#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:23:45 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180859 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/90/2019080.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2019080_Fobs loop_ _publ_author_name 'Wang, Ming-Feng' 'Yue, Cheng-Yang' 'Yuan, Zhuang-Dong' 'Lei, Xiao-Wu' _publ_section_title ; Two polymorphs of tris(ethylenediamine)cobalt(III) tetrathioantimonate(V) ; _journal_coeditor_code FG3290 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 855 _journal_page_last 858 _journal_volume 69 _journal_year 2013 _space_group_IT_number 106 _symmetry_space_group_name_Hall 'P 4c -2ab' _symmetry_space_group_name_H-M 'P 42 b c' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 15.4909 _cell_length_b 15.4909 _cell_length_c 13.6285 _exptl_crystal_F_000 1951.58 _reflns_d_resolution_high 0.7678 _cod_data_source_file fg3290IIsup3.hkl _cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P4(2)bc P42bc' _shelx_refln_list_code 4 _shelx_f_calc_maximum 596.55 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x, z+1/2' '-x, -y, z' 'y, -x, z+1/2' '-x+1/2, y+1/2, z' '-y+1/2, -x+1/2, z+1/2' 'x+1/2, -y+1/2, z' 'y+1/2, x+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 2 -17 10933.84 12038.94 550.86 o 1 2 -17 675.07 692.73 116.78 o 1 3 -17 731.46 748.60 117.56 o 2 3 -17 1141.94 1126.27 130.49 o 0 4 -17 602.78 538.19 177.13 o 1 4 -17 2570.42 2754.50 214.35 o 2 4 -17 5808.50 6193.20 294.06 o 3 4 -17 3499.89 2780.36 284.16 o 1 5 -17 90.32 -74.46 124.85 o 2 5 -17 956.52 1456.10 282.19 o 0 0 -16 1163.35 650.03 316.13 o 1 1 -16 596.95 594.53 145.56 o 0 2 -16 1013.00 1077.24 169.08 o 1 2 -16 229.37 125.77 87.07 o 2 2 -16 1131.16 1183.35 169.08 o 1 3 -16 26.58 -65.73 77.41 o 2 3 -16 135.16 107.65 123.95 o 3 3 -16 1275.89 1052.39 214.54 o 0 4 -16 89.14 90.67 120.93 o 1 4 -16 1205.10 1137.02 123.99 o 2 4 -16 111.16 118.86 90.53 o 3 4 -16 2312.34 2491.22 157.68 o 4 4 -16 1676.13 1657.57 234.68 o 1 5 -16 16.28 -78.11 78.11 o 2 5 -16 288.27 389.13 115.27 o 3 5 -16 360.97 285.34 105.90 o 4 5 -16 1531.75 1665.23 161.57 o 5 5 -16 147.79 47.31 158.75 o 0 6 -16 2858.14 2766.48 233.78 o 1 6 -16 557.93 535.18 154.27 o 2 6 -16 1333.12 1599.48 222.01 o 3 6 -16 873.35 1012.14 149.73 o 4 6 -16 954.93 1200.71 154.16 o 5 6 -16 168.13 274.41 135.02 o 6 6 -16 8635.10 9945.77 856.05 o 1 7 -16 184.17 281.11 119.19 o 2 7 -16 179.17 123.59 115.17 o 3 7 -16 64.46 119.83 119.63 o 4 7 -16 769.13 765.76 178.85 o 5 7 -16 61.48 -120.77 291.27 o 0 8 -16 1057.03 1399.51 365.86 o 1 8 -16 34.05 -154.68 290.98 o 2 8 -16 5272.19 5107.87 625.16 o 3 8 -16 52.22 -248.64 248.64 o 0 2 -15 20937.83 21303.87 489.13 o 1 2 -15 669.77 737.32 105.49 o 1 3 -15 321.92 284.54 90.45 o 2 3 -15 645.64 797.13 107.87 o 0 4 -15 44.08 191.70 120.57 o 1 4 -15 3507.73 3874.95 177.29 o 2 4 -15 11393.61 11570.23 350.91 o 3 4 -15 6715.17 6701.95 221.70 o 1 5 -15 48.18 58.26 79.45 o 2 5 -15 1405.82 1568.06 126.11 o 3 5 -15 421.65 430.57 102.73 o 4 5 -15 4591.25 5273.89 241.06 o 0 6 -15 4497.65 4514.01 268.88 o 1 6 -15 2443.24 