#------------------------------------------------------------------------------ #$Date: 2013-10-24 17:51:33 +0300 (Thu, 24 Oct 2013) $ #$Revision: 89414 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/90/2019085.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2019085_Fobs loop_ _publ_author_name 'G\"orbitz, Carl Henrik' 'Yadav, Vitthal N.' _publ_section_title ; An unexpected tetragonal unit cell for N-(L-2-aminobutyryl)-L-serine ; _journal_coeditor_code QS3026 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 888 _journal_page_last 891 _journal_volume 69 _journal_year 2013 _space_group_IT_number 79 _symmetry_space_group_name_Hall 'I 4' _symmetry_space_group_name_H-M 'I 4' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 18.3346 _cell_length_b 18.3346 _cell_length_c 5.1408 _exptl_crystal_F_000 816.00 _reflns_d_resolution_high 0.8373 _[local]_cod_data_source_file qs3026Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' vnybaslt in I4' _shelx_refln_list_code 4 _shelx_f_calc_maximum 158.91 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' '-y, x, z' 'y, -x, z' 'x+1/2, y+1/2, z+1/2' '-x+1/2, -y+1/2, z+1/2' '-y+1/2, x+1/2, z+1/2' 'y+1/2, -x+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 2 0 3002.73 2794.99 154.44 o 2 2 0 5640.38 5234.11 235.68 o -1 3 0 7.93 29.19 5.44 o 1 3 0 309.89 200.80 12.12 o 3 3 0 2923.11 2297.63 103.90 o -2 4 0 16702.51 16760.81 751.96 o 0 4 0 456.22 502.80 23.77 o 2 4 0 533.87 323.15 28.94 o 4 4 0 8533.43 8957.44 402.81 o -3 5 0 130.87 89.52 10.27 o -1 5 0 1111.34 902.93 61.57 o 1 5 0 1579.04 1764.45 155.41 o 3 5 0 3659.81 2854.43 128.44 o 5 5 0 27.54 17.69 6.96 o -4 6 0 11715.42 11543.45 517.42 o -2 6 0 708.91 768.65 52.58 o 0 6 0 25252.60 27542.72 1234.83 o 2 6 0 7024.92 7251.42 358.16 o 4 6 0 628.67 607.24 37.78 o 6 6 0 3083.50 2826.17 128.49 o -5 7 0 133.01 220.23 19.42 o -3 7 0 4303.08 4312.32 193.54 o -1 7 0 11.35 24.44 7.18 o 1 7 0 2202.58 2199.32 125.45 o 3 7 0 2174.07 2241.81 112.01 o 5 7 0 1201.87 1062.80 70.49 o 7 7 0 3144.29 2937.38 133.44 o -6 8 0 737.17 775.50 37.13 o -4 8 0 537.28 527.43 33.93 o -2 8 0 2068.65 1633.01 74.93 o 0 8 0 1090.01 1186.24 59.11 o 2 8 0 63.81 93.58 8.91 o 4 8 0 11.17 84.68 8.64 o 6 8 0 4104.35 3844.11 191.37 o 8 8 0 1249.07 1252.74 70.49 o -7 9 0 242.70 218.26 14.77 o -5 9 0 543.27 592.96 52.19 o -3 9 0 288.70 309.96 17.11 o -1 9 0 980.89 885.10 41.88 o 1 9 