data_2019650 _cell_angle_alpha 90.000 _cell_angle_beta 118.437 _cell_angle_gamma 90.000 _cell_length_a 10.3160 _cell_length_b 19.7793 _cell_length_c 10.6749 _exptl_crystal_F_000 988.00 _reflns_d_resolution_high 0.7487 _cod_data_source_file bg3179Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 120603d in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 236.82 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 5 -20 0 6.46 -15.98 29.68 o 3 -19 0 325.84 459.89 58.77 o 4 -19 0 1508.98 1473.98 113.58 o 5 -19 0 523.24 363.96 59.54 o 6 -19 0 540.98 477.18 65.41 o 7 -19 0 225.10 255.11 55.47 o 2 -18 0 1492.66 1536.04 106.82 o 3 -18 0 2578.64 2747.61 177.79 o 4 -18 0 161.12 195.51 42.79 o 5 -18 0 11.18 18.31 28.54 o 6 -18 0 147.70 168.10 46.68 o 7 -18 0 15.16 5.80 36.86 o 8 -18 0 35.83 19.81 40.45 o 2 -17 0 379.86 410.94 51.52 o 3 -17 0 975.19 976.51 80.55 o 4 -17 0 1021.84 1008.82 84.02 o 5 -17 0 563.38 625.47 65.53 o 6 -17 0 294.72 343.56 56.37 o 7 -17 0 149.17 115.62 43.45 o 8 -17 0 83.01 133.93 47.87 o 9 -17 0 261.95 372.16 64.45 o 1 -16 0 72.32 65.59 27.83 o 2 -16 0 611.96 616.62 59.60 o 3 -16 0 1036.18 1096.55 84.44 o 4 -16 0 485.86 468.75 54.52 o 5 -16 0 119.32 101.85 37.22 o 6 -16 0 16.83 8.62 31.66 o 7 -16 0 61.90 62.42 37.28 o 8 -16 0 227.23 225.37 52.48 o 1 -15 0 1412.06 1439.45 104.48 o 2 -15 0 1072.47 1129.05 82.22 o 3 -15 0 289.35 294.78 42.79 o 4 -15 0 813.38 851.86 71.57 o 5 -15 0 259.46 272.88 46.08 o 6 -15 0 502.81 494.24 58.47 o 7 -15 0 556.29 630.98 68.88 o 8 -15 0 153.47 200.89 49.91 o 1 -14 0 5089.61 5177.69 279.11 o 2 -14 0 557.39 571.68 53.38 o 3 -14 0 194.48 175.88 31.42 o 4 -14 0 1094.68 1233.23 89.94 o 5 -14 0 625.87 648.45 63.61 o 6 -14 0 322.54 317.34 49.19 o 7 -14 0 155.19 154.57 42.85 o 8 -14 0 188.39 245.17 53.08 o 1 -13 0 3215.59 3129.76 187.01 o 2 -13 0 4587.01 4483.28 249.84 o 3 -13 0 560.64 546.18 52.00 o 4 -13 0 774.80 740.85 65.83 o 5 -13 0 848.39 883.28 73.13 o 6 -13 0 1149.29 1182.37 92.22 o 7 -13 0 1450.73 1753.62 124.71 o 8 -13 0 925.39 1142.45 94.07 o 0 -12 0 8735.63 8811.86 486.58 o 1 -12 0 9107.48 9535.18 504.65 o 2 -12 0 596.00 629.12 52.30 o 3 -12 0 564.21 541.81 47.69 o 4 -12 0 2152.03 2215.01 136.62 o 5 -12 0 2461.52 2535.47 154.45 o 6 -12 0 2463.39 2618.95 157.39 o 7 -12 0 549.11 656.71 64.39 o 8 -12 0 67.58 