#------------------------------------------------------------------------------ #$Date: 2016-04-06 16:26:34 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181864 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/94/2019461.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2019461 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.6619 _cell_length_b 14.1976 _cell_length_c 19.1795 _exptl_crystal_F_000 732.00 _reflns_d_resolution_high 0.7828 _cod_data_source_file qs30372sup3.hkl _cod_data_source_block 2 #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 159.84 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 17629.35 17908.69 242.56 o 2 1 0 2146.20 2021.55 125.50 o 3 1 0 694.08 750.75 115.81 o 4 1 0 442.83 318.23 105.52 o 5 1 0 4.74 25.73 62.88 o 6 1 0 912.91 1308.81 187.98 o 0 2 0 2880.85 3352.65 103.51 o 1 2 0 4194.13 4487.31 131.56 o 2 2 0 1120.44 1073.19 102.21 o 3 2 0 1998.97 1991.51 146.33 o 4 2 0 48.99 97.38 69.87 o 5 2 0 821.91 917.10 149.99 o 1 3 0 329.79 392.95 41.08 o 2 3 0 4803.18 5289.22 152.87 o 3 3 0 3184.51 3054.01 183.12 o 4 3 0 1367.73 1606.19 191.05 o 5 3 0 388.81 545.41 93.00 o 0 4 0 879.47 843.16 72.94 o 1 4 0 5332.71 5172.39 108.88 o 2 4 0 1388.13 1326.78 90.62 o 3 4 0 248.42 302.06 66.52 o 4 4 0 227.44 152.17 64.17 o 5 4 0 129.74 225.20 84.76 o 1 5 0 9.25 32.94 31.79 o 2 5 0 246.69 242.88 26.11 o 3 5 0 3410.88 3352.91 171.08 o 4 5 0 2581.15 2507.31 263.27 o 5 5 0 5321.98 6021.76 505.86 o 0 6 0 630.62 532.52 69.09 o 1 6 0 2048.95 1898.56 84.26 o 2 6 0 1010.45 967.25 71.00 o 3 6 0 457.39 587.07 89.37 o 4 6 0 89.81 99.05 62.36 o 5 6 0 1071.97 1351.54 190.71 o 6 6 0 432.57 750.90 141.30 o 1 7 0 54.65 44.66 34.70 o 2 7 0 2381.78 2272.45 100.01 o 3 7 0 672.41 598.78 92.07 o 4 7 0 2127.35 2374.43 232.11 o 5 7 0 265.63 495.17 128.78 o 0 8 0 2106.92 1784.27 121.99 o 1 8 0 183.65 211.73 48.69 o 2 8 0 928.43 1100.32 82.87 o 3 8 0 1351.36 1394.29 132.61 o 4 8 0 182.40 236.57 74.12 o 5 8 0 16.17 66.91 79.59 o 6 8 0 100.26 314.76 111.86 o 1 9 0 27.57 44.95 41.93 o 2 9 0 3521.94 3774.78 144.30 o 3 9 0 1191.03 1192.78 130.74 o 4 9 0 1163.22 1406.40 143.68 o 5 9 0 562.73 482.17 133.02 o 6 9 0 451.74 673.99 145.35 o 0 10 0 942.56 817.61 140.08 o 1 10 0 2121.44 1954.93 110.97 o 2 10 0 2157.93 2067.48 114.90 o 3 10 0 32.15 26.81 61.87 o 4 10 0 54.97 88.08 52.28 o 5 10 0 76.22 96.18 60.95 o 6 10 0 8.40 174.15 51.13 o 1 11 0 2466.46 