#------------------------------------------------------------------------------ #$Date: 2016-04-06 16:28:35 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181865 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/95/2019584.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2019584 _cell_angle_alpha 88.488 _cell_angle_beta 96.881 _cell_angle_gamma 92.679 _cell_length_a 10.1319 _cell_length_b 20.4267 _cell_length_c 15.9591 _exptl_crystal_F_000 1504.00 _reflns_d_resolution_high 0.7813 _cod_data_source_file bg3174IIsup3.hkl _cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' GJ IPDS2 -160DEGC P-1 Z 4' _shelx_refln_list_code 4 _shelx_f_calc_maximum 282.67 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 76.69 118.95 173.07 o 2 0 0 19780.41 23023.00 1092.20 o 3 0 0 981.55 954.31 169.63 o 4 0 0 7501.77 7331.43 440.32 o 5 0 0 639.60 982.38 170.23 o 6 0 0 20961.14 23271.61 641.32 o 7 0 0 1293.56 1270.36 172.70 o 8 0 0 174.36 410.38 190.82 o 9 0 0 1951.79 2037.00 539.36 o 10 0 0 6.17 213.72 209.23 o 11 0 0 8.15 239.10 237.83 o 12 0 0 6.69 84.97 246.06 o -12 0 -1 1.08 168.51 267.40 o -11 0 -1 1822.55 1785.55 249.66 o -10 0 -1 25.50 -5.54 193.51 o -9 0 -1 44.87 479.17 191.04 o -8 0 -1 18.30 90.50 162.44 o -7 0 -1 3096.33 2877.89 393.98 o -6 0 -1 51.42 86.31 214.47 o -5 0 -1 15773.53 16908.11 329.53 o -4 0 -1 160.36 94.55 162.22 o -3 0 -1 4.95 37.58 150.17 o -2 0 -1 110.33 185.43 178.46 o -1 0 -1 4444.65 5133.11 221.51 o 0 0 -1 221.74 249.88 190.44 o 1 0 -1 56477.27 59308.61 2306.19 o 2 0 -1 220.72 213.80 188.42 o 3 0 -1 12265.70 10748.01 459.19 o 4 0 -1 542.73 645.59 203.99 o 5 0 -1 9764.88 11107.41 270.69 o 6 0 -1 1407.59 1569.20 212.08 o 7 0 -1 4974.11 5728.39 227.12 o 8 0 -1 1234.18 1415.29 192.61 o 9 0 -1 2878.50 2992.95 218.96 o 10 0 -1 17.39 -138.12 310.74 o 11 0 -1 601.52 358.05 241.80 o 12 0 -1 425.25 197.70 306.55 o -12 0 -2 1001.24 855.04 383.88 o -11 0 -2 64.29 356.85 236.11 o -10 0 -2 181.13 336.64 213.20 o -9 0 -2 340.43 429.02 180.41 o -8 0 -2 2844.63 3076.20 207.36 o -7 0 -2 2039.99 2288.45 180.11 o -6 0 -2 676.86 739.16 160.05 o -5 0 -2 24.15 59.89 141.48 o -4 0 -2 1090.04 1015.54 153.01 o -3 0 -2 0.44 56.07 153.76 o -2 0 -2 2011.94 2515.65 163.49 o -1 0 -2 94.09 107.50 148.22 o 0 0 -2 41753.87 48210.11 863.35 o 1 0 -2 5.14 -22.31 144.10 o 2 0 -2 1133.11 1284.06 163.42 o 3 0 -2 155.83 119.03 172.70 o 4 0 -2 4669.58 4695.93 189.84 o 5 0 -2 979.65 1258.01 158.93 o 6 0 -2 537.47 598.35 174.87 o 7 0 -2 507.83 471.02 178.24 o 8 0 -2 1263.35 1194.61 226.08 o 9 0 -2 1416.18 1366.63 212.83 o 10 0 -2 3944.08 4123.03 287.53 o 11 0 -2 256.17 637.20 345.18 o 12 0 -2 146.59 236.63 259.39 o -11 0 -3 453.08 716.55 273.76 o -10 0 -3 634.63 843.59 245.01 o -9 0 -3 1070.84 1173.27 203.62 o -8 0 -3 244.24 360.07 187.37 o -7 0 -3 4775.06 4700.79 327.06 o -6 0 -3 44.56 150.99 