data_2019624 _cell_angle_alpha 90.000 _cell_angle_beta 93.962 _cell_angle_gamma 90.000 _cell_length_a 12.5508 _cell_length_b 10.1916 _cell_length_c 24.7009 _exptl_crystal_F_000 1184.00 _reflns_d_resolution_high 0.8219 _[local]_cod_data_source_file uk3100Iasup2.hkl _[local]_cod_data_source_block Ia _shelx_title ' wa604 in P21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 215.23 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 6.19 6.22 36.30 o 6 0 0 313.82 307.08 23.92 o 8 0 0 6349.80 6590.08 121.94 o 10 0 0 1403.78 1247.58 26.08 o 12 0 0 222.94 225.93 24.63 o 14 0 0 102.83 135.50 19.06 o 2 1 0 13072.43 11746.04 316.59 o 3 1 0 7128.76 6750.57 105.70 o 4 1 0 80.88 92.48 20.71 o 5 1 0 2840.32 2870.59 60.71 o 6 1 0 1246.73 1231.77 22.18 o 7 1 0 5464.85 5723.03 127.21 o 8 1 0 40.78 50.12 17.63 o 9 1 0 1366.25 1342.16 36.03 o 10 1 0 3270.13 3370.85 40.71 o 11 1 0 9.24 9.33 15.83 o 12 1 0 237.06 221.87 16.90 o 13 1 0 118.01 138.40 15.00 o 14 1 0 2.80 23.19 14.26 o 15 1 0 0.12 4.29 12.17 o 0 2 0 17702.11 18315.76 305.64 o 1 2 0 10695.49 9397.80 324.61 o 2 2 0 358.38 209.61 28.08 o 3 2 0 5588.40 5072.03 112.38 o 4 2 0 623.65 535.08 23.50 o 5 2 0 3032.06 2601.34 39.60 o 6 2 0 378.95 488.80 20.23 o 7 2 0 2817.14 2912.18 68.08 o 8 2 0 14.75 12.36 16.15 o 9 2 0 1666.10 1690.88 21.36 o 10 2 0 110.37 175.48 16.03 o 11 2 0 36.27 44.08 12.98 o 12 2 0 68.54 118.53 16.28 o 13 2 0 369.66 342.47 14.32 o 14 2 0 377.59 335.53 12.50 o 15 2 0 9.87 14.07 26.22 o 1 3 0 6949.19 6167.96 205.08 o 2 3 0 187.66 175.10 24.28 o 3 3 0 0.47 -7.81 21.57 o 4 3 0 574.66 444.60 20.74 o 5 3 0 888.31 770.39 20.01 o 6 3 0 116.42 42.80 18.82 o 7 3 0 1569.26 1505.29 27.16 o 8 3 0 125.34 116.05 15.74 o 9 3 0 21.50 25.70 16.88 o 10 3 0 0.82 24.42 14.45 o 11 3 0 97.66 88.14 15.15 o 12 3 0 767.74 776.18 17.43 o 13 3 0 129.20 178.51 14.44 o 14 3 0 23.06 25.77 14.95 o 0 4 0 11613.22 10948.41 175.45 o 1 4 0 141.07 223.13 25.14 o 2 4 0 345.72 310.45 22.50 o 3 4 0 437.54 447.86 25.49 o 4 4 0 232.74 223.88 24.01 o 5 4 0 1375.87 1480.57 38.02 o 6 4 0 428.50 403.41 16.67 o 7 4 0 342.64 279.73 18.23 o 8 4 0 783.01 713.21 18.04 o 9 4 0 0.58 35.22 16.43 o 10 4 0 292.46 340.69 17.04 o 11 4 0 25.77 39.23 14.11 o 12 4 0 10.66 12.05 15.30 o 13 4 0 7.84 6.75 22.02 o 14 