#------------------------------------------------------------------------------ #$Date: 2013-10-24 17:51:33 +0300 (Thu, 24 Oct 2013) $ #$Revision: 89414 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/91/2019121.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2019121_Fobs loop_ _publ_author_name 'Sirianni, Eric R.' 'Yap, Glenn P. A.' 'Akturk, Eser S.' 'Theopold, Klaus H.' _publ_section_title ; Improved syntheses, and structural and electronic characterization of carboxamide-substituted Tp^CONHPh,Me^ and Tp^CONHt^-Bu,Me ligands ; _journal_coeditor_code EG3122 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 947 _journal_page_last 953 _journal_volume 69 _journal_year 2013 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 15.1972 _cell_length_b 15.7870 _cell_length_c 34.9020 _exptl_crystal_F_000 2880.00 _reflns_d_resolution_high 0.7695 _[local]_cod_data_source_file eg3122Vsup5.hkl _[local]_cod_data_source_block V #BEGIN Tags that were not found in dictionaries: _shelx_title ' kla0325 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 350.70 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 5846.98 3717.89 100.45 o 6 0 0 11271.78 10051.48 365.23 o 8 0 0 7704.37 8922.59 274.77 o 10 0 0 210.51 199.47 40.93 o 12 0 0 96.24 108.95 47.14 o 14 0 0 186.62 192.07 59.66 o 16 0 0 446.75 596.81 172.06 o 18 0 0 627.36 751.82 98.69 o 2 1 0 3416.42 3614.59 56.02 o 3 1 0 42168.10 44954.34 829.51 o 4 1 0 2092.35 2250.98 56.55 o 5 1 0 2230.69 2075.39 64.63 o 6 1 0 18160.98 18502.12 413.02 o 7 1 0 1485.72 1493.68 50.34 o 8 1 0 987.32 829.83 39.03 o 9 1 0 256.93 186.03 27.56 o 10 1 0 1197.58 1044.38 48.70 o 11 1 0 8173.22 7658.23 177.45 o 12 1 0 7901.08 7904.68 185.84 o 13 1 0 6.21 -9.26 33.26 o 14 1 0 10.57 17.52 37.75 o 15 1 0 496.74 412.24 55.28 o 16 1 0 1499.81 1575.25 80.43 o 17 1 0 185.41 144.88 50.18 o 18 1 0 550.34 645.76 67.17 o 19 1 0 392.79 447.36 73.18 o 1 2 0 45.80 127.33 10.12 o 2 2 0 2676.32 1829.95 34.99 o 3 2 0 80052.31 78243.69 1276.06 o 4 2 0 3993.80 3517.00 73.25 o 5 2 0 62.88 103.73 18.78 o 6 2 0 1214.09 1398.71 50.92 o 7 2 0 1665.48 1076.00 41.77 o 8 2 0 9575.22 9432.44 204.48 o 9 2 0 1376.11 1432.46 54.18 o 10 2 0 3844.06 4059.17 105.13 o 11 2 0 7.39 -17.25 27.43 o 12 2 0 30.21 -16.17 30.66 o 13 2 0 216.43 192.99 38.63 o 14 2 0 4256.60 4379.01 125.04 o 15 2 0 1449.07 1261.57 70.07 o 16 2 0 2.53 79.46 46.02 o 17 2 0 288.84 179.34 52.62 o 18 2 0 50.23 53.87 59.82 o 19 2 0 58.70 64.51 63.45 o 1 3 0 271.19 419.07 15.85 o 2 3 0 2042.86 1193.54 33.27 o 3 3 0 11281.27 10814.08 181.88 o 4 3 0 7427.57 6972.12 127.90 o 5 3 0 6102.62 5565.79 113.10 o 6 3 0 1113.46 943.72 32.00 o 7 3 0 7970.48 9142.95 196.77 o 8 3 