data_2019488 _cell_angle_alpha 103.065 _cell_angle_beta 112.942 _cell_angle_gamma 96.471 _cell_length_a 12.6931 _cell_length_b 13.0160 _cell_length_c 14.3559 _exptl_crystal_F_000 924.00 _reflns_d_resolution_high 0.8403 _[local]_cod_data_source_file sk3527Isup2.hkl _[local]_cod_data_source_block I _shelx_title ' I in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 256.49 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 7976.41 8530.57 199.71 o 3 0 0 7227.15 7150.51 170.94 o 4 0 0 1137.89 1282.60 39.41 o 5 0 0 1478.02 1511.36 47.24 o 6 0 0 570.00 531.52 31.91 o 7 0 0 103.00 44.00 23.30 o 8 0 0 108.65 62.57 28.36 o 9 0 0 26.49 -0.99 22.10 o 10 0 0 66.82 94.92 39.47 o 11 0 0 4.45 -1.45 32.28 o 12 0 0 545.98 601.32 87.60 o 13 0 0 23.43 38.54 43.53 o -13 1 0 322.02 323.69 71.95 o -12 1 0 132.63 110.36 48.66 o -11 1 0 390.95 358.57 63.10 o -10 1 0 11.79 11.52 28.89 o -9 1 0 1703.04 1873.13 116.55 o -8 1 0 2.21 -0.33 19.97 o -7 1 0 2145.13 2310.18 125.00 o -6 1 0 1712.41 1938.83 146.17 o -5 1 0 153.69 139.46 26.29 o -4 1 0 1919.11 2002.75 70.24 o -3 1 0 16432.47 16533.06 472.93 o -2 1 0 413.66 428.86 29.29 o 1 1 0 4157.19 4292.54 125.46 o 2 1 0 283.64 281.99 11.89 o 3 1 0 114.99 101.49 17.22 o 4 1 0 1954.28 1794.79 51.98 o 5 1 0 2205.07 2259.80 65.26 o 6 1 0 112.74 115.50 17.52 o 7 1 0 868.34 872.32 45.25 o 8 1 0 225.55 353.85 54.58 o 9 1 0 49.11 22.83 28.82 o 10 1 0 37.57 10.18 31.62 o 11 1 0 149.15 87.00 44.33 o 12 1 0 0.09 -1.77 39.34 o 13 1 0 4.47 -1.85 41.14 o -13 2 0 0.10 -1.71 38.07 o -12 2 0 2.95 24.03 34.95 o -11 2 0 3.07 -1.29 28.69 o -10 2 0 18.54 -1.11 24.69 o -9 2 0 261.59 291.08 51.45 o -8 2 0 1431.83 1442.81 93.79 o -7 2 0 2198.68 2428.06 129.73 o -6 2 0 43.94 28.02 18.50 o -5 2 0 1485.02 1698.00 64.85 o -4 2 0 8.31 26.96 9.86 o -3 2 0 3532.50 3785.11 118.04 o -2 2 0 296.27 299.96 27.96 o -1 2 0 433.06 386.46 23.50 o 0 2 0 2898.61 3441.73 101.15 o 1 2 0 111.48 62.17 8.60 o 2 2 0 33009.63 33041.96 923.84 o 3 2 0 110.74 84.14 14.18 o 4 2 0 841.54 1025.30 34.60 o 5 2 0 43.70 20.89 10.10 o 6 2 0 1676.10 1692.42 77.84 o 7 2 0 0.05 4.26 14.05 o 8 2 0 514.69 509.67 36.66 o 9 2 0 698.25 602.66 62.37 o 10 2 0 363.58 480.11 70.76 o 11 2 0 50.25 20.23 35.61 o 12 2 0 151.76 162.55 56.98 o 13 2 0 1.71 28.22 45.66 o -13 3 0 238.07 265.25 64.43 o -12 3 0 79.27 122.94 46.99 o -11 3 0 101.90 74.55 41.67 o -10 3 0 25.91 29.69 30.69 o -9 3 0 186.81 130.53 36.61 o -8 3 0 1636.75 1694.35 104.24 o -7 3 0 456.16 441.64 