2329.93 125.60 o 2 11 0 294.10 325.21 64.56 o 3 11 0 759.80 1002.79 124.26 o 4 11 0 0.79 92.34 50.80 o 5 11 0 693.15 1024.46 185.13 o 0 12 0 912.62 1003.75 170.03 o 1 12 0 1587.47 1414.47 151.33 o 2 12 0 200.33 240.48 60.27 o 3 12 0 4.09 54.72 85.73 o 4 12 0 29.88 -39.50 62.21 o 5 12 0 176.14 322.49 107.14 o 1 13 0 250.47 340.65 70.36 o 2 13 0 182.53 186.08 56.68 o 3 13 0 1106.40 728.64 96.54 o 4 13 0 716.56 720.21 136.40 o 0 14 0 2782.39 2922.37 256.85 o 1 14 0 228.61 312.53 59.67 o 2 14 0 1249.08 947.79 252.61 o 3 14 0 245.22 312.39 142.02 o 1 15 0 48.91 -10.73 34.28 o 2 15 0 173.21 223.52 64.37 o 3 15 0 38.39 0.97 66.40 o 0 16 0 1017.91 1040.40 184.32 o 1 16 0 4.27 80.14 38.15 o 2 16 0 1022.70 569.51 326.54 o 1 17 0 84.89 189.51 67.01 o 0 18 0 120.06 253.09 89.48 o 4 0 1 456.48 413.38 124.86 o 5 0 1 8.09 14.72 43.93 o 6 0 1 1161.03 1408.46 203.68 o -6 1 1 431.01 604.04 131.75 o -5 1 1 35.83 31.93 55.37 o -4 1 1 100.06 85.53 77.32 o -3 1 1 2187.42 2075.10 144.46 o -2 1 1 2377.33 2290.13 124.79 o -1 1 1 4972.43 5378.89 116.66 o 0 1 1 20294.11 13497.05 4034.86 o 1 1 1 5246.28 5417.71 96.42 o 2 1 1 2123.02 2124.77 136.28 o 3 1 1 2113.70 2051.36 153.85 o 4 1 1 99.09 151.45 96.42 o 5 1 1 49.24 57.50 90.13 o 6 1 1 428.10 528.73 127.92 o -6 2 1 167.07 399.49 102.98 o -5 2 1 150.84 195.88 62.39 o -4 2 1 1571.33 1489.66 144.80 o -3 2 1 1049.82 1036.86 128.83 o -2 2 1 6383.98 6584.66 502.87 o -1 2 1 8.44 16.09 17.30 o 0 2 1 72.61 86.95 11.65 o 1 2 1 1.95 1.41 13.33 o 2 2 1 6406.13 6339.25 217.40 o 3 2 1 1195.55 1122.65 140.03 o 4 2 1 1440.13 1300.10 150.45 o 5 2 1 142.81 14.70 79.33 o 6 2 1 166.72 306.76 90.13 o -5 3 1 57.62 115.04 47.91 o -4 3 1 197.26 327.81 71.57 o -3 3 1 2979.18 3292.09 272.59 o -2 3 1 1345.31 1392.61 83.52 o -1 3 1 4115.51 4216.83 84.72 o 0 3 1 3613.62 3735.49 101.36 o 1 3 1 4509.79 4711.98 55.10 o 2 3 1 1265.71 1384.48 125.48 o 3 3 1 3077.57 3309.85 201.72 o 4 3 1 196.19 130.41 107.96 o 5 3 1 64.61 206.15 107.62 o -5 4 1 3144.68 3403.16 245.77 o -4 4 1 269.87 215.20 63.78 o -3 4 1 5097.15 5049.49 220.62 o -2 4 1 2679.28 2835.85 130.54 o -1 4 1 78.63 57.04 31.28 o 0 4 1 39.71 48.44 20.81 o 1 4 1 99.23 89.53 17.41 o 2 4 1 2596.87 2765.41 139.31 o 3 4 1 5073.25 4682.07 255.64 o 4 4 1 267.09 282.73 76.22 o 5 4 1 3335.00 3715.02 340.74 o 6 4 1 199.81 351.91 97.86 o -5 5 1 596.70 939.45 147.81 o -4 5 1 28.28 59.61 49.31 o -3 5 1 1643.89 1668.39 170.33 o -2 5 1 1747.12 1838.09 77.32 o -1 5 1 3671.26 3534.85 96.15 o 0 5 1 1603.13 1414.88 62.99 o 1 5 1 3342.29 3282.17 99.70 o 2 5 1 1835.17 1867.79 59.57 o 3 5 1 1596.53 1574.78 77.10 o 4 5 1 26.12 7.30 50.64 o 5 5 1 627.06 743.78 106.73 o 6 5 1 363.85 425.32 119.28 o -5 6 1 2405.19 3133.33 250.75 o -4 6 1 2747.66 2627.08 527.09 o -3 6 1 2234.06 2163.96 298.43 o -2 6 1 1132.89 1081.82 68.15 o -1 6 1 727.89 906.61 65.19 o 0 6 1 1687.82 1676.37 68.84 o 1 6 1 675.47 740.73 62.87 o 2 6 1 1241.42 1212.11 42.65 o 3 6 1 2198.30 2109.44 133.69 o 4 6 1 2736.74 2620.36 159.10 o 5 6 1 2367.47 2339.71 326.45 o -6 7 1 248.68 292.16 91.61 o -5 7 1 501.05 386.02 106.28 o -4 7 1 212.72 194.15 73.72 o -3 7 1 1499.73 1428.73 114.41 o -2 7 1 757.89 776.98 68.24 o -1 7 1 770.78 853.12 67.29 o 0 7 1 411.11 304.02 49.75 o 1 7 1 889.65 1074.85 78.47 o 2 7 1 605.80 588.05 64.39 o 3 7 1 1538.88 1525.63 138.13 o 4 7 1 200.72 252.86 76.09 o 5 7 1 472.17 546.81 92.26 o 6 7 1 254.34 467.50 120.14 o -6 8 1 471.06 768.04 149.73 o -5 8 1 157.43 210.56 93.28 o -4 8 1 794.21 1063.15 143.48 o -3 8 1 56.60 63.93 60.70 o -2 8 1 3168.81 3048.92 180.24 o -1 8 1 1143.49 1129.51 78.26 o 0 8 1 41.72 25.13 36.55 o 1 8 1 1176.97 1191.03 86.72 o 2 8 1 3025.84 2849.96 120.74 o 3 8 1 55.79 -0.53 64.62 o 4 8 1 786.68 1077.70 201.75 o 5 8 1 169.09 301.93 75.54 o 6 8 1 488.13 993.86 176.30 o -6 9 1 293.42 374.74 88.19 o -5 9 1 91.43 263.77 109.87 o -4 9 1 195.49 272.68 76.15 o -3 9 1 155.56 220.56 77.90 o -2 9 1 711.28 724.00 78.32 o -1 9 1 2092.16 1951.54 135.68 o 0 9 1 4107.91 3857.08 137.52 o 1 9 1 2076.89 1942.61 105.41 o 2 9 1 632.64 731.14 79.53 o 3 9 1 183.04 182.59 53.01 o 4 9 1 211.58 334.62 113.90 o 5 9 1 81.33 269.66 84.64 o 6 9 1 369.43 385.08 81.94 o -6 10 1 263.55 345.16 98.19 o -5 10 1 687.13 710.54 166.15 o -4 10 1 205.12 374.79 131.15 o -3 10 1 2410.49 2147.00 148.85 o -2 10 1 57.73 64.62 42.28 o -1 10 1 613.70 726.84 80.09 o 0 10 1 53.44 6.82 44.41 o 1 10 1 599.77 639.67 79.49 o 2 10 1 83.17 74.72 49.86 o 3 10 1 2459.21 2336.42 121.01 o 4 10 1 205.18 466.52 95.40 o 5 10 1 548.22 709.15 174.91 o 6 10 1 272.12 442.01 133.95 o -5 11 1 9.80 47.20 69.92 o -4 11 1 253.09 371.99 124.74 o -3 11 1 430.04 511.96 150.05 o -2 11 1 369.56 355.11 65.96 o -1 11 1 3894.76 3691.26 179.20 o 0 11 1 2035.12 1970.04 117.11 o 1 11 1 3842.54 3634.26 152.00 o 2 11 1 382.63 468.33 75.37 o 3 11 1 464.96 636.42 108.80 o 4 