4 0 77.62 91.36 13.80 o 1 5 0 3917.40 4034.57 77.36 o 2 5 0 2379.23 2068.82 29.58 o 3 5 0 1084.46 1004.30 25.56 o 4 5 0 1101.92 1007.49 29.22 o 5 5 0 430.54 615.84 18.20 o 6 5 0 1010.73 892.44 19.36 o 7 5 0 109.64 140.04 16.58 o 8 5 0 202.81 234.29 18.01 o 9 5 0 150.58 183.47 16.38 o 10 5 0 1006.88 1079.67 21.32 o 11 5 0 309.71 323.25 15.53 o 12 5 0 158.04 180.53 13.00 o 13 5 0 33.93 34.89 15.72 o 0 6 0 420.55 290.61 31.74 o 1 6 0 1242.79 1220.79 26.37 o 2 6 0 435.76 465.52 22.48 o 3 6 0 1055.40 941.24 27.46 o 4 6 0 210.26 215.05 19.99 o 5 6 0 2295.47 2173.53 30.85 o 6 6 0 382.48 379.02 22.56 o 7 6 0 329.02 269.86 24.68 o 8 6 0 19.28 16.92 16.38 o 9 6 0 156.36 158.34 16.70 o 10 6 0 24.47 56.44 16.85 o 11 6 0 37.75 50.33 17.68 o 12 6 0 598.70 626.22 29.50 o 13 6 0 250.76 233.27 14.64 o 1 7 0 908.56 776.83 24.94 o 2 7 0 109.67 127.42 17.76 o 3 7 0 178.46 178.62 19.57 o 4 7 0 2221.89 2112.93 24.43 o 5 7 0 1287.52 1375.81 31.45 o 6 7 0 2226.79 2049.44 74.44 o 7 7 0 1563.57 1592.04 43.80 o 8 7 0 585.63 545.76 18.31 o 9 7 0 113.02 139.24 19.00 o 10 7 0 27.17 29.26 19.37 o 11 7 0 3.85 11.86 18.20 o 12 7 0 15.64 16.68 17.04 o 0 8 0 1583.49 1638.38 35.99 o 1 8 0 236.60 273.62 20.37 o 2 8 0 429.44 397.12 19.73 o 3 8 0 47.45 64.95 18.62 o 4 8 0 3.73 28.29 19.56 o 5 8 0 8.09 18.36 19.18 o 6 8 0 250.17 268.39 23.66 o 7 8 0 413.55 418.58 17.68 o 8 8 0 68.73 66.70 18.76 o 9 8 0 1332.88 1441.41 41.41 o 10 8 0 252.45 241.50 18.10 o 11 8 0 9.57 55.41 16.49 o 1 9 0 214.94 228.27 21.82 o 2 9 0 33.85 50.66 19.39 o 3 9 0 868.64 834.77 25.83 o 4 9 0 672.03 722.50 17.02 o 5 9 0 46.66 52.56 17.49 o 6 9 0 457.05 412.97 18.57 o 7 9 0 1.46 11.50 17.68 o 8 9 0 470.11 481.87 16.92 o 9 9 0 10.38 8.59 16.25 o 10 9 0 445.71 405.93 16.72 o 0 10 0 284.76 307.57 23.93 o 1 10 0 674.21 616.99 22.75 o 2 10 0 32.60 11.24 16.96 o 3 10 0 390.63 369.29 17.24 o 4 10 0 55.51 80.65 20.34 o 5 10 0 15.04 12.27 14.57 o 6 10 0 1.28 42.09 17.72 o 7 10 0 224.91 247.10 17.35 o 8 10 0 44.12 44.09 13.92 o 9 10 0 29.01 -5.25 45.19 o 1 11 0 26.67 10.12 17.07 o 2 11 0 225.41 246.48 24.17 o 3 11 0 0.30 23.57 19.81 o 4 11 0 66.37 87.70 16.60 o 5 11 0 59.59 70.61 14.71 o 6 11 0 0.15 11.30 14.79 o 0 12 0 160.22 90.23 22.76 o 1 12 0 73.18 95.21 17.34 o 2 12 0 35.80 36.54 16.01 