2596.36 154.34 o 2 6 -15 6288.49 6769.30 245.99 o 3 6 -15 3486.02 3626.55 207.88 o 4 6 -15 1566.65 1554.04 149.85 o 5 6 -15 7432.48 8347.21 297.67 o 1 7 -15 125.19 196.61 106.41 o 2 7 -15 772.42 647.83 113.43 o 3 7 -15 166.95 312.65 114.10 o 4 7 -15 7302.49 6947.43 280.55 o 5 7 -15 130.67 193.19 110.89 o 6 7 -15 290.61 305.84 119.54 o 0 8 -15 9564.69 9593.95 406.50 o 1 8 -15 959.30 1017.23 134.13 o 2 8 -15 1923.17 2032.66 189.26 o 3 8 -15 1182.75 1129.10 172.55 o 4 8 -15 3506.49 3744.75 217.47 o 5 8 -15 296.70 443.63 120.43 o 6 8 -15 1657.67 1824.96 153.25 o 7 8 -15 2072.21 1962.59 223.73 o 1 9 -15 975.27 1057.55 159.00 o 2 9 -15 629.35 737.81 147.03 o 3 9 -15 6.24 34.72 123.52 o 4 9 -15 2425.05 2403.82 203.53 o 5 9 -15 1225.83 1267.55 169.89 o 0 10 -15 628.90 725.93 220.19 o 1 10 -15 55.15 -45.44 129.79 o 2 10 -15 7280.69 7564.06 382.98 o 3 10 -15 256.80 210.27 144.66 o 4 10 -15 724.83 497.29 319.69 o 0 0 -14 20994.47 19081.68 877.36 o 1 1 -14 174.26 179.75 113.31 o 0 2 -14 50.62 -92.32 92.32 o 1 2 -14 669.04 569.28 92.56 o 2 2 -14 8789.20 9109.34 352.73 o 1 3 -14 587.71 699.98 138.12 o 2 3 -14 2533.66 2620.84 143.35 o 3 3 -14 570.64 276.99 120.51 o 0 4 -14 1129.00 925.22 152.13 o 1 4 -14 5554.84 5597.10 198.32 o 2 4 -14 1451.57 1528.81 117.75 o 3 4 -14 3324.63 3182.14 156.33 o 4 4 -14 2560.35 2635.06 208.98 o 1 5 -14 754.68 712.66 99.18 o 2 5 -14 2164.88 2261.18 141.62 o 3 5 -14 458.43 507.29 95.98 o 4 5 -14 5314.11 5032.30 207.79 o 5 5 -14 736.91 377.18 309.62 o 0 6 -14 4741.00 4942.70 268.28 o 1 6 -14 183.88 176.38 83.11 o 2 6 -14 3118.71 3109.03 169.99 o 3 6 -14 3754.26 3489.22 178.15 o 4 6 -14 4545.61 4607.74 200.87 o 5 6 -14 1359.54 1227.21 115.29 o 6 6 -14 6934.98 6733.04 319.09 o 1 7 -14 867.44 890.44 114.96 o 2 7 -14 130.99 28.41 85.27 o 3 7 -14 188.48 14.18 85.07 o 4 7 -14 3314.76 3475.76 169.57 o 5 7 -14 40.69 -4.35 79.88 o 6 7 -14 1432.80 1342.70 121.04 o 7 7 -14 625.68 608.60 146.41 o 0 8 -14 4566.82 4625.84 423.39 o 1 8 -14 274.82 338.38 145.35 o 2 8 -14 9005.65 9089.78 229.21 o 3 8 -14 283.32 241.42 88.24 o 4 8 -14 3940.33 3688.80 173.47 o 5 8 -14 400.79 417.66 92.87 o 6 8 -14 101.46 51.85 95.86 o 7 8 -14 736.84 792.61 113.02 o 8 8 -14 6489.76 7204.66 304.02 o 1 9 -14 518.99 481.65 103.72 o 2 9 -14 955.60 1105.70 138.24 o 3 9 -14 7.10 -60.16 123.45 o 4 9 -14 1250.69 1228.12 121.05 o 5 9 -14 367.63 394.55 98.92 o 6 9 -14 386.96 275.46 88.51 o 7 9 -14 208.76 271.24 90.89 o 8 9 -14 408.76 338.25 103.57 o 0 10 -14 6717.03 7022.69 387.67 o 1 10 -14 1855.91 1851.61 162.47 o 2 10 -14 972.06 1119.29 125.45 o 3 10 -14 1411.26 1341.42 137.38 o 4 10 -14 3089.42 3268.63 184.58 o 5 10 -14 1568.80 1676.40 160.94 o 6 10 -14 4500.42 4546.46 205.39 o 7 10 -14 544.75 534.58 129.36 o 1 11 -14 902.07 615.70 117.43 o 2 11 -14 69.05 -97.29 97.29 o 3 11 -14 80.36 174.99 104.46 o 4 11 -14 2157.06 1994.76 156.34 o 5 11 -14 70.50 46.66 139.19 o 0 12 -14 427.85 274.79 208.06 o 1 12 -14 2908.93 2985.41 178.44 o 2 12 -14 2308.36 2371.92 167.53 o 3 12 -14 3866.46 4251.21 322.94 o 0 2 -13 23041.27 24089.91 480.35 o 1 2 -13 3600.67 3398.30 