data_2019631 _cell_angle_alpha 90.000 _cell_angle_beta 107.526 _cell_angle_gamma 90.000 _cell_length_a 14.5012 _cell_length_b 18.2988 _cell_length_c 15.1952 _exptl_crystal_F_000 1728.00 _reflns_d_resolution_high 0.7654 _[local]_cod_data_source_file sf3233IIIsup4.hkl _[local]_cod_data_source_block III _shelx_title ' matrix_0m in P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 408.59 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 13.61 6.10 7.37 o 2 0 0 589.42 359.33 43.32 o 3 0 0 15.65 -18.17 18.17 o 4 0 0 9935.25 10350.01 170.52 o 5 0 0 3195.05 3060.35 80.32 o 6 0 0 37665.69 36169.86 525.62 o 7 0 0 10388.44 10841.64 199.35 o 8 0 0 565.34 592.16 57.68 o 9 0 0 7449.79 7733.57 272.22 o 10 0 0 23025.90 22742.59 463.24 o 11 0 0 99.54 273.71 74.01 o 12 0 0 6006.46 6010.36 220.91 o 13 0 0 6049.18 6140.38 231.71 o 14 0 0 197.79 16.14 113.36 o 15 0 0 2277.76 2047.14 368.38 o 16 0 0 4584.29 4627.24 316.61 o 17 0 0 1243.50 1248.64 212.32 o 18 0 0 62.13 -228.32 228.32 o 2 1 0 5711.19 5567.57 97.47 o 3 1 0 1104.44 1115.32 28.78 o 4 1 0 5078.66 4846.49 69.03 o 5 1 0 2777.78 3110.19 57.01 o 6 1 0 12876.36 13567.47 161.74 o 7 1 0 25664.34 26295.08 286.74 o 8 1 0 2882.90 2883.81 82.95 o 9 1 0 286.62 321.57 32.74 o 10 1 0 174.15 220.10 46.33 o 11 1 0 4054.99 4038.54 160.17 o 12 1 0 3938.84 3898.83 144.26 o 13 1 0 2837.31 2906.96 124.52 o 14 1 0 1002.12 1033.98 99.78 o 15 1 0 806.42 862.89 117.65 o 16 1 0 503.31 375.59 131.54 o 17 1 0 2890.26 2908.36 206.20 o 18 1 0 547.39 545.39 204.80 o 1 2 0 6085.64 5157.23 164.77 o 2 2 0 223.82 371.15 17.71 o 3 2 0 63.03 9.78 13.84 o 4 2 0 7541.08 7126.78 93.63 o 5 2 0 30691.07 30486.45 314.37 o 6 2 0 2018.50 2573.76 56.44 o 7 2 0 2969.63 2843.30 77.49 o 8 2 0 3539.67 3366.00 72.01 o 9 2 0 232.03 157.57 29.94 o 10 2 0 466.32 520.09 65.66 o 11 2 0 11857.70 11344.79 230.10 o 12 2 0 2974.12 2806.73 112.25 o 13 2 0 1489.13 1557.70 111.42 o 14 2 0 8387.47 8338.66 221.93 o 15 2 0 763.52 732.52 102.29 o 16 2 0 94.96 137.23 101.53 o 17 2 0 1785.86 1640.47 375.34 o 18 2 0 4025.14 4763.94 527.62 o 1 3 0 6100.07 5939.91 77.98 o 2 3 0 1994.18 2081.81 37.02 o 3 3 0 4529.49 4342.27 62.95 o 4 3 0 1411.55 1393.97 37.97 o 5 3 0 3007.79 3154.09 62.72 o 6 3 0 1717.16 1676.98 47.58 o 7 3 0 1343.62 1744.73 52.77 o 8 3 0 399.20 310.62 31.59 o 9 3 0 465.51 601.13 40.96 o 10 3 0 2382.16 2339.95 92.32 o 11 3 0 1341.54 1390.17 85.33 o 12 3 0 92.76 26.38 58.43 o 13 3 0 51.64 100.41 66.99 o 14 3 0 403.76 459.61 87.42 o 15 