Crystallography Open Database

Information card for entry 2019305

2019304 << 2019305 >> 2019306

Preview

Coordinates	2019305.cif
Original IUCr paper	HTML

Structure parameters

Chemical name	{5,7-Bis[2-(2-methylphenyl)diazen-1-yl]quinolin-8-olato-κ^2^<i>N</i>^1^,<i>O</i>}tricarbonyl(pyridine-κ<i>N</i>)rhenium(I)
Formula	C31 H23 N6 O4 Re
Calculated formula	C31 H23 N6 O4 Re
Title of publication	Distorted octahedral environments in tricarbonylrhenium(I) complexes of 5-[2-(2,4,6-trimethylphenyl)diazen-1-yl]quinolin-8-olate and 5,7-bis[2-(2-methylphenyl)diazen-1-yl]quinolin-8-olate
Authors of publication	Schutte-Smith, Marietjie; Muller, Theunis J.; Visser, Hendrik G.; Roodt, Andreas
Journal of publication	Acta Crystallographica Section C
Year of publication	2013
Journal volume	69
Journal issue	12
Pages of publication	1467 - 1471
a	7.9776 ± 0.0006 Å
b	11.6818 ± 0.0008 Å
c	15.3994 ± 0.0011 Å
α	92.113 ± 0.004°
β	98.13 ± 0.003°
γ	92.384 ± 0.004°
Cell volume	1418.13 ± 0.18 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0286
Residual factor for significantly intense reflections	0.0219
Weighted residual factors for all reflections included in the refinement	0.0449
Goodness-of-fit parameter for all reflections included in the refinement	1.088
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176760 (current)	2016-02-20	cif/2/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/01.	2019305.cif
92243	2014-01-12	cif/ Adding structures of 2019304, 2019305 via cif-deposit CGI script.	2019305.cif