153.17 o 1 3 -13 1877.61 1861.70 119.42 o 2 3 -13 2122.53 2418.46 133.04 o 0 4 -13 5113.63 4808.12 253.11 o 1 4 -13 4905.64 4634.44 173.77 o 2 4 -13 5348.79 5556.99 189.75 o 3 4 -13 7101.86 7314.87 287.58 o 1 5 -13 97.09 87.62 76.92 o 2 5 -13 2718.13 2643.73 130.65 o 3 5 -13 142.07 141.85 67.14 o 4 5 -13 3405.55 3476.00 137.91 o 0 6 -13 6495.75 6289.67 305.05 o 1 6 -13 3589.32 3759.22 152.18 o 2 6 -13 7721.54 7800.03 175.57 o 3 6 -13 1078.64 1171.87 100.49 o 4 6 -13 8948.61 8872.38 213.68 o 5 6 -13 4160.19 4401.34 181.41 o 1 7 -13 335.43 330.44 83.72 o 2 7 -13 1423.68 1499.92 110.63 o 3 7 -13 438.77 486.43 85.06 o 4 7 -13 2569.57 2639.39 177.91 o 5 7 -13 718.00 660.47 97.51 o 6 7 -13 1497.26 1678.95 132.41 o 0 8 -13 11994.07 11959.72 348.87 o 1 8 -13 4107.56 4125.15 161.09 o 2 8 -13 278.97 236.09 90.21 o 3 8 -13 2418.60 2333.33 141.47 o 4 8 -13 4329.83 4731.92 187.98 o 5 8 -13 222.30 178.39 90.62 o 6 8 -13 6329.33 6072.56 213.72 o 7 8 -13 1009.25 969.77 112.70 o 1 9 -13 548.12 712.50 91.53 o 2 9 -13 854.20 756.04 108.08 o 3 9 -13 355.73 279.93 86.15 o 4 9 -13 1563.99 1795.01 131.02 o 5 9 -13 4.53 83.58 76.23 o 6 9 -13 2216.31 2067.71 130.03 o 7 9 -13 579.47 574.51 96.60 o 8 9 -13 790.66 666.55 92.86 o 0 10 -13 1169.81 1351.15 148.51 o 1 10 -13 534.23 359.65 82.97 o 2 10 -13 5054.44 5147.86 197.16 o 3 10 -13 1460.05 1622.70 124.86 o 4 10 -13 1427.52 1537.72 152.04 o 5 10 -13 57.34 -73.05 73.05 o 6 10 -13 1042.47 1099.86 111.14 o 7 10 -13 643.97 735.90 96.03 o 8 10 -13 6574.05 6769.75 275.57 o 9 10 -13 2633.71 2708.86 196.62 o 1 11 -13 1449.61 1357.19 112.81 o 2 11 -13 686.29 612.24 100.72 o 3 11 -13 128.12 130.74 82.40 o 4 11 -13 2576.97 2507.24 153.05 o 5 11 -13 5.21 -55.91 79.98 o 6 11 -13 1341.53 1488.54 139.17 o 7 11 -13 108.04 -64.73 84.16 o 8 11 -13 291.68 94.82 162.37 o 0 12 -13 3261.29 3613.72 405.03 o 1 12 -13 5671.46 5665.62 200.34 o 2 12 -13 956.33 738.65 107.82 o 3 12 -13 1089.55 1183.86 125.36 o 4 12 -13 939.53 875.12 113.58 o 5 12 -13 2583.20 2798.47 179.06 o 6 12 -13 2393.61 2623.62 233.71 o 1 13 -13 621.66 732.94 110.05 o 2 13 -13 529.96 456.17 101.80 o 3 13 -13 281.99 246.46 112.43 o 4 13 -13 1699.31 1738.47 166.24 o 0 0 -12 97391.44 89480.00 2149.00 o 1 1 -12 1653.01 1747.55 165.31 o 0 2 -12 5043.28 4858.27 238.17 o 1 2 -12 5681.15 5647.92 204.75 o 2 2 -12 32585.61 32588.54 549.46 o 1 3 -12 969.37 1011.23 97.12 o 2 3 -12 7703.66 7353.29 159.02 o 3 3 -12 1369.85 1529.98 137.48 o 0 4 -12 16784.56 16087.59 372.87 o 1 4 -12 8779.81 8619.00 172.57 o 2 4 -12 2254.79 2168.37 106.33 o 3 4 -12 7970.86 8061.34 168.37 o 4 4 -12 1371.64 1472.30 151.85 o 1 5 -12 568.24 671.71 71.53 o 2 5 -12 5297.91 5450.88 152.11 o 3 5 -12 528.93 567.68 76.48 o 4 5 -12 8931.54 9084.63 181.01 o 5 5 -12 2259.16 2023.39 178.19 o 0 6 -12 8929.40 8327.90 219.22 o 1 6 -12 1899.75 1993.86 100.06 o 2 6 -12 3761.11 3755.94 130.67 o 3 6 -12 10203.93 10492.86 204.65 o 4 6 -12 3214.30 3291.76 139.11 o 5 6 -12 4732.64 4685.70 177.03 o 6 6 -12 2983.50 3215.99 218.16 o 1 7 -12 1195.65 1235.91 83.31 o 2 7 -12 2134.72 2123.51 111.10 o 3 7 -12 17.53 