3 0 519.60 651.51 134.03 o 16 3 0 204.88 149.45 119.91 o 17 3 0 919.91 951.87 144.70 o 0 4 0 128.25 126.52 21.92 o 1 4 0 9165.87 9508.62 119.15 o 2 4 0 6755.33 6617.33 91.72 o 3 4 0 5.23 31.45 15.40 o 4 4 0 53.27 57.09 22.34 o 5 4 0 6915.94 7068.10 105.97 o 6 4 0 8086.89 7590.32 108.42 o 7 4 0 13423.62 13530.78 190.84 o 8 4 0 5078.16 5244.26 105.67 o 9 4 0 1191.70 1245.65 56.29 o 10 4 0 7073.92 7137.45 152.99 o 11 4 0 2091.08 2097.12 110.44 o 12 4 0 89.26 145.84 64.73 o 13 4 0 3783.60 3677.96 135.27 o 14 4 0 117.20 98.22 68.48 o 15 4 0 552.44 625.49 110.67 o 16 4 0 658.21 622.39 146.44 o 17 4 0 2717.30 3104.41 241.57 o 1 5 0 995.73 991.29 38.17 o 2 5 0 7918.58 8297.02 132.77 o 3 5 0 2226.43 2370.74 46.82 o 4 5 0 5198.33 5272.87 79.34 o 5 5 0 698.10 778.78 39.34 o 6 5 0 1665.70 1769.60 53.63 o 7 5 0 403.94 324.50 31.12 o 8 5 0 1254.12 1135.75 50.67 o 9 5 0 2066.19 2088.07 66.19 o 10 5 0 1269.16 1325.38 85.99 o 11 5 0 481.39 303.60 103.46 o 12 5 0 402.82 382.81 74.87 o 13 5 0 2174.89 2232.31 153.70 o 14 5 0 472.20 441.17 98.56 o 15 5 0 210.15 172.19 98.92 o 16 5 0 626.82 706.22 132.97 o 17 5 0 271.42 187.43 124.85 o 0 6 0 43187.27 43018.02 867.07 o 1 6 0 2498.00 2688.80 50.30 o 2 6 0 4232.07 4390.99 78.39 o 3 6 0 667.68 637.89 36.19 o 4 6 0 1155.00 1053.69 37.26 o 5 6 0 2076.73 2206.52 66.27 o 6 6 0 28116.03 28252.53 307.24 o 7 6 0 10160.26 10267.96 142.72 o 8 6 0 2160.89 2422.03 67.41 o 9 6 0 1970.10 1895.38 73.42 o 10 6 0 6568.89 6475.82 165.35 o 11 6 0 151.99 204.80 62.71 o 12 6 0 3316.49 3561.98 254.78 o 13 6 0 9260.37 8586.74 325.12 o 14 6 0 161.04 200.21 104.13 o 15 6 0 841.67 861.40 126.85 o 16 6 0 725.45 973.17 143.97 o 17 6 0 606.78 596.05 142.92 o 1 7 0 7580.12 7911.10 105.32 o 2 7 0 1846.46 1576.94 61.09 o 3 7 0 25483.00 26211.07 304.95 o 4 7 0 431.89 499.74 28.70 o 5 7 0 1.02 -0.09 19.33 o 6 7 0 284.63 257.61 27.96 o 7 7 0 11984.32 11780.84 158.80 o 8 7 0 2779.53 2815.51 80.17 o 9 7 0 2399.17 2423.25 106.19 o 10 7 0 23.36 52.36 72.39 o 11 7 0 735.36 672.11 102.29 o 12 7 0 7298.46 7160.16 231.09 o 13 7 0 1120.33 1020.87 157.07 o 14 7 0 2.99 8.27 90.93 o 15 7 0 319.24 200.24 110.61 o 16 7 0 2344.19 2625.94 194.54 o 17 7 0 2202.83 2354.78 198.27 o 0 8 0 8292.37 8881.14 169.45 o 1 8 0 15421.43 14627.87 173.60 o 2 8 0 2534.17 2758.06 68.46 o 3 8 0 1350.57 1406.95 54.73 o 4 8 0 877.90 902.41 47.40 o 5 8 0 28771.01 28491.81 310.86 o 6 8 0 684.56 758.70 52.67 o 7 8 0 7401.46 7088.82 148.46 o 8 8 0 6184.91 5941.19 186.74 o 