structures: the acetic acid monosolvate, and the propan-2-ol and propan-2-one hemisolvate monohydrates ; _journal_coeditor_code OV3029 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 781 _journal_page_last 786 _journal_volume 69 _journal_year 2013 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 125.790 _cell_angle_gamma 90.000 _cell_length_a 24.5759 _cell_length_b 12.5608 _cell_length_c 15.1607 _exptl_crystal_F_000 1536.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file ov3029IIIsup4.hkl _cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_title ' Ola-propanone-water in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 336.72 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 1157.02 935.09 29.96 o 6 0 0 715.31 599.82 44.24 o 8 0 0 595.16 541.76 56.91 o 10 0 0 503.98 353.29 63.82 o 12 0 0 653.53 694.76 73.02 o 14 0 0 118.61 50.14 75.07 o 16 0 0 26.51 63.87 80.28 o 18 0 0 982.43 1055.20 104.50 o 20 0 0 314.23 219.65 130.43 o 22 0 0 542.12 632.59 134.86 o 1 1 0 41.24 3.80 8.14 o 3 1 0 860.65 804.54 22.44 o 5 1 0 2809.72 2759.31 30.87 o 7 1 0 4742.14 4921.97 47.00 o 9 1 0 475.20 575.23 42.33 o 11 1 0 425.06 439.04 45.88 o 13 1 0 296.32 366.85 51.89 o 15 1 0 47.77 61.34 55.02 o 17 1 0 1.02 0.00 57.38 o 19 1 0 1.34 37.90 84.76 o 21 1 0 7.68 0.85 106.41 o 23 1 0 6.60 0.00 112.19 o 0 2 0 36201.25 35150.59 338.76 o 2 2 0 985.46 741.52 16.08 o 4 2 0 13776.41 12999.34 110.49 o 6 2 0 10137.34 9663.04 112.96 o 8 2 0 3196.84 3278.83 40.99 o 10 2 0 254.62 284.23 41.81 o 12 2 0 377.27 410.00 48.16 o 14 2 0 0.56 6.72 51.71 o 16 2 0 3440.60 3495.58 74.36 o 18 2 0 264.60 264.26 63.19 o 20 2 0 461.33 470.95 101.04 o 22 2 0 8.75 0.00 103.97 o 1 3 0 18151.53 18221.17 122.10 o 3 3 0 90528.03 90066.10 342.94 o 5 3 0 9840.07 9921.53 73.42 o 7 3 0 1021.52 977.84 33.77 o 9 3 0 101.26 213.63 27.74 o 11 3 0 678.13 677.51 36.40 o 13 3 0 345.22 346.44 47.25 o 15 3 0 332.98 379.56 53.21 o 17 3 0 10.31 0.89 56.87 o 19 3 0 1122.99 1197.26 77.62 o 21 3 0 715.05 697.64 137.88 o 23 3 0 110.58 104.80 135.54 o 0 4 0 26099.80 23107.97 127.70 o 2 4 0 6.82 43.60 20.05 o 4 4 0 33.83 36.33 24.29 o 6 4 0 216.81 236.77 30.56 o 8 4 0 1934.80 2005.78 101.37 o 10 4 0 364.37 360.13 37.77 o 12 4 0 1027.07 985.50 42.08 o 14 4 0 1313.54 1433.75 46.67 o 16 4 0 3682.66 3265.62 62.81 o 18 4 0 242.39 207.34 62.54 o 20 4 0 94.49 108.11 