#------------------------------------------------------------------------------ #$Date: 2013-10-24 17:51:33 +0300 (Thu, 24 Oct 2013) $ #$Revision: 89414 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/90/2019095.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2019095_Fobs loop_ _publ_author_name 'Gomes, Ligia Rebelo' 'Low, John Nicolson' 'Rodrigues, Ana S. M. C.' 'Wardell, James L.' 'de Souza, Marcus V. N.' 'Noguiera, Thais C. M.' 'Pinheiro, Alessandra C.' _publ_section_title ; Comparison of the structure of (E)-2-(2-benzylidenehydrazinylidene)quinoxaline with those of its chloro- and bromobenzylidene analogues ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 920 _journal_page_last 926 _journal_volume 69 _journal_year 2013 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.004 _cell_angle_gamma 90.000 _cell_length_a 12.0020 _cell_length_b 9.1700 _cell_length_c 12.6170 _exptl_crystal_F_000 656.00 _reflns_d_resolution_high 0.8400 _[local]_cod_data_source_file sk34883csup8.hkl _[local]_cod_data_source_block 3c #BEGIN Tags that were not found in dictionaries: _shelx_title ' 896_pc P 1 c 1 R = New: P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 290.29 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6663.54 6429.64 57.11 o 3 0 0 2399.61 2399.25 17.38 o 4 0 0 6889.08 6720.21 50.35 o 5 0 0 1870.60 1920.59 21.97 o 6 0 0 240.86 193.31 11.68 o 7 0 0 3085.18 3599.84 42.69 o 8 0 0 1540.95 1804.88 39.08 o 9 0 0 298.38 345.36 31.39 o 10 0 0 936.59 961.72 49.20 o 11 0 0 1647.01 1510.22 110.57 o 12 0 0 1767.70 1677.01 80.73 o 13 0 0 1405.78 1549.49 175.87 o 14 0 0 2306.21 1994.26 128.23 o 2 1 0 30.42 46.58 4.54 o 3 1 0 314.39 387.30 13.11 o 4 1 0 2494.23 2485.13 13.22 o 5 1 0 3494.44 3472.80 19.58 o 6 1 0 4921.14 5023.22 28.33 o 7 1 0 4455.09 4555.90 45.12 o 8 1 0 3502.67 3656.48 38.25 o 9 1 0 1755.11 1838.33 46.80 o 10 1 0 1113.39 1191.33 45.42 o 11 1 0 398.57 457.76 31.48 o 12 1 0 276.26 331.45 23.63 o 13 1 0 209.71 201.64 21.02 o 14 1 0 8.21 56.74 23.43 o 0 2 0 150.03 158.81 13.88 o 1 2 0 9.67 13.42 2.86 o 2 2 0 10480.78 11119.79 39.02 o 3 2 0 16357.90 17074.17 61.07 o 4 2 0 353.05 452.18 16.34 o 5 2 0 2996.06 3367.29 26.20 o 6 2 0 29.29 53.20 3.96 o 7 2 0 0.40 34.45 4.99 o 8 2 0 9.46 32.56 13.30 o 9 2 0 20.50 46.92 8.09 o 10 2 0 477.92 489.08 33.42 o 11 2 0 88.09 87.24 12.76 o 12 2 0 18.44 61.59 17.45 o 13 2 0 353.86 317.16 33.56 o 1 3 0 1557.69 1514.97 20.81 o 2 3 0 3529.11 3558.95 17.48 o 3 3 0 2596.06 2425.99 15.44 o 4 3 0 4914.40 4855.23 22.77 