#------------------------------------------------------------------------------ #$Date: 2016-04-06 16:30:44 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181866 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/96/2019639.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2019639 _cell_angle_alpha 90.000 _cell_angle_beta 106.382 _cell_angle_gamma 90.000 _cell_length_a 9.9611 _cell_length_b 8.8630 _cell_length_c 5.5598 _exptl_crystal_F_000 588.40 _reflns_d_resolution_high 0.7391 _cod_data_source_file eg3165NMnGsup3.hkl _cod_data_source_block NMnG #BEGIN Tags that were not found in dictionaries: _shelx_title ' SrMnGe2O6 Flux NaWolframat, # 3 0.02 Grad bis 950C' _shelx_refln_list_code 4 _shelx_f_calc_maximum 306.40 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6777.85 5225.45 104.64 o 4 0 0 9117.83 9010.65 181.18 o 6 0 0 6607.38 7425.30 153.28 o 8 0 0 2222.84 2256.06 58.48 o 10 0 0 14074.65 15151.95 309.47 o 12 0 0 2208.51 2078.84 238.84 o 1 1 0 578.64 583.36 6.70 o 3 1 0 36288.58 34607.52 860.62 o 5 1 0 11531.55 11482.29 289.13 o 7 1 0 17418.02 18292.83 415.19 o 9 1 0 907.27 958.93 26.71 o 11 1 0 3852.50 4149.11 78.54 o 0 2 0 15158.95 14443.09 249.49 o 2 2 0 3539.46 3546.51 36.85 o 4 2 0 426.36 327.83 7.68 o 6 2 0 82.91 85.05 6.91 o 8 2 0 26.15 41.12 11.15 o 10 2 0 1461.80 1556.12 35.19 o 12 2 0 731.63 713.94 28.59 o 1 3 0 195.54 167.25 6.01 o 3 3 0 1134.98 1301.78 15.63 o 5 3 0 2407.44 2366.31 29.50 o 7 3 0 1799.32 1730.14 28.46 o 9 3 0 431.25 424.50 18.47 o 11 3 0 76.74 91.70 15.34 o 0 4 0 13868.48 13321.76 230.75 o 2 4 0 3358.80 3161.89 36.88 o 4 4 0 16737.21 16938.57 170.89 o 6 4 0 5.25 17.45 6.03 o 8 4 0 497.38 453.64 15.97 o 10 4 0 6937.08 7040.82 107.43 o 12 4 0 694.11 704.05 57.59 o 1 5 0 5334.09 5727.78 72.55 o 3 5 0 28310.36 29224.90 356.09 o 5 5 0 6071.41 5835.50 63.11 o 7 5 0 28822.71 29676.79 323.74 o 9 5 0 216.44 236.18 15.11 o 11 5 0 3398.77 3257.50 70.72 o 0 6 0 41221.41 41020.32 706.75 o 2 6 0 4925.49 4678.87 61.02 o 4 6 0 8209.97 8551.08 108.05 o 6 6 0 261.79 248.39 11.07 o 8 6 0 16.52 32.18 8.86 o 10 6 0 7865.17 7777.45 167.09 o 1 7 0 826.93 773.56 16.44 o 3 7 0 836.77 788.21 28.25 o 5 7 0 4432.95 4360.92 59.11 o 7 7 0 6500.91 6527.70 87.66 o 9 7 0 244.26 242.25 20.78 o 0 8 0 66.20 77.37 12.24 o 2 8 0 454.86 444.10 14.41 o 4 8 0 608.24 578.99 16.76 o 6 8 0 7.58 19.31 13.27 o 8 8 0 10.81 6.47 12.66 o 1 9 0 2.47 9.23 8.14 o 3 9 0 