43.33 o -6 3 0 1222.09 1418.11 83.47 o -5 3 0 522.35 459.81 39.01 o -4 3 0 143.86 135.99 22.83 o -3 3 0 3208.01 3061.80 138.78 o -2 3 0 322.34 307.05 24.83 o -1 3 0 5464.59 5805.26 168.75 o 0 3 0 245.31 186.62 12.57 o 1 3 0 2047.61 1622.66 55.00 o 2 3 0 556.79 457.99 23.60 o 3 3 0 570.95 784.92 27.45 o 4 3 0 1410.65 1389.34 44.10 o 5 3 0 5149.56 5393.40 139.14 o 6 3 0 655.85 596.67 36.35 o 7 3 0 417.35 404.48 38.28 o 8 3 0 245.18 188.91 30.39 o 9 3 0 506.38 585.87 51.78 o 10 3 0 6.23 -1.46 32.48 o 11 3 0 99.32 123.47 54.71 o 12 3 0 0.07 -1.67 37.21 o -13 4 0 5.49 5.13 37.01 o -12 4 0 18.12 -1.33 29.55 o -11 4 0 32.58 7.72 28.69 o -10 4 0 1262.77 1149.07 89.13 o -9 4 0 156.74 147.77 39.54 o -8 4 0 1665.14 1571.01 97.31 o -7 4 0 592.31 543.81 48.59 o -6 4 0 1192.76 1205.51 76.01 o -5 4 0 1159.29 1338.90 77.61 o -4 4 0 246.48 254.47 27.82 o -3 4 0 651.01 607.65 41.93 o -2 4 0 9.94 3.19 9.39 o -1 4 0 2086.00 2294.11 74.36 o 0 4 0 233.22 221.45 15.11 o 1 4 0 20.65 26.69 20.90 o 2 4 0 4417.72 4926.20 151.56 o 3 4 0 1226.13 1191.87 37.81 o 4 4 0 9555.73 10251.57 305.78 o 5 4 0 821.08 848.16 44.40 o 6 4 0 302.09 362.85 58.48 o 7 4 0 101.64 43.78 19.32 o 8 4 0 532.08 544.01 40.63 o 9 4 0 60.71 44.55 25.32 o 10 4 0 46.18 20.19 26.36 o 11 4 0 4.92 -1.54 34.21 o 12 4 0 5.89 -1.55 34.41 o -13 5 0 89.93 26.03 37.34 o -12 5 0 29.86 6.79 36.08 o -11 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501.25 58.84 o 1 6 0 55.08 69.60 32.38 o 2 6 0 901.87 837.57 45.16 o 3 6 0 33.70 0.75 13.23 o 4 6 0 1273.81 1135.45 55.70 o 5 6 0 1.11 -0.61 13.53 o 6 6 0 288.33 350.24 39.99 o 7 6 0 30.03 31.50 22.01 o 8 6 0 506.43 568.66 55.17 o 9 6 0 115.01 81.30 32.22 o 10 6 0 143.74 133.20 35.69 o 11 6 0 2.91 -1.23 27.30 o -13 7 0 323.13 375.48 72.15 o -12 7 0 32.61 10.18 31.28 o -11 7 0 1348.13 1231.47 95.78 o -10 7 0 14.09 12.38 28.16 o -9 7 0 1555.57 1481.15 101.71 o -8 7 0 5.41 -0.89 19.84 o -7 7 0 1619.00 1590.71 99.84 o -6 7 0 255.59 195.83 38.54 o -5 7 0 2734.72 2613.90 137.38 o -4 7 0 691.51 681.93 54.98 o -3 7 0 49.59 38.97 12.83 o -2 7 0 875.01 889.37 55.75 o -1 7 0 1626.68 1691.77 65.47 o 0 7 0 98.70 92.38 16.83 o 1 7 0 24.47 23.45 12.85 o 2 7 0 123.12 171.73 24.15 o 3 7 0 1311.63 1299.15 68.43 o 4 7 0 403.46 431.58 37.75 o 5 7 0 385.58 514.40 46.77 o 6 7 0 2.97 -0.85 18.87 o 7 7 0 184.86 166.35 33.58 o 8 7 0 9.75 -1.02 22.74 o 9 7 0 29.29 -1.06 23.61 o 10 7 0 10.38 -1.99 44.20 o -13 8 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