41.13 60.78 o 4 7 -12 4981.15 4748.17 182.75 o 5 7 -12 238.91 86.90 77.95 o 6 7 -12 6262.39 6480.17 204.81 o 7 7 -12 1062.73 1069.76 152.19 o 0 8 -12 5929.56 6004.48 365.00 o 1 8 -12 1072.43 1057.76 84.39 o 2 8 -12 14885.23 15280.39 225.26 o 3 8 -12 887.27 1064.53 97.05 o 4 8 -12 2180.27 2348.93 127.13 o 5 8 -12 5270.18 5202.52 191.00 o 6 8 -12 1928.69 1664.82 123.71 o 7 8 -12 450.70 434.22 100.99 o 8 8 -12 13717.83 13544.94 456.89 o 1 9 -12 1116.76 1250.69 95.12 o 2 9 -12 1323.10 1318.57 117.93 o 3 9 -12 178.84 127.93 73.02 o 4 9 -12 3146.13 3263.81 138.40 o 5 9 -12 135.68 142.02 71.33 o 6 9 -12 2787.63 2660.44 140.48 o 7 9 -12 424.68 324.13 77.76 o 8 9 -12 1474.06 1463.85 108.53 o 9 9 -12 800.84 767.32 183.03 o 0 10 -12 16836.70 16859.09 391.89 o 1 10 -12 883.48 924.23 90.61 o 2 10 -12 1456.98 1513.80 129.42 o 3 10 -12 2060.05 2191.34 126.57 o 4 10 -12 5690.57 5907.59 190.49 o 5 10 -12 2186.27 2300.24 127.66 o 6 10 -12 2053.90 1922.78 118.54 o 7 10 -12 823.53 870.86 96.34 o 8 10 -12 405.11 263.26 88.56 o 9 10 -12 1292.21 1467.60 130.03 o 10 10 -12 5458.38 5385.97 462.45 o 1 11 -12 1071.60 1262.29 121.17 o 2 11 -12 481.07 572.50 88.97 o 3 11 -12 334.08 349.15 83.88 o 4 11 -12 3105.85 3146.66 158.88 o 5 11 -12 272.34 253.94 82.95 o 6 11 -12 4254.48 4263.95 163.39 o 7 11 -12 320.75 258.71 80.23 o 8 11 -12 984.16 846.25 114.37 o 9 11 -12 143.96 166.07 95.21 o 10 11 -12 382.35 81.52 291.27 o 0 12 -12 710.96 859.61 131.61 o 1 12 -12 402.72 353.43 85.27 o 2 12 -12 5721.71 5887.04 197.94 o 3 12 -12 1613.61 1737.69 154.44 o 4 12 -12 69.86 58.29 80.31 o 5 12 -12 428.15 285.53 91.19 o 6 12 -12 11.74 96.55 78.86 o 7 12 -12 1657.09 1685.34 138.53 o 8 12 -12 2959.53 3032.25 216.92 o 1 13 -12 1352.18 1273.62 110.72 o 2 13 -12 1224.93 1170.66 109.19 o 3 13 -12 429.66 350.27 96.26 o 4 13 -12 2153.95 2004.98 141.90 o 5 13 -12 110.04 95.89 86.52 o 6 13 -12 4064.52 3704.90 253.62 o 7 13 -12 93.21 94.74 172.40 o 0 14 -12 2570.12 2395.27 216.47 o 1 14 -12 1658.06 1582.68 142.29 o 2 14 -12 1768.61 1554.82 133.21 o 3 14 -12 1213.40 1074.64 121.01 o 4 14 -12 185.70 133.31 99.75 o 5 14 -12 2868.81 2646.29 468.87 o 0 2 -11 2242.44 2607.10 154.50 o 1 2 -11 2356.41 2398.67 102.08 o 1 3 -11 550.97 646.83 65.52 o 2 3 -11 1681.14 1742.42 93.90 o 0 4 -11 18896.30 18121.90 296.88 o 1 4 -11 934.20 902.20 70.28 o 2 4 -11 899.70 920.78 72.78 o 3 4 -11 5781.22 6049.45 150.37 o 1 5 -11 529.74 589.07 63.21 o 2 5 -11 6912.42 6840.78 135.61 o 3 5 -11 327.96 151.93 66.15 o 4 5 -11 1341.63 1510.03 111.15 o 0 6 -11 65.17 38.16 73.77 o 1 6 -11 2848.10 2829.39 103.78 o 2 6 -11 8591.80 8458.63 150.50 o 3 6 -11 2318.08 2474.36 136.47 o 4 6 -11 7205.87 7276.76 160.89 o 5 6 -11 4565.95 4475.38 154.06 o 1 7 -11 107.22 111.30 52.93 o 2 7 -11 1854.62 1921.06 99.14 o 3 7 -11 1549.30 1701.55 92.21 o 4 7 -11 1900.22 1968.66 110.29 o 5 7 -11 294.28 194.55 67.54 o 6 7 -11 2380.22 2139.90 119.23 o 0 8 -11 29168.85 28977.71 424.67 o 1 8 -11 288.04 258.63 63.61 o 2 8 -11 6581.69 6490.54 151.49 o 3 8 -11 95.43 35.96 57.46 o 4 8 -11 8356.31 8140.08 174.23 o 5 8 -11 172.59 117.77 