# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_2019412 _shelx_title ' 131014am in C2/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 522.52 _exptl_crystal_F_000 1472.00 _reflns_d_resolution_high 0.8225 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 24.4936 _cell_length_b 6.0061 _cell_length_c 17.3057 _cell_angle_alpha 90.000 _cell_angle_beta 95.796 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 63797.82 39331.16 512.39 o 6 0 0 818.42 624.12 180.92 o 8 0 0 501.77 798.96 212.31 o 10 0 0 21677.85 23248.94 690.95 o 12 0 0 6286.95 5736.88 411.80 o 14 0 0 68309.38 78591.79 1434.56 o 16 0 0 51297.68 60033.22 1343.42 o 18 0 0 39587.33 48703.63 839.65 o 20 0 0 32394.86 40135.74 1713.87 o 22 0 0 6986.55 8148.73 411.56 o 24 0 0 9340.46 11316.46 752.38 o 26 0 0 5733.20 7515.39 667.32 o 28 0 0 3068.42 5168.79 615.00 o 1 1 0 22880.25 17124.96 2773.15 o 3 1 0 1581.39 1718.35 44.14 o 5 1 0 456.99 586.57 44.69 o 7 1 0 2062.28 2312.52 161.26 o 9 1 0 1338.39 1177.27 88.94 o 11 1 0 1171.25 1073.57 126.29 o 13 1 0 815.62 884.80 135.30 o 15 1 0 5434.58 5719.54 316.75 o 17 1 0 3593.69 4125.86 237.93 o 19 1 0 4351.12 5467.06 285.09 o 21 1 0 96.82 352.02 181.13 o 23 1 0 68.39 -18.23 183.82 o 25 1 0 17.49 -42.32 182.92 o 27 1 0 274.92 389.32 266.67 o 29 1 0 218.30 165.79 275.86 o 0 2 0 8390.90 8285.85 1155.75 o 2 2 0 33759.21 33818.89 2101.06 o 4 2 0 10743.51 11095.76 414.36 o 6 2 0 46087.13 46242.84 1226.55 o 8 2 0 82744.82 80213.38 1078.95 o 10 2 0 84272.59 78606.95 1392.16 o 12 2 0 68561.72 66060.66 2332.13 o 14 2 0 14224.17 13228.01 545.71 o 16 2 0 24167.61 25015.01 1307.79 o 18 2 0 5655.98 5418.74 334.19 o 20 2 0 1344.35 1396.65 195.53 o 22 2 0 3685.84 3556.45 256.02 o 24 2 0 3747.44 4746.07 299.58 o 26 2 0 7306.61 8734.56 495.51 o 28 2 0 4857.85 6191.90 449.69 o 1 3 0 14213.31 15495.62 425.65 o 3 3 0 17513.48 18748.77 792.74 o 5 3 0 1023.46 994.63 74.31 o 7 3 0 5378.13 5591.36 329.45 o 9 3 0 6249.53 6250.32 151.10 o 11 3 0 2206.13 2069.90 106.52 o 13 3 0 5799.10 5814.94 281.66 o 15 3 0 4562.11 3996.86 215.74 o 17 3 0 14977.00 14087.23 1418.12 o 19 3 0 2543.83 2259.91 317.29 o 21 3 0 666.46 605.14 204.12 o 23 3 0 323.12 90.72 211.09 o 25 3 0 220.83 217.28 305.98 o 27 3 0 1065.76 1527.43 308.01 o 0 4 0 3442.35 3553.22 159.01 o 2 4 0 10248.37 10949.57 227.86 o 4 4 0 8504.40 7995.86 458.94 o 6 4 0 29323.33 30716.90 1635.39 o 8 4 0 13254.22 12113.98 656.02 o 10 4 0 8221.54 7756.32 236.10 o 12 4 0 1633.25 