data_2019647 _cell_angle_alpha 90.000 _cell_angle_beta 102.300 _cell_angle_gamma 90.000 _cell_length_a 14.0913 _cell_length_b 14.9503 _cell_length_c 22.6588 _exptl_crystal_F_000 2016.00 _reflns_d_resolution_high 0.7214 _cod_data_source_file bg3182Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 302.60 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 52064.86 52744.62 764.68 o 4 0 0 30071.49 31364.75 505.34 o 5 0 0 4511.84 5569.44 157.82 o 6 0 0 6965.01 7830.70 210.32 o 7 0 0 8214.36 9637.76 253.27 o 8 0 0 947.58 1025.64 80.52 o 9 0 0 5028.14 5293.28 201.01 o 10 0 0 4255.43 4976.95 210.53 o 11 0 0 46.81 16.04 44.32 o 12 0 0 195.60 66.90 45.11 o 13 0 0 1512.89 1768.34 142.89 o 14 0 0 38.26 1.37 49.14 o 15 0 0 36.09 67.92 47.73 o 16 0 0 420.46 475.75 89.84 o 17 0 0 128.33 233.12 79.90 o 2 1 0 7065.16 7734.08 144.80 o 3 1 0 36243.97 37309.05 840.63 o 4 1 0 4611.38 5050.77 120.19 o 5 1 0 15262.89 15420.19 219.10 o 6 1 0 16263.71 18621.43 484.07 o 7 1 0 97.59 178.96 25.07 o 8 1 0 551.63 729.94 54.75 o 9 1 0 99.20 14.57 20.23 o 10 1 0 642.44 507.98 39.04 o 11 1 0 1059.57 917.30 74.53 o 12 1 0 5.41 -33.89 37.11 o 13 1 0 102.92 146.77 36.76 o 14 1 0 255.49 161.42 40.27 o 15 1 0 93.38 59.02 41.65 o 16 1 0 19.29 94.21 38.53 o 17 1 0 0.48 -4.17 35.16 o 1 2 0 61.49 27.36 8.69 o 2 2 0 4169.35 4824.31 78.24 o 3 2 0 400.00 344.81 23.45 o 4 2 0 2700.30 3017.44 73.17 o 5 2 0 2702.93 2201.78 66.79 o 6 2 0 282.56 179.20 24.43 o 7 2 0 670.08 608.55 42.13 o 8 2 0 776.48 894.18 53.96 o 9 2 0 1.33 -0.38 16.80 o 10 2 0 1791.88 1985.39 74.26 o 11 2 0 1498.15 1444.87 84.84 o 12 2 0 84.24 174.60 42.57 o 13 2 0 252.49 467.41 56.31 o 14 2 0 40.37 37.94 34.21 o 15 2 0 246.87 162.08 42.27 o 16 2 0 28.22 0.31 34.15 o 17 2 0 50.53 95.76 39.74 o 1 3 0 60704.68 59815.61 822.18 o 2 3 0 45879.59 47230.48 950.06 o 3 3 0 23705.67 23468.95 218.43 o 4 3 0 9690.08 10045.88 120.16 o 5 3 0 4214.80 4537.73 109.39 o 6 3 0 1986.08 1998.37 70.32 o 7 3 0 3150.27 3161.82 96.19 o 8 3 0 470.82 471.43 48.28 o 9 3 0 1953.34 2221.76 65.17 o 10 3 0 4.78 -24.44 31.79 o 11 3 0 10.41 25.63 29.82 o 12 3 0 1949.22 1957.41 100.11 o 13 3 0 3.75 -36.71 36.71 o 14 3 0 38.11 38.44 34.18 o 15 3 0 300.69 367.80 56.99 o 16 3 0 131.22 111.42 39.76 o 17 3 0 369.69 398.11 62.38 o 0 4 0 10404.30 11337.54 