68.46 o 6 8 -11 13059.99 12574.13 245.37 o 7 8 -11 279.51 276.35 71.13 o 1 9 -11 75.51 67.33 61.57 o 2 9 -11 2553.71 2518.28 111.12 o 3 9 -11 510.81 660.48 74.51 o 4 9 -11 2309.87 2351.73 111.81 o 5 9 -11 1091.74 1095.87 87.34 o 6 9 -11 456.11 381.17 76.43 o 7 9 -11 1391.05 1508.07 106.31 o 8 9 -11 984.81 1031.07 90.71 o 0 10 -11 176.46 292.79 97.84 o 1 10 -11 5745.22 5979.41 172.12 o 2 10 -11 4792.11 5245.75 174.47 o 3 10 -11 7501.62 7844.00 179.40 o 4 10 -11 7060.23 7426.49 166.12 o 5 10 -11 1847.50 1749.33 103.11 o 6 10 -11 496.00 631.58 106.05 o 7 10 -11 4903.14 5031.78 170.50 o 8 10 -11 13877.58 13580.81 258.45 o 9 10 -11 5027.47 5281.74 215.26 o 1 11 -11 15.88 85.42 66.62 o 2 11 -11 2043.94 1966.74 119.74 o 3 11 -11 206.64 190.57 80.60 o 4 11 -11 426.53 492.09 85.03 o 5 11 -11 1376.93 1419.53 111.54 o 6 11 -11 1679.86 1865.94 115.52 o 7 11 -11 401.95 308.44 82.71 o 8 11 -11 742.95 939.35 106.75 o 9 11 -11 1374.56 1505.04 126.27 o 10 11 -11 928.01 963.19 148.79 o 0 12 -11 1179.22 1372.13 149.08 o 1 12 -11 6939.41 7777.53 201.69 o 2 12 -11 690.85 674.18 91.65 o 3 12 -11 2391.31 2275.46 137.61 o 4 12 -11 1075.07 989.14 116.34 o 5 12 -11 6859.45 6815.72 203.69 o 6 12 -11 3219.64 3170.03 151.10 o 7 12 -11 4549.65 4405.45 202.85 o 8 12 -11 1404.96 1047.09 118.39 o 9 12 -11 3159.46 3320.83 176.67 o 10 12 -11 2599.48 2309.70 264.04 o 1 13 -11 268.81 205.14 79.74 o 2 13 -11 996.73 1037.48 119.92 o 3 13 -11 1.92 7.03 102.13 o 4 13 -11 1480.22 1777.64 130.08 o 5 13 -11 606.87 501.16 96.65 o 6 13 -11 16.30 -17.77 76.75 o 7 13 -11 292.90 152.25 89.56 o 8 13 -11 357.42 392.66 112.31 o 9 13 -11 792.08 507.94 341.00 o 0 14 -11 919.92 683.09 174.63 o 1 14 -11 4409.55 4544.08 191.73 o 2 14 -11 646.11 797.76 115.14 o 3 14 -11 6415.06 7037.84 229.65 o 4 14 -11 24.58 -89.95 89.95 o 5 14 -11 1946.48 1984.35 158.09 o 6 14 -11 2528.63 2826.17 177.77 o 7 14 -11 4297.07 4441.41 324.60 o 1 15 -11 199.96 68.52 107.04 o 2 15 -11 777.40 705.34 110.09 o 3 15 -11 59.50 -4.10 90.28 o 4 15 -11 467.93 608.88 135.13 o 5 15 -11 72.64 -57.80 177.37 o 0 0 -10 136793.91 131380.11 2735.09 o 1 1 -10 1211.74 1174.77 91.84 o 0 2 -10 2173.99 2083.48 114.04 o 1 2 -10 9358.86 9239.90 142.75 o 2 2 -10 57885.05 56791.25 569.26 o 1 3 -10 667.12 571.29 64.41 o 2 3 -10 5782.18 5857.10 118.94 o 3 3 -10 1024.73 1008.05 94.39 o 0 4 -10 54145.99 53211.34 555.23 o 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3415.96 3117.16 160.99 o 10 16 -1 337.89 284.74 83.05 o 11 16 -1 3334.41 3894.53 189.43 o 12 16 -1 3471.54 3118.90 352.56 o 1 17 -1 156.14 168.00 74.59 o 2 17 -1 377.35 238.68 83.56 o 3 17 -1 498.00 576.10 89.02 o 4 17 -1 892.03 692.42 90.53 o 5 17 -1 1065.53 1057.18 99.82 o 6 17 -1 120.77 209.38 99.89 o 7 17 -1 395.62 299.85 81.18 o 8 17 -1 148.68 137.92 90.91 o 9 17 -1 3398.28 3853.87 206.95 o 10 17 -1 2976.04 3069.63 202.05 o 0 18 -1 10722.52 9953.04 331.11 o 1 18 -1 477.97 488.77 94.06 o 2 18 -1 3289.36 3565.26 179.63 o 3 18 -1 353.71 137.66 93.31 o 4 18 -1 8349.54 8340.41 224.86 o 5 18 -1 2762.61 3134.62 153.08 o 6 18 -1 9052.69 9146.58 223.48 o 7 18 -1 