0 446.36 349.05 35.87 o 3 9 0 424.90 399.49 28.02 o 5 9 0 750.60 720.89 35.05 o 7 9 0 342.74 353.29 24.15 o 9 9 0 628.85 716.80 42.66 o -8 10 0 123.29 154.76 19.21 o -6 10 0 0.01 2.50 8.61 o -4 10 0 2092.54 2041.16 93.80 o -2 10 0 3418.67 3215.41 146.16 o 0 10 0 385.97 373.71 25.79 o 2 10 0 104.63 69.60 9.02 o 4 10 0 277.04 313.92 17.22 o 6 10 0 185.71 171.96 12.53 o 8 10 0 1319.49 1428.38 65.99 o 10 10 0 63.28 32.09 12.88 o -9 11 0 616.03 614.23 50.28 o -7 11 0 69.42 132.45 25.05 o -5 11 0 2315.01 2024.12 93.51 o -3 11 0 3825.42 3829.87 173.13 o -1 11 0 47.91 70.53 9.36 o 1 11 0 95.65 121.94 11.53 o 3 11 0 458.83 400.56 23.92 o 5 11 0 434.92 442.04 23.18 o 7 11 0 681.52 603.06 43.34 o 9 11 0 145.99 141.34 19.39 o 11 11 0 54.10 64.77 16.79 o -10 12 0 550.44 676.93 49.44 o -8 12 0 682.60 679.96 82.30 o -6 12 0 34.78 70.27 11.27 o -4 12 0 184.86 142.27 11.98 o -2 12 0 1471.83 1382.72 64.78 o 0 12 0 599.08 572.06 28.88 o 2 12 0 43.95 52.20 14.79 o 4 12 0 2042.33 1966.88 99.89 o 6 12 0 1966.18 1893.37 99.73 o 8 12 0 574.85 599.24 38.62 o 10 12 0 103.00 82.25 29.65 o 12 12 0 3.46 18.96 14.17 o -11 13 0 232.01 166.20 22.02 o -9 13 0 1052.74 923.43 95.22 o -7 13 0 2.83 40.09 13.30 o -5 13 0 117.62 137.84 17.71 o -3 13 0 309.34 293.08 29.73 o -1 13 0 1.46 5.77 9.24 o 1 13 0 906.64 862.90 42.07 o 3 13 0 49.80 94.39 17.29 o 5 13 0 1.21 98.55 11.74 o 7 13 0 191.59 146.54 15.07 o 9 13 0 144.22 180.00 20.12 o 11 13 0 156.28 195.35 23.56 o 13 13 0 35.41 43.20 18.77 o -12 14 0 12.64 25.60 18.72 o -10 14 0 32.87 15.41 27.72 o -8 14 0 929.47 901.31 55.13 o -6 14 0 165.63 233.66 28.76 o -4 14 0 13.33 26.71 19.28 o -2 14 0 3.00 8.04 10.70 o 0 14 0 223.64 215.53 15.34 o 2 14 0 471.29 437.97 24.24 o 4 14 0 58.79 33.10 10.87 o 6 14 0 676.31 543.99 31.93 o 8 14 0 2094.55 1969.30 113.57 o 10 14 0 2.95 47.70 18.79 o 12 14 0 153.54 174.48 29.31 o 14 14 0 274.39 278.85 29.50 o -13 15 0 24.44 21.16 20.22 o -11 15 0 22.86 25.89 18.70 o -9 15 0 119.34 89.77 19.10 o -7 15 0 254.93 253.05 21.74 o -5 15 0 657.10 608.64 38.93 o -3 15 0 43.10 43.68 11.95 o -1 15 0 394.86 433.46 26.51 o 1 15 0 3763.72 3456.54 157.54 o 3 15 0 260.58 297.14 31.66 o 5 15 0 46.18 66.89 13.01 o 7 15 0 50.08 54.74 13.55 o 9 15 0 9.54 56.59 15.72 o 11 15 0 355.18 203.24 26.44 o 13 15 0 0.56 0.63 20.29 o 15 15 0 0.41 11.79 21.41 o -14 16 0 126.76 120.10 24.23 o -12 16 0 111.59 91.82 22.15 o -10 16 0 3.84 18.30 