1558.52 151.38 o 14 4 0 389.55 358.03 127.81 o 16 4 0 2213.13 2132.03 180.39 o 18 4 0 3187.23 3205.82 407.47 o 20 4 0 5405.18 4939.73 588.77 o 22 4 0 4040.96 3890.50 1073.05 o 24 4 0 2417.18 2794.00 736.35 o 1 5 0 2408.81 2257.85 113.30 o 3 5 0 1732.10 1692.34 126.84 o 5 5 0 5234.49 5127.17 223.83 o 7 5 0 9774.52 9907.75 420.03 o 9 5 0 15171.04 14365.58 397.29 o 11 5 0 6784.89 7044.97 296.33 o 13 5 0 1729.47 1603.45 183.82 o 15 5 0 888.40 1078.49 180.36 o 17 5 0 197.85 269.64 136.15 o 19 5 0 1031.60 1238.80 173.22 o 21 5 0 404.96 263.00 163.68 o 0 6 0 1078.48 1165.25 149.85 o 2 6 0 671.01 750.76 100.12 o 4 6 0 1141.89 1207.84 111.39 o 6 6 0 1505.64 1615.39 183.95 o 8 6 0 110.21 73.02 149.61 o 10 6 0 633.63 540.34 164.31 o 12 6 0 58.34 -1.43 152.48 o 14 6 0 821.94 712.48 233.24 o 16 6 0 601.95 575.15 183.26 o 1 7 0 2387.85 2774.09 178.99 o 3 7 0 1966.79 2172.63 168.60 o 5 7 0 358.76 431.06 129.07 o 7 7 0 1385.67 1278.77 159.68 o -29 1 1 2874.39 3875.00 404.06 o -27 1 1 2651.66 3747.46 299.47 o -25 1 1 4333.66 5725.40 332.90 o -23 1 1 10361.07 12292.78 423.88 o -21 1 1 7083.94 8216.26 344.52 o -19 1 1 18777.12 21024.83 556.03 o -17 1 1 21811.98 23429.18 842.38 o -15 1 1 53195.62 60331.13 1021.72 o -13 1 1 52874.46 54696.34 999.72 o -11 1 1 43828.86 43197.32 3161.63 o -9 1 1 23145.16 20794.78 1337.37 o -7 1 1 53843.81 52215.50 826.83 o -5 1 1 52181.55 51626.05 564.52 o -3 1 1 35659.56 37367.88 398.62 o -1 1 1 65584.37 68520.36 814.10 o 1 1 1 119355.67 116597.60 877.40 o 3 1 1 273026.50 233113.64 1292.17 o 5 1 1 129568.25 124191.84 2979.89 o 7 1 1 14321.41 14396.60 569.03 o 9 1 1 19560.22 19456.12 710.78 o 11 1 1 12089.34 10834.09 616.75 o 13 1 1 41730.23 41658.98 1598.01 o 15 1 1 29252.14 28922.80 1267.65 o 17 1 1 34388.27 37412.21 596.09 o 19 1 1 19616.01 21321.11 748.67 o 21 1 1 20987.21 24001.95 969.18 o 23 1 1 2813.68 3336.71 259.38 o 25 1 1 5001.53 5884.15 327.21 o 27 1 1 2476.84 3330.46 363.38 o 29 1 1 4730.99 6091.63 457.44 o -28 2 1 382.56 508.30 287.33 o -26 2 1 792.74 1147.02 280.43 o -24 2 1 47.27 -1.48 217.14 o -22 2 1 526.84 695.94 188.67 o -20 2 1 379.69 387.50 163.27 o -18 2 1 4357.46 4567.77 269.66 o -16 2 1 11229.97 11956.46 775.62 o -14 2 1 24052.86 24003.32 1479.66 o -12 2 1 18289.29 18033.97 603.79 o -10 2 1 65.43 -1.86 62.87 o -8 2 1 7662.52 6831.13 295.47 o -6 2 1 3013.05 2604.22 140.24 o -4 2 1 460.54 531.59 57.64 o -2 2 1 22757.51 24023.54 325.22 o 0 2 1 36993.32 38509.60 645.50 o 2 2 1 