data_2019568 _cell_angle_alpha 70.779 _cell_angle_beta 80.031 _cell_angle_gamma 79.353 _cell_length_a 8.1979 _cell_length_b 14.0424 _cell_length_c 14.1697 _exptl_crystal_F_000 837.00 _reflns_d_resolution_high 0.7271 _[local]_cod_data_source_file sk3545Isup2.hkl _[local]_cod_data_source_block I _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 296.17 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 68.89 282.08 32.20 o 3 0 0 2287.08 3654.11 146.34 o 4 0 0 8180.22 8505.15 190.09 o 5 0 0 956.00 1029.62 85.81 o 6 0 0 619.41 557.82 119.93 o 7 0 0 3769.59 4098.55 261.39 o 8 0 0 575.42 617.25 91.54 o 9 0 0 498.98 643.27 127.65 o 10 0 0 57.54 40.23 64.70 o 11 0 0 316.24 637.23 215.58 o -10 1 0 513.40 678.48 147.80 o -9 1 0 24.48 138.63 75.08 o -8 1 0 31.40 83.91 57.44 o -7 1 0 3483.65 3720.38 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14784.44 14506.32 248.30 o 2 4 0 600.59 562.35 31.19 o 3 4 0 4720.19 4622.58 111.23 o 4 4 0 373.98 325.19 23.49 o 5 4 0 935.47 792.37 43.36 o 6 4 0 20.48 32.59 22.40 o 7 4 0 523.20 643.24 163.21 o 8 4 0 2469.61 2565.36 319.35 o 9 4 0 351.44 675.49 212.94 o 10 4 0 113.79 42.31 90.25 o -9 5 0 180.71 111.48 127.61 o -8 5 0 530.75 488.53 120.12 o -7 5 0 2008.26 1881.26 176.97 o -6 5 0 11009.09 11303.55 398.30 o -5 5 0 4525.76 4436.58 235.43 o -4 5 0 6726.52 5310.54 283.76 o -3 5 0 5723.76 5869.80 170.17 o -2 5 0 4278.46 3724.53 333.38 o -1 5 0 3457.52 3133.59 91.60 o 0 5 0 4130.13 3859.65 120.24 o 1 5 0 11784.78 10703.04 152.39 o 2 5 0 253.44 298.01 41.07 o 3 5 0 2580.11 2657.97 76.56 o 4 5 0 184.57 139.92 19.82 o 5 5 0 2609.78 2381.85 172.19 o 6 5 0 606.09 459.23 77.76 o 7 5 0 372.17 285.19 83.37 o 8 5 0 1157.69 1104.97 212.67 o 9 5 0 1151.75 1378.89 262.11 o 10 5 0 2.77 284.62 169.37 o -8 6 0 400.45 502.11 199.67 o -7 6 0 50.58 -6.25 64.64 o -6 6 0 3006.59 3098.18 338.83 o -5 6 0 5038.27 4237.62 506.74 o -4 6 0 1123.68 1071.12 75.35 o -3 6 0 4793.05 4511.15 156.39 o -2 6 0 5442.29 4952.03 139.81 o -1 6 0 8421.71 7463.55 649.41 o 0 6 0 1277.67 1062.01 88.59 o 1 6 0 6811.15 6605.60 172.83 o 2 6 0 3620.17 3361.80 97.16 o 3 6 0 707.44 604.05 38.15 o 4 6 0 767.51 717.88 43.01 o 5 6 0 5436.46 4964.68 118.64 o 6 6 0 9427.14 8407.73 312.38 o 7 6 0 798.36 664.51 73.42 o 8 6 0 208.54 223.63 142.83 o 9 6 0 1171.09 1252.33 258.39 o 10 6 0 472.12 613.26 198.12 o -8 7 0 1819.79 1672.72 308.57 o -7 7 0 155.58 131.79 130.05 o -6 7 0 1956.81 3398.16 1129.88 o -5 7 0 4053.92 3375.10 235.13 o -4 7 0 5516.41 5421.98 224.67 o -3 7 0 422.00 542.43 48.47 o -2 7 0 3986.70 3942.60 181.27 o -1 7 0 9677.82 10320.77 289.55 o 0 7 0 492.82 392.89 40.31 o 1 7 0 5962.85 5169.96 159.56 o 2 7 0 3485.43 3043.04 153.25 o 3 7 0 8952.64 8487.60 181.82 o 4 7 0 2410.50 2086.00 71.59 o 5 7 0 703.78 509.72 62.04 o 6 7 0 1766.82 1526.32 89.35 o 7 7 0 2498.69 2701.62 140.16 o 8 7 0 439.82 318.25 147.52 o 9 7 0 22.27 228.23 123.04 o 10 7 0 725.19 1184.51 273.29 o -8 8 0 1377.95 1288.24 256.68 o -7 8 0 1719.65 1682.89 272.67 o -6 8 0 41.75 90.65 74.25 o -5 8 0 1589.26 1303.02 193.92 o -4 8 0 4457.40 4234.36 366.09 o -3 8 0 4218.39 4401.45 132.80 o -2 8 0 63.07 45.25 30.41 o -1 8 0 4663.56 4609.55 208.39 o 0 8 0 337.57 375.36 48.36 o 1 8 0 62.34 23.62 29.75 o 2 8 0 626.85 574.46 62.57 o 3 8 0 1525.14 1425.97 80.57 o 4 8 0 4291.16 3904.55 119.74 o 5 8 0 1666.66 1666.06 87.11 o 6 8 0 63.52 92.55 35.08 o 7 8 0 1705.90 1793.76 118.27 o 8 8 0 848.15 986.42 234.59 o 9 8 0 214.48 222.42 112.44 o 10 8 0 239.14 587.30 212.89 o -7 9 0 1548.32 1554.00 281.38 o -6 9 0 774.84 754.92 202.92 o -5 9 0 141.78 77.68 79.24 o -4 9 0 1527.77 1473.51 143.47 o -3 9 0 2896.06 2896.48 167.86 o -2 9 0 185.20 116.58 41.28 o -1 9 0 1641.71 1599.93 109.39 o 0 9 0 3154.64 3119.56 119.36 o 1 9 0 1800.78 1921.21 116.99 o 2 9 0 1317.55 1035.02 53.14 o 3 9 0 71.17 61.46 28.87 o 4 9 0 2548.15 2507.74 103.39 o 5 9 0 1485.35 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