2143.13 2150.05 34.81 o 5 9 0 856.72 877.09 26.89 o 7 9 0 2803.03 2809.99 71.70 o 0 10 0 16951.63 16724.37 297.16 o 2 10 0 815.92 820.76 23.93 o 4 10 0 5009.05 4827.98 67.93 o 6 10 0 907.15 913.26 35.98 o 1 11 0 2.07 16.24 10.14 o 3 11 0 6672.25 6546.55 89.14 o -11 1 1 108.27 139.89 15.96 o -9 1 1 1787.75 1755.54 26.64 o -7 1 1 3159.37 3144.66 73.90 o -5 1 1 13425.35 13226.68 184.10 o -3 1 1 9383.05 9778.65 121.86 o -1 1 1 4950.08 4783.27 50.10 o 1 1 1 2299.62 1931.57 23.99 o 3 1 1 7376.96 7547.59 81.50 o 5 1 1 7992.92 7640.55 76.22 o 7 1 1 1798.45 1717.16 24.46 o 9 1 1 2556.85 2621.03 47.59 o 11 1 1 517.93 502.89 23.13 o -12 2 1 11553.40 12458.61 183.54 o -10 2 1 2099.40 2167.36 56.62 o -8 2 1 8661.69 8732.40 101.55 o -6 2 1 5032.83 5044.17 126.09 o -4 2 1 913.17 1079.48 16.64 o -2 2 1 67373.98 67814.62 790.07 o 0 2 1 14441.69 13653.80 134.86 o 2 2 1 55084.78 53935.92 573.19 o 4 2 1 319.02 252.12 7.76 o 6 2 1 9538.90 9846.14 107.69 o 8 2 1 6789.04 6734.64 86.39 o 10 2 1 1129.90 1149.54 30.96 o -11 3 1 377.88 325.72 18.52 o -9 3 1 13194.61 13739.69 248.59 o -7 3 1 9537.91 9485.30 119.39 o -5 3 1 56406.29 55506.68 1193.21 o -3 3 1 615.96 925.85 13.71 o -1 3 1 20371.04 21130.51 218.49 o 1 3 1 1814.29 1669.48 20.97 o 3 3 1 207.15 119.52 4.73 o 5 3 1 56103.79 55228.71 640.42 o 7 3 1 4238.36 4031.62 47.94 o 9 3 1 10945.14 10986.37 245.01 o 11 3 1 18.83 41.93 31.08 o -12 4 1 4729.84 4917.62 96.61 o -10 4 1 1830.07 1745.05 68.24 o -8 4 1 1435.68 1508.29 27.08 o -6 4 1 139.34 134.22 9.79 o -4 4 1 19.88 33.37 4.67 o -2 4 1 19698.51 19667.39 203.77 o 0 4 1 22231.51 22835.70 235.69 o 2 4 1 13228.84 12999.11 147.51 o 4 4 1 672.81 685.00 11.96 o 6 4 1 1462.08 1418.04 22.32 o 8 4 1 1255.33 1263.50 24.99 o 10 4 1 1184.45 1198.71 44.87 o -11 5 1 0.45 4.19 14.28 o -9 5 1 251.50 242.37 14.90 o -7 5 1 60.16 63.18 7.61 o -5 5 1 1836.44 1766.80 28.98 o -3 5 1 140.40 136.98 5.68 o -1 5 1 1272.81 1219.62 16.96 o 1 5 1 362.84 358.23 8.06 o 3 5 1 578.88 559.43 12.80 o 5 5 1 1764.53 1708.49 23.20 o 7 5 1 11.52 0.58 10.79 o 9 5 1 254.39 242.38 14.08 o -10 6 1 211.45 144.95 30.37 o -8 6 1 368.07 358.22 18.06 o -6 6 1 299.15 290.16 11.70 o -4 6 1 377.13 373.18 9.83 o -2 6 1 3288.28 3116.52 37.91 o 0 6 1 5149.43 5168.38 60.07 o 2 6 1 1380.89 1306.92 18.08 o 4 6 1 356.13 345.64 11.41 o 6 6 1 46.28 69.67 7.62 o 8 6 1 6.49 1.54 12.10 o 10 6 1 242.87 209.99 30.67 o -9 7 1 4611.39 4696.27 99.26 o -7 