204.72 o 1 4 0 6016.28 5584.08 84.16 o 2 4 0 9766.31 10138.86 179.41 o 3 4 0 202.62 210.81 14.14 o 4 4 0 642.98 704.97 24.08 o 5 4 0 1070.16 918.14 26.95 o 6 4 0 6155.65 5786.59 77.80 o 7 4 0 1141.20 1198.02 39.44 o 8 4 0 2326.25 2084.74 57.72 o 9 4 0 113.76 104.91 21.78 o 10 4 0 260.77 256.15 29.00 o 11 4 0 382.19 410.92 35.22 o 12 4 0 678.13 680.62 60.69 o 13 4 0 2.71 -32.29 32.29 o 14 4 0 741.79 1016.13 135.69 o 15 4 0 3.44 -26.04 31.12 o 16 4 0 382.11 330.97 75.62 o 17 4 0 79.30 79.98 52.52 o 1 5 0 178.42 211.32 22.60 o 2 5 0 535.33 452.98 22.96 o 3 5 0 357.25 296.54 30.87 o 4 5 0 15.36 38.10 10.03 o 5 5 0 1281.58 1404.35 37.73 o 6 5 0 17680.14 18718.64 186.95 o 7 5 0 1249.19 1215.82 39.88 o 8 5 0 219.44 213.01 18.51 o 9 5 0 8.73 -3.00 26.46 o 10 5 0 3209.40 2942.14 96.20 o 11 5 0 842.45 726.87 46.16 o 12 5 0 213.74 191.21 27.40 o 13 5 0 56.69 60.33 47.65 o 14 5 0 237.68 263.09 51.27 o 15 5 0 101.16 90.58 64.59 o 16 5 0 103.58 175.22 46.37 o 17 5 0 0.23 68.02 53.21 o 0 6 0 6488.23 6987.33 162.77 o 1 6 0 6516.59 6513.59 89.72 o 2 6 0 230.30 180.28 33.87 o 3 6 0 12939.55 14026.23 194.94 o 4 6 0 355.54 314.54 17.18 o 5 6 0 4393.16 4794.02 84.37 o 6 6 0 283.13 262.43 24.40 o 7 6 0 1057.85 1034.40 41.72 o 8 6 0 367.37 292.87 21.91 o 9 6 0 253.83 185.04 25.20 o 10 6 0 158.74 119.33 36.54 o 11 6 0 635.77 597.58 58.99 o 12 6 0 363.31 342.80 34.63 o 13 6 0 629.94 586.13 69.88 o 14 6 0 118.45 147.85 41.76 o 15 6 0 46.71 18.03 31.40 o 16 6 0 54.93 125.46 45.14 o 17 6 0 2.41 -57.55 57.55 o 1 7 0 2169.89 2131.63 51.85 o 2 7 0 3868.86 3994.01 133.36 o 3 7 0 387.00 315.29 17.25 o 4 7 0 7282.66 7206.55 91.48 o 5 7 0 771.55 863.59 32.55 o 6 7 0 9814.78 10212.78 173.31 o 7 7 0 13083.28 13736.28 183.73 o 8 7 0 572.99 558.54 49.05 o 9 7 0 1277.44 1471.67 76.03 o 10 7 0 683.61 782.72 89.16 o 11 7 0 133.05 98.33 31.47 o 12 7 0 123.46 120.12 27.83 o 13 7 0 122.70 151.30 57.31 o 14 7 0 5.31 -47.50 47.50 o 15 7 0 175.18 131.05 53.94 o 16 7 0 8.86 8.60 46.57 o 0 8 0 1541.94 1502.36 78.56 o 1 8 0 855.00 859.93 42.99 o 2 8 0 928.68 1019.83 36.25 o 3 8 0 4616.03 4697.63 140.29 o 4 8 0 1478.83 1381.63 37.21 o 5 8 0 181.16 246.89 19.69 o 6 8 0 663.53 658.60 40.42 o 7 8 0 0.23 9.93 13.77 o 8 8 0 12.81 14.86 31.18 o 9 8 0 287.47 345.33 64.21 o 10 8 0 529.93 493.88 