# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_2019403 _cell_angle_alpha 90 _cell_angle_beta 98.359(4) _cell_angle_gamma 90 _cell_length_a 8.2189(5) _cell_length_b 9.6676(6) _cell_length_c 9.8361(4) _exptl_crystal_F_000 392 _reflns_d_resolution_high 0.7252 _cod_data_source_file lg3130IIsup3.hkl _cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 111.86 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 935.53 951.75 5.56 o 3 0 0 1150.16 1000.38 6.96 o 4 0 0 496.21 546.52 9.10 o 5 0 0 1786.42 1907.47 12.43 o 6 0 0 82.77 74.58 2.17 o 7 0 0 107.66 111.61 3.30 o 8 0 0 1.08 0.95 0.62 < 9 0 0 916.39 903.72 17.22 o 10 0 0 281.47 264.26 9.91 o 11 0 0 0.09 0.41 1.28 < 1 1 0 831.93 857.06 4.76 o 2 1 0 3468.50 3704.36 13.10 o 3 1 0 313.54 348.70 2.57 o 4 1 0 48.25 66.90 1.10 o 5 1 0 7.90 7.04 0.47 o 6 1 0 51.41 55.03 1.37 o 7 1 0 412.13 420.72 6.46 o 8 1 0 339.02 332.32 5.21 o 9 1 0 6.21 7.16 1.33 o 10 1 0 1.98 0.81 0.84 < 11 1 0 89.00 85.74 6.12 o 0 2 0 2424.63 2126.18 12.81 o 1 2 0 961.47 881.03 5.87 o 2 2 0 14.44 23.77 0.85 o 3 2 0 97.22 108.71 1.72 o 4 2 0 14.31 12.61 1.04 o 5 2 0 117.56 106.46 1.76 o 6 2 0 20.43 24.26 1.18 o 7 2 0 129.96 118.55 3.10 o 8 2 0 1.76 2.02 1.09 < 9 2 0 74.15 72.00 4.81 o 10 2 0 8.47 10.13 1.58 o 11 2 0 103.14 106.82 6.93 o 1 3 0 1165.08 1123.30 7.57 o 2 3 0 29.93 51.76 1.39 o 3 3 0 582.89 630.11 4.61 o 4 3 0 286.36 259.75 3.18 o 5 3 0 445.72 450.59 4.23 o 6 3 0 187.46 192.90 3.25 o 7 3 0 0.60 1.15 0.53 < 8 3 0 336.70 339.01 5.78 o 9 3 0 1.11 0.69 0.96 < 10 3 0 71.11 66.10 4.93 o 0 4 0 99.51 132.76 3.94 o 1 4 0 13.50 24.37 1.04 o 2 4 0 674.91 667.70 5.64 o 3 4 0 4203.71 4399.69 19.63 o 4 4 0 300.32 299.35 3.01 o 5 4 0 10.18 9.56 0.80 o 6 4 0 1506.19 1456.53 14.06 o 7 4 0 401.22 395.42 5.08 o 8 4 0 112.93 112.68 3.45 o 9 4 0 160.21 162.63 4.36 o 10 4 0 261.50 278.02 9.97 o 1 5 0 581.02 611.89 7.01 o 2 5 0 1022.98 1073.38 7.95 o 3 5 0 729.14 756.53 6.94 o 4 5 0 382.39 372.02 4.37 o 5 5 0 858.11 864.73 7.11 o 6 5 0 317.70 320.97 4.14 o 7 5 0 12.58 11.40 1.10 o 8 5 0 235.99 235.37 5.14 o 9 5 0 5.94 9.01 1.59 o 0 6 0 623.34 716.88 12.09 o 1 6 0 6.16 5.73 0.80 o 2 6 0 37.60 40.99 1.72 o 3 6 0 92.33 106.92 2.46 o 4 6 0 783.30 796.71 8.07 o 5 6 0 24.49 28.89 1.66 o 6 6 0 586.17 