83683.77 83744.44 1053.38 o 4 2 1 20853.65 22436.53 357.82 o 6 2 1 92.23 207.04 38.88 o 8 2 1 7.81 73.02 46.99 o 10 2 1 718.99 624.74 91.35 o 12 2 1 1379.95 1499.34 112.79 o 14 2 1 3004.87 2677.10 149.84 o 16 2 1 2884.01 2606.22 206.63 o 18 2 1 6294.59 5952.83 476.42 o 20 2 1 3943.86 4162.53 249.86 o 22 2 1 3678.10 3663.74 331.94 o 24 2 1 272.70 141.43 171.08 o 26 2 1 11.37 165.52 223.68 o 28 2 1 213.00 239.99 411.46 o -27 3 1 2584.93 3124.90 362.13 o -25 3 1 5757.88 6571.51 761.50 o -23 3 1 7761.02 9159.71 582.26 o -21 3 1 7264.76 7304.09 1134.48 o -19 3 1 1686.80 1556.58 294.84 o -17 3 1 1517.10 1454.18 171.89 o -15 3 1 3866.78 3943.96 444.37 o -13 3 1 8567.03 8345.26 202.96 o -11 3 1 17023.99 16977.12 266.94 o -9 3 1 32601.96 33740.07 345.03 o -7 3 1 70753.79 71943.20 1543.06 o -5 3 1 47386.33 48670.27 2519.75 o -3 3 1 30738.87 30118.79 1368.59 o -1 3 1 14548.54 14934.12 601.67 o 1 3 1 1002.41 1047.21 68.00 o 3 3 1 5216.38 5587.48 120.24 o 5 3 1 20466.25 21701.64 396.58 o 7 3 1 13341.46 12217.69 405.36 o 9 3 1 54682.13 52719.61 1843.92 o 11 3 1 39728.88 36739.73 959.72 o 13 3 1 26721.35 25810.75 439.32 o 15 3 1 10775.88 11020.00 324.43 o 17 3 1 303.69 299.17 140.38 o 19 3 1 7719.43 6875.11 1290.93 o 21 3 1 812.09 955.71 229.92 o 23 3 1 5095.72 5127.11 1021.57 o 25 3 1 2732.80 3314.10 461.25 o -24 4 1 2727.51 3609.72 565.22 o -22 4 1 2264.80 2577.55 479.14 o -20 4 1 313.10 289.32 152.49 o -18 4 1 192.09 82.40 136.15 o -16 4 1 583.38 508.97 141.20 o -14 4 1 8401.18 8427.65 516.63 o -12 4 1 3528.94 3751.02 152.71 o -10 4 1 9097.55 9396.72 214.09 o -8 4 1 14466.70 14485.27 555.50 o -6 4 1 13744.54 14312.84 931.24 o -4 4 1 15294.40 15538.75 936.07 o -2 4 1 3418.69 3169.80 125.75 o 0 4 1 4350.56 4094.45 124.38 o 2 4 1 1475.74 1170.24 94.39 o 4 4 1 3955.32 3858.28 180.17 o 6 4 1 2490.50 2536.09 162.63 o 8 4 1 5204.11 5118.92 226.16 o 10 4 1 10799.88 10346.31 403.83 o 12 4 1 23879.50 22506.83 794.44 o 14 4 1 7132.86 6901.45 307.09 o 16 4 1 2251.87 2504.92 314.97 o 18 4 1 945.04 894.48 157.51 o 20 4 1 392.43 398.44 148.02 o 22 4 1 560.47 288.80 209.81 o 24 4 1 309.57 231.31 226.49 o -21 5 1 1483.72 1712.64 356.84 o -19 5 1 2267.22 2122.27 325.29 o -17 5 1 4884.13 4608.68 395.12 o -15 5 1 605.39 474.91 161.83 o -13 5 1 3859.61 3780.44 246.05 o -11 5 1 200.31 141.66 139.78 o -9 5 1 943.75 1001.33 121.99 o -7 5 1 965.14 801.65 109.89 o -5 5 1 3045.22 2822.10 148.13 o -3 5 1 6775.95 6696.59 195.50 o -1 5 1 3683.81 3818.68 