o 3 12 0 50.81 60.48 15.04 o -15 0 1 0.28 -8.48 20.27 o -13 0 1 115.58 126.29 18.48 o -11 0 1 317.19 257.37 21.33 o -9 0 1 1559.83 1444.28 82.47 o -7 0 1 4072.43 4207.85 39.79 o -5 0 1 1627.78 1809.18 54.93 o -3 0 1 6043.74 5455.35 82.46 o 3 0 1 8190.35 7547.19 310.60 o 5 0 1 231.47 138.34 30.31 o 7 0 1 8357.10 8265.67 248.12 o 9 0 1 7697.29 7282.21 112.56 o 11 0 1 15.95 50.28 22.83 o 13 0 1 212.89 170.85 23.92 o 15 0 1 100.47 147.01 18.20 o -15 1 1 3.19 29.49 12.97 o -14 1 1 3.72 2.90 14.37 o -13 1 1 57.69 98.58 21.03 o -12 1 1 579.00 621.07 13.99 o -11 1 1 26.87 39.84 14.66 o -10 1 1 746.55 737.51 24.47 o -9 1 1 419.69 413.92 17.28 o -8 1 1 73.53 71.19 17.76 o -7 1 1 117.60 138.18 16.74 o -6 1 1 318.38 359.62 19.54 o -5 1 1 72.56 69.09 20.30 o -4 1 1 260.89 221.75 21.98 o -3 1 1 1.63 48.58 25.23 o -2 1 1 4619.93 4492.39 85.86 o 2 1 1 5.32 13.48 20.08 o 3 1 1 3.52 10.46 22.44 o 4 1 1 127.47 75.37 21.31 o 5 1 1 756.17 696.85 22.45 o 6 1 1 3564.67 3504.00 44.27 o 7 1 1 63.15 68.16 19.52 o 8 1 1 1036.22 1042.57 17.95 o 9 1 1 3178.49 3030.33 47.21 o 10 1 1 4.34 -0.40 18.67 o 11 1 1 168.89 139.33 13.78 o 12 1 1 4.05 25.36 12.33 o 13 1 1 1009.07 1077.32 18.22 o 14 1 1 66.92 56.60 14.06 o 15 1 1 14.63 30.22 14.19 o -15 2 1 53.72 67.44 21.09 o -14 2 1 173.10 203.85 18.54 o -13 2 1 27.27 11.38 16.31 o -12 2 1 98.55 102.39 15.40 o -11 2 1 305.50 298.53 13.20 o -10 2 1 0.03 28.34 16.30 o -9 2 1 154.13 220.45 16.60 o -8 2 1 55.10 31.69 15.60 o -7 2 1 109.77 123.31 17.44 o -6 2 1 96.22 94.72 20.16 o -5 2 1 985.64 945.05 23.86 o -4 2 1 3758.89 3632.78 78.23 o -3 2 1 353.65 405.40 22.17 o -2 2 1 539.80 556.77 28.60 o -1 2 1 29.21 41.12 30.07 o 0 2 1 22042.37 20304.46 399.65 o 1 2 1 10499.00 9721.37 160.38 o 2 2 1 48.24 91.66 27.47 o 3 2 1 251.85 117.64 24.18 o 4 2 1 1459.45 1469.62 27.13 o 5 2 1 148.11 132.07 18.36 o 6 2 1 2402.10 2811.63 31.27 o 7 2 1 1344.69 1457.06 27.67 o 8 2 1 539.79 517.76 16.91 o 9 2 1 566.78 573.05 19.92 o 10 2 1 1403.98 1334.61 29.93 o 11 2 1 10.22 20.16 16.20 o 12 2 1 937.45 944.22 15.89 o 13 2 1 10.02 3.12 13.16 o 14 2 1 99.25 121.65 13.96 o -14 3 1 139.27 148.90 15.55 o -13 3 1 6.78 -11.70 13.42 o -12 3 1 37.90 69.25 16.13 o -11 3 1 58.41 63.93 14.12 o -10 3 1 182.18 218.12 15.17 o -9 3 1 136.45 132.88 