83.72 37.52 o 1 -11 0 2505.06 2295.50 136.44 o 2 -11 0 4915.06 5095.35 264.62 o 3 -11 0 312.75 313.56 40.57 o 4 -11 0 156.39 172.18 20.59 o 5 -11 0 1847.18 1856.91 119.98 o 6 -11 0 1622.58 1839.86 118.37 o 7 -11 0 1964.15 2188.08 137.16 o 8 -11 0 552.18 697.34 68.22 o 0 -10 0 8502.19 9042.68 471.02 o 1 -10 0 2405.01 2253.79 130.82 o 2 -10 0 1248.60 1254.58 51.98 o 3 -10 0 1001.71 1003.80 44.79 o 4 -10 0 196.04 185.31 20.48 o 5 -10 0 1297.50 1193.31 73.40 o 6 -10 0 2497.94 2675.02 155.53 o 7 -10 0 302.69 365.70 49.37 o 8 -10 0 331.54 409.92 53.80 o 1 -9 0 214.97 177.53 20.23 o 2 -9 0 741.42 763.09 37.97 o 3 -9 0 343.55 330.42 22.46 o 4 -9 0 3428.72 3552.31 128.85 o 5 -9 0 3567.71 3786.50 191.44 o 6 -9 0 252.41 349.06 44.04 o 7 -9 0 530.66 641.51 59.24 o 0 -8 0 3514.64 3392.83 191.56 o 1 -8 0 2044.65 2333.41 131.14 o 2 -8 0 3807.77 3723.96 213.07 o 3 -8 0 2632.53 2659.24 99.25 o 4 -8 0 4130.40 4429.64 157.39 o 5 -8 0 119.15 164.78 19.54 o 6 -8 0 2046.25 2033.04 137.85 o 7 -8 0 520.27 588.43 53.92 o 8 -8 0 883.89 869.51 76.00 o 9 -8 0 457.29 587.71 73.73 o 10 -8 0 182.42 229.91 56.19 o 1 -7 0 4205.33 4232.71 153.24 o 2 -7 0 1796.08 1757.81 146.79 o 3 -7 0 4270.74 4352.81 182.46 o 4 -7 0 9493.73 9617.38 316.06 o 5 -7 0 12143.62 12500.13 415.43 o 6 -7 0 998.72 1042.96 43.38 o 7 -7 0 175.92 202.38 26.41 o 8 -7 0 1806.26 1690.91 114.06 o 9 -7 0 776.38 759.46 75.22 o 10 -7 0 583.20 599.92 73.49 o 11 -7 0 289.20 256.60 61.82 o 0 -6 0 9900.45 9820.09 510.99 o 1 -6 0 3908.46 4083.20 159.39 o 2 -6 0 8399.53 8618.37 424.01 o 3 -6 0 5858.71 5773.96 291.31 o 4 -6 0 7041.91 7014.70 194.41 o 5 -6 0 252.33 326.03 26.63 o 6 -6 0 738.29 767.31 32.89 o 7 -6 0 209.82 265.68 28.19 o 8 -6 0 19.58 15.14 26.99 o 9 -6 0 176.31 153.50 44.76 o 10 -6 0 243.88 208.91 53.14 o 11 -6 0 370.71 353.37 67.50 o 1 -5 0 9669.38 10043.12 465.72 o 2 -5 0 1614.19 1701.72 57.20 o 3 -5 0 1076.53 1065.21 76.33 o 4 -5 0 7256.87 7572.15 208.60 o 5 -5 0 9928.25 9888.71 272.78 o 6 -5 0 962.43 927.97 37.55 o 7 -5 0 391.25 407.31 31.74 o 8 -5 0 1360.04 1462.73 103.77 o 9 -5 0 626.66 697.58 73.43 o 10 -5 0 962.27 938.15 90.42 o 11 -5 0 533.25 659.52 89.46 o 0 -4 0 1629.21 1540.56 70.43 o 1 -4 0 3190.37 3065.90 111.29 o 2 -4 0 11136.11 11226.12 595.43 o 3 -4 0 3021.62 3020.93 85.61 o 4 -4 0 3973.16 4098.14 