614.17 9.86 o 7 6 0 362.62 374.10 8.10 o 8 6 0 75.44 74.30 3.86 o 9 6 0 296.45 309.16 10.39 o 1 7 0 252.75 274.86 4.48 o 2 7 0 572.52 524.52 6.30 o 3 7 0 351.09 331.92 6.54 o 4 7 0 294.48 302.45 6.59 o 5 7 0 528.72 515.74 9.03 o 6 7 0 0.87 1.28 0.89 < 7 7 0 82.35 82.85 4.02 o 8 7 0 133.66 138.22 5.42 o 0 8 0 8.82 6.08 1.44 o 1 8 0 9.68 9.18 1.19 o 2 8 0 25.80 24.65 1.89 o 3 8 0 569.26 557.80 8.76 o 4 8 0 447.24 429.35 12.58 o 5 8 0 2.86 3.89 1.07 o 6 8 0 301.21 317.21 7.76 o 7 8 0 18.89 20.17 2.20 o 8 8 0 24.13 25.50 3.22 o 1 9 0 23.86 26.48 1.47 o 2 9 0 66.74 67.54 3.20 o 3 9 0 227.52 222.05 5.91 o 4 9 0 249.00 258.83 6.59 o 5 9 0 400.69 404.09 8.53 o 6 9 0 122.50 125.27 7.85 o 0 10 0 126.59 125.94 6.43 o 1 10 0 156.02 152.32 5.02 o 2 10 0 31.69 39.46 2.65 o 3 10 0 49.28 46.00 2.95 o 4 10 0 0.60 0.04 0.85 < 5 10 0 144.44 157.71 5.58 o 1 11 0 228.44 213.30 6.27 o 2 11 0 575.58 559.59 10.28 o 3 11 0 19.26 15.92 1.92 o 4 11 0 383.26 388.97 8.95 o 0 12 0 442.66 451.82 13.68 o 1 12 0 79.46 78.84 4.08 o 2 12 0 56.14 47.86 3.27 o 3 12 0 7.02 8.17 1.62 o 1 13 0 23.85 25.66 2.61 o -11 1 1 19.80 22.22 2.28 o -10 1 1 23.23 24.84 2.32 o -9 1 1 267.51 279.63 6.99 o -8 1 1 1205.22 1162.67 9.77 o -7 1 1 214.43 208.81 4.42 o -6 1 1 73.72 61.79 2.08 o -5 1 1 246.95 314.18 3.30 o -4 1 1 1875.05 1948.60 7.80 o -3 1 1 68.07 48.84 1.05 o -2 1 1 2052.03 1942.86 10.23 o -1 1 1 1385.98 1311.88 5.21 o 0 1 1 567.63 619.82 3.85 o 1 1 1 296.35 321.26 2.36 o 2 1 1 1.87 1.91 0.35 o 3 1 1 190.95 203.58 2.06 o 4 1 1 292.38 326.94 2.36 o 5 1 1 256.81 266.61 2.65 o 6 1 1 123.31 133.40 2.35 o 7 1 1 163.73 171.04 3.63 o 8 1 1 6.93 6.31 0.84 o 9 1 1 564.74 551.17 7.22 o 10 1 1 210.15 213.06 6.09 o -11 2 1 61.85 63.14 3.80 o -10 2 1 347.30 340.78 8.22 o -9 2 1 26.34 25.51 3.08 o -8 2 1 300.88 293.01 9.30 o -7 2 1 1029.25 1019.57 8.80 o -6 2 1 283.00 262.15 3.83 o -5 2 1 148.54 139.25 2.57 o -4 2 1 2267.78 2255.25 13.21 o -3 2 1 1153.39 1165.59 8.66 o -2 2 1 2164.01 2058.46 9.36 o -1 2 1 10762.30 11555.40 33.45 o 0 2 1 6711.80 6544.15 16.95 o 1 2 1 8061.19 9254.12 25.45 o 2 2 1 1136.47 1100.14 4.79 o 3 2 1 35.61 53.30 1.05 o 4 2 1 1532.53 1569.38 8.13 o 5 2 1 369.39 371.90 2.93 o 6 2 1 324.73 307.78 3.32 o 7 2 1 2.34 3.15 0.56 o 8 2 1 487.00 478.74 