16.66 o -8 3 1 21.14 24.90 16.24 o -7 3 1 859.63 913.45 24.83 o -6 3 1 0.20 -2.05 17.75 o -5 3 1 0.06 18.73 19.39 o -4 3 1 1069.69 1287.90 34.72 o -3 3 1 66.62 42.78 21.03 o -2 3 1 696.63 479.95 26.90 o -1 3 1 729.92 673.99 30.35 o 0 3 1 52.81 58.26 29.19 o 1 3 1 1182.88 1064.04 33.50 o 2 3 1 0.36 11.92 25.59 o 3 3 1 1.57 8.57 21.15 o 4 3 1 9.79 27.32 20.30 o 5 3 1 4.82 23.49 21.30 o 6 3 1 2818.96 3155.61 29.92 o 7 3 1 212.45 206.09 17.75 o 8 3 1 615.77 670.35 26.73 o 9 3 1 1272.86 1271.57 20.12 o 10 3 1 46.93 60.57 15.47 o 11 3 1 325.83 324.04 27.02 o 12 3 1 175.67 195.67 12.96 o 13 3 1 366.00 397.27 14.96 o 14 3 1 134.50 143.40 16.08 o -14 4 1 1.80 12.75 17.92 o -13 4 1 32.13 60.67 15.12 o -12 4 1 71.81 104.58 15.47 o -11 4 1 185.11 205.23 16.82 o -10 4 1 134.25 162.41 14.44 o -9 4 1 517.94 460.28 17.59 o -8 4 1 448.72 469.06 19.39 o -7 4 1 137.43 126.87 15.39 o -6 4 1 72.53 75.74 17.20 o -5 4 1 1.49 15.51 15.52 o -4 4 1 718.51 838.42 26.05 o -3 4 1 1441.52 1391.11 28.31 o -2 4 1 415.42 515.34 25.51 o -1 4 1 19.10 5.16 23.87 o 0 4 1 10.66 -7.80 22.90 o 1 4 1 961.63 992.17 27.52 o 2 4 1 1373.67 1237.73 32.49 o 3 4 1 223.87 267.63 24.27 o 4 4 1 246.24 190.50 21.75 o 5 4 1 1715.54 1650.76 22.84 o 6 4 1 423.55 434.10 17.47 o 7 4 1 3814.25 3874.39 48.03 o 8 4 1 2.08 -3.04 16.77 o 9 4 1 0.91 13.33 14.96 o 10 4 1 269.62 288.97 16.53 o 11 4 1 132.35 158.54 15.69 o 12 4 1 283.40 290.80 15.78 o 13 4 1 473.75 447.57 14.54 o 14 4 1 239.22 231.69 14.57 o -13 5 1 24.84 6.52 14.68 o -12 5 1 167.72 192.44 18.03 o -11 5 1 0.55 10.21 13.40 o -10 5 1 260.34 305.81 14.90 o -9 5 1 1915.31 1818.73 35.01 o -8 5 1 30.08 33.17 14.85 o -7 5 1 22.11 46.99 17.56 o -6 5 1 0.58 -12.35 17.65 o -5 5 1 810.64 802.69 28.07 o -4 5 1 1455.76 1521.79 26.36 o -3 5 1 1019.33 1032.15 25.68 o -2 5 1 33.62 47.97 21.02 o -1 5 1 187.04 389.13 23.09 o 0 5 1 2815.58 2680.78 46.69 o 1 5 1 10.54 39.51 21.61 o 2 5 1 8.51 30.99 22.95 o 3 5 1 4153.80 4421.06 103.06 o 4 5 1 202.50 114.73 17.65 o 5 5 1 39.21 44.09 18.41 o 6 5 1 1089.23 1026.56 24.94 o 7 5 1 17.05 -8.36 18.45 o 8 5 1 603.35 583.01 18.81 o 9 5 1 19.07 33.05 16.17 o 10 5 1 8.00 17.09 13.74 o 11 5 1 1071.83 943.45 23.29 o 12 5 1 19.25 19.32 13.73 o 13 5 1 82.94 94.13 13.99 o -13 6 1 220.18 206.23 14.77 