data_2019481 _cell_angle_alpha 90.000 _cell_angle_beta 112.680 _cell_angle_gamma 90.000 _cell_length_a 10.8920 _cell_length_b 11.3011 _cell_length_c 13.1986 _exptl_crystal_F_000 912.00 _reflns_d_resolution_high 0.8002 _[local]_cod_data_source_file uk3089IIIsup4.hkl _[local]_cod_data_source_block III _shelx_title ' CHI5 in P21/n No.14' _shelx_refln_list_code 4 _shelx_f_calc_maximum 342.49 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 51402.20 53060.19 508.64 o 4 0 0 14403.66 14999.23 210.61 o 6 0 0 19565.70 19001.36 328.34 o 8 0 0 22601.59 22517.47 385.24 o 10 0 0 6665.11 6890.29 275.82 o 12 0 0 4143.38 4624.32 254.95 o 2 1 0 60929.62 62943.65 416.56 o 3 1 0 34798.05 35230.46 276.87 o 4 1 0 14732.89 14966.48 142.66 o 5 1 0 16106.75 16012.69 145.61 o 6 1 0 839.00 1012.46 40.63 o 7 1 0 51.84 80.57 11.43 o 8 1 0 1121.76 1185.40 70.95 o 9 1 0 9803.28 9903.23 208.37 o 10 1 0 8059.75 8813.52 219.87 o 11 1 0 8684.99 9195.89 240.64 o 12 1 0 4620.82 5003.73 188.42 o 0 2 0 6905.12 6543.01 242.11 o 1 2 0 62083.80 63421.04 886.93 o 2 2 0 3877.45 4041.61 49.70 o 3 2 0 8432.24 9208.96 90.24 o 4 2 0 4313.79 4349.04 85.30 o 5 2 0 24653.96 24336.45 252.80 o 6 2 0 774.07 739.77 34.31 o 7 2 0 39530.20 37349.94 832.19 o 8 2 0 710.56 739.08 51.30 o 9 2 0 9529.15 9857.21 230.50 o 10 2 0 152.52 113.07 20.40 o 11 2 0 71.93 73.20 16.16 o 12 2 0 1.97 24.06 26.86 o 1 3 0 3740.82 3788.93 61.91 o 2 3 0 723.98 707.67 22.84 o 3 3 0 38290.04 39164.55 449.27 o 4 3 0 31049.04 30458.72 636.89 o 5 3 0 20185.76 20515.43 332.82 o 6 3 0 7537.03 7622.46 158.17 o 7 3 0 361.12 291.78 41.36 o 8 3 0 5028.25 5154.17 131.06 o 9 3 0 4720.36 4902.50 164.06 o 10 3 0 8012.24 8591.56 233.08 o 11 3 0 5775.72 5833.87 228.55 o 12 3 0 3375.94 3443.73 176.42 o 0 4 0 27805.47 27291.84 478.82 o 1 4 0 66.93 100.43 9.12 o 2 4 0 19088.14 19710.82 277.68 o 3 4 0 805.96 892.64 31.25 o 4 4 0 99.85 98.95 12.86 o 5 4 0 1446.92 1379.06 54.58 o 6 4 0 39311.01 38444.47 683.32 o 7 4 0 73.58 59.12 10.37 o 8 4 0 23187.98 22911.92 375.15 o 9 4 0 459.52 433.09 43.75 o 10 4 0 1014.20 1021.56 83.62 o 11 4 0 64.41 49.86 28.79 o 12 4 0 3062.04 3149.61 194.67 o 1 5 0 4696.91 4655.82 92.78 o 2 5 0 9432.13 9603.51 142.78 o 3 5 0 21403.29 22013.59 322.03 o 4 5 0 30330.09 31999.03 529.77 o 5 5 0 10291.84 10052.28 221.04 o 6 5 0 7811.00 7939.57 171.48 o 7 5 0 2070.20 2019.48 86.56 o 8 5 0 4553.52 4525.96 155.16 o 9 5 0 6222.06 6407.30 210.76 o 10 5 0 10526.34 11006.07 312.70 o 11 5 0 13213.03 