76.97 o 22 4 0 6.92 0.00 132.83 o 1 5 0 798.25 775.16 17.73 o 3 5 0 3851.85 3820.64 45.39 o 5 5 0 753.87 708.99 27.96 o 7 5 0 39.94 21.83 29.06 o 9 5 0 41.35 40.51 38.98 o 11 5 0 507.99 450.12 32.09 o 13 5 0 1013.86 1050.54 47.43 o 15 5 0 79.90 74.52 49.10 o 17 5 0 527.95 522.46 71.39 o 19 5 0 200.26 254.47 88.01 o 21 5 0 141.40 118.21 243.69 o 0 6 0 1144.75 1337.84 33.43 o 2 6 0 743.39 768.50 27.27 o 4 6 0 498.46 456.85 23.30 o 6 6 0 218.98 224.78 21.77 o 8 6 0 248.02 278.72 30.09 o 10 6 0 523.73 564.49 41.43 o 12 6 0 1829.76 1652.62 55.57 o 14 6 0 448.50 494.38 53.99 o 16 6 0 152.26 152.10 61.59 o 18 6 0 1.98 0.00 95.56 o 20 6 0 19.18 99.09 130.10 o 1 7 0 453.80 444.62 22.36 o 3 7 0 866.18 806.29 29.50 o 5 7 0 7108.24 7529.16 122.84 o 7 7 0 625.71 576.83 28.19 o 9 7 0 1697.14 1599.86 34.41 o 11 7 0 824.59 822.53 41.96 o 13 7 0 4453.36 4516.49 67.31 o 15 7 0 611.29 484.56 64.95 o 17 7 0 217.52 204.57 128.63 o 19 7 0 137.25 114.83 129.42 o 0 8 0 1292.86 1413.79 45.11 o 2 8 0 4774.28 4641.49 56.02 o 4 8 0 2613.99 2775.74 39.25 o 6 8 0 14.79 23.38 35.20 o 8 8 0 27.20 36.91 46.24 o 10 8 0 59.74 55.60 15.93 o 12 8 0 70.75 44.04 33.19 o 14 8 0 4.99 71.34 108.84 o 16 8 0 40.38 1.98 107.27 o 18 8 0 11.26 0.00 105.60 o 20 8 0 5.72 74.11 116.22 o 1 9 0 55.87 50.58 22.12 o 3 9 0 614.14 589.39 44.84 o 5 9 0 240.35 208.02 27.73 o 7 9 0 1651.00 1721.52 91.77 o 9 9 0 2449.83 2414.56 63.25 o 11 9 0 4.22 0.00 69.35 o 13 9 0 4.14 50.35 105.58 o 15 9 0 39.77 39.72 107.05 o 17 9 0 158.76 197.91 114.04 o 0 10 0 1405.48 1447.36 46.64 o 2 10 0 1902.73 2000.60 56.61 o 4 10 0 3.10 0.00 43.80 o 6 10 0 369.12 346.17 48.83 o 8 10 0 7.18 0.00 69.10 o 10 10 0 13.54 0.00 72.25 o 12 10 0 7.43 25.29 108.55 o 14 10 0 97.37 132.31 113.67 o 16 10 0 340.39 390.13 119.01 o 1 11 0 65.94 101.63 39.31 o 3 11 0 563.27 590.05 52.01 o 5 11 0 601.98 659.20 59.43 o 7 11 0 634.45 650.48 71.86 o 9 11 0 126.40 161.91 67.90 o 11 11 0 20.22 29.49 83.20 o 13 11 0 46.33 41.69 111.12 o 15 11 0 4.77 0.00 120.42 o 0 12 0 173.57 234.77 115.11 o 2 12 0 184.28 233.94 76.19 o 4 12 0 814.42 843.18 90.68 o 6 12 0 807.30 837.52 115.94 o 8 12 0 187.31 189.98 111.60 o 10 12 0 81.92 125.87 111.99 o 12 12 0 120.70 145.80 111.36 o 14 12 0 6.49 18.42 118.28 o 1 13 0 26.53 62.66 100.60 o 3 13 0 121.21 108.10 88.74 o 5 13 0 20.54 18.11 117.31 o 7 13 0 4.61 24.93 114.20 o 9 13 0 