74.45 o 11 8 0 0.36 -0.36 46.99 o 12 8 0 182.38 208.58 57.62 o 13 8 0 126.73 75.48 51.43 o 14 8 0 146.61 130.40 43.71 o 15 8 0 4.40 -49.88 49.88 o 16 8 0 85.05 46.67 53.00 o 1 9 0 3091.09 2986.17 126.97 o 2 9 0 151.64 129.22 22.82 o 3 9 0 755.32 763.67 33.67 o 4 9 0 728.79 688.45 31.28 o 5 9 0 552.14 528.57 28.68 o 6 9 0 1135.22 1230.58 39.02 o 7 9 0 16.51 -11.71 13.32 o 8 9 0 192.09 29.83 51.89 o 9 9 0 401.55 416.03 65.09 o 10 9 0 83.10 80.65 43.44 o 11 9 0 0.54 -3.07 14.64 o 12 9 0 602.21 756.09 95.84 o 13 9 0 4.57 -35.59 38.73 o 14 9 0 135.60 126.36 45.89 o 15 9 0 0.92 -1.34 44.24 o 16 9 0 20.53 -24.08 49.92 o 0 10 0 6815.02 6410.72 189.60 o 1 10 0 20.53 21.46 19.27 o 2 10 0 4154.28 3930.37 101.59 o 3 10 0 115.14 110.47 18.23 o 4 10 0 1995.46 1896.28 49.59 o 5 10 0 4738.60 5129.47 113.11 o 6 10 0 753.65 907.34 34.56 o 7 10 0 233.66 53.77 91.47 o 8 10 0 1775.36 1497.88 321.89 o 9 10 0 2385.77 2735.64 154.69 o 10 10 0 290.75 355.01 63.54 o 11 10 0 548.77 604.30 83.05 o 12 10 0 1.91 73.38 46.90 o 13 10 0 97.16 162.14 56.44 o 14 10 0 1.26 17.61 38.27 o 15 10 0 58.04 37.45 47.40 o 16 10 0 11.64 -43.44 52.75 o 1 11 0 2297.97 2116.07 76.09 o 2 11 0 74.29 79.54 22.31 o 3 11 0 585.15 533.23 40.38 o 4 11 0 11.28 7.27 9.87 o 5 11 0 28.17 8.54 8.27 o 6 11 0 212.08 276.87 30.04 o 7 11 0 85.59 38.23 36.26 o 8 11 0 691.87 682.77 79.24 o 9 11 0 1452.96 1480.89 116.20 o 10 11 0 685.57 713.93 86.28 o 11 11 0 47.44 66.05 40.83 o 12 11 0 49.04 71.27 48.19 o 13 11 0 31.04 32.23 40.83 o 14 11 0 13.49 4.84 36.16 o 15 11 0 2.06 38.55 46.18 o 0 12 0 926.77 965.25 78.46 o 1 12 0 2147.97 2016.57 87.50 o 2 12 0 38.26 35.95 23.07 o 3 12 0 811.60 776.82 49.81 o 4 12 0 2310.15 2138.54 59.25 o 5 12 0 248.02 203.27 17.83 o 6 12 0 2.93 1.99 12.59 o 7 12 0 75.47 100.67 29.21 o 8 12 0 135.23 110.11 40.92 o 9 12 0 475.74 434.20 68.58 o 10 12 0 0.50 -27.89 38.83 o 11 12 0 60.75 49.54 38.02 o 12 12 0 39.48 54.02 45.69 o 13 12 0 135.03 107.88 54.38 o 14 12 0 76.75 42.47 43.23 o 15 12 0 0.17 -17.60 50.17 o 1 13 0 33.02 39.60 24.86 o 2 13 0 3638.15 3600.22 111.59 o 3 13 0 142.39 179.62 23.21 o 4 13 0 1731.61 1721.23 62.41 o 5 13 0 912.40 853.54 44.83 o 6 13 0 317.16 344.84 30.61 o 7 13 0 366.76 368.12 44.36 o 8 13 0 8.50 -11.11 66.88 o 9 13 0 72.84 81.46 27.01 o 10 13 0 105.96 