11 1 227.81 159.99 106.68 o 5 11 1 7.85 -5.03 64.27 o -5 12 1 663.21 777.40 165.17 o -4 12 1 166.53 122.27 118.83 o -3 12 1 1275.50 1063.51 115.77 o -2 12 1 35.54 30.86 43.65 o -1 12 1 699.16 772.88 90.73 o 0 12 1 26.79 2.38 51.77 o 1 12 1 677.36 698.27 90.35 o 2 12 1 47.05 73.33 45.38 o 3 12 1 1314.56 1210.03 502.84 o 4 12 1 173.81 286.92 134.11 o 5 12 1 787.69 892.03 168.98 o -4 13 1 15.64 24.44 65.95 o -3 13 1 675.07 733.91 100.19 o -2 13 1 166.75 210.53 88.02 o -1 13 1 1389.13 1303.45 198.38 o 0 13 1 112.65 167.25 65.26 o 1 13 1 1275.32 1259.32 193.40 o 2 13 1 205.91 164.59 90.68 o 3 13 1 697.45 635.51 96.96 o 4 13 1 10.61 -15.20 51.56 o -4 14 1 405.00 180.94 91.92 o -3 14 1 200.79 134.82 147.42 o -2 14 1 457.65 561.65 91.96 o -1 14 1 328.87 389.01 143.09 o 0 14 1 703.99 730.49 108.79 o 1 14 1 344.09 359.90 72.42 o 2 14 1 543.82 366.61 67.82 o 3 14 1 292.29 293.23 67.84 o 4 14 1 456.20 246.82 83.04 o -2 15 1 1226.75 642.71 283.61 o -1 15 1 363.39 355.04 82.64 o 0 15 1 787.59 728.77 128.71 o 1 15 1 404.74 443.93 74.70 o 2 15 1 1290.39 781.64 265.50 o 3 15 1 45.82 148.97 60.29 o -2 16 1 288.17 395.76 229.33 o -1 16 1 175.16 339.28 78.23 o 0 16 1 31.07 22.60 76.90 o 1 16 1 199.16 383.64 108.25 o 2 16 1 222.11 194.33 106.62 o 3 16 1 133.71 291.73 77.89 o -1 17 1 415.73 632.38 143.34 o 0 17 1 418.39 807.23 394.60 o 1 17 1 464.88 548.56 161.88 o 2 17 1 745.24 613.79 117.67 o 0 18 1 8.50 -0.28 61.28 o 0 0 2 25550.41 7225.78 1010.63 o 1 0 2 134.11 153.65 20.95 o 2 0 2 1351.37 1318.75 106.67 o 4 0 2 9.36 -63.53 63.53 o 5 0 2 134.47 137.60 57.38 o 6 0 2 630.23 964.04 162.75 o 7 0 2 7.98 113.13 43.02 o -6 1 2 859.91 1270.18 193.82 o -5 1 2 34.39 54.46 48.54 o -4 1 2 1374.88 1256.03 132.76 o -3 1 2 1084.21 1077.74 105.18 o -2 1 2 3339.62 3198.63 106.19 o -1 1 2 284.07 330.60 41.62 o 0 1 2 2619.30 2563.39 47.58 o 1 1 2 268.93 258.05 27.08 o 2 1 2 3453.89 3135.47 204.51 o 3 1 2 1156.81 1028.81 122.61 o 4 1 2 1402.31 1524.37 188.56 o 5 1 2 59.89 57.04 81.70 o 6 1 2 860.64 1022.16 173.09 o -6 2 2 245.63 284.09 101.47 o -4 2 2 31.55 82.27 47.83 o -3 2 2 2012.80 2215.67 122.84 o -2 2 2 3098.67 3257.52 90.24 o -1 2 2 2424.97 2443.09 59.51 o 0 2 2 21701.31 18520.05 2615.09 o 1 2 2 2353.19 2436.78 57.28 o 2 2 2 3225.52 3298.69 86.57 o 3 2 2 1932.51 1761.47 152.70 o 4 2 2 26.00 -57.19 71.07 o 5 2 2 378.51 389.97 126.37 o 6 2 2 301.33 328.85 100.71 o -7 3 2 194.04 371.77 77.73 o -5 3 2 1659.58 2042.12 175.63 o -4 3 2 60.83 74.21 49.71 o -3 3 2 2895.60 2787.13 327.74 o -2 3 2 3212.55 3344.38 307.79 o -1 3 2 313.98 330.68 31.81 o 0 3 2 310.45 366.56 24.02 o 1 3 2 398.66 394.71 27.78 o 2 3 2 3164.44 3247.22 82.20 o 3 3 2 3302.71 2899.85 200.07 o 4 3 2 31.43 35.00 96.83 o 5 3 2 1719.55 1964.25 208.64 o 6 3 2 143.39 205.94 77.63 o -5 4 2 1228.34 1522.84 163.92 o -4 4 2 911.82 999.85 93.10 o -3 4 2 865.99 931.93 81.00 o -2 4 2 270.74 282.90 51.60 o -1 4 2 1691.30 1534.91 58.29 o 0 4 2 2989.79 3128.99 111.10 o 1 4 2 1560.69 1478.12 38.24 o 2 4 2 241.08 294.31 40.35 o 3 4 2 956.37 999.31 79.22 o 4 4 2 998.17 1087.07 96.38 o 5 4 2 1224.20 1464.29 205.50 o 6 4 2 1003.39 1190.86 113.49 o -5 5 2 1631.31 2016.86 193.97 o -4 5 2 432.50 459.34 79.83 o -3 5 2 3185.51 3262.48 140.40 o -2 5 2 26.48 -3.81 25.49 o -1 5 2 165.01 169.88 27.79 o 0 5 2 5.80 28.25 17.47 o 1 5 2 114.54 137.13 20.82 o 2 5 2 19.59 13.08 16.28 o 3 5 2 3299.84 3294.30 141.37 o 4 5 2 376.56 347.33 88.08 o 5 5 2 1539.92 1658.52 134.24 o 6 5 2 447.58 552.72 120.09 o -5 6 2 209.23 234.18 88.76 o -4 6 2 504.92 511.58 83.45 o -3 6 2 459.69 556.54 104.75 o -2 6 2 1347.22 1393.66 71.55 o -1 6 2 2570.59 2505.29 88.47 o 0 6 2 4078.00 4198.55 127.32 o 1 6 2 2663.36 2648.81 61.82 o 2 6 2 1202.74 1294.22 51.21 o 3 6 2 486.22 539.70 112.33 o 4 6 2 454.91 637.95 103.72 o 5 6 2 218.90 389.63 88.22 o 6 6 2 111.14 315.57 79.09 o -5 7 2 1145.52 1215.02 180.56 o -4 7 2 3440.79 3417.04 170.67 o -3 7 2 324.52 367.66 76.96 o -2 7 2 4665.05 4374.24 123.46 o -1 7 2 76.26 86.12 35.88 o 0 7 2 0.31 8.54 12.89 o 1 7 2 90.07 106.03 18.65 o 2 7 2 4637.69 4565.06 141.99 o 3 7 2 356.77 312.08 83.28 o 4 7 2 3363.31 3184.68 260.67 o 5 7 2 1077.78 1316.31 139.76 o 6 7 2 366.20 726.72 153.37 o -5 8 2 108.20 192.87 81.10 o -4 8 2 229.51 256.20 116.48 o -3 8 2 207.10 260.58 73.48 o -2 8 2 2114.41 1907.81 96.32 o -1 8 2 228.64 214.80 47.65 o 0 8 2 2736.14 2771.06 83.44 o 1 8 2 204.46 252.77 54.81 o 2 8 2 1952.09 1931.30 163.72 o 3 8 2 250.21 369.45 90.04 o 4 8 2 240.55 194.24 78.22 o 5 8 2 94.62 188.93 65.63 o 6 8 2 229.87 498.88 93.21 o -6 9 2 389.56 461.13 117.96 o -5 9 2 137.05 277.48 127.08 o -4 9 2 806.37 896.20 163.78 o -3 9 2 654.38 728.27 105.00 o -2 9 2 645.98 832.80 76.91 o -1 9 2 897.37 894.04 103.93 o 0 9 2 2443.59 2330.38 81.43 o 1 9 2 864.04 963.50 88.21 o 2 9 2 732.76 731.95 80.62 o 3 9 2 591.27 610.29 