19.29 o -8 16 0 34.92 15.21 21.91 o -6 16 0 90.98 85.13 15.76 o -4 16 0 19.44 19.06 13.95 o -2 16 0 11.06 43.28 12.25 o 0 16 0 1.18 94.23 14.02 o 2 16 0 113.92 130.18 19.03 o 4 16 0 185.82 234.05 35.16 o 6 16 0 23.17 13.61 12.74 o 8 16 0 169.69 137.04 19.16 o 10 16 0 18.20 48.26 19.61 o 12 16 0 8.12 61.31 24.58 o 14 16 0 85.55 125.94 25.47 o -13 17 0 17.15 27.83 21.67 o -11 17 0 4.11 25.90 20.72 o -9 17 0 158.14 142.65 23.34 o -7 17 0 13.18 24.18 17.96 o -5 17 0 10.30 18.09 14.74 o -3 17 0 42.94 23.92 14.79 o -1 17 0 6.05 8.21 12.59 o 1 17 0 1001.21 940.05 50.95 o 3 17 0 1.30 21.05 15.03 o 5 17 0 40.36 28.56 13.44 o 7 17 0 58.24 135.83 24.84 o 9 17 0 156.35 198.70 26.63 o 11 17 0 85.84 92.99 24.24 o 13 17 0 157.20 174.78 26.96 o -12 18 0 33.14 27.45 21.44 o -10 18 0 13.12 30.39 21.22 o -8 18 0 33.29 28.71 20.08 o -6 18 0 156.50 180.25 23.42 o -4 18 0 68.34 64.63 16.58 o -2 18 0 567.57 663.50 63.35 o 0 18 0 16.16 17.64 13.62 o 2 18 0 15.57 31.96 15.70 o 4 18 0 288.15 276.15 24.75 o 6 18 0 294.78 286.00 38.61 o 8 18 0 25.94 29.84 20.68 o 10 18 0 747.37 635.11 89.64 o 12 18 0 234.62 214.56 34.88 o -9 19 0 14.78 -20.28 20.28 o -7 19 0 1.19 65.65 21.18 o -5 19 0 108.78 111.02 21.96 o -3 19 0 210.59 235.89 26.57 o -1 19 0 1004.47 914.23 56.68 o 1 19 0 35.16 37.50 16.76 o 3 19 0 0.57 44.59 16.65 o 5 19 0 347.61 400.93 36.52 o 7 19 0 63.27 116.51 29.19 o 9 19 0 2.86 104.61 29.75 o -8 20 0 0.00 12.46 28.21 o -6 20 0 179.87 181.05 26.53 o -4 20 0 156.53 154.36 24.79 o -2 20 0 150.45 204.29 51.72 o 0 20 0 51.43 19.32 19.90 o 2 20 0 0.02 22.75 17.62 o 4 20 0 5.16 7.90 17.16 o 6 20 0 85.78 106.33 24.20 o 8 20 0 504.89 498.12 53.63 o -5 21 0 4.89 6.57 20.90 o -3 21 0 78.62 36.90 26.82 o -1 21 0 0.20 6.69 24.94 o 1 21 0 14.97 19.22 21.09 o 3 21 0 9.81 13.34 18.37 o 5 21 0 67.81 64.52 24.20 o 0 1 1 1249.90 1157.61 38.85 o -1 2 1 7709.86 8140.57 269.66 o 1 2 1 5160.10 4490.34 148.89 o -2 3 1 10943.84 12496.88 577.41 o 0 3 1 11057.16 10275.13 340.88 o 2 3 1 7160.97 7807.44 270.80 o -3 4 1 9769.33 12468.96 556.07 o -1 4 1 378.68 1245.72 76.73 o 1 4 1 4159.42 4179.18 139.48 o 3 4 1 4517.03 4805.81 208.47 o -4 5 1 1937.77 2343.83 87.23 o -2 5 1 4084.60 4024.25 171.30 o 0 5 1 7402.15 7101.89 246.65 o 2 5 1 163.34 216.95 9.34 o 4 5 1 4944.93 4804.31 168.06 o -5 6 1 423.38 476.31 26.47 o -3 6 1 843.29 773.79 30.14 o -1 6 1 1125.53 885.94 30.49 o 1 6 1 585.01 575.45 23.53 