116.53 o 5 -4 0 1375.29 1435.82 47.50 o 6 -4 0 2390.16 2469.72 76.42 o 7 -4 0 660.09 586.46 58.11 o 8 -4 0 448.81 478.38 61.34 o 9 -4 0 20.85 -1.97 35.55 o 10 -4 0 474.22 489.99 71.69 o 11 -4 0 265.37 322.97 65.41 o 1 -3 0 4490.49 4691.74 239.94 o 2 -3 0 224.13 254.68 22.99 o 3 -3 0 2439.82 2475.73 71.70 o 4 -3 0 817.29 831.32 30.03 o 5 -3 0 2378.34 2413.07 73.73 o 6 -3 0 900.80 945.84 37.27 o 7 -3 0 818.34 870.77 72.71 o 8 -3 0 123.82 129.80 39.44 o 9 -3 0 581.33 686.75 73.97 o 10 -3 0 211.48 200.47 56.07 o 11 -3 0 229.09 145.54 53.68 o 1 -2 0 1383.96 1579.49 43.80 o 2 -2 0 3196.57 3186.22 134.99 o 3 -2 0 452.28 466.67 29.92 o 4 -2 0 180.82 191.76 15.06 o 5 -2 0 6332.85 6700.38 187.13 o 6 -2 0 4304.54 4437.04 128.49 o 7 -2 0 865.68 875.08 74.20 o 8 -2 0 392.32 376.89 55.89 o 9 -2 0 23.29 -6.10 35.31 o 10 -2 0 526.07 474.25 73.37 o 11 -2 0 13.23 -5.98 45.54 o 1 -1 0 25746.27 25681.25 791.46 o 2 -1 0 140.03 146.22 8.51 o 3 -1 0 2052.75 2181.88 61.77 o 4 -1 0 2865.93 2814.98 91.34 o 5 -1 0 81.41 87.11 13.36 o 6 -1 0 4485.91 4750.98 137.06 o 7 -1 0 2841.96 3340.47 187.67 o 8 -1 0 758.40 824.45 76.90 o 9 -1 0 686.71 787.83 81.33 o 10 -1 0 370.31 485.20 73.49 o 11 -1 0 24.10 -4.25 41.83 o 2 0 0 442.32 628.38 23.89 o 3 0 0 607.89 530.06 30.00 o 4 0 0 434.70 399.45 17.66 o 5 0 0 2329.59 2199.23 66.26 o 6 0 0 4987.60 5391.40 151.48 o 7 0 0 218.11 285.45 47.87 o 8 0 0 252.94 268.81 49.91 o 9 0 0 99.76 125.43 46.86 o 10 0 0 568.60 581.49 82.76 o 11 0 0 25.41 36.62 45.84 o 12 0 0 35.11 55.17 50.51 o 2 1 0 115.76 127.39 8.16 o 3 1 0 1935.04 2093.87 66.42 o 4 1 0 2838.88 2809.30 100.37 o 5 1 0 86.17 106.27 18.10 o 6 1 0 4405.96 4716.09 158.29 o 7 1 0 2853.53 3014.03 173.00 o 8 1 0 746.56 774.78 74.92 o 9 1 0 553.25 626.49 73.01 o 10 1 0 355.12 366.00 67.86 o 11 1 0 30.25 -8.32 43.92 o 1 2 0 1216.28 1280.87 68.82 o 2 2 0 3157.10 2902.06 142.19 o 3 2 0 599.86 523.07 22.14 o 4 2 0 166.62 162.52 10.10 o 5 2 0 6308.44 6626.46 212.39 o 6 2 0 4211.02 4381.01 231.53 o 7 2 0 786.22 808.83 71.87 o 8 2 0 393.20 390.83 58.23 o 9 2 0 26.93 -18.67 31.06 o 10 2 0 550.39 619.91 81.80 o 11 2 0 6.19 38.24 45.00 o 1 3 0 4129.58 4465.24 158.94 o 2 3 0 208.81 181.98 19.57 o 3 3 0 2488.66 2411.70 80.39 o 4 3 0 857.42 875.31 34.63 o 5 3 0 2309.79 2425.76 84.96 o 6 3 0 971.07 1058.31 78.75 o 7 3 0 