9 8 0 7758.76 7568.96 195.49 o 10 8 0 4178.02 4249.10 165.23 o 11 8 0 13177.99 12843.15 308.75 o 12 8 0 3277.58 3064.99 171.70 o 13 8 0 194.94 314.06 101.96 o 14 8 0 5579.02 5305.41 238.44 o 15 8 0 674.24 574.07 127.39 o 16 8 0 336.39 345.85 130.01 o 17 8 0 1143.14 211.05 278.20 o 1 9 0 557.99 767.80 36.03 o 2 9 0 16094.40 15989.09 211.36 o 3 9 0 586.12 623.71 42.68 o 4 9 0 10738.27 10674.51 160.90 o 5 9 0 242.80 261.36 35.50 o 6 9 0 4740.47 4777.76 103.41 o 7 9 0 4092.10 4212.25 122.57 o 8 9 0 9987.41 9735.56 184.61 o 9 9 0 229.48 326.74 56.69 o 10 9 0 925.66 1134.50 112.43 o 11 9 0 4011.07 4245.41 266.13 o 12 9 0 7629.69 7708.31 319.58 o 13 9 0 17.22 51.81 91.39 o 14 9 0 70.00 219.47 108.90 o 15 9 0 3264.59 3514.06 218.15 o 16 9 0 315.77 381.11 157.57 o 0 10 0 2325.38 1745.76 78.35 o 1 10 0 881.41 988.68 43.38 o 2 10 0 11607.00 11178.48 195.18 o 3 10 0 2192.62 2399.54 79.55 o 4 10 0 20438.72 20008.72 260.41 o 5 10 0 633.73 677.65 48.26 o 6 10 0 13121.42 12560.96 214.13 o 7 10 0 5359.61 5431.35 135.31 o 8 10 0 114.51 85.18 48.01 o 9 10 0 3400.22 3459.97 118.91 o 10 10 0 1150.97 1251.47 114.10 o 11 10 0 807.49 878.10 106.34 o 12 10 0 6591.94 6338.66 234.27 o 13 10 0 1732.91 1896.87 161.84 o 14 10 0 1208.20 1275.87 164.77 o 15 10 0 2446.04 2590.96 204.37 o 16 10 0 1237.08 1038.15 160.31 o 1 11 0 3763.71 3937.73 79.69 o 2 11 0 825.63 836.47 53.56 o 3 11 0 5889.98 5629.09 114.44 o 4 11 0 4432.58 4617.80 104.44 o 5 11 0 4459.71 4601.12 121.39 o 6 11 0 984.90 1026.96 71.51 o 7 11 0 272.27 180.41 59.93 o 8 11 0 1473.04 1454.91 90.05 o 9 11 0 2464.58 2566.53 128.99 o 10 11 0 7149.45 7153.62 228.84 o 11 11 0 3.80 -69.03 80.42 o 12 11 0 123.02 49.12 91.79 o 13 11 0 2036.61 2140.43 169.20 o 14 11 0 13.05 19.32 121.06 o 15 11 0 30.54 -1.65 210.19 o 16 11 0 1143.39 1121.66 586.14 o 0 12 0 402.02 345.89 76.55 o 1 12 0 5851.10 6178.53 130.66 o 2 12 0 2994.02 3181.80 112.61 o 3 12 0 2104.95 2062.93 74.74 o 4 12 0 538.39 526.13 57.76 o 5 12 0 5828.24 5675.17 139.38 o 6 12 0 4389.67 4388.82 131.56 o 7 12 0 6149.22 6009.22 153.07 o 8 12 0 2946.32 2932.96 117.76 o 9 12 0 6682.01 6780.28 173.68 o 10 12 0 1442.09 1417.46 136.53 o 11 12 0 41.66 133.33 85.20 o 12 12 0 4777.60 4374.77 210.09 o 13 12 0 321.23 144.16 97.51 o 14 12 0 911.04 642.35 140.14 o 15 12 0 122.79 253.22 130.13 o 1 13 0 2058.91 2196.76 161.03 o 2 13 0 2508.91 2457.21 121.20 o 3 13 0 1020.49 849.20 84.41 o 4 13 0 63.33 -13.66 46.59 o 5 13 0 4282.35 4525.35 132.65 o 6 13 0 873.04 