o -12 6 1 27.09 27.28 14.46 o -11 6 1 519.01 522.35 16.86 o -10 6 1 99.74 53.03 16.08 o -9 6 1 64.29 78.18 15.67 o -8 6 1 47.21 66.81 16.30 o -7 6 1 962.49 1000.73 31.50 o -6 6 1 574.33 621.96 20.41 o -5 6 1 133.34 153.69 18.59 o -4 6 1 51.06 50.39 17.63 o -3 6 1 636.00 717.04 21.80 o -2 6 1 1722.92 1929.22 26.93 o -1 6 1 1890.71 2104.03 33.51 o 0 6 1 723.81 700.84 21.93 o 1 6 1 1789.61 2173.04 43.74 o 2 6 1 0.71 13.86 18.82 o 3 6 1 419.31 355.30 20.29 o 4 6 1 2034.98 2159.72 23.17 o 5 6 1 8.71 -0.28 18.73 o 6 6 1 212.16 252.06 18.98 o 7 6 1 98.08 109.68 19.24 o 8 6 1 0.09 22.46 16.30 o 9 6 1 113.70 128.12 16.85 o 10 6 1 1787.68 1635.69 43.85 o 11 6 1 89.81 110.76 15.66 o 12 6 1 53.59 49.11 18.20 o 13 6 1 4.35 21.96 15.15 o -12 7 1 56.39 87.63 20.39 o -11 7 1 306.43 281.14 18.04 o -10 7 1 14.42 9.83 17.24 o -9 7 1 215.74 271.35 17.67 o -8 7 1 424.37 460.25 22.57 o -7 7 1 443.30 459.82 17.53 o -6 7 1 1304.13 1192.52 23.92 o -5 7 1 631.14 696.72 27.30 o -4 7 1 372.31 345.13 23.20 o -3 7 1 0.04 9.94 19.50 o -2 7 1 291.70 297.12 20.21 o -1 7 1 13.74 15.47 19.92 o 0 7 1 1074.07 1123.31 23.48 o 1 7 1 1824.61 1803.35 29.61 o 2 7 1 418.40 453.53 19.35 o 3 7 1 1077.93 1009.31 22.15 o 4 7 1 232.60 267.29 20.45 o 5 7 1 5.13 18.91 17.00 o 6 7 1 1082.96 1014.81 30.52 o 7 7 1 164.65 167.22 16.59 o 8 7 1 1158.15 1117.73 18.12 o 9 7 1 135.49 182.08 14.50 o 10 7 1 261.80 262.69 17.19 o 11 7 1 23.11 42.06 15.93 o 12 7 1 269.08 249.80 16.95 o -11 8 1 84.96 87.07 14.91 o -10 8 1 742.00 757.86 18.99 o -9 8 1 507.75 521.65 19.74 o -8 8 1 263.80 255.36 22.00 o -7 8 1 1.24 2.40 19.36 o -6 8 1 387.49 394.77 16.79 o -5 8 1 247.22 247.13 18.37 o -4 8 1 0.52 24.77 17.70 o -3 8 1 6.78 -0.71 17.06 o -2 8 1 1272.87 1356.07 48.87 o -1 8 1 828.33 866.06 23.25 o 0 8 1 1.22 -1.29 19.73 o 1 8 1 493.14 488.61 25.29 o 2 8 1 26.38 10.52 18.36 o 3 8 1 2.52 3.02 17.90 o 4 8 1 160.22 167.77 18.09 o 5 8 1 100.08 85.73 15.92 o 6 8 1 123.28 137.20 16.05 o 7 8 1 529.83 443.08 17.90 o 8 8 1 63.58 69.60 17.07 o 9 8 1 158.81 137.53 15.79 o 10 8 1 5.85 13.98 16.99 o 11 8 1 50.10 35.91 17.29 o -10 9 1 16.54 38.03 15.47 o -9 9 1 703.95 658.38 19.69 o -8 9 1 304.97 284.87 16.65 o -7 9 1 0.19 9.03 17.72 o -6 9 1 118.30 145.46 15.78 o -5 9 1 450.69 442.87 18.87 o -4 9 1 