34.06 0.00 115.43 o 11 13 0 1.87 0.00 119.88 o 0 14 0 1080.10 1401.30 212.48 o 2 14 0 321.15 344.26 130.48 o 4 14 0 158.75 165.72 118.67 o 6 14 0 72.66 120.83 120.75 o 8 14 0 63.85 82.78 118.95 o -23 1 1 4.70 35.80 105.98 o -21 1 1 100.44 56.09 92.91 o -19 1 1 1436.69 1526.38 79.10 o -17 1 1 12.67 1.70 58.06 o -15 1 1 19.68 0.00 55.70 o -13 1 1 8.02 9.16 51.16 o -11 1 1 839.81 916.11 48.89 o -9 1 1 0.62 0.69 30.68 o -7 1 1 0.53 48.19 28.86 o -5 1 1 9372.22 8965.45 57.55 o -3 1 1 5356.98 4894.39 21.87 o 1 1 1 507.69 555.30 17.67 o 3 1 1 16282.55 16004.78 88.49 o 5 1 1 5239.63 4898.31 60.60 o 7 1 1 11749.94 11648.21 108.72 o 9 1 1 2725.53 2799.94 52.48 o 11 1 1 1953.28 2008.55 55.11 o 13 1 1 181.59 156.81 51.75 o 15 1 1 219.97 260.30 56.89 o 17 1 1 7732.34 7683.72 108.83 o 19 1 1 755.58 721.96 92.83 o 21 1 1 42.17 79.80 107.73 o -24 2 1 189.23 265.93 139.08 o -22 2 1 655.65 574.85 108.27 o -20 2 1 270.09 313.82 72.38 o -18 2 1 65.46 49.69 58.42 o -16 2 1 1054.10 1012.75 60.00 o -14 2 1 342.85 316.51 52.00 o -12 2 1 3665.45 3746.27 59.39 o -10 2 1 11764.72 12661.56 76.83 o -8 2 1 7744.96 8129.47 46.20 o -6 2 1 489.63 451.91 23.27 o -4 2 1 9217.17 9405.23 44.91 o -2 2 1 526.86 452.10 12.23 o 0 2 1 125.08 157.82 12.16 o 2 2 1 7985.17 8482.50 51.25 o 4 2 1 9196.92 9233.46 81.76 o 6 2 1 75.46 28.21 29.57 o 8 2 1 6.13 16.73 31.00 o 10 2 1 1075.68 947.98 45.63 o 12 2 1 823.70 875.51 52.17 o 14 2 1 3627.91 3633.44 70.53 o 16 2 1 164.69 187.02 58.12 o 18 2 1 143.89 92.83 64.98 o 20 2 1 493.63 530.85 113.66 o 22 2 1 120.59 133.33 132.81 o -23 3 1 66.66 3.34 133.33 o -21 3 1 12.21 0.00 97.34 o -19 3 1 188.02 102.86 69.37 o -17 3 1 192.78 173.44 54.08 o -15 3 1 1138.78 1163.67 55.40 o -13 3 1 692.30 776.41 49.10 o -11 3 1 996.64 1137.92 37.26 o -9 3 1 2421.84 2445.98 30.18 o -7 3 1 955.06 900.16 26.91 o -5 3 1 1933.91 2024.06 29.37 o -3 3 1 5065.78 4235.22 34.75 o -1 3 1 12.75 21.56 14.50 o 1 3 1 113378.62 116338.14 377.20 o 3 3 1 781.14 897.17 29.35 o 5 3 1 877.60 936.46 30.29 o 7 3 1 91.98 100.92 36.70 o 9 3 1 373.21 381.54 35.36 o 11 3 1 0.00 0.00 40.60 o 13 3 1 208.33 178.83 47.78 o 15 3 1 1598.02 1610.85 61.06 o 17 3 1 41.66 5.21 68.36 o 19 3 1 616.78 615.23 101.59 o 21 3 1 6.70 38.89 125.95 o -22 4 1 0.88 0.00 131.95 o -20 4 1 18.21 50.01 72.59 o -18 4 1 491.62 517.71 65.47 o -16 4 1 1525.78 1381.49 53.23 o -14 4 1 