14173.59 375.86 o 0 6 0 69.73 57.59 11.64 o 1 6 0 41469.45 42430.61 651.36 o 2 6 0 1381.04 1443.09 59.13 o 3 6 0 385.09 418.92 30.44 o 4 6 0 242.44 177.99 16.33 o 5 6 0 8111.47 7888.27 153.24 o 6 6 0 83.24 92.77 14.26 o 7 6 0 19489.05 19298.28 541.90 o 8 6 0 0.28 28.47 25.16 o 9 6 0 15635.44 16075.40 447.94 o 10 6 0 79.84 52.20 20.92 o 11 6 0 1280.51 1485.17 131.06 o 1 7 0 4717.07 4901.94 125.71 o 2 7 0 8829.09 8393.98 324.03 o 3 7 0 11726.05 11125.04 384.76 o 4 7 0 15326.95 14467.14 356.11 o 5 7 0 9688.81 9631.40 231.53 o 6 7 0 4664.25 4724.05 143.55 o 7 7 0 590.78 624.02 60.82 o 8 7 0 4199.08 4151.79 173.94 o 9 7 0 7453.70 7679.06 271.34 o 10 7 0 10432.81 10861.46 418.34 o 0 8 0 35016.82 37458.91 598.52 o 1 8 0 0.88 21.61 9.89 o 2 8 0 14182.00 13406.49 514.34 o 3 8 0 11.39 9.32 11.45 o 4 8 0 596.28 534.96 44.74 o 5 8 0 814.06 724.04 58.31 o 6 8 0 16648.34 16833.42 466.30 o 7 8 0 403.77 385.84 52.16 o 8 8 0 21775.98 21826.47 847.20 o 9 8 0 1857.35 1825.00 134.44 o 10 8 0 1075.15 999.20 112.06 o 1 9 0 2145.04 1909.89 94.64 o 2 9 0 7016.36 6805.72 170.85 o 3 9 0 16361.27 17095.60 588.15 o 4 9 0 14038.66 14751.29 513.37 o 5 9 0 7598.67 7740.59 284.06 o 6 9 0 5169.62 5573.94 267.99 o 7 9 0 1451.35 1451.80 113.82 o 8 9 0 579.41 493.98 64.85 o 9 9 0 4102.23 4225.62 242.62 o 0 10 0 2118.51 2165.76 158.08 o 1 10 0 27589.60 29619.78 814.48 o 2 10 0 2.15 -13.02 14.99 o 3 10 0 3261.94 3315.78 144.91 o 4 10 0 460.32 339.93 49.92 o 5 10 0 11790.90 11837.66 550.47 o 6 10 0 371.91 286.23 42.21 o 7 10 0 15684.26 16534.61 698.66 o 8 10 0 93.22 111.06 41.79 o 1 11 0 1074.49 1167.73 97.05 o 2 11 0 11764.64 11721.33 313.32 o 3 11 0 12196.44 12471.48 426.22 o 4 11 0 6411.77 6372.05 256.89 o 5 11 0 8892.05 8999.20 555.52 o 6 11 0 856.85 797.36 97.16 o 7 11 0 143.16 116.45 38.22 o 0 12 0 25469.69 28285.44 933.67 o 1 12 0 15.94 18.84 31.84 o 2 12 0 5686.92 5749.19 231.70 o 3 12 0 0.22 -32.06 32.06 o 4 12 0 2965.11 2946.80 194.06 o 5 12 0 39.38 -19.76 52.18 o 6 12 0 10994.16 11403.75 478.51 o 1 13 0 1095.07 1104.61 107.54 o 2 13 0 11382.33 11636.95 418.08 o 3 13 0 5662.10 5762.68 298.64 o 4 13 0 7124.18 7104.61 315.71 o 0 14 0 549.72 944.43 207.34 o 1 14 0 13756.52 13666.19 470.53 o -11 0 1 4951.48 4989.98 244.14 o -9 0 1 37831.05 38905.76 546.64 o -7 0 1 16837.35 16478.87 294.66 o -5 0 1 11281.00 12908.82 153.93 o -3 0 1 57470.14 58017.73 624.15 o 1 0 1 31440.63 34422.91 937.29 o 3 0 1 47647.38 49625.49 775.59 o 5 0 1 23534.41 23275.75 454.69 o 7 0 