587.36 591.66 16.55 o -3 9 1 49.72 70.40 18.15 o -2 9 1 347.10 360.96 19.42 o -1 9 1 18.98 31.90 17.00 o 0 9 1 7.37 0.12 21.35 o 1 9 1 561.59 621.11 21.24 o 2 9 1 284.02 343.43 20.34 o 3 9 1 24.93 30.35 17.09 o 4 9 1 96.24 127.83 14.52 o 5 9 1 147.00 168.62 16.90 o 6 9 1 564.04 565.78 16.59 o 7 9 1 299.34 292.18 18.18 o 8 9 1 3.37 8.91 16.02 o 9 9 1 220.77 218.66 15.58 o 10 9 1 164.87 114.14 16.49 o -8 10 1 97.73 79.17 14.52 o -7 10 1 339.65 317.47 19.28 o -6 10 1 53.22 42.35 15.92 o -5 10 1 117.74 128.10 16.33 o -4 10 1 312.57 352.35 17.19 o -3 10 1 125.56 132.41 18.73 o -2 10 1 76.68 74.07 20.27 o -1 10 1 51.79 76.54 17.35 o 0 10 1 233.55 216.40 18.35 o 1 10 1 185.75 207.16 17.84 o 2 10 1 70.85 57.22 17.56 o 3 10 1 177.22 191.01 16.02 o 4 10 1 124.72 159.37 16.98 o 5 10 1 197.10 235.66 15.90 o 6 10 1 7.09 18.58 16.65 o 7 10 1 80.88 91.78 14.69 o 8 10 1 65.03 67.62 16.24 o -7 11 1 18.31 41.74 27.74 o -6 11 1 337.95 334.31 17.40 o -5 11 1 6.04 5.13 14.71 o -4 11 1 472.11 424.76 16.49 o -3 11 1 94.49 67.15 17.90 o -2 11 1 0.01 20.80 21.40 o -1 11 1 225.09 209.89 17.08 o 0 11 1 26.42 27.27 15.72 o 1 11 1 0.13 14.17 16.61 o 2 11 1 165.40 175.48 17.24 o 3 11 1 150.53 141.75 15.29 o 4 11 1 1.49 7.32 13.78 o 5 11 1 123.72 124.51 14.62 o 6 11 1 47.87 58.76 13.32 o -3 12 1 0.42 0.30 16.41 o -2 12 1 486.89 469.05 17.72 o -1 12 1 30.74 67.14 16.71 o 0 12 1 103.70 77.63 19.06 o 1 12 1 0.07 30.85 17.90 o 2 12 1 24.09 37.07 15.77 o 3 12 1 164.29 168.51 17.31 o -14 0 2 458.14 500.80 36.61 o -12 0 2 3577.35 3561.44 76.61 o -10 0 2 24.18 3.84 27.58 o -8 0 2 14.66 35.64 24.80 o -6 0 2 84.97 114.72 24.31 o -4 0 2 1410.09 1079.52 34.09 o -2 0 2 90.48 34.98 28.77 o 2 0 2 11842.61 12083.12 356.93 o 4 0 2 40.47 28.62 29.73 o 6 0 2 3341.01 3679.50 52.92 o 8 0 2 5395.80 5456.87 135.29 o 10 0 2 175.78 196.85 27.91 o 12 0 2 176.87 149.59 20.39 o 14 0 2 1631.45 1499.34 35.55 o -15 1 2 116.13 112.21 13.79 o -14 1 2 27.53 36.47 14.72 o -13 1 2 140.03 143.98 15.35 o -12 1 2 192.51 236.89 13.30 o -11 1 2 9.08 22.49 15.88 o -10 1 2 1229.11 1213.66 34.15 o -9 1 2 17.48 32.17 17.32 o -8 1 2 231.70 313.86 18.58 o -7 1 2 5.51 14.57 17.37 o -6 1 2 333.99 289.40 20.90 o -5 1 2 1307.40 1360.22 21.51 o -4 1 2 35.62 20.04 21.66 o -3 1 2 963.58 995.13 26.55 