32.85 35.75 34.61 o -12 4 1 151.66 166.42 28.50 o -10 4 1 660.55 563.66 25.42 o -8 4 1 573.13 624.58 41.15 o -6 4 1 126.07 195.11 23.93 o -4 4 1 3195.98 3150.75 32.54 o -2 4 1 2151.35 2128.22 22.19 o 0 4 1 31.41 44.57 16.94 o 2 4 1 52.15 53.76 15.30 o 4 4 1 168.14 143.72 17.83 o 6 4 1 5399.17 5801.43 63.44 o 8 4 1 154.44 184.98 33.72 o 10 4 1 271.45 216.24 41.71 o 12 4 1 0.38 0.00 23.41 o 14 4 1 3457.89 3304.99 71.82 o 16 4 1 1509.33 1367.56 71.84 o 18 4 1 103.03 137.02 75.13 o 20 4 1 835.01 836.58 135.79 o -23 5 1 0.00 0.00 184.78 o -21 5 1 237.60 200.39 129.81 o -19 5 1 508.96 530.29 75.70 o -17 5 1 1428.09 1414.40 83.91 o -15 5 1 1933.11 2165.05 57.38 o -13 5 1 240.32 187.57 35.81 o -11 5 1 121.18 85.06 46.55 o -9 5 1 1178.42 1031.30 41.77 o -7 5 1 9142.10 8541.40 76.39 o -5 5 1 7321.74 6846.61 158.21 o -3 5 1 26.32 32.09 16.11 o -1 5 1 216.39 231.63 18.78 o 1 5 1 1312.88 1313.77 25.84 o 3 5 1 3.15 11.35 17.87 o 5 5 1 374.01 320.31 18.28 o 7 5 1 21.68 26.73 17.80 o 9 5 1 1194.85 1123.80 34.96 o 11 5 1 359.06 329.11 38.83 o 13 5 1 813.76 733.83 49.16 o 15 5 1 3203.17 3303.72 74.50 o 17 5 1 17.72 16.68 71.11 o 19 5 1 186.03 162.68 170.22 o 21 5 1 110.22 147.36 183.11 o -22 6 1 1.64 19.73 189.73 o -20 6 1 158.02 177.34 121.07 o -18 6 1 26.86 15.30 67.46 o -16 6 1 1142.93 1148.63 68.58 o -14 6 1 1414.04 1509.80 61.49 o -12 6 1 602.80 572.53 47.94 o -10 6 1 3.15 15.03 38.41 o -8 6 1 213.25 196.71 19.11 o -6 6 1 2.04 2.16 31.57 o -4 6 1 584.08 639.92 28.81 o -2 6 1 2976.38 2702.31 30.01 o 0 6 1 7175.61 6790.03 114.75 o 2 6 1 1746.06 1661.53 29.17 o 4 6 1 2243.24 2149.14 51.76 o 6 6 1 414.93 412.78 19.84 o 8 6 1 37.72 42.28 31.03 o 10 6 1 162.55 214.11 40.30 o 12 6 1 3103.82 2966.62 120.61 o 14 6 1 587.16 548.26 59.31 o 16 6 1 269.53 329.23 61.75 o 18 6 1 39.18 27.30 126.00 o 20 6 1 81.75 16.00 126.10 o -21 7 1 5.06 8.24 136.71 o -19 7 1 27.44 70.94 134.66 o -17 7 1 174.81 92.41 87.25 o -15 7 1 352.07 364.30 51.95 o -13 7 1 8.87 24.33 43.52 o -11 7 1 3.30 0.00 36.24 o -9 7 1 0.01 0.36 24.30 o -7 7 1 1.63 7.28 30.33 o -5 7 1 2208.03 2023.08 36.23 o -3 7 1 990.90 903.61 26.24 o -1 7 1 245.05 269.72 25.10 o 1 7 1 341.58 313.40 30.70 o 3 7 1 72.62 112.93 25.05 o 5 7 1 13.66 15.33 20.42 o 7 7 1 3.56 20.67 33.95 o 9 7 1 133.39 104.31 27.64 o 11 7 1 14.48 6.07 38.47 o 13 7 1 582.15 661.81 50.30 o 15 7 1 287.12 334.92 