#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:24:05 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180860 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/91/2019120.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2019120_Fobs loop_ _publ_author_name 'Sirianni, Eric R.' 'Yap, Glenn P. A.' 'Akturk, Eser S.' 'Theopold, Klaus H.' _publ_section_title ; Improved syntheses, and structural and electronic characterization of carboxamide-substituted Tp^CONHPh,Me^ and Tp^CONHt^-Bu,Me ligands ; _journal_coeditor_code EG3122 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 947 _journal_page_last 953 _journal_volume 69 _journal_year 2013 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 97.840 _cell_angle_beta 107.809 _cell_angle_gamma 97.599 _cell_length_a 13.1310 _cell_length_b 19.4036 _cell_length_c 19.7708 _exptl_crystal_F_000 1936.00 _reflns_d_resolution_high 0.7671 _cod_data_source_file eg3122IVsup4.hkl _cod_data_source_block IV #BEGIN Tags that were not found in dictionaries: _shelx_title ' kla0343 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 357.17 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 0.34 1.15 2.74 o 2 0 0 1404.36 1424.57 26.19 o 3 0 0 8.86 17.50 7.46 o 4 0 0 14.86 12.29 8.09 o 5 0 0 4371.61 4228.11 107.09 o 6 0 0 94.87 113.15 16.29 o 7 0 0 127.57 222.64 27.65 o 8 0 0 576.16 437.60 33.14 o 9 0 0 380.22 443.37 36.61 o 10 0 0 93.54 90.51 23.23 o 11 0 0 0.81 -21.90 21.90 o 12 0 0 668.85 602.26 61.88 o 13 0 0 81.85 8.60 32.22 o 14 0 0 409.37 501.64 82.84 o 15 0 0 34.34 34.42 47.15 o -16 1 0 221.78 307.25 86.81 o -15 1 0 187.82 195.61 65.82 o -14 1 0 277.07 261.86 68.16 o -13 1 0 506.18 423.74 58.00 o -12 1 0 3014.46 2975.52 205.00 o -11 1 0 63.40 53.16 28.62 o -10 1 0 2557.13 2654.03 101.25 o -9 1 0 278.67 282.55 29.93 o -8 1 0 2433.53 2235.72 66.05 o -7 1 0 378.53 451.76 30.98 o -6 1 0 88.78 124.29 16.84 o -5 1 0 8329.67 8703.23 149.57 o -4 1 0 59.16 32.98 8.94 o -3 1 0 7668.86 7354.70 119.92 o -2 1 0 180.82 142.80 9.93 o -1 1 0 36511.95 35895.31 515.11 o 1 1 0 26556.45 26739.80 314.70 o 2 1 0 3206.77 3583.30 62.56 o 3 1 0 14092.35 13869.19 214.64 o 4 1 0 150.43 113.94 15.19 o 5 1 0 1618.45 1421.51 41.71 o 6 1 0 6551.31 7047.42 131.68 o 7 1 0 1148.90 1293.07 50.04 o 8 1 0 1627.89 1579.86 79.44 o 9 1 0 335.42 304.95 30.45 o 10 1 0 13.65 -5.69 24.53 o 11 1 0 798.22 713.31 65.28 o 12 1 0 636.58 657.87 72.60 o 13 1 0 389.24 359.54 78.05 o 14 1 0 148.25 208.98 49.92 o 15 1 0 650.80 753.16 108.01 o -16 2 0 73.67 85.71 112.64 o -15 2 0 329.21 319.80 107.92 o -14 2 0 35.87 34.71 47.15 o -13 2 0 316.89 285.91 64.92 o -12 2 0 17.93 -4.62 28.83 o -11 2 0 9105.35 9291.37 227.74 o -10 2 0 33.74 29.26 18.64 o -9 2 0 1694.52 1776.99 62.81 o -8 2 0 102.23 129.12 20.36 o -7 2 0 53.63 3.92 11.43 o -6 2 0 389.48 