791.74 70.89 o 7 13 0 111.55 208.11 59.63 o 8 13 0 237.22 214.20 63.48 o 9 13 0 7724.63 7644.32 190.10 o 10 13 0 73.83 89.22 87.07 o 11 13 0 46.14 -85.25 91.15 o 12 13 0 9.12 -3.53 96.34 o 13 13 0 2645.11 2962.38 228.40 o 14 13 0 649.09 701.07 141.91 o 15 13 0 777.51 741.76 186.82 o 0 14 0 4622.08 4721.85 182.71 o 1 14 0 3575.03 3586.12 106.00 o 2 14 0 1384.02 1458.69 97.10 o 3 14 0 200.80 287.72 63.21 o 4 14 0 71.26 76.51 52.79 o 5 14 0 172.35 154.10 57.18 o 6 14 0 236.82 215.83 71.79 o 7 14 0 26.73 -28.59 57.86 o 8 14 0 4174.03 4037.44 144.09 o 9 14 0 479.38 489.49 78.70 o 10 14 0 20.33 -20.72 84.50 o 11 14 0 978.18 1036.96 134.72 o 12 14 0 581.76 611.34 119.82 o 13 14 0 1215.86 1249.65 157.26 o 14 14 0 231.18 305.07 190.80 o 1 15 0 1294.15 1440.46 87.17 o 2 15 0 11827.75 11324.02 244.29 o 3 15 0 8.58 12.55 57.86 o 4 15 0 4482.62 4431.55 156.30 o 5 15 0 839.67 990.24 94.10 o 6 15 0 1306.23 1267.99 93.21 o 7 15 0 5199.00 5058.16 223.62 o 8 15 0 4026.41 4299.44 156.47 o 9 15 0 348.91 284.84 109.69 o 10 15 0 2192.65 2220.67 167.91 o 11 15 0 1603.91 1807.49 161.90 o 12 15 0 18.66 -20.94 105.58 o 13 15 0 109.51 106.25 154.80 o 14 15 0 1653.23 1415.65 251.57 o 0 16 0 6966.32 6993.22 302.13 o 1 16 0 5.64 22.38 57.56 o 2 16 0 232.49 209.51 59.46 o 3 16 0 26.44 -21.94 64.47 o 4 16 0 7085.59 6406.01 192.43 o 5 16 0 1285.44 1315.33 109.43 o 6 16 0 1544.93 1435.46 106.02 o 7 16 0 5.17 -28.10 66.10 o 8 16 0 196.89 290.73 77.74 o 9 16 0 2669.60 2701.15 142.19 o 10 16 0 2663.60 2812.87 192.22 o 11 16 0 100.56 97.00 112.25 o 12 16 0 1014.31 1099.83 150.23 o 13 16 0 2807.93 3177.65 234.28 o 1 17 0 7642.72 7513.25 203.62 o 2 17 0 7.66 109.01 66.62 o 3 17 0 8207.05 8258.91 222.73 o 4 17 0 471.38 543.50 110.65 o 5 17 0 183.18 169.00 78.32 o 6 17 0 1449.31 1179.41 112.06 o 7 17 0 1030.77 993.04 110.82 o 8 17 0 438.54 355.94 86.19 o 9 17 0 2352.24 2486.18 146.33 o 10 17 0 2722.30 2905.51 278.31 o 11 17 0 484.42 703.22 171.70 o 12 17 0 890.90 932.12 181.11 o 0 18 0 19.68 171.75 125.38 o 1 18 0 3825.57 3921.57 158.16 o 2 18 0 547.36 483.53 89.07 o 3 18 0 1155.99 973.75 144.38 o 4 18 0 258.23 165.27 82.08 o 5 18 0 4306.68 4146.57 181.03 o 6 18 0 16.51 36.76 85.30 o 7 18 0 216.53 258.60 94.79 o 8 18 0 589.03 654.46 103.62 o 9 18 0 445.35 543.13 110.50 o 10 18 0 1531.21 1671.96 324.89 o 11 18 0 448.16 657.46 147.39 o 1 19 0 1866.87 1867.72 148.99 o 2 19 0 1676.41 1660.02 125.04 o 3 19 0 0.19 -54.57 75.37 o 4 19 0 1065.54 1330.51 108.90 o 5 19 0 416.36 