o 3 6 1 1124.67 925.49 31.83 o 5 6 1 1439.27 1340.81 48.27 o -6 7 1 139.65 150.72 11.00 o -4 7 1 4546.46 4435.01 155.73 o -2 7 1 1966.58 1944.47 65.28 o 0 7 1 14521.20 14825.80 471.04 o 2 7 1 2204.94 2336.39 78.14 o 4 7 1 1121.84 1654.10 66.90 o 6 7 1 1026.75 1176.89 67.71 o -7 8 1 1742.18 1523.46 55.08 o -5 8 1 1903.65 1833.17 65.07 o -3 8 1 1580.35 1588.20 53.30 o -1 8 1 1571.86 1420.91 48.18 o 1 8 1 1086.42 1120.67 36.90 o 3 8 1 3447.82 3415.20 114.46 o 5 8 1 275.60 311.22 16.06 o 7 8 1 364.15 375.30 15.04 o -8 9 1 70.95 97.46 8.94 o -6 9 1 182.13 347.70 15.10 o -4 9 1 666.92 582.72 22.49 o -2 9 1 2282.53 2444.83 81.55 o 0 9 1 1314.90 1712.07 88.58 o 2 9 1 332.07 359.72 13.40 o 4 9 1 3459.09 3429.44 115.22 o 6 9 1 40.59 79.49 7.12 o 8 9 1 418.46 332.04 15.37 o -9 10 1 0.76 61.74 8.97 o -7 10 1 36.99 170.46 10.21 o -5 10 1 764.66 742.49 28.86 o -3 10 1 876.17 839.67 29.67 o -1 10 1 919.68 1291.49 44.64 o 1 10 1 1810.88 1919.12 61.71 o 3 10 1 1331.67 1256.09 42.86 o 5 10 1 608.81 577.40 21.52 o 7 10 1 355.66 354.65 15.68 o 9 10 1 639.08 553.65 23.78 o -10 11 1 718.40 724.51 29.89 o -8 11 1 201.05 209.83 12.62 o -6 11 1 380.09 419.95 17.73 o -4 11 1 1252.77 1287.34 44.67 o -2 11 1 1446.83 1504.06 51.81 o 0 11 1 496.67 469.24 17.93 o 2 11 1 307.00 380.88 29.29 o 4 11 1 2642.60 2802.85 104.87 o 6 11 1 7.03 29.43 8.70 o 8 11 1 145.95 153.44 10.89 o 10 11 1 1406.29 1410.57 54.82 o -11 12 1 87.61 77.27 12.01 o -9 12 1 110.90 109.89 10.37 o -7 12 1 192.81 210.51 13.66 o -5 12 1 151.70 219.13 11.89 o -3 12 1 465.19 470.13 18.54 o -1 12 1 135.55 217.12 10.91 o 1 12 1 735.80 730.01 25.37 o 3 12 1 292.70 290.33 13.21 o 5 12 1 129.11 183.93 11.94 o 7 12 1 288.47 380.14 33.61 o 9 12 1 625.98 565.98 38.19 o 11 12 1 975.01 1022.62 43.74 o -12 13 1 143.23 214.00 21.42 o -10 13 1 92.31 75.12 12.05 o -8 13 1 236.09 176.11 12.24 o -6 13 1 131.04 129.03 10.62 o -4 13 1 686.73 718.28 29.47 o -2 13 1 346.81 384.89 26.22 o 0 13 1 449.72 412.99 17.79 o 2 13 1 58.01 109.18 9.33 o 4 13 1 1018.43 1013.41 36.20 o 6 13 1 283.51 394.96 18.68 o 8 13 1 703.90 696.62 29.21 o 10 13 1 234.77 258.75 16.30 o 12 13 1 76.11 70.60 12.85 o -13 14 1 35.44 53.65 13.31 o -11 14 1 341.10 331.04 22.52 o -9 14 1 381.08 320.81 19.30 o -7 14 1 164.77 156.79 12.53 o -5 14 1 70.42 113.60 11.05 o -3 14 1 83.58 87.73 9.78 o -1 14 1 1259.05 1145.19 40.46 o 1 14 1 123.44 156.19 16.40 o 3 14 1 441.76 