o 5 3 0 5295.25 5216.68 30.70 o 6 3 0 2918.79 2749.90 23.92 o 7 3 0 2616.32 2581.27 41.96 o 8 3 0 3042.19 2961.36 50.68 o 9 3 0 2216.42 2351.02 44.30 o 10 3 0 2175.05 2186.33 72.55 o 11 3 0 849.97 823.09 31.41 o 12 3 0 92.15 102.30 11.38 o 13 3 0 147.02 166.58 23.36 o 0 4 0 8644.59 8573.89 122.17 o 1 4 0 6917.23 6699.43 50.15 o 2 4 0 4001.32 3922.43 34.06 o 3 4 0 3385.40 3303.57 25.28 o 4 4 0 3159.67 3091.38 26.84 o 5 4 0 7165.83 7579.69 38.33 o 6 4 0 384.72 441.05 19.83 o 7 4 0 106.57 109.37 9.94 o 8 4 0 11.17 46.87 13.42 o 9 4 0 298.15 288.92 19.63 o 10 4 0 239.16 271.89 20.59 o 11 4 0 1118.50 1264.72 54.56 o 12 4 0 2282.30 2128.25 83.67 o 13 4 0 336.82 365.48 32.85 o 1 5 0 175.83 246.30 15.78 o 2 5 0 1282.66 1347.90 28.49 o 3 5 0 203.33 219.94 10.53 o 4 5 0 468.97 525.14 34.47 o 5 5 0 421.10 442.73 22.54 o 6 5 0 1414.21 1443.95 47.84 o 7 5 0 749.33 754.63 33.97 o 8 5 0 206.81 225.25 19.55 o 9 5 0 624.88 700.98 43.98 o 10 5 0 33.11 40.07 8.56 o 11 5 0 41.90 60.70 15.16 o 12 5 0 28.38 80.78 24.32 o 0 6 0 1130.30 1070.62 16.49 o 1 6 0 1272.15 1230.75 30.62 o 2 6 0 544.40 493.42 32.28 o 3 6 0 540.59 514.14 30.68 o 4 6 0 183.69 146.50 15.95 o 5 6 0 283.25 290.79 17.80 o 6 6 0 8.86 23.12 6.25 o 7 6 0 4.86 26.45 10.05 o 8 6 0 209.69 171.46 17.02 o 9 6 0 473.49 458.58 28.83 o 10 6 0 17.23 58.45 10.72 o 11 6 0 56.37 51.69 15.26 o 1 7 0 287.57 315.94 21.94 o 2 7 0 352.12 303.80 30.00 o 3 7 0 448.55 486.19 28.25 o 4 7 0 355.69 354.53 41.80 o 5 7 0 2037.32 2021.26 58.69 o 6 7 0 4445.40 4680.36 97.48 o 7 7 0 857.73 865.85 51.24 o 8 7 0 1480.57 1664.73 80.39 o 9 7 0 877.91 942.78 66.54 o 10 7 0 1177.88 1276.42 99.35 o 0 8 0 1931.83 2064.94 78.67 o 1 8 0 2010.37 1950.52 95.29 o 2 8 0 1795.36 1874.54 55.04 o 3 8 0 626.10 737.76 52.98 o 4 8 0 336.05 358.89 34.75 o 5 8 0 60.27 75.67 14.77 o 6 8 0 20.55 61.75 12.68 o 7 8 0 2.04 65.25 19.37 o 8 8 0 42.34 42.67 20.10 o 9 8 0 74.74 95.98 16.11 o 1 9 0 119.99 128.04 31.10 o 2 9 0 15.96 130.67 29.11 o 3 9 0 523.88 502.36 55.99 o 4 9 0 201.72 263.67 35.83 o 5 9 0 3.33 60.13 18.64 o 6 9 0 241.54 226.75 22.74 o 7 9 0 50.47 99.42 21.10 o 0 10 0 13.69 83.26 26.69 o 1 10 0 413.56 320.86 46.45 o 2 10 0 221.07 203.22 30.27 o 3 10 0 446.46 397.22 44.62 o 4 10 0 283.74 241.48 27.62 o 5 10 0 278.87 239.84 25.36 o -14 1 1 235.58 241.89 25.25 o -13 1 1 22.77 55.62 17.97 o -12 1 1 8.63 35.01 9.60 o -11 1 1 84.23 126.32 22.65 o -10 1 1 25.61 51.98 8.40 o -9 1 1 563.13 544.74 24.66 o -8 1 1 2665.44 2746.38 31.76 o -7 1 1 2003.18 2008.96 23.98 o -6 1 1 