7 1 1335.28 1322.87 26.72 o -5 7 1 19593.14 20288.46 256.57 o -3 7 1 1306.80 1174.79 18.76 o -1 7 1 6986.30 7169.92 75.37 o 1 7 1 5446.92 5523.61 64.96 o 3 7 1 291.34 266.31 10.16 o 5 7 1 12635.05 13076.00 162.58 o 7 7 1 1091.49 1075.53 33.68 o 9 7 1 6117.98 5836.98 112.12 o -8 8 1 5079.92 4959.97 148.33 o -6 8 1 1750.73 1682.85 30.59 o -4 8 1 11.10 12.85 7.07 o -2 8 1 21653.78 22017.62 244.32 o 0 8 1 3276.28 3061.57 43.79 o 2 8 1 18379.80 19112.63 282.78 o 4 8 1 460.96 513.48 16.76 o 6 8 1 4386.49 4260.91 70.07 o 8 8 1 3446.32 3295.08 70.98 o -7 9 1 2846.17 2735.77 52.52 o -5 9 1 9695.58 9648.86 147.50 o -3 9 1 916.49 898.28 18.00 o -1 9 1 1343.03 1313.93 24.78 o 1 9 1 414.53 439.98 14.28 o 3 9 1 756.75 748.20 21.70 o 5 9 1 7348.83 7642.57 123.46 o 7 9 1 1779.10 1748.59 46.50 o -6 10 1 7.22 23.11 16.17 o -4 10 1 177.21 196.89 15.91 o -2 10 1 3399.35 3255.23 48.48 o 0 10 1 1236.77 1180.63 24.96 o 2 10 1 1039.79 1024.13 23.70 o 4 10 1 113.97 121.76 11.43 o 6 10 1 550.49 563.70 40.45 o -3 11 1 312.74 283.87 14.66 o -1 11 1 8.62 29.07 10.75 o 1 11 1 30.06 30.70 11.12 o 3 11 1 202.88 214.09 16.18 o -12 0 2 2078.47 2182.52 64.55 o -10 0 2 18748.57 18846.09 666.39 o -8 0 2 45.53 39.97 10.11 o -6 0 2 15094.35 15476.30 249.81 o -4 0 2 26130.79 26899.32 428.53 o -2 0 2 10833.29 10536.90 139.07 o 0 0 2 93879.11 91580.30 1465.05 o 2 0 2 455.40 242.61 15.16 o 4 0 2 39111.84 40912.91 609.21 o 6 0 2 85.04 111.93 11.93 o 8 0 2 240.37 249.55 15.11 o 10 0 2 10421.27 10093.61 230.72 o -13 1 2 1143.80 1081.26 61.90 o -11 1 2 387.53 342.14 18.86 o -9 1 2 849.43 848.55 21.22 o -7 1 2 36231.99 37549.54 416.87 o -5 1 2 9604.49 9303.37 121.70 o -3 1 2 10228.36 9719.23 189.80 o -1 1 2 78.81 112.79 5.49 o 1 1 2 10924.93 11998.34 140.93 o 3 1 2 13258.91 13075.95 153.90 o 5 1 2 7910.46 7538.15 83.22 o 7 1 2 15773.67 15520.55 151.91 o 9 1 2 1353.00 1413.19 34.02 o -12 2 2 791.03 789.62 28.91 o -10 2 2 3304.16 3213.48 50.76 o -8 2 2 673.39 646.49 18.76 o -6 2 2 334.34 361.78 11.29 o -4 2 2 3778.70 3772.07 49.35 o -2 2 2 771.19 750.51 8.88 o 0 2 2 214.85 100.28 4.01 o 2 2 2 3327.85 3258.98 41.49 o 4 2 2 8062.78 7872.44 84.75 o 6 2 2 395.17 379.35 13.45 o 8 2 2 945.43 902.04 20.22 o 10 2 2 1220.12 1141.38 32.05 o -11 3 2 90.23 85.71 18.26 o -9 3 2 404.25 370.55 15.02 o -7 3 2 8.78 13.33 7.13 o -5 3 2 772.05 833.82 14.40 o -3 3 2 1239.97 1251.89 17.84 o -1 3 2 2088.74 2315.05 26.29 o 1 3 2 752.09 