374.32 25.55 o -5 2 0 165.15 167.05 16.63 o -4 2 0 2252.72 2223.46 49.58 o -3 2 0 21576.63 20835.09 363.19 o -2 2 0 5425.63 4706.42 69.17 o -1 2 0 213.15 131.70 7.51 o 0 2 0 3340.56 3408.12 56.32 o 1 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o 4 3 0 10074.18 9757.44 171.96 o 5 3 0 501.40 536.32 34.49 o 6 3 0 27.07 13.36 13.25 o 7 3 0 29.11 17.33 14.41 o 8 3 0 794.10 751.13 44.27 o 9 3 0 533.29 526.11 40.43 o 10 3 0 593.18 582.20 57.56 o 11 3 0 452.40 507.14 56.76 o 12 3 0 1577.44 1530.78 174.96 o 13 3 0 24.93 6.45 37.11 o 14 3 0 547.43 685.79 75.90 o 15 3 0 11.88 33.02 43.58 o -16 4 0 69.88 61.81 58.77 o -15 4 0 3.36 -12.58 48.16 o -14 4 0 110.22 230.88 69.47 o -13 4 0 499.32 552.54 85.71 o -12 4 0 52.76 -4.80 38.62 o -11 4 0 32.67 23.24 41.90 o -10 4 0 215.50 230.99 29.67 o -9 4 0 620.61 523.14 37.66 o -8 4 0 1238.40 1416.70 67.44 o -7 4 0 23.11 37.67 14.00 o -6 4 0 304.56 487.84 28.54 o -5 4 0 27.62 13.12 9.38 o -4 4 0 2769.22 2774.11 59.83 o -3 4 0 10643.54 10357.50 166.63 o -2 4 0 41201.24 41191.81 600.87 o -1 4 0 4260.56 4290.06 74.53 o 0 4 0 1331.56 1224.94 23.77 o 1 4 0 2540.31 2427.29 59.93 o 2 4 0 13.68 9.86 11.41 o 3 4 0 43.73 51.26 10.60 o 4 4 0 7164.88 6933.39 125.73 o 5 4 0 6312.59 6308.24 121.20 o 6 4 0 1590.05 1581.03 51.16 o 7 4 0 799.56 780.04 43.93 o 8 4 0 43.30 58.91 18.85 o 9 4 0 204.43 277.88 32.25 o 10 4 0 115.68 104.33 35.27 o 11 4 0 1147.85 1136.05 88.35 o 12 4 0 66.39 19.40 31.53 o 13 4 0 172.38 103.32 40.91 o 14 4 0 288.71 294.88 57.90 o 15 4 0 32.51 29.92 49.91 o -16 5 0 77.42 161.35 65.30 o -15 5 0 17.38 -10.58 47.83 o -14 5 0 83.66 88.73 81.61 o -13 5 0 101.05 54.42 73.52 o -12 5 0 9.33 -24.85 34.91 o -11 5 0 3.35 -6.86 20.40 o -10 5 0 194.89 187.92 36.72 o -9 5 0 512.99 429.80 34.27 o -8 5 0 3321.67 3462.38 84.52 o -7 5 0 6313.77 6560.16 136.48 o -6 5 0 3240.09 2948.79 80.79 o -5 5 0 167.74 62.05 17.13 o -4 5 0 2.45 6.42 9.64 o -3 5 0 20602.65 20120.04 307.93 o -2 5 0 1934.03 1926.30 63.28 o -1 5 0 1351.63 1318.76 33.38 o 0 5 0 325.83 317.51 11.54 o 1 5 0 12671.08 12171.56 226.61 o 2 5 0 3674.19 3640.69 60.37 o 3 5 0 12943.00 12897.60 209.00 o 4 5 0 41.13 54.67 13.71 o 5 5 0 414.08 352.92 26.98 o 6 5 0 121.64 186.24 22.46 o 7 5 0 245.27 225.10 26.42 o 8 5 0 527.88 550.44 40.93 o 9 5 0 44.97 40.65 22.61 o 10 5 0 0.00 -21.37 42.87 o 11 5 0 559.58 533.82 73.36 o 12 5 0 8.76 3.35 32.05 o 13 5 0 561.55 713.70 76.03 o 14 5 0 8.35 -46.01 46.01 o 15 5 0 172.46 100.68 60.07 o -16 6 0 2.44 -62.73 62.73 o -15 6 0 401.70 316.42 81.97 o -14 6 0 80.49 88.25 54.84 o -13 6 0 1571.51 1466.10 165.93 o -12 6 0 0.11 -23.36 39.80 o -11 6 0 5834.93 5911.35 165.17 o -10 6 0 80.29 116.86 24.85 o -9 6 0 1310.96 1165.46 51.58 o -8 6 0 965.42 1197.98 58.82 o -7 6 0 5698.58 6515.86 128.06 o -6 6 0 144.90 196.41 27.75 o -5 6 0 675.36 