132.71 o 1 5 1 5236.99 5214.99 147.24 o 3 5 1 5641.56 6016.05 241.85 o 5 5 1 1634.19 1699.60 126.33 o 7 5 1 6450.86 6250.11 262.58 o 9 5 1 2817.28 2521.59 191.51 o 11 5 1 3087.85 2852.71 216.98 o 13 5 1 130.47 185.48 140.42 o 15 5 1 966.84 810.35 166.67 o 17 5 1 169.51 73.51 134.94 o 19 5 1 1022.35 864.42 169.21 o 21 5 1 2253.19 2178.50 302.96 o -16 6 1 1225.25 1347.30 221.26 o -14 6 1 594.03 659.84 189.27 o -12 6 1 1320.24 1294.85 190.19 o -10 6 1 760.75 860.87 181.47 o -8 6 1 2744.94 2554.97 211.60 o -6 6 1 5079.50 4818.52 200.06 o -4 6 1 4331.06 4298.56 161.77 o -2 6 1 1911.08 1941.76 124.18 o 0 6 1 656.72 753.77 99.52 o 2 6 1 6771.86 7521.92 195.25 o 4 6 1 1983.72 2348.91 154.46 o 6 6 1 5051.47 5223.74 396.28 o 8 6 1 2086.65 2185.12 212.61 o 10 6 1 2572.35 2304.81 219.30 o 12 6 1 1881.32 1705.72 210.39 o 14 6 1 509.19 498.85 178.68 o 16 6 1 648.84 571.73 194.54 o -7 7 1 132.22 52.17 127.11 o -5 7 1 19.29 -10.69 116.08 o -3 7 1 179.13 188.24 125.00 o -1 7 1 714.82 627.24 114.00 o 1 7 1 29.03 8.06 113.64 o 3 7 1 417.34 304.84 128.76 o 5 7 1 16.08 49.00 119.47 o 7 7 1 225.12 221.77 130.42 o -28 0 2 6319.67 8493.93 721.33 o -26 0 2 9168.74 11750.22 997.27 o -24 0 2 2329.03 3013.64 304.88 o -22 0 2 12289.44 14379.12 1866.95 o -20 0 2 5897.60 6362.68 557.28 o -18 0 2 26948.46 29832.04 1051.45 o -16 0 2 37042.53 41719.28 1205.03 o -14 0 2 67515.84 78008.52 1574.97 o -12 0 2 81464.31 85785.84 1413.29 o -10 0 2 93804.75 99275.07 1341.40 o -8 0 2 12325.63 12855.32 383.45 o -6 0 2 2473.69 3119.23 166.75 o -4 0 2 40131.39 42733.60 467.16 o -2 0 2 208012.22 180255.30 1271.52 o 0 0 2 68652.98 71005.13 982.79 o 2 0 2 200351.30 165967.09 2698.03 o 4 0 2 126364.96 126569.11 1023.43 o 6 0 2 140618.95 140157.63 3712.13 o 8 0 2 53733.13 55845.78 734.83 o 10 0 2 6392.67 5500.56 204.38 o 12 0 2 18532.10 17075.55 375.54 o 14 0 2 11647.60 10808.72 333.41 o 16 0 2 38704.52 41715.10 691.59 o 18 0 2 35363.96 41252.60 1552.36 o 20 0 2 14611.87 18160.73 537.75 o 22 0 2 19357.48 20880.74 908.33 o 24 0 2 8552.30 9070.11 671.71 o 26 0 2 3011.63 4606.45 555.60 o 28 0 2 1235.07 1359.96 443.53 o -29 1 2 364.47 774.39 242.77 o -27 1 2 50.76 180.69 203.63 o -25 1 2 149.20 -52.25 189.03 o -23 1 2 317.09 288.01 182.67 o -21 1 2 21.47 -148.24 160.36 o -19 1 2 400.56 586.91 179.11 o -17 1 2 4225.39 4533.39 305.07 o -15 1 2 20515.31 22597.47 473.86 o -13 1 2 9113.86 8513.79 291.03 o -11 1 2 27541.35 29597.23 1192.33 o -9 1 2 170.31 173.91 77.04 