192.67 52.50 o 11 13 0 15.53 1.55 39.64 o 12 13 0 210.41 295.71 68.43 o 13 13 0 1.02 48.76 44.25 o 14 13 0 22.31 33.14 37.97 o 0 14 0 458.87 450.46 59.80 o 1 14 0 522.39 471.19 42.84 o 2 14 0 7.66 24.55 20.36 o 3 14 0 358.48 389.52 35.23 o 4 14 0 0.98 24.26 15.35 o 5 14 0 238.48 226.67 26.43 o 6 14 0 9.49 -1.06 15.17 o 7 14 0 95.19 121.10 46.60 o 8 14 0 190.69 208.24 39.29 o 9 14 0 9.22 -23.14 30.45 o 10 14 0 31.31 61.67 36.63 o 11 14 0 310.84 307.10 49.50 o 12 14 0 22.86 65.65 41.16 o 13 14 0 14.95 0.39 34.33 o 1 15 0 81.65 102.73 25.57 o 2 15 0 306.60 286.16 39.26 o 3 15 0 1198.98 1329.86 70.13 o 4 15 0 68.29 68.19 20.08 o 5 15 0 198.75 184.53 24.63 o 6 15 0 27.48 22.99 15.08 o 7 15 0 21.75 36.58 22.29 o 8 15 0 8.96 42.38 25.88 o 9 15 0 10.88 34.18 26.32 o 10 15 0 179.31 129.36 34.51 o 11 15 0 68.60 99.08 45.39 o 12 15 0 1.48 23.61 39.68 o 0 16 0 880.49 809.18 82.82 o 1 16 0 9.87 33.09 20.47 o 2 16 0 11.92 33.45 26.30 o 3 16 0 521.65 561.58 46.89 o 4 16 0 340.07 353.85 33.23 o 5 16 0 92.48 121.05 22.89 o 6 16 0 131.03 174.45 35.08 o 7 16 0 81.68 130.25 31.66 o 8 16 0 30.39 41.38 24.18 o 9 16 0 3.28 -19.69 26.18 o 10 16 0 109.11 115.70 55.08 o 1 17 0 266.44 341.94 41.56 o 2 17 0 526.17 555.13 49.56 o 3 17 0 105.52 137.29 23.30 o 4 17 0 280.88 333.82 43.48 o 5 17 0 21.91 67.64 27.16 o 6 17 0 5.59 -6.02 29.33 o 7 17 0 3.34 24.02 38.13 o 8 17 0 23.15 41.08 36.46 o 9 17 0 73.24 -39.71 43.71 o 0 18 0 14.26 78.15 35.07 o 1 18 0 10.18 34.15 21.21 o 2 18 0 26.29 3.37 32.72 o 3 18 0 78.60 48.61 39.17 o 4 18 0 52.83 74.95 42.45 o 5 18 0 67.84 40.56 34.57 o 6 18 0 29.96 -14.95 36.82 o 7 18 0 23.70 -38.51 38.51 o 1 19 0 99.01 81.69 38.08 o 2 19 0 8.24 -1.94 28.39 o 3 19 0 63.48 65.21 37.69 o 4 19 0 1.04 97.24 47.71 o 5 19 0 14.05 9.05 32.85 o 6 19 0 0.77 -12.83 33.46 o 3 20 0 92.42 63.10 45.46 o 4 20 0 23.78 23.66 38.93 o 5 20 0 1.41 24.83 44.22 o -17 1 1 15.07 45.60 37.47 o -16 1 1 6.28 -32.98 32.98 o -15 1 1 492.75 547.53 63.05 o -14 1 1 197.96 180.17 42.66 o -13 1 1 286.50 272.26 45.96 o -12 1 1 125.56 128.90 38.42 o -11 1 1 878.40 914.43 67.45 o -10 1 1 1655.89 1760.02 59.77 o -9 1 1 0.89 9.09 16.07 o -8 1 1 3889.79 4212.46 116.20 o -7 1 1 3506.78 3595.23 100.79 o -6 1 1 877.34 883.96 46.21 o -5 1 1 11195.78 11232.13 173.49 o -4 1 1 6948.09 7511.53 