418.36 18.33 o 5 14 1 527.59 503.83 21.19 o 7 14 1 934.34 945.56 38.02 o 9 14 1 167.16 178.92 13.75 o 11 14 1 227.59 191.02 15.85 o 13 14 1 192.80 144.74 15.22 o -14 15 1 87.22 65.63 14.61 o -12 15 1 119.02 131.14 15.06 o -10 15 1 122.10 166.81 15.18 o -8 15 1 154.10 149.97 18.58 o -6 15 1 274.86 314.44 18.97 o -4 15 1 355.21 425.95 28.28 o -2 15 1 75.36 69.94 9.92 o 0 15 1 626.49 633.05 29.72 o 2 15 1 44.77 109.12 10.54 o 4 15 1 108.38 107.54 10.32 o 6 15 1 486.12 476.37 21.86 o 8 15 1 913.69 839.21 37.05 o 10 15 1 22.18 44.11 12.78 o 12 15 1 60.97 48.21 13.67 o 14 15 1 32.45 20.89 13.71 o -13 16 1 2.90 12.28 13.59 o -11 16 1 28.81 40.01 13.28 o -9 16 1 354.57 267.30 18.34 o -7 16 1 64.71 98.16 13.08 o -5 16 1 247.07 342.32 32.49 o -3 16 1 118.15 98.31 11.30 o -1 16 1 143.75 217.61 15.40 o 1 16 1 91.50 228.06 18.95 o 3 16 1 265.44 234.59 13.57 o 5 16 1 190.22 174.18 13.78 o 7 16 1 176.34 118.46 13.59 o 9 16 1 564.12 469.33 27.78 o 11 16 1 152.34 201.29 22.66 o 13 16 1 69.44 54.95 14.66 o -12 17 1 8.26 43.44 14.06 o -10 17 1 39.14 46.77 16.06 o -8 17 1 113.24 155.18 15.02 o -6 17 1 42.26 88.37 13.02 o -4 17 1 57.89 112.70 12.32 o -2 17 1 224.29 197.14 15.55 o 0 17 1 199.53 205.82 18.16 o 2 17 1 279.22 262.35 14.70 o 4 17 1 116.74 101.97 12.26 o 6 17 1 17.30 27.55 12.42 o 8 17 1 71.07 116.93 14.47 o 10 17 1 48.80 42.54 14.95 o 12 17 1 149.74 187.82 20.35 o -11 18 1 7.37 30.31 15.93 o -9 18 1 5.73 7.29 13.01 o -7 18 1 215.32 217.23 17.10 o -5 18 1 132.31 137.22 14.38 o -3 18 1 332.28 347.14 20.69 o -1 18 1 300.60 242.23 22.09 o 1 18 1 18.99 53.40 12.37 o 3 18 1 514.48 464.41 25.60 o 5 18 1 257.76 188.24 16.41 o 7 18 1 134.19 168.31 21.60 o 9 18 1 60.22 66.90 16.07 o 11 18 1 57.34 102.83 17.28 o -10 19 1 233.93 245.99 20.65 o -8 19 1 25.53 47.99 14.03 o -6 19 1 150.03 100.49 14.72 o -4 19 1 186.51 197.69 17.99 o -2 19 1 10.51 19.53 12.29 o 0 19 1 81.60 118.99 14.28 o 2 19 1 175.06 154.57 16.94 o 4 19 1 76.16 71.90 15.20 o 6 19 1 26.48 61.34 14.33 o 8 19 1 33.06 68.62 16.63 o 10 19 1 44.07 73.60 17.23 o -7 20 1 29.26 27.76 14.11 o -5 20 1 61.59 74.45 15.67 o -3 20 1 78.03 64.11 15.40 o -1 20 1 92.59 126.35 14.97 o 1 20 1 241.79 273.21 20.75 o 3 20 1 45.09 30.24 17.84 o 5 20 1 9.06 24.36 16.41 o 7 20 1 78.07 83.21 17.27 o -4 21 1 88.21 136.32 17.43 o -2 21 1 8.27 13.44 15.23 o 0 21 1 24.93 48.86 15.27 o 2 21 1 1.24 8.17 18.68 o 4 21 1 0.33 21.14 19.09 o 0 0 