399.56 238.92 95.64 o 8 18 -1 38.21 60.35 93.78 o 9 18 -1 286.72 264.27 219.50 o 1 19 -1 477.86 533.32 101.30 o 2 19 -1 449.06 428.70 100.07 o 3 19 -1 165.84 90.41 88.65 o 4 19 -1 882.03 872.14 116.02 o 5 19 -1 49.74 21.38 95.54 o 6 19 -1 397.69 249.84 114.13 o 0 20 -1 690.74 787.45 183.20 o 1 20 -1 765.60 701.42 141.25 o 2 20 -1 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5033.01 5031.98 68.67 o 3 8 1 6811.73 6762.29 98.19 o 4 8 1 49430.97 49341.59 281.94 o 5 8 1 609.49 663.04 40.48 o 6 8 1 37539.59 35944.72 253.97 o 7 8 1 2183.40 2196.06 80.49 o 1 9 1 559.74 573.85 36.30 o 2 9 1 4810.90 4789.91 73.06 o 3 9 1 287.11 352.41 34.68 o 4 9 1 1933.82 1904.73 56.11 o 5 9 1 1303.60 1338.50 53.58 o 6 9 1 666.95 709.50 56.09 o 7 9 1 2595.14 2689.63 91.14 o 8 9 1 816.33 972.05 65.23 o 0 10 1 5670.90 5466.42 135.48 o 1 10 1 19547.74 19167.02 153.66 o 2 10 1 22412.07 22489.31 177.25 o 3 10 1 14028.97 13824.52 143.10 o 4 10 1 15365.51 15476.40 150.19 o 5 10 1 2490.74 2403.15 79.62 o 6 10 1 2332.98 2316.07 86.60 o 7 10 1 9198.13 9389.79 148.57 o 8 10 1 34637.59 34045.15 303.44 o 9 10 1 16723.78 16969.45 208.93 o 1 11 1 275.08 299.75 39.99 o 2 11 1 3889.28 4109.23 86.51 o 3 11 1 2013.47 2204.86 74.22 o 4 11 1 2463.17 2499.24 83.62 o 5 11 1 2483.30 2417.95 93.94 o 6 11 1 5309.99 5194.99 118.29 o 7 11 1 1367.29 1407.90 82.56 o 8 11 1 155.73 177.05 52.83 o 9 11 1 2251.17 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315.92 384.73 90.89 o 11 16 1 3427.45 3701.67 183.82 o 12 16 1 3205.64 3087.57 282.42 o 1 17 1 177.53 79.53 70.03 o 2 17 1 323.59 228.92 72.84 o 3 17 1 552.53 562.95 97.67 o 4 17 1 912.49 811.72 99.20 o 5 17 1 978.16 938.49 103.20 o 6 17 1 116.70 -4.66 78.05 o 7 17 1 365.86 362.69 94.73 o 8 17 1 120.00 89.99 86.36 o 9 17 1 3643.07 3786.73 195.34 o 10 17 1 2839.05 3190.74 203.10 o 0 18 1 10769.14 11791.94 409.87 o 1 18 1 498.42 391.51 84.25 o 2 18 1 3304.61 3557.22 177.38 o 3 18 1 431.32 378.39 87.37 o 4 18 1 8503.14 8610.95 224.42 o 5 18 1 2939.71 2950.64 170.41 o 6 18 1 9005.94 8959.29 250.66 o 7 18 1 404.85 311.89 101.11 o 8 18 1 41.95 46.91 93.70 o 9 18 1 318.81 245.09 323.24 o 1 19 1 459.40 336.33 99.83 o 2 19 1 399.69 625.72 106.51 o 3 19 1 198.26 136.22 87.05 o 4 19 1 977.26 984.30 142.09 o 5 19 1 39.57 -54.90 86.91 o 6 19 1 406.39 354.53 128.01 o 0 20 1 826.20 1051.41 326.79 o 1 20 1 779.05 1098.29 236.15 o 2 20 1 1145.31 1186.63 199.21 o 1 1 2 22.82 -15.68 15.68 o 0 2 2 477.27 462.75 25.52 o 1 2 2 17695.27 18208.60 94.87 o 2 2 2 156958.33 161138.88 973.35 o 1 3 2 2886.11 2992.13 39.00 o 2 3 2 19572.74 19793.17 106.97 o 3 3 2 14044.67 15414.17 156.45 o 0 4 2 91798.87 97711.05 561.69 o 1 4 2 42916.93 43426.84 208.31 o 2 4 2 16058.40 16071.99 110.19 o 3 4 2 28554.76 29171.48 182.09 o 4 4 2 12966.85 12604.19 174.31 o 1 5 2 2469.40 2483.19 43.74 o 2 5 2 16071.25 16701.65 111.18 o 3 5 2 2275.37 2282.29 50.99 o 4 5 2 30438.55 30744.38 199.24 o 5 5 2 3073.18 3174.50 79.45 o 0 6 2 26506.80 25838.67 205.50 o 1 6 2 9706.97 9923.63 82.39 o 2 6 2 11354.41 11538.88 96.73 o 3 6 2 38946.35 39395.94 216.13 o 4 6 2 14093.39 