874.03 13.40 o 3 3 2 333.66 280.67 9.48 o 5 3 2 543.52 521.60 14.10 o 7 3 2 42.02 47.46 8.06 o 9 3 2 363.58 333.53 15.37 o -12 4 2 1779.27 1861.60 51.80 o -10 4 2 5224.09 5360.84 152.85 o -8 4 2 59.09 60.72 8.99 o -6 4 2 1774.92 1815.60 30.81 o -4 4 2 2949.49 2950.17 37.86 o -2 4 2 3076.53 2973.45 30.83 o 0 4 2 25146.92 25860.18 291.34 o 2 4 2 4741.39 4806.44 57.41 o 4 4 2 8196.97 8186.40 90.14 o 6 4 2 5.28 11.23 7.29 o 8 4 2 18.52 33.05 11.12 o 10 4 2 2284.16 2066.62 64.34 o -11 5 2 2836.16 2836.83 82.22 o -9 5 2 44.47 24.52 10.00 o -7 5 2 22819.79 24171.07 328.01 o -5 5 2 4001.85 3776.87 48.40 o -3 5 2 42538.27 44729.02 462.24 o -1 5 2 16.29 10.09 4.29 o 1 5 2 2508.66 2864.15 36.13 o 3 5 2 28072.18 29297.89 331.37 o 5 5 2 1004.21 904.30 23.79 o 7 5 2 12847.69 12842.77 167.06 o 9 5 2 925.99 1093.72 32.49 o -10 6 2 5493.82 5941.63 105.43 o -8 6 2 22.15 22.36 12.07 o -6 6 2 5211.26 5211.47 76.22 o -4 6 2 2707.97 2792.29 33.16 o -2 6 2 8590.64 8495.25 84.04 o 0 6 2 38125.12 38830.03 425.87 o 2 6 2 2422.02 2389.31 32.13 o 4 6 2 7006.00 7302.50 86.87 o 6 6 2 2.25 10.94 9.61 o 8 6 2 168.99 172.99 16.42 o -9 7 2 342.01 336.56 19.18 o -7 7 2 4685.82 4641.90 105.73 o -5 7 2 1694.65 1631.02 28.38 o -3 7 2 2628.76 2639.88 34.17 o -1 7 2 728.79 685.50 13.09 o 1 7 2 376.65 358.90 10.88 o 3 7 2 3527.98 3474.94 68.87 o 5 7 2 1833.68 1810.56 31.44 o 7 7 2 1892.81 1817.00 40.88 o -8 8 2 381.62 369.31 40.31 o -6 8 2 247.91 226.37 15.91 o -4 8 2 28.36 38.67 8.37 o -2 8 2 67.48 83.56 7.54 o 0 8 2 678.03 667.16 15.56 o 2 8 2 358.60 362.51 16.19 o 4 8 2 81.84 90.36 9.64 o 6 8 2 128.19 113.18 13.06 o -7 9 2 3705.31 3686.14 56.51 o -5 9 2 813.01 799.54 23.08 o -3 9 2 1397.46 1405.26 23.40 o -1 9 2 32.00 43.50 9.10 o 1 9 2 763.15 779.99 23.24 o 3 9 2 639.73 671.89 19.52 o 5 9 2 1032.74 1101.81 28.82 o -6 10 2 1444.50 1282.78 45.72 o -4 10 2 4700.68 4570.78 66.48 o -2 10 2 291.34 316.04 12.58 o 0 10 2 10775.62 10806.92 114.40 o 2 10 2 854.37 951.74 21.30 o 4 10 2 7473.15 7294.64 113.13 o -3 11 2 5759.43 5564.68 153.85 o -1 11 2 28.14 50.07 9.85 o 1 11 2 324.53 249.81 36.49 o -13 1 3 0.71 -20.92 20.92 o -11 1 3 56.39 35.45 9.71 o -9 1 3 1155.02 1142.88 20.68 o -7 1 3 2949.49 2869.79 41.06 o -5 1 3 10915.30 10709.81 134.98 o -3 1 3 7201.04 7316.78 161.48 o -1 1 3 3290.02 3186.62 51.92 o 1 1 3 932.17 902.90 17.65 o 3 1 3 1430.48 1402.92 22.35 o 5 1 3 2103.00 1999.42 30.45 o 7 1 3 1323.78 1282.99 