1 16702.61 16569.68 376.43 o 9 0 1 1108.56 1178.92 103.45 o 11 0 1 9954.76 11018.71 381.44 o -12 1 1 7073.13 7652.25 228.65 o -11 1 1 8440.18 9292.34 236.68 o -10 1 1 3784.81 3977.34 142.82 o -9 1 1 209.95 208.39 24.29 o -8 1 1 1198.02 1249.06 53.00 o -7 1 1 12553.11 12692.69 161.25 o -6 1 1 14755.19 14160.23 137.34 o -5 1 1 31700.44 32036.62 234.47 o -4 1 1 23556.37 23103.82 192.47 o -3 1 1 28126.96 28504.97 214.06 o -2 1 1 6532.01 6887.31 54.92 o -1 1 1 2594.32 3433.72 196.15 o 1 1 1 52229.05 55568.73 570.99 o 2 1 1 49616.96 51471.30 492.14 o 3 1 1 7810.60 7926.94 90.13 o 4 1 1 13508.51 14030.92 163.75 o 5 1 1 913.41 992.53 35.61 o 6 1 1 1199.79 1179.86 43.76 o 7 1 1 1645.67 1571.96 57.43 o 8 1 1 7646.29 7522.28 164.53 o 9 1 1 12496.15 12872.35 268.27 o 10 1 1 8591.50 8941.87 227.59 o 11 1 1 5724.40 6075.07 198.73 o 12 1 1 435.44 290.48 39.42 o -12 2 1 1026.12 984.73 80.12 o -11 2 1 209.38 266.34 32.48 o -10 2 1 12874.83 13041.50 293.38 o -9 2 1 0.62 28.88 9.90 o -8 2 1 27729.12 27906.07 404.37 o -7 2 1 30.94 62.42 12.76 o -6 2 1 8420.68 8259.24 109.75 o -5 2 1 2475.54 2704.91 60.48 o -4 2 1 29671.45 30637.31 257.12 o -3 2 1 6.50 38.68 5.35 o -2 2 1 117297.98 116994.00 1234.85 o -1 2 1 2114.94 2218.58 33.64 o 0 2 1 33014.82 31923.36 386.57 o 1 2 1 9382.50 9802.35 100.00 o 2 2 1 939.91 970.31 26.10 o 3 2 1 3286.17 3343.58 54.90 o 4 2 1 25713.00 24547.61 371.44 o 5 2 1 530.62 514.42 26.37 o 6 2 1 40096.59 38692.26 716.16 o 7 2 1 119.28 125.83 14.21 o 8 2 1 3364.11 3349.66 133.83 o 9 2 1 833.22 784.67 66.05 o 10 2 1 2964.00 3308.52 145.67 o 11 2 1 21.93 9.43 23.78 o 12 2 1 10524.65 11171.64 306.64 o -12 3 1 4837.05 5243.16 213.16 o -11 3 1 5122.80 5219.75 189.13 o -10 3 1 2101.15 2168.41 112.92 o -9 3 1 105.45 127.57 24.59 o -8 3 1 466.33 501.24 44.66 o -7 3 1 7816.36 7490.83 171.13 o -6 3 1 24030.66 23626.70 394.99 o -5 3 1 31492.46 31893.37 343.35 o -4 3 1 33847.23 34825.14 409.30 o -3 3 1 8332.71 8602.79 97.05 o -2 3 1 2509.09 2704.92 45.40 o -1 3 1 3921.97 3924.70 55.17 o 0 3 1 41640.39 41283.44 451.19 o 1 3 1 6730.75 6603.54 66.42 o 2 3 1 22456.82 22651.01 276.12 o 3 3 1 31314.38 31217.78 476.60 o 4 3 1 4837.15 4973.59 95.63 o 5 3 1 2496.09 2288.71 59.16 o 6 3 1 3598.27 3305.85 97.68 o 7 3 1 11556.86 11267.82 379.15 o 8 3 1 11718.57 12255.36 249.65 o 9 3 1 13151.69 13695.50 282.20 o 10 3 1 5858.82 6003.65 207.19 o 11 3 1 680.35 699.69 76.10 o -12 4 1 17.67 51.08 40.72 o -11 4 1 8296.95 8385.42 260.07 o -10 4 1 1041.66 