123.25 o -3 1 1 9540.26 9851.40 412.05 o -2 1 1 8902.61 9480.55 163.74 o 2 1 1 913.00 824.41 40.09 o 3 1 1 43032.37 42173.22 446.98 o 4 1 1 9777.04 10166.45 368.38 o 5 1 1 692.25 788.45 62.03 o 6 1 1 157.33 157.38 22.99 o 7 1 1 1469.98 1624.20 67.47 o 8 1 1 138.97 163.40 25.54 o 9 1 1 602.84 573.78 45.93 o 10 1 1 787.77 915.44 67.55 o 11 1 1 3180.50 3288.50 271.14 o 12 1 1 481.43 535.03 58.22 o 13 1 1 79.01 -25.62 31.28 o 14 1 1 887.04 985.73 81.37 o 15 1 1 66.10 83.46 35.80 o 16 1 1 173.27 163.90 50.69 o 17 1 1 70.82 48.60 34.97 o -17 2 1 343.62 412.34 63.18 o -16 2 1 42.02 -22.05 29.51 o -15 2 1 31.44 -8.89 34.42 o -14 2 1 329.17 405.84 55.75 o -13 2 1 835.53 901.82 73.67 o -12 2 1 702.22 619.92 61.28 o -11 2 1 733.56 747.50 63.05 o -10 2 1 5.12 19.91 20.61 o -9 2 1 4511.17 4578.74 106.04 o -8 2 1 2643.66 2619.01 90.17 o -7 2 1 3607.57 3873.60 106.18 o -6 2 1 8924.30 9208.26 164.50 o -5 2 1 2726.99 2899.01 77.32 o -4 2 1 126.15 116.28 18.58 o -3 2 1 38325.24 39294.94 417.15 o -2 2 1 1951.13 1883.28 76.55 o -1 2 1 14534.55 14268.60 233.43 o 1 2 1 1805.33 1857.46 51.36 o 2 2 1 14255.73 14357.66 148.09 o 3 2 1 31944.72 33204.25 365.77 o 4 2 1 584.94 724.66 35.88 o 5 2 1 3850.64 3932.78 93.58 o 6 2 1 850.73 1013.24 50.87 o 7 2 1 4090.09 4504.63 116.55 o 8 2 1 1090.89 1185.46 61.91 o 9 2 1 1318.84 1347.66 50.59 o 10 2 1 3636.08 3761.10 127.40 o 11 2 1 18.93 44.54 34.00 o 12 2 1 546.24 528.92 57.98 o 13 2 1 997.44 1060.88 78.86 o 14 2 1 139.03 94.60 37.69 o 15 2 1 200.35 163.64 43.27 o 16 2 1 202.64 138.47 58.94 o 17 2 1 111.21 191.83 85.73 o -17 3 1 19.76 22.90 37.23 o -16 3 1 60.91 33.27 36.05 o -15 3 1 176.67 124.87 36.35 o -14 3 1 63.63 28.87 31.05 o -13 3 1 168.58 171.88 38.15 o -12 3 1 506.14 481.66 54.73 o -11 3 1 1303.18 1170.26 77.09 o -10 3 1 1434.99 1478.28 74.36 o -9 3 1 503.84 477.63 32.27 o -8 3 1 65.59 92.84 40.00 o -7 3 1 6376.59 6678.82 144.15 o -6 3 1 2710.74 2599.99 65.32 o -5 3 1 1086.43 1347.36 73.91 o -4 3 1 86.49 90.71 12.06 o -3 3 1 388.57 447.90 18.31 o -2 3 1 1325.63 1223.96 55.03 o -1 3 1 39.57 67.23 35.23 o 0 3 1 12899.69 13925.67 230.75 o 1 3 1 14289.52 14358.04 234.98 o 2 3 1 6616.35 6915.05 83.52 o 3 3 1 13.11 6.37 10.52 o 4 3 1 114.10 116.38 13.18 o 5 3 1 6630.67 6942.61 103.69 o 6 3 1 326.57 277.50 21.16 o 7 3 