8.52 o 9 2 1 735.48 736.68 9.96 o 10 2 1 17.77 15.02 2.55 o -10 3 1 40.89 37.09 3.93 o -9 3 1 15.26 14.54 1.62 o -8 3 1 62.22 56.57 2.85 o -7 3 1 170.32 168.46 3.31 o -6 3 1 194.45 204.18 3.06 o -5 3 1 1602.79 1660.95 10.48 o -4 3 1 122.07 129.61 2.29 o -3 3 1 1088.23 1085.06 5.94 o -2 3 1 938.76 908.76 6.29 o -1 3 1 293.85 320.70 2.93 o 0 3 1 497.64 466.97 4.11 o 1 3 1 2212.53 2190.96 10.67 o 2 3 1 32.96 35.08 0.98 o 3 3 1 52.60 46.64 1.02 o 4 3 1 46.18 35.25 1.01 o 5 3 1 259.59 273.79 3.68 o 6 3 1 1682.95 1740.61 13.16 o 7 3 1 239.96 237.44 3.77 o 8 3 1 243.02 244.48 4.72 o 9 3 1 8.26 7.22 1.40 o -10 4 1 38.93 40.80 4.08 o -9 4 1 116.07 128.54 4.56 o -8 4 1 358.88 345.98 6.19 o -7 4 1 453.85 430.38 6.46 o -6 4 1 386.01 387.48 4.50 o -5 4 1 1004.24 982.16 6.09 o -4 4 1 129.53 135.95 2.34 o -3 4 1 52.27 59.20 1.44 o -2 4 1 1438.25 1518.55 6.44 o -1 4 1 588.81 648.17 4.27 o 0 4 1 132.48 144.88 2.66 o 1 4 1 38.29 48.04 1.36 o 2 4 1 903.91 1030.51 6.87 o 3 4 1 10.64 14.66 0.78 o 4 4 1 3.38 5.28 0.44 o 5 4 1 955.34 978.30 6.20 o 6 4 1 786.72 782.82 7.86 o 7 4 1 0.03 1.21 0.47 < 8 4 1 102.57 105.55 3.25 o 9 4 1 0.08 1.12 0.96 < -10 5 1 2.08 1.72 1.27 < -9 5 1 66.17 54.08 2.69 o -8 5 1 58.39 54.33 2.60 o -7 5 1 843.91 869.37 8.68 o -6 5 1 295.65 288.83 3.96 o -5 5 1 717.57 721.31 5.40 o -4 5 1 65.37 73.56 2.05 o -3 5 1 0.36 5.45 0.61 o -2 5 1 245.86 248.15 2.99 o -1 5 1 1214.21 1293.44 7.52 o 0 5 1 106.66 118.36 3.94 o 1 5 1 168.44 179.32 2.95 o 2 5 1 670.67 777.50 8.25 o 3 5 1 1013.35 1036.24 6.99 o 4 5 1 1283.17 1238.82 8.10 o 5 5 1 28.16 28.36 1.30 o 6 5 1 289.04 301.39 3.90 o 7 5 1 52.28 58.26 3.08 o 8 5 1 53.50 50.78 2.36 o 9 5 1 73.12 82.53 6.42 o -9 6 1 18.67 16.88 1.86 o -8 6 1 1.14 2.24 0.89 < -7 6 1 353.14 370.58 8.20 o -6 6 1 0.01 -0.22 0.94 < -5 6 1 506.11 499.77 6.71 o -4 6 1 338.58 351.61 5.40 o -3 6 1 352.80 378.72 4.68 o -2 6 1 550.64 570.16 4.96 o -1 6 1 0.17 1.10 0.37 < 0 6 1 85.03 108.76 4.55 o 1 6 1 1.58 -0.04 0.58 < 2 6 1 1241.78 1175.73 7.73 o 3 6 1 2027.78 1990.29 15.33 o 4 6 1 40.71 45.33 1.90 o 5 6 1 224.82 235.98 4.46 o 6 6 1 376.62 381.44 5.87 o 7 6 1 493.35 497.04 9.22 o 8 6 1 181.94 195.61 6.06 o -9 7 1 99.84 106.20 4.60 o -8 7 1 95.14 103.32 4.75 o -7 7 1 21.34 23.37 2.24 o -6 7 1 