4705.02 4735.24 28.70 o -5 1 1 5928.75 5842.56 43.04 o -4 1 1 6550.11 6518.82 42.38 o -3 1 1 11923.24 11843.31 113.22 o -2 1 1 7454.25 7315.01 30.74 o -1 1 1 1673.84 1559.45 14.05 o 1 1 1 591.97 571.59 8.44 o 2 1 1 20.94 44.42 3.92 o 3 1 1 630.00 690.65 14.55 o 4 1 1 4.11 23.92 3.67 o 5 1 1 793.76 801.18 15.81 o 6 1 1 2717.54 2702.36 27.92 o 7 1 1 962.90 926.58 29.54 o 8 1 1 2152.16 2101.97 68.97 o 9 1 1 2364.11 2389.42 47.70 o 10 1 1 2464.52 2464.21 68.27 o 11 1 1 1568.55 1629.00 63.82 o 12 1 1 1370.86 1235.00 68.84 o 13 1 1 737.19 717.77 55.34 o -13 2 1 774.84 713.50 37.03 o -12 2 1 4991.99 4544.67 241.94 o -11 2 1 1002.53 1039.60 46.01 o -10 2 1 5236.05 5283.69 155.62 o -9 2 1 3459.85 3556.29 59.15 o -8 2 1 1991.16 1996.28 39.69 o -7 2 1 1245.66 1154.34 33.66 o -6 2 1 35.14 82.42 4.59 o -5 2 1 2208.81 2503.17 27.28 o -4 2 1 2108.86 2342.58 14.56 o -3 2 1 10745.62 11100.13 42.31 o -2 2 1 2484.80 2309.39 13.66 o -1 2 1 174.67 178.30 7.97 o 0 2 1 5192.18 4898.84 17.35 o 1 2 1 3348.00 3127.24 19.93 o 2 2 1 84268.09 87292.59 514.58 o 3 2 1 2461.20 2265.89 20.98 o 4 2 1 5536.96 5524.38 31.42 o 5 2 1 6219.26 6361.35 35.38 o 6 2 1 7319.06 7552.66 51.36 o 7 2 1 2850.36 2819.41 50.70 o 8 2 1 799.14 800.85 26.06 o 9 2 1 21.75 46.86 11.51 o 10 2 1 407.01 410.58 25.68 o 11 2 1 4.34 65.90 13.47 o 12 2 1 62.35 61.62 20.35 o 13 2 1 498.52 449.34 38.70 o -13 3 1 6.14 50.73 14.28 o -12 3 1 202.51 239.77 17.28 o -11 3 1 8.39 78.29 18.62 o -10 3 1 199.28 208.05 17.47 o -9 3 1 51.25 64.93 11.52 o -8 3 1 258.38 257.54 19.89 o -7 3 1 542.22 563.20 24.16 o -6 3 1 2230.67 2266.28 26.38 o -5 3 1 4295.64 4315.28 37.05 o -4 3 1 3942.89 4067.87 30.53 o -3 3 1 2325.60 2397.84 16.82 o -2 3 1 1309.47 1390.67 14.97 o -1 3 1 1046.79 1094.69 13.77 o 0 3 1 1557.76 1573.19 14.61 o 1 3 1 59.64 82.09 5.55 o 2 3 1 358.21 397.67 11.82 o 3 3 1 10.87 23.23 3.93 o 4 3 1 417.60 504.69 15.20 o 5 3 1 292.38 358.71 11.95 o 6 3 1 797.06 829.28 25.73 o 7 3 1 948.52 963.38 36.07 o 8 3 1 1741.47 1770.51 55.45 o 9 3 1 585.66 663.38 25.70 o 10 3 1 755.92 835.08 41.97 o 11 3 1 1577.63 1552.57 68.62 o 12 3 1 210.94 202.68 32.47 o 13 3 1 240.29 258.75 29.91 o -13 4 1 268.06 217.12 26.09 o -12 4 1 184.51 191.77 24.45 o -11 4 1 331.01 262.12 22.90 o -10 4 1 20.37 55.42 13.12 o -9 4 1 211.96 227.95 17.79 o -8 4 1 37.65 63.78 9.11 o -7 4 1 695.08 721.63 27.85 o -6 4 1 46.53 73.42 4.26 o -5 4 1 87.62 124.94 11.04 o -4 4 1 10.18 20.21 3.37 o -3 4 1 3466.50 3676.06 26.85 o -2 4 1 32.87 68.71 6.87 o -1 4 1 218.63 207.40 7.63 o 0 4 