994.20 73.04 o -9 4 1 19151.97 19696.61 344.39 o -8 4 1 377.59 394.50 41.25 o -7 4 1 17265.79 16766.80 416.01 o -6 4 1 1509.81 1431.40 64.81 o -5 4 1 1548.85 1609.10 53.31 o -4 4 1 489.06 484.41 28.71 o -3 4 1 57614.11 58128.70 791.29 o -2 4 1 1667.77 1642.94 43.50 o -1 4 1 31663.26 31150.10 362.09 o 0 4 1 2273.01 2312.65 44.92 o 1 4 1 8373.30 8684.65 128.03 o 2 4 1 71.49 66.97 7.68 o 3 4 1 10103.90 10246.04 163.27 o 4 4 1 2.78 37.24 7.01 o 5 4 1 64681.43 65034.98 988.77 o 6 4 1 353.58 423.28 31.74 o 7 4 1 26327.73 27596.29 366.38 o 8 4 1 11.92 40.78 14.23 o 9 4 1 1192.28 1321.25 100.42 o 10 4 1 72.95 30.73 30.33 o 11 4 1 8588.18 8951.19 316.52 o -12 5 1 9244.85 10027.88 349.54 o -11 5 1 3684.67 3860.92 190.23 o -10 5 1 2041.48 2180.24 126.03 o -9 5 1 156.99 121.22 34.54 o -8 5 1 11222.20 11368.83 245.02 o -7 5 1 6120.94 5848.20 225.16 o -6 5 1 13648.49 13494.13 258.54 o -5 5 1 18716.01 18790.72 320.55 o -4 5 1 5752.06 5493.29 124.70 o -3 5 1 2677.49 2318.00 98.48 o -2 5 1 5597.21 5991.41 105.91 o -1 5 1 1954.70 1817.87 74.58 o 0 5 1 7427.94 7368.72 110.47 o 1 5 1 21194.68 21569.31 241.89 o 2 5 1 31509.20 31693.35 452.65 o 3 5 1 19595.80 19269.97 362.22 o 4 5 1 6020.88 5877.37 148.87 o 5 5 1 431.58 460.52 36.05 o 6 5 1 6228.96 6368.85 148.74 o 7 5 1 12530.94 12809.26 250.38 o 8 5 1 14431.13 15041.05 360.96 o 9 5 1 11392.77 11752.62 312.72 o 10 5 1 8523.98 8845.67 286.83 o 11 5 1 2295.92 2249.17 150.26 o -11 6 1 0.38 20.37 17.75 o -10 6 1 20279.91 21359.18 423.77 o -9 6 1 12.77 33.34 12.17 o -8 6 1 24479.82 24391.21 699.74 o -7 6 1 19.80 24.51 17.19 o -6 6 1 96.77 138.43 22.14 o -5 6 1 55.08 49.86 7.71 o -4 6 1 4770.35 3953.05 227.71 o -3 6 1 420.05 411.63 43.50 o -2 6 1 30138.97 30372.53 647.20 o -1 6 1 77.73 70.95 10.99 o 0 6 1 35485.46 35410.73 550.25 o 1 6 1 452.29 477.63 31.50 o 2 6 1 117.01 179.35 17.51 o 3 6 1 1269.40 1382.18 51.10 o 4 6 1 30639.62 30224.12 589.80 o 5 6 1 116.16 86.36 20.52 o 6 6 1 31687.24 32549.50 650.94 o 7 6 1 108.26 122.54 24.09 o 8 6 1 4613.62 4705.72 199.79 o 9 6 1 51.26 1.52 23.85 o 10 6 1 5215.54 5528.53 232.70 o 11 6 1 15.05 4.71 34.39 o -11 7 1 4698.74 4666.95 220.56 o -10 7 1 2263.87 2201.44 147.54 o -9 7 1 62.72 80.42 31.08 o -8 7 1 4871.41 5010.88 185.40 o -7 7 1 2236.52 2010.64 91.96 o -6 7 1 7023.13 6712.03 216.00 o -5 7 1 9766.43 9175.53 316.07 o -4 7 1 4513.65 3711.73 183.74 o -3 7 1 3775.04 3544.09 111.73 o -2 7 1 2786.68 2753.98 98.44 o -1 7 1 2807.55 2492.49 94.98 o 0 7 1 7870.55 