107.24 105.69 4.34 o -5 7 1 932.47 954.06 12.52 o -4 7 1 206.48 226.10 5.76 o -3 7 1 428.46 471.41 7.98 o -2 7 1 269.96 287.34 3.69 o -1 7 1 183.54 196.80 3.02 o 0 7 1 198.93 210.52 4.89 o 1 7 1 59.92 61.08 2.67 o 2 7 1 25.66 29.66 1.96 o 3 7 1 123.49 117.20 3.89 o 4 7 1 1178.97 1165.77 12.80 o 5 7 1 181.45 180.21 5.27 o 6 7 1 76.69 78.92 3.67 o 7 7 1 67.16 70.09 3.69 o 8 7 1 17.49 13.54 3.11 o -8 8 1 15.76 17.80 2.89 o -7 8 1 12.27 14.19 1.91 o -6 8 1 119.61 125.52 5.03 o -5 8 1 14.62 17.48 1.92 o -4 8 1 0.02 0.61 1.55 < -3 8 1 139.24 133.95 4.42 o -2 8 1 124.44 115.56 2.77 o -1 8 1 504.41 504.87 5.95 o 0 8 1 3.79 2.20 0.77 < 1 8 1 15.68 14.93 1.47 o 2 8 1 216.60 202.82 5.08 o 3 8 1 384.08 357.81 6.95 o 4 8 1 10.51 10.88 1.47 o 5 8 1 34.19 39.08 4.21 o 6 8 1 90.01 84.45 6.31 o 7 8 1 94.38 84.63 4.22 o -8 9 1 196.29 205.71 9.44 o -7 9 1 6.18 7.91 2.08 o -6 9 1 398.51 397.76 9.27 o -5 9 1 292.54 301.98 11.36 o -4 9 1 0.04 0.75 0.91 < -3 9 1 893.65 903.95 12.12 o -2 9 1 259.26 258.68 6.29 o -1 9 1 261.10 255.95 4.48 o 0 9 1 298.22 289.29 6.41 o 1 9 1 516.16 502.49 8.49 o 2 9 1 187.12 194.97 5.35 o 3 9 1 186.05 187.32 5.37 o 4 9 1 339.67 342.14 7.43 o 5 9 1 22.22 21.68 2.09 o 6 9 1 468.15 451.39 15.03 o -6 10 1 0.24 2.09 1.69 < -5 10 1 230.35 224.15 6.71 o -4 10 1 461.65 462.45 9.35 o -3 10 1 24.29 22.90 2.16 o -2 10 1 2.99 3.75 1.14 o -1 10 1 0.12 -0.29 0.84 < 0 10 1 129.53 134.29 4.72 o 1 10 1 6.86 7.66 1.25 o 2 10 1 3.01 1.59 0.90 < 3 10 1 158.65 147.99 5.04 o 4 10 1 63.54 64.61 3.43 o 5 10 1 888.29 912.60 21.27 o -5 11 1 35.75 35.87 2.95 o -4 11 1 2.03 1.17 1.03 < -3 11 1 11.76 13.34 1.88 o -2 11 1 316.85 297.36 7.53 o -1 11 1 22.24 21.98 2.18 o 0 11 1 2.47 2.36 0.99 < 1 11 1 183.54 176.34 5.73 o 2 11 1 16.36 18.71 1.99 o 3 11 1 331.25 318.74 7.81 o 4 11 1 8.29 8.26 2.71 o -4 12 1 167.96 176.34 8.44 o -3 12 1 67.15 70.90 4.00 o -2 12 1 46.24 45.23 3.19 o -1 12 1 56.59 52.96 3.41 o 0 12 1 4.46 5.24 1.34 o 1 12 1 0.07 0.36 1.05 < 2 12 1 1.60 0.60 1.59 < -2 13 1 309.90 297.27 11.53 o -1 13 1 11.58 9.12 1.77 o 0 13 1 377.42 374.11 9.20 o -11 0 2 170.83 172.34 9.02 o -10 0 2 267.21 246.26 10.13 o -9 0 2 357.99 327.35 10.97 o -8 0 2 1486.78 1408.82 21.45 o -7 0 2 624.94 619.02 13.10 o -6 0 2 216.47 225.70 7.22 o -5 0 2 566.99 539.30 7.38 o -4 0 2 102.96 117.89 2.46 o -3 0 2 2797.10 2597.46 14.17 o -2 0 2 3262.17 2686.17 13.08 o -1 0 2 2803.70 2614.69 9.11 o 0 0 2 5725.68 6211.27 15.78 o 2 0 2 244.09 193.30 2.62 o 3 0 2 115.10 108.75 2.36 o 4 0 2 355.73 344.84 4.89 o 5 0 2 53.67 65.97 2.41 o 6 0 2 34.56 37.08 1.66 o 7 0 2 606.86 601.59 8.08 o 8 0 2 732.09 713.69 9.46 o 9 0 2 22.52 17.65 1.64 o -11 1 2 12.39 10.72 2.59 o -10 1 2 151.63 168.65 5.95 o -9 1 2 240.89 236.59 6.61 o -8 1 2 123.06 104.21 4.08 o -7 1 2 548.53 536.41 6.83 o -6 1 2 151.40 168.74 2.51 o -5 1 2 340.38 365.39 4.26 o -4 1 2 628.79 594.21 4.88 o -3 1 2 50.90 49.17 1.47 o -2 1 2 418.05 441.61 3.25 o -1 1 2 2609.88 2450.56 8.71 o 0 1 2 10.23 14.89 0.59 o 1 1 2 2196.65 2323.31 6.76 o 2 1 2 261.86 216.20 1.53 o 3 1 2 354.42 423.30 2.37 o 4 1 2 68.78 80.61 1.30 o 5 1 2 92.40 84.64 1.71 o 6 1 2 556.78 549.04 4.81 o 7 1 2 26.25 24.00 1.24 o 8 1 2 102.77 103.21 2.96 o 9 1 2 244.40 236.80 4.10 o -11 2 2 192.06 206.74 9.71 o -10 2 2 9.75 8.46 1.54 o -9 2 2 2.46 3.97 1.09 o -8 2 2 258.27 220.51 4.05 o -7 2 2 99.45 97.16 3.56 o -6 2 2 628.48 620.05 6.75 o -5 2 2 228.03 235.80 4.01 o -4 2 2 37.32 52.62 1.41 o -3 2 2 1889.86 1912.84 11.09 o -2 2 2 1943.57 1942.53 7.27 o -1 2 2 143.56 132.07 1.42 o 0 2 2 750.58 777.48 3.21 o 1 2 2 9846.13 12512.40 31.96 o 2 2 2 3921.38 4330.09 9.43 o 3 2 2 319.65 370.77 2.62 o 4 2 2 117.94 120.98 1.89 o 5 2 2 366.62 386.56 2.92 o 6 2 2 64.98 71.96 1.44 o 7 2 2 0.28 0.83 0.50 < 8 2 2 184.18 194.75 5.30 o 9 2 2 53.52 54.33 2.78 o 10 2 2 77.53 85.38 5.52 o -11 3 2 6.66 7.42 2.29 o -10 3 2 29.56 29.16 2.62 o -9 3 2 45.39 42.27 2.72 o -8 3 2 113.01 125.82 4.38 o -7 3 2 228.41 234.51 5.62 o -6 3 2 60.99 59.54 1.94 o -5 3 2 230.29 238.44 2.77 o -4 3 2 564.88 542.84 4.83 o -3 3 2 8.44 18.36 0.94 o -2 3 2 2823.24 2885.27 8.63 o -1 3 2 14.41 26.94 0.80 o 0 3 2 125.22 114.91 1.43 o 1 3 2 781.48 854.01 3.85 o 2 3 2 1709.34 1779.04 7.14 o 3 3 2 701.89 686.01 3.50 o 4 3 2 46.62 53.47 1.29 o 5 3 2 137.63 140.31 2.59 o 6 3 2 9.58 8.90 0.73 o 7 3 2 28.08 29.04 1.13 o 8 3 2 162.44 171.62 5.04 o 9 3 2 224.30 221.14 9.82 o -10 4 2 7.23 6.90 1.38 o -9 4 2 216.16 228.29 6.35 o -8 4 2 93.39 104.79 3.13 o -7 4 2 277.56 287.30 4.42 o -6 4 2 834.51 834.67 