13743.26 123.25 o 5 6 2 22738.31 22882.37 171.30 o 6 6 2 13629.76 13453.98 202.15 o 1 7 2 6167.52 6164.51 73.75 o 2 7 2 8063.79 7843.83 83.67 o 3 7 2 1268.69 1470.56 60.73 o 4 7 2 18259.18 18098.57 147.32 o 5 7 2 4562.31 4626.54 77.51 o 6 7 2 16808.24 17193.06 150.61 o 7 7 2 1029.99 951.60 77.85 o 0 8 2 13691.69 13022.70 150.81 o 1 8 2 13432.74 13136.90 108.66 o 2 8 2 67778.75 67099.13 344.16 o 3 8 2 2034.91 2076.23 54.05 o 4 8 2 25024.89 24708.09 173.38 o 5 8 2 20190.77 20329.41 166.71 o 6 8 2 5202.46 5121.58 94.40 o 7 8 2 1909.67 1873.45 73.64 o 8 8 2 33803.49 34973.51 452.75 o 1 9 2 1127.22 1216.30 44.35 o 2 9 2 7659.80 7836.68 93.69 o 3 9 2 4599.70 4731.04 75.38 o 4 9 2 12787.83 12517.91 130.13 o 5 9 2 576.92 507.32 42.48 o 6 9 2 10141.34 9502.56 131.33 o 7 9 2 378.36 393.42 52.31 o 8 9 2 1462.77 1433.51 81.38 o 9 9 2 3648.53 3672.89 225.56 o 0 10 2 62005.30 62152.31 467.32 o 1 10 2 12714.35 12565.59 116.38 o 2 10 2 6617.77 6506.54 90.94 o 3 10 2 14577.82 14182.42 139.51 o 4 10 2 19050.52 18457.21 167.64 o 5 10 2 7935.60 7714.02 136.75 o 6 10 2 14090.09 14169.40 177.10 o 7 10 2 6842.82 6825.88 128.78 o 8 10 2 1302.84 1478.18 78.77 o 9 10 2 5659.59 5672.71 135.89 o 10 10 2 14769.63 14238.61 331.57 o 1 11 2 1265.03 1318.45 54.31 o 2 11 2 4871.29 5020.85 91.98 o 3 11 2 822.62 820.32 51.58 o 4 11 2 16701.18 16426.94 171.54 o 5 11 2 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5 940.72 866.00 112.79 o 10 15 5 228.89 210.66 75.33 o 11 15 5 445.64 337.93 84.47 o 12 15 5 1211.03 1752.17 202.29 o 0 16 5 2365.21 2555.17 170.23 o 1 16 5 512.74 470.69 79.31 o 2 16 5 10515.55 10355.28 227.76 o 3 16 5 1778.82 1952.50 117.90 o 4 16 5 137.94 71.75 93.24 o 5 16 5 1193.91 1197.28 109.27 o 6 16 5 316.80 379.90 80.82 o 7 16 5 1669.84 1930.05 125.68 o 8 16 5 1801.79 1772.53 121.12 o 9 16 5 8.87 -24.55 73.44 o 10 16 5 98.07 123.50 83.08 o 1 17 5 2282.29 2269.99 134.71 o 2 17 5 1888.25 2170.73 148.02 o 3 17 5 1709.51 1540.88 130.26 o 4 17 5 2551.01 2778.77 148.95 o 5 17 5 61.80 -5.59 72.84 o 6 17 5 1155.22 1151.45 123.80 o 7 17 5 394.21 331.36 106.63 o 8 17 5 634.22 707.38 120.70 o 9 17 5 3237.02 3228.99 221.64 o 0 18 5 8485.67 8812.77 378.92 o 1 18 5 964.59 899.40 112.88 o 2 18 5 821.72 561.90 109.72 o 3 18 5 477.14 380.32 106.75 o 4 18 5 3315.58 3736.59 206.76 o 5 18 5 3767.38 3749.05 191.53 o 6 18 5 970.21 856.39 122.11 o 7 18 5 1050.15 589.76 223.16 o 1 19 5 1729.49 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12 8 8351.80 8794.62 193.70 o 3 12 8 10446.09 10555.71 185.87 o 4 12 8 504.50 467.45 66.72 o 5 12 8 946.39 911.87 78.42 o 6 12 8 612.04 696.86 76.79 o 7 12 8 5309.14 5373.25 169.12 o 8 12 8 5538.95 5520.70 200.23 o 9 12 8 2998.09 2819.05 151.24 o 10 12 8 1224.27 1124.25 112.85 o 11 12 8 1202.28 979.15 108.26 o 12 12 8 2324.63 2661.98 247.63 o 1 13 8 1069.40 1142.28 83.21 o 2 13 8 719.99 830.05 80.13 o 3 13 8 431.91 364.29 80.32 o 4 13 8 1835.49 1840.28 106.37 o 5 13 8 910.91 921.34 82.87 o 6 13 8 5145.25 4874.98 162.69 o 7 13 8 78.39 -7.26 65.60 o 8 13 8 371.04 423.80 87.75 o 9 13 8 415.79 518.92 93.45 o 10 13 8 