1 58.29 32.00 17.90 o 8 3 1 1667.64 1926.95 65.32 o 9 3 1 587.23 666.37 47.60 o 10 3 1 838.44 799.02 62.37 o 11 3 1 965.58 1014.58 72.15 o 12 3 1 12.98 60.36 31.72 o 13 3 1 163.25 217.28 42.06 o 14 3 1 239.86 245.48 80.81 o 15 3 1 328.58 389.10 63.02 o 16 3 1 47.88 71.84 70.60 o 17 3 1 20.49 12.16 57.78 o -17 4 1 99.25 124.84 44.37 o -16 4 1 102.78 107.83 40.65 o -15 4 1 208.46 297.97 50.92 o -14 4 1 14.50 13.00 45.11 o -13 4 1 169.15 176.94 39.28 o -12 4 1 116.26 145.01 28.28 o -11 4 1 27.29 25.63 47.55 o -10 4 1 4.81 9.79 21.45 o -9 4 1 8.34 -2.59 11.88 o -8 4 1 5161.84 5131.91 99.58 o -7 4 1 129.29 130.69 17.00 o -6 4 1 9818.27 9930.41 117.11 o -5 4 1 413.81 421.37 19.90 o -4 4 1 658.31 640.91 27.28 o -3 4 1 3946.04 3665.64 58.69 o -2 4 1 1657.49 1579.37 29.51 o -1 4 1 158.24 202.36 13.07 o 0 4 1 36585.03 37506.47 390.77 o 1 4 1 795.02 802.18 42.72 o 2 4 1 10685.79 10539.26 114.67 o 3 4 1 8173.66 7799.74 96.24 o 4 4 1 1405.48 1620.30 37.98 o 5 4 1 4134.36 4153.87 67.73 o 6 4 1 3168.53 3357.61 64.23 o 7 4 1 1291.07 1318.89 42.22 o 8 4 1 27.85 29.38 13.13 o 9 4 1 288.71 326.02 28.02 o 10 4 1 113.92 114.93 30.41 o 11 4 1 2071.00 2067.89 75.78 o 12 4 1 5.02 -16.90 29.24 o 13 4 1 28.93 29.58 29.45 o 14 4 1 337.90 294.18 49.02 o 15 4 1 35.42 98.56 36.12 o 16 4 1 56.30 15.82 67.00 o 17 4 1 282.32 335.11 89.19 o -17 5 1 90.98 29.34 42.61 o -16 5 1 354.47 423.89 81.20 o -15 5 1 193.56 116.16 39.99 o -14 5 1 527.01 512.72 61.36 o -13 5 1 333.97 351.07 49.57 o -12 5 1 111.20 134.97 24.84 o -11 5 1 1153.57 1182.59 56.36 o -10 5 1 21.96 -0.54 29.03 o -9 5 1 600.77 573.96 36.15 o -8 5 1 2101.41 2279.69 51.69 o -7 5 1 8064.73 8176.72 125.05 o -6 5 1 1022.85 1258.14 36.80 o -5 5 1 13386.14 12298.56 129.56 o -4 5 1 12171.50 11846.49 114.90 o -3 5 1 16721.61 17092.84 164.58 o -2 5 1 36770.90 38118.15 327.49 o -1 5 1 1212.39 1104.91 50.45 o 0 5 1 2294.05 2449.54 58.82 o 1 5 1 8580.45 8911.04 129.49 o 2 5 1 952.67 1181.56 32.31 o 3 5 1 25330.60 25664.59 259.28 o 4 5 1 19589.99 20792.88 233.70 o 5 5 1 17548.00 17618.91 204.48 o 6 5 1 12945.40 11820.11 138.73 o 7 5 1 244.95 182.97 17.58 o 8 5 1 145.40 50.11 18.58 o 9 5 1 324.78 372.12 30.31 o 10 5 1 3683.37 3246.46 91.81 o 11 5 1 35.89 71.74 21.76 o 12 5 1 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