398.41 99.60 o 6 19 0 651.78 868.65 117.88 o 7 19 0 50.65 -62.35 89.04 o 8 19 0 7566.88 7973.12 256.16 o 9 19 0 758.63 681.52 181.93 o 10 19 0 45.33 72.21 141.87 o 0 20 0 4266.96 4323.84 307.39 o 1 20 0 302.17 91.20 94.26 o 2 20 0 21.45 138.78 100.66 o 3 20 0 132.28 190.27 89.81 o 4 20 0 419.64 506.20 103.77 o 5 20 0 100.29 86.61 85.99 o 6 20 0 244.90 397.50 109.17 o 7 20 0 68.17 4.11 100.26 o 8 20 0 23.36 224.59 110.33 o 9 20 0 265.49 116.13 127.94 o 1 21 0 384.68 270.70 112.41 o 2 21 0 282.77 515.44 120.22 o 3 21 0 1920.01 1912.37 167.96 o 4 21 0 328.37 408.28 108.06 o 5 21 0 1345.95 1238.79 129.35 o 6 21 0 504.41 396.63 112.83 o 7 21 0 1229.20 1186.48 146.07 o 8 21 0 1986.15 2033.87 202.81 o 0 22 0 649.87 794.39 190.67 o 1 22 0 438.59 407.17 126.06 o 2 22 0 205.08 302.93 124.07 o 3 22 0 3.28 -94.54 151.36 o 4 22 0 20.89 5.46 144.28 o 5 22 0 714.49 820.66 125.77 o 6 22 0 73.17 78.69 106.15 o 7 22 0 13.30 -164.44 168.84 o 1 23 0 62.52 146.34 124.90 o 2 23 0 2.89 23.65 114.81 o 3 23 0 1942.75 1758.71 191.16 o 4 23 0 314.40 289.93 125.23 o -18 1 1 868.04 923.46 145.16 o -17 1 1 75.26 73.91 106.02 o -16 1 1 419.14 459.39 104.62 o -15 1 1 3713.29 3745.77 395.08 o -14 1 1 5462.07 5271.86 178.27 o -13 1 1 1291.27 1367.48 103.68 o -12 1 1 4280.93 4125.69 127.37 o -11 1 1 31.06 -3.19 42.69 o -10 1 1 244.74 245.70 34.53 o -9 1 1 5480.21 6036.47 104.83 o -8 1 1 16622.52 16652.76 207.68 o -7 1 1 967.67 836.42 40.47 o -6 1 1 12699.55 13056.36 167.44 o -5 1 1 20.84 15.96 16.12 o -4 1 1 1851.13 1793.81 41.01 o -3 1 1 3658.59 3662.96 53.14 o -2 1 1 3187.45 2822.13 71.29 o 1 1 1 455.61 224.62 22.05 o 2 1 1 5547.81 5310.68 64.57 o 3 1 1 145.84 108.98 14.27 o 4 1 1 67318.69 69095.88 665.33 o 5 1 1 9413.73 9637.61 119.37 o 6 1 1 14435.64 15748.21 182.33 o 7 1 1 587.09 528.24 35.68 o 8 1 1 5437.39 5731.23 95.39 o 9 1 1 999.01 998.73 63.72 o 10 1 1 3259.12 3455.81 108.62 o 11 1 1 5884.95 5781.26 203.93 o 12 1 1 1599.63 1589.87 96.40 o 13 1 1 575.29 636.36 76.43 o 14 1 1 2057.48 2028.05 134.08 o 15 1 1 356.26 390.40 178.34 o 16 1 1 2316.96 2166.35 169.94 o 17 1 1 4344.65 4597.77 234.12 o -18 2 1 673.23 940.51 173.33 o -17 2 1 27.98 -34.86 102.21 o -16 2 1 657.28 793.47 120.55 o -15 2 1 3487.96 3595.70 179.60 o -14 2 1 890.02 1003.41 99.29 o -13 2 1 1831.44 1926.68 117.37 o -12 2 1 378.84 340.23 59.48 o -11 2 1 207.78 140.29 49.91 o -10 2 1 3808.39 3693.78 86.09 o -9 2 1 587.50 557.03 38.67 o -8 2 1 495.76 519.60 36.83 o -7 2 1 1287.31 1482.98 56.82 