393.32 370.92 88.55 o 11 13 8 544.21 400.15 95.99 o 12 13 8 3490.62 3407.05 230.86 o 0 14 8 4784.42 4553.20 303.41 o 1 14 8 4949.34 5044.29 164.52 o 2 14 8 6333.03 6187.13 177.84 o 3 14 8 2637.79 2700.01 132.92 o 4 14 8 182.93 123.78 67.69 o 5 14 8 4807.73 5010.97 177.48 o 6 14 8 271.14 209.96 76.67 o 7 14 8 3935.86 3906.21 164.78 o 8 14 8 4139.43 4179.00 233.77 o 9 14 8 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4315.76 564.78 o 0 2 15 22076.32 22742.37 575.16 o 1 2 15 757.93 748.66 94.81 o 1 3 15 312.97 291.34 81.84 o 2 3 15 640.27 609.12 84.71 o 0 4 15 85.12 146.95 119.48 o 1 4 15 3714.30 3683.00 152.57 o 2 4 15 11326.05 12193.77 270.92 o 3 4 15 6678.39 6593.94 217.74 o 1 5 15 65.96 -15.77 68.82 o 2 5 15 1482.62 1556.40 117.69 o 3 5 15 398.17 302.90 81.03 o 4 5 15 4655.96 4695.18 177.53 o 0 6 15 4429.11 4700.47 423.89 o 1 6 15 2421.16 2331.58 148.03 o 2 6 15 6227.73 6331.63 208.52 o 3 6 15 3429.00 3669.57 159.45 o 4 6 15 1382.41 1474.38 132.41 o 5 6 15 7364.06 7579.87 228.43 o 1 7 15 137.16 111.20 92.72 o 2 7 15 795.07 758.05 97.67 o 3 7 15 170.00 189.48 73.20 o 4 7 15 7198.37 7620.69 216.01 o 5 7 15 122.56 73.89 75.99 o 6 7 15 375.88 205.04 73.46 o 0 8 15 9354.85 9387.09 388.78 o 1 8 15 837.60 947.78 122.91 o 2 8 15 2024.73 2019.17 146.02 o 3 8 15 1375.79 1520.02 123.44 o 4 8 15 3490.29 3728.48 166.88 o 5 8 15 302.82 314.00 85.93 o 6 8 15 1587.12 1617.76 125.95 o 7 8 15 2033.52 2106.46 156.75 o 1 9 15 965.16 871.55 128.67 o 2 9 15 598.24 578.36 106.34 o 3 9 15 14.52 127.33 94.40 o 4 9 15 2429.94 2218.53 149.69 o 5 9 15 1197.63 1319.00 141.76 o 0 10 15 623.29 242.19 179.38 o 1 10 15 36.30 179.41 116.65 o 2 10 15 7329.48 7172.63 409.64 o 3 10 15 313.40 499.99 161.91 o 4 10 15 624.84 397.83 294.82 o 0 0 16 1184.93 1395.96 341.00 o 1 1 16 607.65 709.41 138.45 o 0 2 16 1051.66 1050.54 150.69 o 1 2 16 267.52 294.88 80.37 o 2 2 16 1170.54 1349.36 203.54 o 1 3 16 25.24 -63.21 68.81 o 2 3 16 195.77 74.03 87.81 o 3 3 16 1304.65 1482.34 203.03 o 0 4 16 69.85 113.35 149.28 o 1 4 16 1197.50 1243.49 131.92 o 2 4 16 161.03 16.28 83.10 o 3 4 16 2253.22 2247.90 164.46 o 4 4 16 1627.69 1964.09 191.43 o 1 5 16 15.99 -22.63 85.88 o 2 5 16 263.57 379.65 92.75 o 3 5 16 376.59 469.67 99.18 o 4 5 16 1474.91 1603.23 130.38 o 5 5 16 150.49 103.98 115.13 o 0 6 16 2843.80 2930.69 264.89 o 1 6 16 558.85 474.47 109.76 o 2 6 16 1233.21 1327.41 154.36 o 3 6 16 864.69 825.57 104.38 o 4 6 16 920.07 848.60 107.99 o 5 6 16 175.67 216.05 92.73 o 6 6 16 8330.21 8958.29 393.68 o 1 7 16 196.33 334.51 103.46 o 2 7 16 214.61 236.84 103.20 o 3 7 16 51.45 -44.34 85.10 o 4 7 16 726.64 949.33 119.68 o 5 7 16 60.95 128.16 110.93 o 0 8 16 1060.39 845.39 326.79 o 1 8 16 25.09 143.74 169.74 o 2 8 16 5217.62 5389.24 430.62 o 3 8 16 39.00 165.87 167.86 o 0 2 17 10107.36 11491.08 369.27 o 1 2 17 652.05 742.62 101.58 o 1 3 17 673.53 723.36 123.82 o 2 3 17 1121.14 1181.19 137.71 o 0 4 17 623.30 374.38 232.66 o 1 4 17 2499.39 2532.38 181.15 o 2 4 17 5699.90 6065.51 260.99 o 3 4 17 3321.44 3587.41 252.89 o 1 5 17 114.72 19.11 191.54 o 2 5 17 1013.67 927.44 190.13 o