21.95 o 9 1 3 2799.99 2747.91 45.89 o -12 2 3 10844.42 10008.67 261.35 o -10 2 3 1302.37 1346.69 24.05 o -8 2 3 12457.00 13128.51 166.92 o -6 2 3 295.53 316.10 11.20 o -4 2 3 563.30 642.70 13.51 o -2 2 3 40230.14 41689.78 429.69 o 0 2 3 3248.67 2970.44 34.62 o 2 2 3 32872.59 33597.97 391.90 o 4 2 3 2282.03 2146.43 28.09 o 6 2 3 6943.36 6949.17 86.75 o 8 2 3 3255.45 3095.52 45.22 o -11 3 3 1354.77 1256.07 36.17 o -9 3 3 12238.98 12837.12 164.64 o -7 3 3 5968.52 5844.23 77.49 o -5 3 3 31416.88 32484.14 455.60 o -3 3 3 667.69 577.23 10.87 o -1 3 3 30749.65 32096.11 314.59 o 1 3 3 1732.91 1793.35 22.84 o 3 3 3 273.87 213.26 9.02 o 5 3 3 21364.38 21358.65 261.62 o 7 3 3 1705.29 1754.99 33.63 o 9 3 3 9687.75 8916.12 129.69 o -12 4 3 3998.54 3935.74 200.74 o -10 4 3 915.03 931.52 23.86 o -8 4 3 3890.03 3985.46 56.47 o -6 4 3 731.08 652.96 16.15 o -4 4 3 152.81 173.69 7.80 o -2 4 3 16856.81 16755.20 175.33 o 0 4 3 6044.51 6183.84 73.01 o 2 4 3 6610.02 6798.32 80.69 o 4 4 3 2313.09 2265.90 35.47 o 6 4 3 1964.51 1953.67 33.45 o 8 4 3 629.13 665.87 28.61 o -11 5 3 78.66 50.72 22.38 o -9 5 3 98.25 93.94 12.21 o -7 5 3 134.18 126.31 10.78 o -5 5 3 2010.13 1967.86 28.87 o -3 5 3 278.21 252.03 8.61 o -1 5 3 487.98 494.86 12.43 o 1 5 3 795.56 727.22 15.61 o 3 5 3 59.98 68.61 6.96 o 5 5 3 208.58 199.96 11.40 o 7 5 3 7.35 26.11 11.12 o -10 6 3 513.15 504.87 22.16 o -8 6 3 650.80 701.37 22.02 o -6 6 3 181.89 178.51 9.91 o -4 6 3 105.43 117.81 7.85 o -2 6 3 1054.44 996.09 14.80 o 0 6 3 2516.30 2453.07 30.47 o 2 6 3 1496.93 1533.70 24.34 o 4 6 3 546.89 537.58 17.55 o 6 6 3 105.74 112.15 11.48 o 8 6 3 2.52 -0.25 17.78 o -9 7 3 4289.70 4296.49 81.28 o -7 7 3 1053.75 1056.50 22.23 o -5 7 3 13453.48 13923.78 165.87 o -3 7 3 1371.03 1380.06 20.98 o -1 7 3 8912.81 9205.67 99.45 o 1 7 3 1619.90 1687.60 25.90 o 3 7 3 20.74 34.84 7.81 o 5 7 3 7084.50 6951.05 95.34 o 7 7 3 569.39 629.43 70.01 o -8 8 3 5462.87 5493.21 93.93 o -6 8 3 655.91 652.33 20.12 o -4 8 3 219.45 219.98 12.10 o -2 8 3 11030.89 11337.94 129.53 o 0 8 3 1548.08 1595.81 25.67 o 2 8 3 17493.53 18428.43 227.99 o 4 8 3 1232.73 1255.11 30.09 o 6 8 3 2667.74 2651.43 83.51 o -7 9 3 2276.22 2295.32 40.98 o -5 9 3 4918.49 4991.10 71.56 o -3 9 3 1007.41 1007.09 23.67 o -1 9 3 4175.11 4139.01 48.32 o 1 9 3 58.08 71.55 10.24 o 3 9 3 705.09 757.45 21.78 o 5 9 3 4249.28 4288.85 120.16 o -6 10 3 1.85 13.69 26.42 o -4 10 3 39.85 52.93 15.25 