o -6 2 1 1224.98 1514.10 45.70 o -5 2 1 8046.95 7968.06 99.71 o -4 2 1 1636.58 1694.40 39.59 o -3 2 1 40800.12 41671.27 405.80 o -2 2 1 5135.51 5480.77 72.16 o -1 2 1 765.15 701.69 38.18 o 0 2 1 23264.07 21794.02 475.04 o 1 2 1 14692.32 14784.82 154.54 o 2 2 1 4598.80 4384.12 58.64 o 3 2 1 1967.26 2175.76 41.53 o 4 2 1 4615.51 4458.15 67.39 o 5 2 1 538.65 453.08 35.87 o 6 2 1 253.51 180.74 23.76 o 7 2 1 4472.06 4861.08 83.02 o 8 2 1 1354.86 1543.86 51.04 o 9 2 1 813.91 911.73 80.66 o 10 2 1 3442.63 3411.21 109.91 o 11 2 1 17.96 -14.76 44.69 o 12 2 1 215.15 190.86 59.62 o 13 2 1 269.82 252.51 76.13 o 14 2 1 1574.59 1733.86 126.11 o 15 2 1 1170.72 1271.16 121.64 o 16 2 1 232.88 211.94 111.45 o 17 2 1 32.21 -36.17 127.82 o -18 3 1 332.70 402.97 146.81 o -17 3 1 2209.34 2339.87 231.51 o -16 3 1 6542.63 5874.12 280.92 o -15 3 1 31.55 -12.62 76.66 o -14 3 1 4693.92 4818.24 176.90 o -13 3 1 17754.44 17426.71 327.04 o -12 3 1 69.70 61.80 56.52 o -11 3 1 3379.32 3261.07 108.28 o -10 3 1 5325.63 5250.47 102.54 o -9 3 1 14029.86 13503.42 179.39 o -8 3 1 2635.74 3198.04 71.61 o -7 3 1 26587.89 25893.89 284.44 o -6 3 1 934.35 1115.98 41.68 o -5 3 1 12953.48 12971.56 152.59 o -4 3 1 148.14 197.45 20.30 o -3 3 1 32405.49 31684.38 315.25 o -2 3 1 5515.13 5505.23 75.46 o -1 3 1 14120.55 14716.05 159.54 o 0 3 1 258.64 248.63 15.35 o 1 3 1 1754.32 1607.54 32.70 o 2 3 1 17984.33 18374.04 191.20 o 3 3 1 33657.52 34276.60 342.67 o 4 3 1 3014.61 3245.34 57.26 o 5 3 1 1163.30 1115.54 37.52 o 6 3 1 13458.30 13196.04 161.37 o 7 3 1 1167.10 1174.17 55.65 o 8 3 1 426.30 356.44 32.86 o 9 3 1 5073.37 4907.18 126.66 o 10 3 1 8567.55 7931.14 165.84 o 11 3 1 1267.63 1135.15 77.48 o 12 3 1 15605.13 16003.58 305.81 o 13 3 1 1058.15 1044.53 97.32 o 14 3 1 558.71 431.91 114.95 o 15 3 1 630.29 698.17 111.58 o 16 3 1 6921.07 6950.02 266.57 o 17 3 1 167.12 172.66 140.64 o -18 4 1 126.09 212.21 318.49 o -17 4 1 1277.00 1335.11 237.03 o -16 4 1 919.62 1019.41 196.52 o -15 4 1 1021.64 1056.20 107.57 o -14 4 1 14142.56 13920.11 268.79 o -13 4 1 2776.50 2562.19 132.88 o -12 4 1 2649.12 2566.48 147.29 o -11 4 1 60.69 92.36 54.04 o -10 4 1 15261.29 15139.81 231.42 o -9 4 1 3032.37 2938.17 90.37 o -8 4 1 5630.90 5627.75 97.69 o -7 4 1 9.35 24.95 22.41 o -6 4 1 21046.16 22350.87 246.93 o -5 4 1 6529.42 6395.77 91.14 o -4 4 1 46458.66 47071.46 465.27 o -3 4 1 8625.34 8839.12 105.31 o -2 4 1 22343.26 22821.22 232.91 o -1 4 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