7473.61 196.49 o 1 7 1 24489.72 25373.15 358.67 o 2 7 1 27011.72 27222.56 737.18 o 3 7 1 9625.07 9315.62 206.30 o 4 7 1 5757.22 5604.19 153.89 o 5 7 1 29.06 32.89 13.90 o 6 7 1 39.74 42.54 16.31 o 7 7 1 3514.92 3597.17 157.73 o 8 7 1 9187.51 8987.26 416.35 o 9 7 1 9625.07 10187.41 400.94 o 10 7 1 7817.02 8000.86 307.06 o -10 8 1 1323.63 1235.86 115.81 o -9 8 1 18431.02 19034.74 859.60 o -8 8 1 184.41 106.65 40.35 o -7 8 1 9987.74 9830.26 307.48 o -6 8 1 2119.51 1972.96 103.67 o -5 8 1 767.99 655.90 47.73 o -4 8 1 252.04 181.95 22.58 o -3 8 1 22316.90 22432.75 791.06 o -2 8 1 363.00 318.12 31.86 o -1 8 1 34574.94 35390.59 530.41 o 0 8 1 1602.55 1424.88 69.01 o 1 8 1 7604.71 7967.57 200.37 o 2 8 1 55.90 43.24 13.44 o 3 8 1 8318.90 8025.89 206.14 o 4 8 1 507.13 455.80 40.61 o 5 8 1 26143.37 25616.95 909.25 o 6 8 1 0.39 -12.78 25.18 o 7 8 1 10277.61 9958.50 316.69 o 8 8 1 85.22 60.39 23.92 o 9 8 1 35.73 94.84 31.64 o 10 8 1 199.23 164.29 41.97 o -9 9 1 77.10 77.83 20.89 o -8 9 1 44.33 68.25 31.82 o -7 9 1 9110.30 9079.33 332.99 o -6 9 1 11755.26 12178.89 374.36 o -5 9 1 14205.98 13941.81 470.93 o -4 9 1 14681.24 14980.57 501.52 o -3 9 1 3327.85 3234.78 128.29 o -2 9 1 373.47 288.14 33.23 o -1 9 1 1026.13 909.05 51.59 o 0 9 1 9814.05 9236.58 399.03 o 1 9 1 15580.93 15145.96 489.19 o 2 9 1 7579.27 7330.70 281.63 o 3 9 1 15885.77 15531.88 684.75 o 4 9 1 3037.38 2915.31 158.91 o 5 9 1 639.19 633.18 64.16 o 6 9 1 1113.15 1238.93 109.20 o 7 9 1 5067.53 5253.30 258.62 o 8 9 1 6291.65 6189.44 297.54 o 9 9 1 6062.37 5610.22 353.39 o -9 10 1 27.22 24.18 31.17 o -8 10 1 16047.59 16166.99 626.04 o -7 10 1 3.57 6.74 13.86 o -6 10 1 3488.81 3572.89 180.97 o -5 10 1 10.56 11.36 23.87 o -4 10 1 14257.98 14609.10 514.17 o -3 10 1 0.10 11.95 18.72 o -2 10 1 36447.77 38094.34 1044.84 o -1 10 1 231.43 207.20 31.18 o 0 10 1 6624.89 6721.60 196.94 o 1 10 1 14.67 10.82 17.85 o 2 10 1 157.53 139.15 32.95 o 3 10 1 540.69 469.81 58.07 o 4 10 1 16788.44 16768.73 776.10 o 5 10 1 162.82 152.78 32.29 o 6 10 1 21713.16 22901.95 1115.20 o 7 10 1 155.54 123.53 34.64 o 8 10 1 1304.49 1132.43 131.66 o -8 11 1 445.57 385.86 80.39 o -7 11 1 3729.28 3504.63 224.91 o -6 11 1 12299.62 13359.62 496.01 o -5 11 1 11107.19 11837.67 381.14 o -4 11 1 14906.72 14857.31 630.78 o -3 11 1 4078.25 4108.96 212.29 o -2 11 1 4.10 -0.41 23.17 o -1 11 1 942.96 998.31 88.16 o 0 11 1 4782.34 5198.12 206.58 o 1 11 1 15416.67 16262.36 368.97 o 2 11 1 7261.99 7581.76 253.44 o 3 11 