93.22 o 4 9 2 732.98 928.86 124.01 o 5 9 2 112.83 316.88 74.11 o 6 9 2 414.03 637.48 122.75 o -6 10 2 60.07 83.59 46.46 o -5 10 2 178.76 218.86 86.46 o -4 10 2 230.43 250.75 112.96 o -3 10 2 57.66 102.52 67.21 o -2 10 2 445.03 500.33 67.83 o -1 10 2 2353.93 2366.13 115.76 o 0 10 2 1597.88 1543.23 158.41 o 1 10 2 2418.14 2203.04 119.82 o 2 10 2 519.82 625.50 102.37 o 3 10 2 95.41 77.54 37.50 o 4 10 2 192.90 215.67 81.05 o 5 10 2 201.53 347.02 96.30 o 6 10 2 40.95 11.90 68.25 o -5 11 2 1636.47 2010.40 225.78 o -4 11 2 78.10 28.75 73.46 o -3 11 2 1659.46 1598.57 134.92 o -2 11 2 795.99 912.27 87.84 o -1 11 2 1671.79 1687.92 110.38 o 0 11 2 349.45 324.77 66.08 o 1 11 2 1776.58 1613.22 114.70 o 2 11 2 813.33 832.28 93.44 o 3 11 2 1489.17 1372.85 105.67 o 4 11 2 67.73 47.15 65.79 o 5 11 2 1547.44 1779.76 211.90 o -5 12 2 48.37 170.60 73.82 o -4 12 2 97.27 34.04 67.41 o -3 12 2 517.54 726.87 107.43 o -2 12 2 633.90 700.89 112.43 o -1 12 2 1431.02 1343.80 120.96 o 0 12 2 270.44 223.38 65.77 o 1 12 2 1243.80 1067.03 144.37 o 2 12 2 596.53 521.77 80.09 o 3 12 2 593.38 526.01 98.10 o 4 12 2 99.99 203.99 66.39 o 5 12 2 63.26 107.24 71.72 o -4 13 2 477.55 734.48 144.06 o -3 13 2 1184.00 1011.82 153.89 o -2 13 2 163.19 219.23 80.12 o -1 13 2 304.56 291.38 77.48 o 0 13 2 1364.94 1279.16 130.36 o 1 13 2 351.97 434.10 77.06 o 2 13 2 224.83 248.94 63.66 o 3 13 2 1101.54 559.73 95.94 o 4 13 2 432.99 285.84 96.16 o -4 14 2 6.98 39.93 58.89 o -3 14 2 314.24 282.87 87.66 o -2 14 2 460.43 587.88 98.80 o -1 14 2 314.02 342.82 81.55 o 0 14 2 560.62 732.93 108.22 o 1 14 2 359.55 364.11 78.35 o 2 14 2 536.76 479.36 76.10 o 3 14 2 292.86 295.02 72.89 o 4 14 2 12.88 62.18 185.01 o -3 15 2 4.56 -46.68 46.68 o -2 15 2 173.56 252.28 159.13 o -1 15 2 50.09 94.12 99.68 o 0 15 2 79.36 140.03 52.05 o 1 15 2 75.18 97.87 39.48 o 2 15 2 201.69 209.37 44.75 o 3 15 2 1.20 99.30 133.07 o -2 16 2 1139.38 772.15 146.52 o -1 16 2 147.19 129.53 85.74 o 0 16 2 2473.34 2378.36 166.61 o 1 16 2 122.76 282.72 68.61 o 2 16 2 1195.66 989.46 178.29 o 3 16 2 302.51 388.20 117.73 o -1 17 2 64.92 184.82 84.50 o 0 17 2 88.53 44.48 44.05 o 1 17 2 91.72 164.87 78.06 o 2 17 2 443.38 455.64 166.21 o 0 18 2 145.92 125.86 63.08 o 1 0 3 108.68 114.77 20.67 o 2 0 3 3236.19 3445.24 190.72 o 3 0 3 776.54 838.61 94.36 o 4 0 3 3089.16 3033.34 138.89 o 5 0 3 12.03 22.67 64.46 o 6 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