2 8266.89 7132.96 451.12 o 1 1 2 642.70 567.88 25.04 o 0 2 2 5102.92 5106.79 170.27 o 2 2 2 1982.53 1967.64 66.30 o -1 3 2 540.90 830.01 49.07 o 1 3 2 459.59 537.83 25.57 o 3 3 2 303.19 472.23 27.63 o -2 4 2 829.10 1206.74 41.20 o 0 4 2 2055.72 1934.29 64.99 o 2 4 2 2461.24 2588.52 86.84 o 4 4 2 4225.23 4287.34 143.23 o -3 5 2 3.27 14.86 6.65 o -1 5 2 411.01 445.15 20.35 o 1 5 2 374.28 422.09 16.51 o 3 5 2 1213.86 1178.40 42.49 o 5 5 2 329.43 369.46 15.58 o -4 6 2 487.73 482.95 28.06 o -2 6 2 673.53 671.07 27.31 o 0 6 2 1771.31 1690.91 57.23 o 2 6 2 2502.93 2502.61 87.96 o 4 6 2 4821.92 5149.91 180.31 o 6 6 2 875.78 789.39 31.45 o -5 7 2 909.72 830.40 32.77 o -3 7 2 263.15 246.23 12.43 o -1 7 2 722.31 850.17 34.94 o 1 7 2 1407.70 1370.63 44.85 o 3 7 2 1187.04 1189.56 43.11 o 5 7 2 1094.19 1426.29 53.82 o 7 7 2 1785.49 1767.24 66.91 o -6 8 2 246.93 361.93 20.74 o -4 8 2 295.92 436.95 32.59 o -2 8 2 270.73 287.39 16.94 o 0 8 2 299.07 341.46 14.56 o 2 8 2 938.49 931.67 32.51 o 4 8 2 555.25 719.74 27.36 o 6 8 2 519.63 606.26 25.24 o 8 8 2 516.60 539.44 23.27 o -7 9 2 29.70 87.24 9.41 o -5 9 2 8.61 27.18 8.29 o -3 9 2 310.75 342.16 18.75 o -1 9 2 184.75 255.77 15.78 o 1 9 2 452.00 498.59 26.51 o 3 9 2 204.56 192.52 10.75 o 5 9 2 1287.14 1220.59 47.24 o 7 9 2 12.14 51.78 8.23 o 9 9 2 66.32 50.65 10.33 o -8 10 2 132.20 119.28 10.50 o -6 10 2 396.78 470.74 20.78 o -4 10 2 118.47 200.76 12.08 o -2 10 2 1430.70 1169.10 44.83 o 0 10 2 404.24 511.91 29.53 o 2 10 2 1016.48 951.61 35.52 o 4 10 2 155.70 185.56 10.69 o 6 10 2 298.10 276.25 13.68 o 8 10 2 671.70 626.21 26.36 o 10 10 2 791.21 694.61 29.00 o -9 11 2 581.46 593.18 25.84 o -7 11 2 586.75 543.11 23.58 o -5 11 2 1451.78 1432.10 55.33 o -3 11 2 2618.93 2437.09 91.64 o -1 11 2 559.19 442.35 18.55 o 1 11 2 144.75 113.36 8.98 o 3 11 2 451.30 459.51 20.40 o 5 11 2 892.81 846.76 34.04 o 7 11 2 100.73 167.46 15.08 o 9 11 2 103.09 147.31 11.71 o 11 11 2 135.31 158.65 11.92 o -10 12 2 691.82 653.67 28.19 o -8 12 2 497.28 506.26 28.70 o -6 12 2 1540.05 1404.88 54.31 o -4 12 2 142.74 123.65 10.91 o -2 12 2 1134.94 1083.61 44.93 o 0 12 2 1138.44 1194.25 53.07 o 2 12 2 462.29 498.34 23.35 o 4 12 2 104.35 112.26 10.96 o 6 12 2 267.06 199.85 13.44 o 8 12 2 1199.23 1012.00 40.70 o 10 12 2 224.08 192.90 14.35 o 12 12 2 185.92 192.71 13.38 o -11 13 2 54.35 65.31 11.32 o -9 13 2 336.55 307.67 17.71 o -7 13 2 671.36 615.03 