118.20 o 17 7 1 71.95 122.41 120.59 o 19 7 1 73.79 2.02 128.75 o -20 8 1 268.24 312.72 118.54 o -18 8 1 36.35 53.71 114.66 o -16 8 1 246.04 250.82 111.64 o -14 8 1 86.83 88.54 67.27 o -12 8 1 54.70 71.25 31.79 o -10 8 1 90.42 99.61 55.78 o -8 8 1 101.67 75.42 32.20 o -6 8 1 557.81 510.29 35.89 o -4 8 1 426.63 418.15 34.40 o -2 8 1 1865.01 1745.08 32.23 o 0 8 1 4439.55 4346.39 68.01 o 2 8 1 1948.54 1958.66 43.12 o 4 8 1 463.88 451.76 27.24 o 6 8 1 6.70 14.93 30.53 o 8 8 1 884.77 944.70 56.15 o 10 8 1 2599.09 2447.31 83.38 o 12 8 1 3865.83 3973.62 117.04 o 14 8 1 207.44 232.72 104.75 o 16 8 1 12.42 36.48 104.88 o 18 8 1 39.98 3.99 109.95 o -19 9 1 114.55 155.76 116.46 o -17 9 1 538.21 508.45 118.42 o -15 9 1 1024.60 1178.37 125.94 o -13 9 1 471.84 547.47 74.74 o -11 9 1 49.46 81.33 56.04 o -9 9 1 126.21 137.01 38.84 o -7 9 1 230.24 242.80 40.21 o -5 9 1 963.90 1004.98 38.67 o -3 9 1 937.85 819.93 46.19 o -1 9 1 25.90 49.89 27.02 o 1 9 1 266.78 320.78 45.29 o 3 9 1 94.89 73.56 38.20 o 5 9 1 676.43 579.86 35.49 o 7 9 1 203.93 205.09 24.74 o 9 9 1 319.46 262.88 71.42 o 11 9 1 106.19 81.47 73.40 o 13 9 1 0.08 75.67 105.97 o 15 9 1 557.28 614.79 112.66 o 17 9 1 219.61 307.15 114.18 o -18 10 1 15.49 0.00 116.92 o -16 10 1 0.01 9.09 113.63 o -14 10 1 164.20 204.71 116.04 o -12 10 1 14.30 29.29 73.34 o -10 10 1 382.63 387.63 71.23 o -8 10 1 215.28 242.38 48.52 o -6 10 1 486.60 497.01 42.84 o -4 10 1 117.92 176.41 44.30 o -2 10 1 201.16 222.66 24.66 o 0 10 1 156.34 133.20 17.24 o 2 10 1 353.62 435.14 49.82 o 4 10 1 549.34 568.25 51.28 o 6 10 1 546.58 578.42 55.68 o 8 10 1 78.92 44.23 70.99 o 10 10 1 38.52 42.71 75.28 o 12 10 1 134.25 159.61 108.68 o 14 10 1 135.59 127.71 111.92 o 16 10 1 0.62 45.29 113.66 o -15 11 1 3.36 47.37 116.30 o -13 11 1 36.84 78.08 116.00 o -11 11 1 0.84 11.62 66.34 o -9 11 1 129.14 105.29 67.59 o -7 11 1 2.10 0.00 48.94 o -5 11 1 134.22 126.69 45.14 o -3 11 1 1117.02 1264.61 50.92 o -1 11 1 1213.17 1224.71 42.49 o 1 11 1 359.18 409.58 46.86 o 3 11 1 431.97 450.12 50.96 o 5 11 1 348.28 332.43 56.54 o 7 11 1 140.24 143.87 70.10 o 9 11 1 1.60 0.00 71.14 o 11 11 1 72.75 66.17 112.45 o 13 11 1 179.29 184.31 113.65 o 15 11 1 339.46 406.26 122.65 o -14 12 1 63.60 0.00 113.50 o -12 12 1 245.34 322.62 117.79 o -10 12 1 772.76 691.42 97.61 o -8 12 1 335.93 357.93 114.46 o -6 12 1 327.38 234.70 84.95 o -4 