6.69 o -5 4 2 1686.85 1688.57 8.92 o -4 4 2 727.98 765.69 5.41 o -3 4 2 623.98 660.84 5.09 o -2 4 2 3646.26 3656.10 12.41 o -1 4 2 83.87 82.21 1.56 o 0 4 2 319.27 320.71 3.18 o 1 4 2 68.89 45.76 1.08 o 2 4 2 32.78 44.17 1.19 o 3 4 2 478.89 457.80 3.55 o 4 4 2 1339.04 1397.41 5.68 o 5 4 2 280.76 266.34 3.27 o 6 4 2 34.15 33.37 1.32 o 7 4 2 1027.07 1025.94 7.86 o 8 4 2 168.94 165.63 5.08 o 9 4 2 4.52 5.08 2.17 < -10 5 2 144.66 152.09 8.18 o -9 5 2 126.43 137.11 5.10 o -8 5 2 19.37 19.19 1.66 o -7 5 2 327.86 326.70 4.54 o -6 5 2 317.54 304.20 4.13 o -5 5 2 410.18 395.21 5.24 o -4 5 2 1157.06 1214.47 7.16 o -3 5 2 76.87 72.68 1.95 o -2 5 2 1015.10 1061.72 8.27 o -1 5 2 2612.57 2511.08 10.10 o 0 5 2 82.10 81.61 2.15 o 1 5 2 17.69 29.03 1.00 o 2 5 2 104.86 130.95 1.85 o 3 5 2 196.73 200.44 3.22 o 4 5 2 556.01 554.53 5.26 o 5 5 2 466.74 462.09 3.90 o 6 5 2 574.93 556.05 5.18 o 7 5 2 0.18 0.27 0.80 < 8 5 2 29.05 36.13 2.59 o 9 5 2 114.14 105.89 7.26 o -10 6 2 37.17 46.96 4.68 o -9 6 2 9.02 10.55 1.63 o -8 6 2 144.89 150.91 4.49 o -7 6 2 5.13 7.22 1.34 o -6 6 2 197.39 188.19 3.35 o -5 6 2 497.45 499.43 8.63 o -4 6 2 12.46 9.64 1.35 o -3 6 2 2.38 4.71 0.66 o -2 6 2 8.74 11.11 0.71 o -1 6 2 534.81 532.26 4.87 o 0 6 2 12.17 17.53 1.31 o 1 6 2 10.49 11.74 0.67 o 2 6 2 111.57 120.77 1.99 o 3 6 2 135.09 145.53 3.01 o 4 6 2 454.11 470.02 7.48 o 5 6 2 121.45 134.37 3.29 o 6 6 2 37.86 39.75 2.54 o 7 6 2 101.53 101.22 4.14 o 8 6 2 111.75 128.15 7.84 o -9 7 2 15.12 12.74 1.78 o -8 7 2 35.91 32.74 2.80 o -7 7 2 259.04 257.82 7.20 o -6 7 2 115.44 109.17 4.47 o -5 7 2 329.52 350.26 7.58 o -4 7 2 61.24 62.25 3.10 o -3 7 2 389.26 404.28 7.42 o -2 7 2 238.85 235.51 3.45 o -1 7 2 795.58 754.16 6.06 o 0 7 2 763.93 779.93 7.49 o 1 7 2 1.35 0.70 0.53 < 2 7 2 862.22 855.17 7.80 o 3 7 2 609.02 606.43 6.69 o 4 7 2 80.92 73.80 3.20 o 5 7 2 295.55 296.75 6.73 o 6 7 2 328.69 316.57 11.60 o 7 7 2 27.60 27.86 2.32 o 8 7 2 58.75 72.59 6.19 o -9 8 2 392.32 410.38 13.65 o -8 8 2 53.72 51.21 4.76 o -7 8 2 28.28 29.39 2.70 o -6 8 2 199.67 212.42 6.54 o -5 8 2 44.44 52.48 3.20 o -4 8 2 27.23 31.70 2.43 o -3 8 2 9.39 8.27 1.88 o -2 8 2 9.53 10.00 0.98 o -1 8 2 0.02 0.13 0.42 < 0 8 2 9.99 7.04 0.85 o 1 8 2 513.86 494.40 6.97 o 2 8 2 489.67 507.42 12.76 