40.68 o -5 13 2 698.91 688.71 32.97 o -3 13 2 1036.44 938.48 37.80 o -1 13 2 834.64 887.07 37.92 o 1 13 2 291.37 300.47 16.96 o 3 13 2 36.89 34.10 10.51 o 5 13 2 78.01 92.00 10.96 o 7 13 2 168.26 175.94 16.00 o 9 13 2 198.46 221.02 14.33 o 11 13 2 35.80 79.21 11.26 o 13 13 2 65.89 62.11 13.00 o -12 14 2 37.77 26.47 12.31 o -10 14 2 93.44 105.44 12.14 o -8 14 2 520.73 402.19 20.13 o -6 14 2 21.16 29.24 9.90 o -4 14 2 2155.22 2145.78 80.50 o -2 14 2 568.44 549.85 25.80 o 0 14 2 72.46 111.96 11.54 o 2 14 2 710.94 700.40 31.02 o 4 14 2 303.71 241.85 16.59 o 6 14 2 426.50 393.60 20.74 o 8 14 2 301.83 280.38 17.03 o 10 14 2 354.16 352.22 18.67 o 12 14 2 115.19 110.28 13.78 o 14 14 2 10.00 14.11 14.14 o -13 15 2 40.42 57.60 17.21 o -11 15 2 17.57 26.05 13.03 o -9 15 2 143.07 170.77 13.75 o -7 15 2 88.62 124.71 12.13 o -5 15 2 176.61 191.68 17.42 o -3 15 2 10.98 110.68 12.56 o -1 15 2 234.54 225.48 15.30 o 1 15 2 1661.15 1544.79 67.69 o 3 15 2 469.04 532.82 27.45 o 5 15 2 149.35 109.31 13.30 o 7 15 2 66.79 51.51 11.67 o 9 15 2 43.13 52.65 11.89 o 11 15 2 27.43 37.22 13.36 o 13 15 2 64.46 72.11 14.96 o -12 16 2 131.04 109.11 15.92 o -10 16 2 25.47 52.42 13.64 o -8 16 2 47.56 39.85 11.93 o -6 16 2 187.42 178.83 13.56 o -4 16 2 12.11 87.03 12.47 o -2 16 2 52.63 38.54 11.47 o 0 16 2 224.03 272.32 20.03 o 2 16 2 272.58 338.90 37.84 o 4 16 2 120.04 122.97 14.03 o 6 16 2 555.71 536.70 28.20 o 8 16 2 13.94 13.67 11.59 o 10 16 2 347.38 299.77 21.24 o 12 16 2 54.93 50.67 16.06 o -11 17 2 147.09 145.02 16.31 o -9 17 2 160.85 124.82 14.30 o -7 17 2 10.80 31.86 12.17 o -5 17 2 10.99 63.85 12.35 o -3 17 2 25.03 54.27 12.26 o -1 17 2 6.12 6.43 12.23 o 1 17 2 126.38 97.94 14.78 o 3 17 2 22.92 46.19 14.02 o 5 17 2 508.42 529.88 28.04 o 7 17 2 8.47 23.01 12.92 o 9 17 2 12.53 1.68 14.18 o 11 17 2 147.01 133.66 18.20 o -10 18 2 34.96 67.00 15.20 o -8 18 2 76.56 77.78 13.65 o -6 18 2 330.73 275.34 19.10 o -4 18 2 283.81 278.91 21.67 o -2 18 2 114.84 62.74 13.85 o 0 18 2 27.78 45.70 13.28 o 2 18 2 25.51 38.51 14.18 o 4 18 2 114.83 92.11 15.49 o 6 18 2 18.84 34.15 13.46 o 8 18 2 20.89 30.03 15.75 o 10 18 2 15.24 20.56 15.57 o -7 19 2 84.79 64.62 16.15 o -5 19 2 102.92 207.91 17.47 o -3 19 2 230.55 253.53 27.03 o -1 19 2 32.16 13.16 13.70 o 1 19 2 1.60 21.05 14.55 o 3 19 2 31.43 46.17 15.25 o 5 19 2 19.70 31.91 15.59 o 7 19 2 2.23 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