145.23 o -5 0 -3 546.01 588.77 157.58 o -4 0 -3 68.56 -5.84 189.99 o -3 0 -3 10119.54 10643.50 407.98 o -2 0 -3 407.37 430.22 161.47 o -1 0 -3 27740.46 31147.41 966.58 o 0 0 -3 245.81 271.96 170.31 o 1 0 -3 3964.35 4163.53 260.96 o 2 0 -3 733.40 879.07 170.31 o 3 0 -3 19481.87 19722.22 518.63 o 4 0 -3 22.16 29.64 134.90 o 5 0 -3 2426.30 2472.23 198.53 o 6 0 -3 447.53 466.37 195.16 o 7 0 -3 219.09 279.97 185.13 o 8 0 -3 194.96 156.23 202.79 o 9 0 -3 5.30 280.72 253.32 o 10 0 -3 2678.21 2321.01 312.16 o 11 0 -3 1855.05 1694.37 343.75 o 12 0 -3 87.64 223.53 385.53 o -11 0 -4 1757.41 1481.92 249.73 o -10 0 -4 9.44 179.06 259.24 o -9 0 -4 875.01 990.09 234.91 o -8 0 -4 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0 -8 28412.72 31717.46 1132.62 o -3 0 -8 8.19 24.55 155.71 o -2 0 -8 6179.06 6612.55 177.12 o -1 0 -8 417.13 414.57 131.23 o 0 0 -8 3557.93 3587.78 159.75 o 1 0 -8 89.23 98.29 153.39 o 2 0 -8 21359.27 21634.36 1350.61 o 3 0 -8 5334.18 5988.30 273.61 o 4 0 -8 7068.32 7992.81 201.37 o 5 0 -8 0.27 95.89 178.84 o 6 0 -8 272.18 148.45 158.18 o 7 0 -8 218.04 218.22 204.29 o 8 0 -8 197.52 112.89 244.72 o 9 0 -8 92.23 115.88 321.37 o 10 0 -8 4.92 -173.22 285.36 o 11 0 -8 804.65 855.42 311.41 o -10 0 -9 8.70 107.42 318.83 o -9 0 -9 9.48 319.57 263.13 o -8 0 -9 201.93 51.28 220.69 o -7 0 -9 1963.17 2010.80 204.89 o -6 0 -9 113.10 127.04 204.89 o -5 0 -9 574.59 683.32 180.34 o -4 0 -9 80.59 155.33 183.26 o -3 0 -9 7793.54 8119.10 362.99 o -2 0 -9 142.63 264.25 131.23 o -1 0 -9 1116.52 1390.14 150.39 o 0 0 -9 33.87 29.27 132.58 o 1 0 -9 4688.10 5265.16 200.40 o 2 0 -9 2819.47 3082.78 148.60 o 3 0 -9 6016.23 6522.87 586.07 o 4 0 -9 2779.10 2983.74 249.21 o 5 0 -9 30.77 81.60 176.37 o 6 0 -9 689.37 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11.62 74.93 146.05 o -3 0 -11 1638.68 1554.75 186.70 o -2 0 -11 2.00 12.05 177.94 o -1 0 -11 22.62 45.44 138.41 o 0 0 -11 50.16 207.29 173.97 o 1 0 -11 4721.09 5179.97 417.57 o 2 0 -11 1.29 26.05 159.90 o 3 0 -11 20.32 -23.58 148.97 o 4 0 -11 194.30 434.86 147.92 o 5 0 -11 1063.08 1044.89 190.97 o 6 0 -11 599.37 685.71 210.21 o 7 0 -11 2891.05 2776.08 208.56 o 8 0 -11 1703.57 1852.17 219.94 o 9 0 -11 4.84 -107.05 212.97 o 10 0 -11 17.47 -344.65 375.79 o -8 0 -12 592.22 618.86 258.26 o -7 0 -12 260.28 542.43 224.43 o -6 0 -12 413.45 377.22 210.13 o -5 0 -12 45.76 218.74 160.50 o -4 0 -12 1187.86 1295.82 196.66 o -3 0 -12 5.17 2.02 166.11 o -2 0 -12 829.01 812.07 163.49 o -1 0 -12 154.74 138.86 182.88 o 0 0 -12 6791.17 6608.21 306.70 o 1 0 -12 677.90 863.20 160.42 o 2 0 -12 11.35 -9.21 157.28 o 3 0 -12 21.67 119.85 168.36 o 4 0 -12 995.06 1112.78 169.86 o 5 0 -12 136.38 19.16 171.20 o 6 0 -12 107.98 287.31 171.73 o 7 0 -12 13.47 119.10 204.07 o 8 0 -12 1105.91 1149.91 247.56 o 9 0 -12 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