o 3 8 2 3.83 6.44 1.91 o 4 8 2 1335.03 1315.87 22.70 o 5 8 2 216.04 222.89 5.87 o 6 8 2 238.69 277.64 11.34 o 7 8 2 222.17 230.93 10.82 o -8 9 2 99.15 94.35 6.73 o -7 9 2 56.57 61.57 3.90 o -6 9 2 6.99 8.25 1.69 o -5 9 2 37.94 35.01 2.77 o -4 9 2 388.22 388.97 12.13 o -3 9 2 260.72 262.24 6.57 o -2 9 2 838.38 828.75 11.48 o -1 9 2 35.63 41.93 1.89 o 0 9 2 0.09 0.38 0.73 < 1 9 2 30.75 36.21 1.70 o 2 9 2 521.96 502.18 8.54 o 3 9 2 499.13 479.55 8.42 o 4 9 2 0.01 1.12 0.86 < 5 9 2 115.26 121.74 7.67 o 6 9 2 17.53 12.21 2.82 o -7 10 2 5.74 6.71 2.17 o -6 10 2 129.55 112.92 7.66 o -5 10 2 3.33 4.10 1.30 o -4 10 2 9.65 7.14 1.45 o -3 10 2 92.35 88.97 4.11 o -2 10 2 209.83 216.51 6.21 o -1 10 2 59.48 55.77 3.12 o 0 10 2 37.28 36.28 2.53 o 1 10 2 1.90 1.98 0.97 < 2 10 2 25.51 17.20 1.80 o 3 10 2 6.41 6.35 1.35 o 4 10 2 32.67 29.28 3.93 o 5 10 2 0.10 0.07 1.75 < -6 11 2 155.99 146.22 7.84 o -5 11 2 107.44 110.15 5.08 o -4 11 2 449.76 466.62 9.98 o -3 11 2 676.95 680.72 11.83 o -2 11 2 9.62 5.62 1.38 o -1 11 2 349.85 345.12 8.01 o 0 11 2 257.02 251.75 6.83 o 1 11 2 5.35 4.83 1.25 o 2 11 2 156.78 142.48 5.14 o 3 11 2 268.69 275.90 11.55 o -4 12 2 0.49 0.68 1.46 < -3 12 2 157.04 165.35 6.13 o -2 12 2 61.18 65.61 3.82 o -1 12 2 30.70 31.05 2.72 o 0 12 2 60.68 66.57 3.76 o 1 12 2 254.38 260.29 11.29 o 2 12 2 34.67 38.89 4.51 o -10 1 3 25.73 26.77 2.57 o -9 1 3 0.13 0.71 0.89 < -8 1 3 426.76 467.19 8.91 o -7 1 3 787.78 770.95 10.71 o -6 1 3 109.15 111.97 2.96 o -5 1 3 235.67 221.88 3.05 o -4 1 3 339.85 446.79 5.16 o -3 1 3 2331.98 2228.44 11.21 o -2 1 3 7.99 3.82 0.34 o -1 1 3 886.92 841.65 4.07 o 0 1 3 910.80 886.84 3.84 o 1 1 3 1058.28 989.90 3.99 o 2 1 3 704.59 644.99 3.32 o 3 1 3 18.48 23.17 0.62 o 4 1 3 55.96 55.04 1.12 o 5 1 3 1.80 1.70 0.37 o 6 1 3 0.50 1.14 0.47 < 7 1 3 25.13 24.85 1.27 o 8 1 3 213.00 215.52 3.43 o 9 1 3 0.16 1.55 0.70 < -10 2 3 30.08 27.58 2.61 o -9 2 3 694.84 668.05 11.48 o -8 2 3 121.50 129.55 4.55 o -7 2 3 224.88 234.27 5.73 o -6 2 3 2372.31 2203.38 16.63 o -5 2 3 0.03 1.20 0.33 o -4 2 3 1657.87 1606.08 9.99 o -3 2 3 4348.95 4158.34 18.90 o -2 2 3 60.74 47.21 1.01 o -1 2 3 873.71 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2.62 o -2 2 13 47.18 49.73 4.64 o -1 2 13 289.51 300.98 8.18 o