o -2 1 2 10550.30 10655.69 367.73 o 2 1 2 16.94 13.18 23.18 o 3 1 2 8.81 28.99 23.10 o 4 1 2 941.33 903.78 22.98 o 5 1 2 3646.91 3628.64 57.81 o 6 1 2 574.53 525.66 19.23 o 7 1 2 171.16 155.88 16.81 o 8 1 2 5.11 3.07 15.12 o 9 1 2 391.17 376.13 16.21 o 10 1 2 2997.94 3058.69 51.54 o 11 1 2 322.95 293.80 13.57 o 12 1 2 414.57 450.69 15.78 o 13 1 2 385.91 396.75 19.15 o 14 1 2 75.88 74.66 13.76 o 15 1 2 373.56 333.32 13.77 o -15 2 2 534.45 502.93 52.16 o -14 2 2 17.98 4.74 14.95 o -13 2 2 6.82 0.62 13.97 o -12 2 2 29.73 46.57 13.62 o -11 2 2 10.30 -10.34 13.10 o -10 2 2 770.43 762.30 18.03 o -9 2 2 168.20 144.23 16.16 o -8 2 2 404.63 423.14 17.36 o -7 2 2 136.38 107.36 18.13 o -6 2 2 57.45 82.75 19.25 o -5 2 2 895.36 1031.93 28.76 o -4 2 2 876.00 852.75 30.51 o -3 2 2 10.17 25.37 25.66 o -2 2 2 476.21 379.28 27.97 o -1 2 2 188.92 247.23 32.98 o 0 2 2 23859.67 23187.68 428.65 o 1 2 2 34.30 33.26 32.07 o 2 2 2 376.32 383.05 28.52 o 3 2 2 2036.24 1850.90 32.23 o 4 2 2 77.56 143.30 18.41 o 5 2 2 606.60 584.16 18.80 o 6 2 2 72.66 109.64 18.05 o 7 2 2 2490.90 2449.58 57.41 o 8 2 2 5.80 6.38 16.34 o 9 2 2 1728.56 1542.17 47.08 o 10 2 2 246.63 247.41 21.59 o 11 2 2 99.17 121.77 16.40 o 12 2 2 3.48 15.82 13.99 o 13 2 2 809.79 841.20 22.55 o 14 2 2 172.65 174.69 14.20 o -14 3 2 64.24 83.50 14.38 o -13 3 2 26.49 35.67 12.63 o -12 3 2 106.22 116.43 15.32 o -11 3 2 681.90 785.99 15.97 o -10 3 2 90.39 82.98 15.55 o -9 3 2 1742.85 1733.24 27.46 o -8 3 2 1.35 4.51 15.94 o -7 3 2 1076.80 1088.42 20.74 o -6 3 2 43.35 94.49 18.77 o -5 3 2 361.79 469.27 22.42 o -4 3 2 343.14 329.32 23.40 o -3 3 2 1942.39 2362.07 72.42 o -2 3 2 4373.64 4408.87 67.54 o -1 3 2 2449.05 2124.21 53.24 o 0 3 2 253.46 240.01 33.62 o 1 3 2 2778.24 2346.52 47.67 o 2 3 2 282.11 273.00 28.71 o 3 3 2 296.12 303.47 27.35 o 4 3 2 772.74 819.47 28.41 o 5 3 2 843.28 1067.58 24.61 o 6 3 2 2411.69 2713.08 41.50 o 7 3 2 779.96 741.16 20.83 o 8 3 2 520.41 540.91 17.15 o 9 3 2 202.60 232.30 17.11 o 10 3 2 1279.45 1243.79 25.23 o 11 3 2 0.19 37.51 15.83 o 12 3 2 56.42 88.86 15.32 o 13 3 2 383.55 410.26 14.80 o 14 3 2 30.08 30.75 19.97 o -14 4 2 60.04 72.08 13.70 o -13 4 2 0.91 44.36 14.79 o -12 4 2 1.45 15.17 14.99 o -11 4 2 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