518.36 28.11 o -4 6 0 22589.74 22806.52 351.59 o -3 6 0 5294.41 5304.73 98.07 o -2 6 0 2315.36 2172.68 49.89 o -1 6 0 771.48 671.06 28.84 o 0 6 0 1936.98 1976.45 36.88 o 1 6 0 1268.63 1420.36 50.21 o 2 6 0 236.17 287.14 14.14 o 3 6 0 5874.34 5318.36 100.88 o 4 6 0 2330.86 2099.42 77.69 o 5 6 0 6428.57 6518.05 172.71 o 6 6 0 156.47 259.54 26.16 o 7 6 0 764.22 699.25 55.49 o 8 6 0 52.74 20.89 20.06 o 9 6 0 135.22 100.57 25.11 o 10 6 0 148.74 83.51 44.86 o 11 6 0 204.14 106.08 43.36 o 12 6 0 399.02 459.63 62.19 o 13 6 0 50.31 1.91 47.04 o 14 6 0 17.68 38.08 52.93 o -16 7 0 5.94 -38.05 68.12 o -15 7 0 0.31 6.70 51.48 o -14 7 0 241.05 309.01 75.72 o -13 7 0 30.51 61.40 63.40 o -12 7 0 1347.06 1356.78 140.30 o -11 7 0 144.64 92.61 33.79 o -10 7 0 1581.92 1566.17 106.21 o -9 7 0 785.68 759.72 43.97 o -8 7 0 2984.21 2976.83 76.77 o -7 7 0 5.54 4.70 11.12 o -6 7 0 108.27 152.06 19.05 o -5 7 0 14.53 1.84 9.88 o -4 7 0 1557.74 1471.54 72.11 o -3 7 0 36.61 10.79 9.38 o -2 7 0 1511.95 1560.08 42.27 o -1 7 0 465.05 438.14 23.93 o 0 7 0 5749.72 5481.49 85.52 o 1 7 0 6559.57 6939.40 149.22 o 2 7 0 7888.86 8283.76 215.69 o 3 7 0 1124.84 1490.72 69.51 o 4 7 0 8002.23 8150.74 148.80 o 5 7 0 1166.33 1230.75 48.61 o 6 7 0 1485.69 1353.00 55.11 o 7 7 0 17.12 17.21 16.38 o 8 7 0 2688.50 2683.08 81.80 o 9 7 0 3.58 -18.84 18.84 o 10 7 0 784.31 887.36 103.41 o 11 7 0 386.09 196.42 161.88 o 12 7 0 481.91 388.99 101.18 o 13 7 0 36.82 150.91 59.05 o 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109.94 o -12 9 0 22.34 3.80 84.99 o -11 9 0 127.55 197.39 40.14 o -10 9 0 241.32 210.98 53.23 o -9 9 0 6.98 -20.41 21.92 o -8 9 0 180.16 165.38 21.22 o -7 9 0 1177.32 1076.93 45.20 o -6 9 0 118.66 154.94 19.54 o -5 9 0 240.74 246.10 22.03 o -4 9 0 3437.25 3437.72 78.77 o -3 9 0 4802.72 4860.81 99.39 o -2 9 0 424.75 481.17 28.70 o -1 9 0 13862.33 13268.42 218.97 o 0 9 0 1987.45 2373.09 55.38 o 1 9 0 3820.74 3424.55 95.25 o 2 9 0 1185.17 1222.53 63.78 o 3 9 0 1714.33 1735.80 68.27 o 4 9 0 1142.92 1347.44 46.37 o 5 9 0 7.59 -2.47 15.12 o 6 9 0 108.40 138.96 23.47 o 7 9 0 34.05 44.23 20.09 o 8 9 0 13.95 9.33 24.96 o 9 9 0 585.60 579.87 57.82 o 10 9 0 936.78 875.21 98.45 o 11 9 0 358.38 347.42 145.69 o 12 9 0 4.75 -1.91 43.74 o 13 9 0 638.05 636.99 162.55 o -15 10 0 203.63 252.84 76.24 o -14 10 0 9.48 17.86 78.24 o -13 10 0 1643.18 1468.72 134.97 o -12 10 0 17.61 5.40 39.07 o -11 10 0 360.82 350.99 55.07 o -10 10 0 17.22 -5.04 23.58 o -9 10 0 8.39 52.01 26.53 o -8 10 0 660.63 728.82 95.47 o 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177.64 21.85 o -2 11 0 900.58 1021.38 59.78 o -1 11 0 213.76 240.12 22.10 o 0 11 0 2152.32 2288.63 56.34 o 1 11 0 81.36 42.18 46.97 o 2 11 0 3996.28 3713.10 111.45 o 3 11 0 255.55 291.82 39.85 o 4 11 0 1454.10 1513.69 82.89 o 5 11 0 67.13 17.59 