12 1 120.29 116.18 87.50 o -2 12 1 464.42 491.89 84.97 o 0 12 1 15.94 5.26 74.32 o 2 12 1 76.15 60.90 87.43 o 4 12 1 3.51 37.68 112.51 o 6 12 1 11.96 6.41 111.77 o 8 12 1 72.29 93.57 88.87 o 10 12 1 102.22 105.64 113.16 o 12 12 1 18.60 80.76 115.20 o -11 13 1 13.53 72.95 117.25 o -9 13 1 204.15 218.08 115.14 o -7 13 1 21.18 33.01 115.73 o -5 13 1 34.42 9.36 116.29 o -3 13 1 1.70 47.73 101.78 o -1 13 1 46.99 78.68 84.70 o 1 13 1 57.25 96.67 90.11 o 3 13 1 137.45 119.66 113.64 o 5 13 1 103.72 99.22 113.44 o 7 13 1 220.51 172.69 114.97 o 9 13 1 24.54 18.19 117.92 o -8 14 1 11.83 35.53 120.48 o -6 14 1 15.67 11.04 117.59 o -4 14 1 62.93 9.51 134.54 o -2 14 1 22.87 2.08 117.94 o 0 14 1 165.99 159.05 122.80 o 2 14 1 90.82 153.83 114.67 o 4 14 1 75.08 65.15 118.67 o 6 14 1 170.02 207.00 120.43 o -24 0 2 196.32 184.52 129.81 o -22 0 2 1381.90 1501.10 152.40 o -20 0 2 885.95 1006.22 112.33 o -18 0 2 1806.61 1588.15 99.27 o -16 0 2 145.68 168.50 85.41 o -14 0 2 1017.27 1209.05 85.59 o -12 0 2 21918.07 23343.24 240.87 o -10 0 2 2647.85 2375.05 72.41 o -8 0 2 310.37 400.17 46.14 o -6 0 2 5652.41 6335.50 59.31 o -4 0 2 2291.15 2536.44 28.12 o -2 0 2 367.64 391.45 58.04 o 0 0 2 9537.11 8905.57 76.63 o 2 0 2 5958.35 5322.62 51.03 o 4 0 2 2720.23 2461.47 52.52 o 6 0 2 817.07 1003.36 66.36 o 8 0 2 1.24 14.90 66.79 o 10 0 2 566.07 517.83 66.36 o 12 0 2 1923.43 2135.79 88.10 o 14 0 2 992.91 1004.89 87.21 o 16 0 2 484.94 514.07 97.98 o 18 0 2 785.96 854.59 133.88 o 20 0 2 130.33 131.60 181.41 o -25 1 2 31.32 0.00 111.67 o -23 1 2 393.09 435.65 95.33 o -21 1 2 2102.30 1830.79 101.96 o -19 1 2 753.76 765.06 63.10 o -17 1 2 30.52 27.98 57.48 o -15 1 2 382.74 318.29 57.04 o -13 1 2 2036.21 2098.55 59.99 o -11 1 2 3311.85 3443.06 51.93 o -9 1 2 740.98 761.47 35.32 o -7 1 2 631.76 640.20 29.76 o -5 1 2 74277.48 76278.95 395.02 o -3 1 2 13417.30 13210.00 81.49 o -1 1 2 323.11 241.33 12.09 o 1 1 2 19244.24 18212.75 66.40 o 3 1 2 468.15 475.95 28.15 o 5 1 2 1630.01 1551.44 42.26 o 7 1 2 826.29 806.03 50.14 o 9 1 2 113.00 118.12 42.08 o 11 1 2 14.71 23.34 48.16 o 13 1 2 88.29 78.98 52.35 o 15 1 2 118.02 143.18 58.01 o 17 1 2 40.48 80.84 87.70 o 19 1 2 2.40 28.42 103.18 o 21 1 2 125.45 212.13 106.04 o -24 2 2 75.80 47.12 135.85 o -22 2 2 266.28 284.79 104.61 o -20 2 2 10.07 0.42 66.10 o 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