o -7 1 2 26020.89 24431.71 1125.16 o -5 1 2 46110.70 43847.34 924.48 o -3 1 2 19844.78 20092.04 318.36 o -1 1 2 1253.15 1499.05 36.16 o 1 1 2 13109.48 13519.71 281.06 o 3 1 2 112024.19 109480.37 1223.19 o 5 1 2 80279.88 79822.59 1310.86 o 7 1 2 14374.81 15435.92 190.73 o 9 1 2 432.83 544.00 73.56 o 11 1 2 3466.63 3548.45 192.74 o 13 1 2 4337.94 4188.67 192.61 o 15 1 2 893.76 857.48 133.79 o 17 1 2 473.74 616.61 167.91 o 19 1 2 740.15 921.61 174.06 o 21 1 2 830.52 993.19 187.63 o 23 1 2 2512.43 2946.16 250.18 o 25 1 2 748.73 1061.26 255.08 o 27 1 2 261.87 305.69 258.85 o -28 2 2 3510.74 4146.17 401.82 o -26 2 2 4847.11 5953.22 428.44 o -24 2 2 5132.38 6607.70 451.29 o -22 2 2 4461.43 5145.52 298.95 o -20 2 2 16497.81 19345.06 496.65 o -18 2 2 6475.75 6781.71 413.82 o -16 2 2 8651.92 8531.29 319.38 o -14 2 2 20546.32 21332.95 1324.05 o -12 2 2 28404.35 27564.89 1208.11 o -10 2 2 62814.28 65072.65 1051.67 o -8 2 2 26586.97 24977.65 240.72 o -6 2 2 63296.34 63092.52 619.02 o -4 2 2 49185.23 49998.28 465.40 o -2 2 2 49783.72 51447.73 554.09 o 0 2 2 58148.85 58268.67 934.65 o 2 2 2 24543.96 25695.52 301.87 o 4 2 2 19482.12 21615.09 283.41 o 6 2 2 58913.50 63407.59 576.71 o 8 2 2 35047.58 36570.81 247.18 o 10 2 2 31987.56 32276.07 1058.49 o 12 2 2 20600.33 20821.06 441.36 o 14 2 2 42106.22 42188.38 744.93 o 16 2 2 15987.52 14761.30 675.46 o 18 2 2 10949.41 9839.67 364.51 o 20 2 2 6432.93 6112.04 531.89 o 22 2 2 5073.53 5126.78 280.56 o 24 2 2 5972.32 5505.71 304.70 o 26 2 2 3453.50 4017.37 365.66 o 28 2 2 2544.99 4357.34 607.24 o -27 3 2 1683.12 2189.11 330.00 o -25 3 2 2077.91 2872.54 340.95 o -23 3 2 2439.34 2835.43 317.62 o -21 3 2 642.86 738.41 231.53 o -19 3 2 2353.62 2041.47 276.11 o -17 3 2 357.66 188.42 344.12 o -15 3 2 305.21 97.15 124.93 o -13 3 2 8357.07 7844.00 482.18 o -11 3 2 10202.81 9535.91 362.92 o -9 3 2 25841.92 25968.84 371.98 o -7 3 2 3572.71 3406.45 117.95 o -5 3 2 15518.15 16999.25 379.92 o -3 3 2 5041.82 5075.79 116.94 o -1 3 2 18684.32 20360.87 337.59 o 1 3 2 11218.76 11670.31 267.13 o 3 3 2 7544.14 7711.96 101.46 o 5 3 2 4154.07 4445.79 96.07 o 7 3 2 4476.60 4837.98 96.64 o 9 3 2 298.41 307.93 55.57 o 11 3 2 1276.50 1252.07 121.38 o 13 3 2 6135.26 5958.49 253.20 o 15 3 2 16680.06 16036.36 664.25 o 17 3 2 10862.13 10050.02 1045.50 o 19 3 2 2612.68 2367.94 203.81 o 21 3 2 2676.74 2715.63 593.74 o 23 3 2 34.83 -122.99 184.61 o 25 3 2 485.30 451.79 225.14 o -24 4 2 1963.73 2032.32 409.95 o -22 