1 4846.22 4926.45 314.42 o 4 11 1 4696.74 4705.83 237.00 o 5 11 1 62.43 15.25 32.83 o 6 11 1 707.22 589.56 88.21 o 7 11 1 1296.49 1277.18 140.74 o -6 12 1 408.31 360.39 81.58 o -5 12 1 30.17 59.78 43.33 o -4 12 1 71.35 52.00 36.56 o -3 12 1 16072.36 16174.13 561.97 o -2 12 1 251.90 245.88 55.23 o -1 12 1 21029.67 21767.97 602.56 o 0 12 1 33.10 9.45 23.22 o 1 12 1 768.93 809.50 87.45 o 2 12 1 83.74 101.90 35.95 o 3 12 1 5682.08 5917.50 273.88 o 4 12 1 0.07 -10.59 29.37 o 5 12 1 8688.28 8591.88 468.43 o 6 12 1 0.52 -13.43 34.39 o -5 13 1 5113.72 4805.66 284.72 o -4 13 1 6217.57 5879.42 299.89 o -3 13 1 3001.99 2980.58 215.61 o -2 13 1 1014.98 913.78 113.30 o -1 13 1 2962.67 2930.27 203.64 o 0 13 1 4570.10 4297.83 240.50 o 1 13 1 14803.69 15110.50 417.67 o 2 13 1 7097.42 7017.54 328.68 o 3 13 1 4376.72 4084.15 254.25 o 4 13 1 1367.90 1205.33 122.94 o -1 14 1 669.53 878.00 130.33 o 0 14 1 9133.12 9167.86 417.74 o 1 14 1 226.57 306.17 76.02 o -12 0 2 7328.77 7766.96 345.78 o -10 0 2 37949.84 39663.20 740.84 o -8 0 2 7057.42 7360.55 179.94 o -6 0 2 19652.48 20092.21 218.63 o -4 0 2 79833.73 80826.99 922.87 o -2 0 2 19044.51 18717.28 206.72 o 0 0 2 1630.94 1718.20 51.82 o 2 0 2 69217.58 69130.77 1469.56 o 4 0 2 45280.89 46242.27 756.57 o 6 0 2 6298.93 6046.36 155.88 o 8 0 2 617.35 633.60 68.88 o 10 0 2 19453.33 19932.61 556.43 o -13 1 2 4406.59 4822.69 188.64 o -12 1 2 6196.26 6938.51 232.67 o -11 1 2 100.54 99.08 19.27 o -10 1 2 91.54 90.03 13.77 o -9 1 2 5072.76 5323.52 135.36 o -8 1 2 26546.18 27020.48 243.19 o -7 1 2 33301.89 33802.30 242.10 o -6 1 2 20760.62 21015.87 171.28 o -5 1 2 6763.67 6463.55 86.34 o -4 1 2 718.53 759.86 23.36 o -3 1 2 6517.23 6642.77 74.68 o -2 1 2 15251.82 15219.19 141.19 o -1 1 2 21388.06 21641.77 141.55 o 0 1 2 41021.34 41031.79 358.66 o 1 1 2 14154.38 14441.23 123.48 o 2 1 2 6363.81 6598.67 75.56 o 3 1 2 1240.67 1301.27 39.50 o 4 1 2 804.23 786.36 36.47 o 5 1 2 4276.56 4068.12 81.83 o 6 1 2 5172.22 4984.33 111.20 o 7 1 2 11546.37 11007.15 341.01 o 8 1 2 11036.23 11176.69 241.16 o 9 1 2 2813.73 2861.39 121.38 o 10 1 2 3837.58 3874.20 153.01 o 11 1 2 499.09 548.57 52.84 o -12 2 2 416.07 379.63 47.55 o -11 2 2 19980.67 21413.79 416.25 o -10 2 2 532.69 549.15 49.67 o -9 2 2 14820.95 14879.50 253.31 o -8 2 2 69.96 49.66 10.50 o -7 2 2 9.10 38.60 9.22 o -6 2 2 416.38 415.17 24.45 o -5 2 2 47261.00 47229.22 434.23 o -4 2 2 774.21 912.77 26.80 o -3 2 2 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