0 6177.33 5434.00 126.54 o 9 3 0 24.52 81.88 27.59 o 10 3 0 191.74 158.43 29.29 o 11 3 0 2844.34 2923.49 87.74 o 12 3 0 603.89 560.38 44.30 o 13 3 0 42.99 5.73 43.24 o 14 3 0 66.69 6.07 36.91 o 15 3 0 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0 7.67 8.46 26.91 o 11 5 0 171.78 119.06 31.55 o 12 5 0 52.06 29.05 32.51 o 13 5 0 1293.32 1347.46 66.26 o 14 5 0 68.34 59.18 45.33 o 15 5 0 163.55 127.84 51.16 o 16 5 0 14.06 -7.70 49.35 o 17 5 0 82.51 1.79 54.92 o 18 5 0 248.45 255.03 81.90 o 19 5 0 509.51 477.81 78.14 o 0 6 0 4900.81 5786.93 155.23 o 1 6 0 446.43 461.49 21.18 o 2 6 0 51.53 30.07 10.56 o 3 6 0 451.45 349.48 23.49 o 4 6 0 343.46 438.90 26.59 o 5 6 0 126.09 254.37 23.85 o 6 6 0 9960.46 11321.15 208.79 o 7 6 0 119.25 124.82 19.05 o 8 6 0 486.31 377.13 30.03 o 9 6 0 3525.64 3172.63 87.47 o 10 6 0 93.84 117.43 29.46 o 11 6 0 12.78 -5.58 29.17 o 12 6 0 419.46 474.97 51.59 o 13 6 0 512.97 575.62 58.16 o 14 6 0 4762.61 4620.53 148.35 o 15 6 0 1224.43 1173.85 80.28 o 16 6 0 74.05 -30.97 50.95 o 17 6 0 11.96 9.87 55.72 o 18 6 0 4.45 -16.38 60.54 o 1 7 0 238.03 170.13 17.21 o 2 7 0 26297.53 25506.79 449.71 o 3 7 0 819.93 1145.24 40.29 o 4 7 0 3631.87 3431.95 80.84 o 5 7 0 1831.09 1546.11 50.15 o 6 7 0 740.08 729.73 35.08 o 7 7 0 43.77 20.41 22.11 o 8 7 0 361.20 339.66 29.78 o 9 7 0 739.53 676.10 56.71 o 10 7 0 41.00 41.06 35.93 o 11 7 0 722.47 662.12 56.25 o 12 7 0 80.26 3.49 41.57 o 13 7 0 2502.41 2314.17 102.07 o 14 7 0 59.71 -23.00 46.98 o 15 7 0 1520.05 1617.56 92.61 o 16 7 0 3.18 32.74 54.97 o 17 7 0 990.69 842.94 79.75 o 18 7 0 379.88 341.62 71.96 o 0 8 0 3742.47 3689.58 109.98 o 1 8 0 8805.50 8256.38 155.12 o 2 8 0 54.92 45.69 15.73 o 3 8 0 5150.92 5422.58 127.20 o 4 8 0 2125.56 1888.76 56.33 o 5 8 0 2090.63 1688.69 53.79 o 6 8 0 1495.18 1577.35 53.60 o 7 8 0 2018.54 1796.67 59.39 o 8 8 0 2339.30 2084.27 80.61 o 9 8 0 1061.41 996.36 58.94 o 10 8 0 737.49 858.77 58.76 o 11 8 0 12.83 -7.90 39.39 o 12 8 0 19.90 96.01 42.67 o 13 8 0 239.77 192.57 57.54 o 14 8 0 278.58 339.32 64.72 o 15 8 0 28.58 51.09 53.64 o 16 8 0 100.39 211.28 61.55 o 17 8 0 210.10 132.50 63.29 o 18 8 0 6.86 -2.97 63.92 o 1 9 0 357.06 349.90 23.75 o 2 9 0 276.45 338.21 27.92 o 3 9 0 1080.95 1283.63 47.21 o 4 9 0 3655.41 4025.88 102.80 o 5 9 0 2314.87 2364.47 68.00 o 6 9 0 2444.09 2294.46 67.95 o 7 9 0 2809.95 2833.09 78.70 o 8 9 0 4190.99 4473.53 130.79 o 9 9 0 622.89 665.95 52.95 o 10 9 0 506.15 518.58 57.69 o 11 9 0 38.40 -32.48 40.17 o 12 9 0 3823.87 3634.10 173.20 o 13 9 0 1323.25 1304.59 80.92 o 14 9 0 87.01 77.35 52.23 o 15 9 0 3.64 -19.93 51.70 o 16 9 0 17.69 -2.69 57.00 o 17 9 0 141.35 172.61 64.33 o 0 10 0 957.52 780.60 46.79 o 1 10 0 1.16 -10.36 17.95 o 2 10 0 1808.79 1878.04 51.98 o 3 10 0 831.49 887.56 41.22 o 4 10 0 2719.38 2603.65 72.00 o 5 10 0 336.45 295.90 36.64 o 6 10 0 10719.97 10170.98 210.69 o 7 10 0 235.74 264.67 36.67 o 8 10 0 287.42 275.21 44.50 o 9 10 0 738.72 724.81 56.71 o 10 10 0 581.67 578.11 54.30 o 11 10 0 12.90 -38.34 47.04 o 12 10 0 21.11 24.39 47.14 o 13 10 0 2.57 -33.18 49.54 o 14 10 0 305.54 296.08 60.40 o 15 10 0 2.91 38.87 56.95 o 16 10 0 283.46 282.26 83.54 o 17 10 0 87.35 96.19 80.32 o 1 11 0 1262.20 1346.52 45.78 o 2 11 0 2348.82 2016.78 62.44 o 3 11 0 967.23 988.31 45.72 o 4 11 0 3.78 -2.52 25.28 o 5 11 0 5402.76 5623.61 128.47 o 6 11 0 20.43 88.14 35.59 o 7 11 0 317.91 290.01 40.01 o 8 11 0 1728.16 1722.42 80.16 o 9 11 0 1332.63 1259.99 71.34 o 10 11 0 2198.83 2167.18 95.93 o 11 11 0 2130.61 2028.07 95.44 o 12 11 0 602.80 626.62 63.87 o 13 11 0 147.90 193.32 56.26 o 14 11 0 19.43 12.08 55.94 o 15 11 0 0.49 23.05 68.43 o 16 11 0 85.70 -34.57 80.88 o 0 12 0 122.84 147.97 37.18 o 1 12 0 7919.48 7774.10 155.08 o 2 12 0 4401.89 4205.12 109.63 o 3 12 0 831.49 836.43 45.36 o 4 12 0 329.10 398.93 36.61 o 5 12 0 287.77 383.69 36.66 o 6 12 0 1769.56 1694.30 65.35 o 7 12 0 2300.23 2386.26 126.75 o 8 12 0 5362.10 5626.40 161.96 o 9 12 0 222.38 127.27 46.12 o 10 12 0 1716.06 1852.65 90.79 o 11 12 0 17.86 14.91 46.11 o 12 12 0 11.62 23.97 51.62 o 13 12 0 662.40 587.08 113.00 o 14 12 0 1330.60 1428.40 110.09 o 15 12 0 19.41 1.18 76.38 o 16 12 0 153.32 116.39 158.39 o 1 13 0 2352.85 2462.11 77.18 o 2 13 0 1389.76 1490.31 60.08 o 3 13 0 3836.13 3788.11 100.51 o 4 13 0 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889.51 60.77 o 3 5 28 639.14 578.27 53.69 o 4 5 28 916.55 945.21 70.76 o 5 5 28 632.00 709.71 65.10 o 6 5 28 2511.90 2487.23 92.22 o 7 5 28 34.00 -30.75 40.79 o 8 5 28 226.06 250.15 48.13 o 9 5 28 160.98 151.35 47.26 o 10 5 28 162.65 221.08 51.83 o 11 5 28 437.70 481.38 75.42 o 12 5 28 165.62 222.27 70.29 o 13 5 28 204.83 257.26 87.29 o 14 5 28 110.01 5.00 70.87 o -14 6 28 202.71 350.13 96.51 o -13 6 28 32.53 -69.17 77.72 o -12 6 28 920.91 803.86 121.03 o -11 6 28 551.39 644.78 76.52 o -10 6 28 615.46 666.64 78.82 o -9 6 28 82.99 154.83 101.31 o -8 6 28 2271.47 2216.45 115.51 o -7 6 28 418.79 293.39 61.97 o -6 6 28 1649.21 1779.33 110.97 o -5 6 28 563.40 554.77 82.94 o -4 6 28 238.81 282.32 67.00 o -3 6 28 455.42 444.91 71.01 o -2 6 28 1409.61 1413.91 97.44 o -1 6 28 570.27 504.20 108.38 o 0 6 28 1114.69 1026.56 75.73 o 1 6 28 619.29 658.37 64.13 o 2 6 28 1463.14 1444.71 75.73 o 3 6 28 398.78 447.52 58.44 o 4 6 28 271.04 282.97 50.15 o 5 6 28 580.32 506.81 55.61 o 6 6 28 1575.47 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