1 164.10 135.22 8.26 o 1 4 1 1388.30 1324.80 28.40 o 2 4 1 567.49 566.22 23.63 o 3 4 1 565.59 540.74 12.96 o 4 4 1 1279.00 1451.90 18.64 o 5 4 1 7533.99 8019.42 47.96 o 6 4 1 14.57 33.50 5.30 o 7 4 1 195.53 207.46 16.89 o 8 4 1 165.91 168.25 16.68 o 9 4 1 88.17 103.23 16.88 o 10 4 1 1.10 81.39 26.97 o 11 4 1 27.08 78.19 13.88 o 12 4 1 199.15 160.08 31.70 o -12 5 1 3.02 47.94 11.28 o -11 5 1 25.33 58.71 9.70 o -10 5 1 177.54 198.18 13.25 o -9 5 1 965.68 1070.23 38.08 o -8 5 1 2071.00 2171.65 55.49 o -7 5 1 1476.43 1470.28 51.78 o -6 5 1 2649.47 2724.35 37.40 o -5 5 1 2735.61 2634.20 28.91 o -4 5 1 4972.34 4862.98 29.78 o -3 5 1 6166.43 6155.62 32.09 o -2 5 1 3722.92 3645.97 25.23 o -1 5 1 2556.51 2374.54 19.85 o 0 5 1 1727.27 1484.86 15.85 o 1 5 1 1572.15 1545.49 27.89 o 2 5 1 200.85 220.30 10.58 o 3 5 1 52.59 44.33 6.59 o 4 5 1 504.39 522.24 19.28 o 5 5 1 188.90 187.03 14.28 o 6 5 1 279.37 326.21 27.70 o 7 5 1 1855.86 1824.44 58.11 o 8 5 1 3443.74 3471.70 99.22 o 9 5 1 607.29 689.94 44.34 o 10 5 1 1977.30 1921.22 74.81 o 11 5 1 1191.57 1140.51 57.63 o 12 5 1 1116.38 1061.31 77.25 o -11 6 1 921.42 887.60 60.00 o -10 6 1 1501.42 1443.92 58.83 o -9 6 1 1848.63 1890.78 49.48 o -8 6 1 633.45 577.87 39.42 o -7 6 1 880.36 838.74 54.28 o -6 6 1 290.08 246.81 17.37 o -5 6 1 22.88 37.20 6.53 o -4 6 1 0.43 14.99 6.35 o -3 6 1 134.07 116.88 13.21 o -2 6 1 657.51 640.36 23.08 o -1 6 1 1684.63 1642.57 26.54 o 0 6 1 1085.93 1153.09 30.58 o 1 6 1 2845.48 2809.04 37.45 o 2 6 1 3659.41 3734.77 52.69 o 3 6 1 4493.64 4618.08 58.88 o 4 6 1 3939.25 3940.43 69.77 o 5 6 1 1536.48 1524.59 37.29 o 6 6 1 1452.02 1434.58 63.44 o 7 6 1 2886.61 2714.19 82.83 o 8 6 1 240.61 242.75 28.93 o 9 6 1 304.45 381.24 28.05 o 10 6 1 62.53 98.28 18.51 o 11 6 1 3.70 64.32 11.84 o -10 7 1 41.17 59.20 15.28 o -9 7 1 17.17 16.45 16.79 o -8 7 1 3.94 63.89 21.14 o -7 7 1 50.27 76.60 16.44 o -6 7 1 10.84 30.97 12.52 o -5 7 1 197.73 196.69 20.87 o -4 7 1 766.98 787.85 78.08 o -3 7 1 639.82 700.91 26.24 o -2 7 1 37.34 37.52 9.42 o -1 7 1 149.32 128.98 24.18 o 0 7 1 110.97 127.68 11.86 o 1 7 1 103.63 139.12 18.49 o 2 7 1 16.27 22.24 5.95 o 3 7 1 257.35 290.59 27.85 o 4 7 1 41.27 42.88 9.65 o 5 7 1 976.69 979.12 69.79 o 6 7 1 845.13 711.48 74.65 o 7 7 1 41.23 33.04 12.08 o 8 7 1 473.26 482.10 39.84 o 9 7 1 196.61 225.43 31.38 o 10 7 1 27.86 33.60 20.18 o -9 8 1 186.87 275.79 47.61 o -8 8 1 32.37 41.78 15.83 o -7 8 1 182.31 205.04 19.65 o -6 8 1 94.06 87.50 26.24 o -5 8 1 18.65 26.20 9.23 o -4 8 1 4.57 54.15 12.90 o -3 