4 2 5314.50 4955.92 547.66 o -20 4 2 8779.07 8095.10 1665.27 o -18 4 2 3305.19 3390.06 481.94 o -16 4 2 4293.30 3839.87 261.68 o -14 4 2 129.95 139.89 93.69 o -12 4 2 1211.92 1209.51 111.93 o -10 4 2 4694.26 4657.28 197.41 o -8 4 2 11139.33 11225.39 220.43 o -6 4 2 18096.29 18121.07 891.29 o -4 4 2 26807.65 27331.36 1165.82 o -2 4 2 14802.39 14952.36 322.40 o 0 4 2 9634.68 9848.77 168.82 o 2 4 2 1644.61 1540.79 178.27 o 4 4 2 5646.50 5924.89 236.24 o 6 4 2 2948.66 3038.56 117.31 o 8 4 2 15512.18 15527.74 481.31 o 10 4 2 9532.82 8848.04 377.99 o 12 4 2 15396.20 13830.59 389.42 o 14 4 2 7461.70 6603.20 252.41 o 16 4 2 3136.30 2704.95 194.68 o 18 4 2 2044.34 1666.80 181.29 o 20 4 2 114.37 -62.08 135.56 o 22 4 2 1422.86 1358.94 441.34 o 24 4 2 1880.97 1780.37 287.81 o -21 5 2 3533.68 3676.24 514.53 o -19 5 2 2388.64 2258.27 348.66 o -17 5 2 2956.02 3116.10 365.87 o -15 5 2 227.10 211.32 131.77 o -13 5 2 2524.58 2589.07 212.43 o -11 5 2 2595.73 2653.90 207.86 o -9 5 2 3700.00 3769.71 169.27 o -7 5 2 6935.78 7078.42 211.95 o -5 5 2 3557.17 3556.49 195.65 o -3 5 2 14682.27 13998.01 450.81 o -1 5 2 3468.22 3246.03 125.64 o 1 5 2 2410.81 2538.52 116.16 o 3 5 2 1827.06 1966.76 127.13 o 5 5 2 2767.16 2818.32 349.53 o 7 5 2 9258.68 9103.02 454.33 o 9 5 2 4894.38 4589.68 245.15 o 11 5 2 6674.59 6482.59 386.49 o 13 5 2 4733.72 4305.34 404.38 o 15 5 2 2497.69 2492.66 224.32 o 17 5 2 1643.40 1333.39 174.07 o 19 5 2 33.73 -173.17 134.96 o 21 5 2 331.88 245.20 161.81 o -16 6 2 947.80 986.40 222.78 o -14 6 2 1919.70 1827.67 440.49 o -12 6 2 1191.81 956.35 176.92 o -10 6 2 243.27 380.99 159.90 o -8 6 2 1591.97 1364.27 179.28 o -6 6 2 280.92 344.72 113.30 o -4 6 2 1325.49 1388.76 120.31 o -2 6 2 74.00 34.27 85.53 o 0 6 2 1361.56 1294.62 109.92 o 2 6 2 2908.72 3155.36 185.69 o 4 6 2 1218.82 1367.08 133.87 o 6 6 2 3356.55 3926.44 443.53 o 8 6 2 493.09 590.32 149.65 o 10 6 2 254.19 241.59 161.01 o 12 6 2 186.66 226.95 161.23 o 14 6 2 86.32 86.20 162.66 o 16 6 2 373.99 271.47 178.30 o -7 7 2 567.75 514.26 210.29 o -5 7 2 1110.64 961.29 176.89 o -3 7 2 2226.60 2343.92 180.80 o -1 7 2 1280.59 1340.84 186.16 o 1 7 2 1622.42 1850.39 199.49 o 3 7 2 338.24 557.63 164.68 o 5 7 2 2478.94 2786.88 240.31 o 7 7 2 788.36 1000.13 189.62 o -29 1 3 3216.99 4092.75 317.45 o -27 1 3 7408.92 8994.00 403.23 o -25 1 3 8461.67 10566.42 417.97 o -23 1 3 8323.21 10466.64 593.70 o -21 1 3 7380.11 8860.85 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