o -2 10 3 2336.62 2404.04 35.73 o 0 10 3 283.97 320.92 12.30 o 2 10 3 1029.75 994.53 32.28 o -12 0 4 1219.73 1293.09 45.48 o -10 0 4 10245.17 10619.07 223.78 o -8 0 4 758.87 762.17 29.33 o -6 0 4 20779.53 20879.25 424.55 o -4 0 4 10054.97 10512.36 215.67 o -2 0 4 4129.37 3807.54 64.12 o 0 0 4 42533.46 47402.87 875.08 o 2 0 4 1203.20 1167.83 34.02 o 4 0 4 18100.74 19640.75 373.96 o 6 0 4 42.97 48.14 15.87 o 8 0 4 1419.08 1290.68 29.25 o -11 1 4 713.16 668.04 21.27 o -9 1 4 432.32 436.95 17.38 o -7 1 4 10822.88 10640.04 137.89 o -5 1 4 3043.89 2932.75 42.21 o -3 1 4 26101.85 27120.59 298.15 o -1 1 4 3194.12 3101.49 33.21 o 1 1 4 602.17 689.99 17.70 o 3 1 4 7938.28 8304.98 115.68 o 5 1 4 448.47 515.34 19.34 o 7 1 4 5494.40 5485.75 64.62 o -12 2 4 871.08 824.79 26.56 o -10 2 4 714.42 715.80 18.50 o -8 2 4 92.07 100.85 9.05 o -6 2 4 669.70 614.98 18.48 o -4 2 4 5.98 6.27 4.69 o -2 2 4 911.12 925.58 15.10 o 0 2 4 3548.26 3546.74 46.37 o 2 2 4 2450.40 2474.79 40.13 o 4 2 4 1135.24 1172.95 19.86 o 6 2 4 3.09 14.79 8.40 o 8 2 4 0.51 32.48 11.62 o -11 3 4 70.11 79.38 10.99 o -9 3 4 333.35 301.09 14.06 o -7 3 4 710.36 687.82 16.86 o -5 3 4 581.82 555.51 19.61 o -3 3 4 49.33 66.81 5.13 o -1 3 4 423.71 388.38 9.31 o 1 3 4 319.70 292.73 9.71 o 3 3 4 80.29 83.58 8.19 o 5 3 4 839.39 806.48 19.60 o 7 3 4 359.90 400.95 32.78 o -12 4 4 967.63 856.55 60.73 o -10 4 4 6562.39 7017.98 103.63 o -8 4 4 938.65 985.69 26.26 o -6 4 4 963.77 1013.07 22.77 o -4 4 4 3085.41 3005.17 40.54 o -2 4 4 89.60 109.24 6.53 o 0 4 4 6274.25 6628.82 79.19 o 2 4 4 4248.35 4122.45 76.42 o 4 4 4 9244.42 9169.12 121.76 o 6 4 4 6.06 20.32 10.26 o 8 4 4 1.74 26.89 23.44 o -11 5 4 452.20 347.60 23.09 o -9 5 4 39.30 39.92 15.38 o -7 5 4 19578.04 20471.65 280.16 o -5 5 4 2317.06 2332.75 33.99 o -3 5 4 21866.15 22715.97 238.12 o -1 5 4 67.90 70.03 6.23 o 1 5 4 4418.27 4548.60 56.79 o 3 5 4 6764.90 6657.48 90.71 o 5 5 4 238.92 264.81 13.69 o 7 5 4 10364.11 10911.23 271.58 o -10 6 4 6473.98 6640.19 100.85 o -8 6 4 1474.91 1494.56 31.99 o -6 6 4 3790.84 3788.48 51.47 o -4 6 4 4900.65 5041.65 64.91 o -2 6 4 1775.66 1696.50 20.74 o 0 6 4 9575.78 10124.06 119.14 o 2 6 4 2403.10 2499.59 39.83 o 4 6 4 10281.96 10318.98 140.52 o 6 6 4 38.16 50.32 17.92 o -9 7 4 593.75 558.84 32.31 o -7 7 4 4158.50 4292.27 67.53 o -5 7 4 472.31 475.81 16.08 o -3 7 4 1709.25 1752.74 26.40 o 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