8 1 102.37 145.79 16.82 o -2 8 1 233.21 206.94 18.97 o -1 8 1 711.31 797.48 37.73 o 0 8 1 697.22 646.98 73.62 o 1 8 1 653.95 562.45 42.27 o 2 8 1 198.98 177.31 21.05 o 3 8 1 573.97 626.80 46.40 o 4 8 1 156.82 182.74 26.72 o 5 8 1 350.09 378.86 31.58 o 6 8 1 471.56 496.90 52.14 o 7 8 1 465.72 549.43 61.08 o 8 8 1 99.14 105.75 21.86 o 9 8 1 30.31 49.33 12.68 o -8 9 1 474.84 549.86 68.94 o -7 9 1 801.39 818.16 83.54 o -6 9 1 1069.89 1036.28 83.47 o -5 9 1 244.64 263.44 47.04 o -4 9 1 3096.80 2983.94 217.51 o -3 9 1 814.67 907.16 65.35 o -2 9 1 466.10 508.02 44.79 o -1 9 1 487.41 497.38 46.35 o 0 9 1 649.24 601.84 88.57 o 1 9 1 974.70 1121.51 126.95 o 2 9 1 868.39 823.16 73.04 o 3 9 1 1236.89 1245.71 70.31 o 4 9 1 45.46 66.18 15.76 o 5 9 1 162.66 186.89 20.12 o 6 9 1 197.48 215.29 53.34 o 7 9 1 951.04 946.26 97.45 o -5 10 1 61.94 113.95 20.14 o -4 10 1 1.94 34.04 18.01 o -3 10 1 4.77 56.37 15.54 o -2 10 1 79.04 92.50 18.37 o -1 10 1 318.94 327.55 36.58 o 0 10 1 291.40 272.87 34.17 o 1 10 1 835.33 873.10 70.45 o 2 10 1 297.83 311.57 39.45 o 3 10 1 240.81 282.89 35.94 o 4 10 1 369.20 433.77 36.37 o 5 10 1 312.58 364.26 43.66 o -14 0 2 157.21 210.72 31.25 o -13 0 2 178.49 124.14 38.54 o -12 0 2 1082.74 1047.50 87.22 o -11 0 2 2535.54 2411.96 77.11 o -10 0 2 9422.69 9744.36 172.36 o -9 0 2 483.42 459.65 27.19 o -8 0 2 13388.26 14012.25 139.50 o -7 0 2 7220.86 7250.04 86.37 o -6 0 2 3772.47 3686.73 36.04 o -5 0 2 4608.67 4531.18 33.42 o -4 0 2 4795.37 4662.26 54.99 o -3 0 2 94.28 132.53 10.63 o 0 0 2 1303.72 1163.54 17.35 o 1 0 2 1282.22 1345.19 26.48 o 2 0 2 1342.16 1260.48 26.15 o 3 0 2 5620.75 5255.86 39.40 o 4 0 2 10788.21 10699.48 137.54 o 5 0 2 5214.69 4998.18 44.55 o 6 0 2 4919.82 4754.41 55.66 o 7 0 2 7210.57 7264.95 80.01 o 8 0 2 8481.21 8372.12 180.18 o 9 0 2 4032.26 4127.79 90.19 o 10 0 2 1077.48 1167.29 73.31 o 11 0 2 201.15 200.03 44.58 o 12 0 2 134.22 163.70 31.00 o 13 0 2 191.49 252.88 38.41 o -14 1 2 510.79 496.98 34.09 o -13 1 2 258.20 221.75 17.87 o -12 1 2 141.59 192.20 15.72 o -11 1 2 91.76 97.67 10.92 o -10 1 2 370.01 381.51 21.81 o -9 1 2 42.08 73.84 6.92 o -8 1 2 4.79 12.16 6.94 o -7 1 2 123.18 119.11 6.06 o -6 1 2 1165.46 1074.09 21.60 o -5 1 2 59.09 33.34 6.91 o -4 1 2 3412.70 3454.81 17.94 o -3 1 2 4390.64 4188.37 22.96 o -2 1 2 4708.65 4655.85 19.16 o -1 1 2 9095.62 9050.12 34.49 o 0 1 2 9799.40 9673.38 34.66 o 1 1 2 10945.76 10756.10 55.30 o 2 1 2 11172.97 11220.14 85.45 o 3 1 2 1233.98 1180.14 16.70 o 4 1 2 300.19 344.49 12.31 o 5 1 2 46.99 61.13 