23.65 o 6 11 0 737.09 752.38 63.74 o 7 11 0 1451.79 1537.35 184.22 o 8 11 0 65.88 84.88 33.30 o 9 11 0 5.57 32.09 51.94 o 10 11 0 58.74 78.61 52.88 o 11 11 0 6.95 104.95 52.63 o 12 11 0 41.25 9.04 97.80 o 13 11 0 21.95 95.78 87.69 o -15 12 0 523.83 655.47 237.42 o -14 12 0 28.68 56.60 53.84 o -13 12 0 139.54 139.75 59.57 o -12 12 0 245.44 149.33 43.30 o -11 12 0 620.31 614.76 83.40 o -10 12 0 21.43 32.34 40.03 o -9 12 0 1392.24 1436.90 90.21 o -8 12 0 57.93 68.70 30.17 o -7 12 0 139.18 37.88 25.51 o -6 12 0 773.84 771.16 42.93 o -5 12 0 78.81 37.65 16.85 o -4 12 0 1654.38 1593.09 57.71 o -3 12 0 9.43 27.98 15.14 o -2 12 0 400.22 426.63 31.63 o -1 12 0 2162.31 2077.55 58.83 o 0 12 0 89.37 55.95 10.32 o 1 12 0 6814.83 6676.47 282.61 o 2 12 0 280.59 223.25 35.03 o 3 12 0 3426.46 3467.46 113.34 o 4 12 0 68.09 116.98 31.43 o 5 12 0 1017.26 1086.80 73.93 o 6 12 0 28.66 45.92 43.89 o 7 12 0 1092.92 1140.32 82.23 o 8 12 0 15.96 -4.71 28.56 o 9 12 0 288.06 267.46 64.53 o 10 12 0 68.61 8.91 45.67 o 11 12 0 146.98 293.25 72.93 o 12 12 0 16.30 -38.31 93.76 o -15 13 0 0.57 -54.63 54.63 o -14 13 0 29.55 9.33 78.92 o -13 13 0 27.75 50.29 51.48 o -12 13 0 60.28 44.38 52.75 o -11 13 0 503.04 463.98 58.65 o -10 13 0 91.44 75.55 34.36 o -9 13 0 2094.09 1936.94 106.59 o -8 13 0 232.20 198.90 39.60 o -7 13 0 1392.95 1431.18 86.02 o -6 13 0 362.39 478.43 36.80 o -5 13 0 5593.00 5843.31 127.08 o -4 13 0 19.18 37.83 17.60 o -3 13 0 1240.59 1120.35 50.77 o -2 13 0 3.89 6.20 13.41 o -1 13 0 1012.07 1000.55 42.85 o 0 13 0 1063.82 1066.79 77.96 o 1 13 0 646.89 660.37 54.59 o 2 13 0 365.18 262.83 58.77 o 3 13 0 2863.60 3053.39 116.23 o 4 13 0 742.40 783.42 75.59 o 5 13 0 191.78 118.39 34.25 o 6 13 0 556.35 497.74 74.39 o 7 13 0 833.28 771.11 87.63 o 8 13 0 1643.07 1484.60 155.64 o 9 13 0 300.60 428.37 76.57 o 10 13 0 299.01 167.98 83.64 o 11 13 0 35.45 23.73 50.87 o 12 13 0 19.50 5.51 52.78 o -14 14 0 0.89 -52.30 61.38 o -13 14 0 78.51 68.71 91.73 o -12 14 0 22.27 33.70 39.10 o -11 14 0 13.49 -61.68 66.78 o -10 14 0 26.23 -15.38 28.22 o -9 14 0 356.19 417.88 54.94 o -8 14 0 5930.77 5942.77 172.57 o -7 14 0 225.08 229.60 41.04 o -6 14 0 2566.17 2747.95 167.57 o -5 14 0 313.37 290.42 30.84 o -4 14 0 3840.93 3726.16 117.02 o -3 14 0 9.20 23.36 16.43 o -2 14 0 173.19 154.81 23.07 o -1 14 0 29.40 53.87 17.12 o 0 14 0 5850.29 5949.25 160.63 o 1 14 0 1202.60 1188.36 126.21 o 2 14 0 144.38 64.16 36.43 o 3 14 0 329.34 384.28 107.25 o 4 14 0 1152.88 1378.41 189.76 o 5 14 0 70.26 109.44 35.60 o 6 14 0 9.57 1.86 29.90 o 7 14 0 51.36 46.31 36.45 o 8 14 0 183.89 246.51 49.46 o 9 14 0 24.63 1.90 43.98 o 10 14 0 459.83 478.77 90.38 o 11 14 0 19.30 112.78 61.82 o -14 15 0 289.73 294.71 97.80 o -13 15 0 0.83 1.95 47.04 o -12 15 0 162.85 242.05 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