6.55 o 6 1 2 94.63 121.63 7.57 o 7 1 2 182.20 203.15 15.77 o 8 1 2 464.83 422.85 37.09 o 9 1 2 197.96 218.45 30.90 o 10 1 2 667.92 663.96 57.77 o 11 1 2 367.68 366.58 31.79 o 12 1 2 615.41 631.50 53.70 o 13 1 2 1707.59 1576.21 161.43 o -14 2 2 468.61 399.74 27.21 o -13 2 2 8.42 46.71 21.89 o -12 2 2 86.41 88.80 12.56 o -11 2 2 181.41 190.78 17.29 o -10 2 2 22.35 34.18 8.33 o -9 2 2 5.99 38.71 5.77 o -8 2 2 26.27 51.84 8.46 o -7 2 2 848.95 888.48 28.10 o -6 2 2 1521.70 1784.67 33.92 o -5 2 2 1708.16 1866.77 20.24 o -4 2 2 83.47 91.32 4.91 o -3 2 2 24.95 29.51 6.36 o -2 2 2 111.70 113.14 5.15 o -1 2 2 65.41 76.00 4.43 o 0 2 2 14.05 9.90 2.02 o 1 2 2 7677.55 7785.17 28.82 o 2 2 2 8586.96 8569.87 48.58 o 3 2 2 2499.64 2531.72 17.59 o 4 2 2 361.23 363.22 13.99 o 5 2 2 205.22 233.24 9.10 o 6 2 2 55.30 83.45 10.02 o 7 2 2 75.05 94.86 16.24 o 8 2 2 20.46 44.02 14.18 o 9 2 2 35.93 70.83 12.11 o 10 2 2 79.24 78.04 25.38 o 11 2 2 17.25 73.15 14.00 o 12 2 2 16.18 56.36 25.15 o 13 2 2 15.00 58.49 25.10 o -13 3 2 1144.53 1057.98 53.78 o -12 3 2 792.98 806.49 45.41 o -11 3 2 205.67 242.66 23.82 o -10 3 2 88.77 127.81 14.49 o -9 3 2 0.09 31.95 8.35 o -8 3 2 2.13 32.12 5.84 o -7 3 2 1034.39 1011.34 32.83 o -6 3 2 2518.12 2650.37 32.99 o -5 3 2 825.90 769.66 16.87 o -4 3 2 6164.79 6302.16 36.19 o -3 3 2 7034.47 7012.69 35.43 o -2 3 2 7209.03 6974.94 42.52 o -1 3 2 12131.99 11961.18 46.92 o 0 3 2 5277.47 5087.59 29.75 o 1 3 2 2171.05 1936.75 19.55 o 2 3 2 843.53 682.60 20.38 o 3 3 2 1860.45 1877.75 18.30 o 4 3 2 694.26 689.67 17.18 o 5 3 2 1979.73 2140.91 43.33 o 6 3 2 74.79 98.54 7.63 o 7 3 2 15.71 33.76 9.20 o 8 3 2 106.13 111.11 19.91 o 9 3 2 248.78 253.81 22.31 o 10 3 2 3410.94 3418.20 86.74 o 11 3 2 239.39 272.78 23.63 o 12 3 2 1624.00 1573.47 102.33 o 13 3 2 835.96 731.72 55.59 o -13 4 2 304.20 268.37 20.91 o -12 4 2 1176.18 1045.14 48.70 o -11 4 2 162.13 280.88 18.34 o -10 4 2 2814.78 3023.26 75.05 o -9 4 2 2089.62 2146.63 55.94 o -8 4 2 3868.89 4017.25 47.51 o -7 4 2 4238.28 4317.96 49.73 o -6 4 2 4683.02 4665.98 42.60 o -5 4 2 2010.40 1961.51 19.42 o -4 4 2 90.39 66.27 5.87 o -3 4 2 4347.17 4783.65 29.91 o -2 4 2 530.76 548.69 14.66 o -1 4 2 1.11 16.61 4.20 o 0 4 2 131.81 137.55 6.42 o 1 4 2 234.56 223.07 8.50 o 2 4 2 2236.42 2162.26 22.17 o 3 4 2 1467.29 1398.34 17.76 o 4 4 2 23340.12 24313.81 207.75 o 5 4 2 2387.03 2359.77 29.00 o 6 4 2 4085.47 4080.37 57.37 o 7 4 2 2732.93 2780.11 54.88 o 8 4 2 3488.66 3826.20 72.14 o 9 4 2 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