754.58 758.50 69.66 o 8 3 0 89.32 56.79 36.44 o 9 3 0 566.62 507.64 69.72 o 10 3 0 205.86 194.73 56.67 o 11 3 0 227.47 174.56 59.30 o 0 4 0 2053.65 1778.16 79.41 o 1 4 0 3455.63 3532.27 111.37 o 2 4 0 10794.80 10608.66 355.96 o 3 4 0 2847.81 2738.99 144.82 o 4 4 0 3878.92 4042.01 131.86 o 5 4 0 1282.71 1323.06 90.12 o 6 4 0 2301.12 2348.94 142.37 o 7 4 0 660.86 614.82 64.99 o 8 4 0 450.17 354.39 56.85 o 9 4 0 20.36 44.70 37.46 o 10 4 0 478.56 415.25 69.66 o 11 4 0 248.38 191.85 62.24 o 1 5 0 10691.25 11421.09 488.25 o 2 5 0 1318.10 1369.47 56.70 o 3 5 0 948.68 768.26 55.06 o 4 5 0 7286.50 7790.71 374.25 o 5 5 0 10086.18 11010.48 511.23 o 6 5 0 829.86 817.33 72.53 o 7 5 0 349.55 322.67 50.81 o 8 5 0 1466.63 1622.63 116.27 o 9 5 0 718.73 724.51 78.09 o 10 5 0 892.32 886.57 92.94 o 11 5 0 524.44 536.61 84.26 o 0 6 0 9747.72 9837.80 455.22 o 1 6 0 4183.25 4369.18 310.55 o 2 6 0 8080.26 8339.35 414.17 o 3 6 0 5536.73 5248.63 184.92 o 4 6 0 7301.42 7062.73 342.90 o 5 6 0 270.39 247.69 38.60 o 6 6 0 650.46 574.91 60.44 o 7 6 0 248.64 257.74 47.10 o 8 6 0 17.85 43.03 35.85 o 9 6 0 179.78 157.09 46.86 o 10 6 0 275.42 300.41 62.42 o 11 6 0 361.14 256.07 64.75 o 1 7 0 4760.90 4805.44 153.04 o 2 7 0 1964.09 1953.88 69.42 o 3 7 0 3888.86 3760.47 141.35 o 4 7 0 9238.92 9217.23 317.20 o 5 7 0 12042.13 12408.94 596.03 o 6 7 0 949.90 991.41 80.19 o 7 7 0 203.39 116.33 38.90 o 8 7 0 1757.65 1656.68 118.49 o 9 7 0 729.76 670.36 75.76 o 10 7 0 586.82 634.63 84.02 o 11 7 0 304.68 307.35 67.44 o 0 8 0 3683.81 3647.52 171.51 o 1 8 0 2116.54 2386.09 118.67 o 2 8 0 3828.79 3958.22 263.94 o 3 8 0 2882.01 2828.54 101.50 o 4 8 0 4300.96 4572.70 160.64 o 5 8 0 117.57 128.76 22.33 o 6 8 0 2133.45 1933.75 84.96 o 7 8 0 429.49 446.96 60.98 o 8 8 0 891.45 781.42 78.57 o 9 8 0 434.53 394.00 64.63 o 10 8 0 209.41 204.24 56.67 o 11 8 0 312.12 322.49 71.27 o 1 9 0 233.71 180.92 26.33 o 2 9 0 944.66 975.86 41.02 o 3 9 0 292.34 284.30 23.22 o 4 9 0 3487.10 3589.15 131.44 o 5 9 0 3729.34 3993.50 145.44 o 6 9 0 238.11 236.55 29.07 o 7 9 0 575.73 508.80 58.32 o 8 9 0 952.08 833.07 101.85 o 9 9 0 275.12 185.35 31.53 o 10 9 0 140.10 81.24 30.34 o 11 9 0 35.31 14.35 18.16 o 0 10 0 8076.50 8809.05 419.26 o 1 10 0 2331.72 2187.79 81.53 o 2 10 0 1176.21 1215.42 52.38 o 3 10 0 973.18 942.65 47.46 o 4 10 0 242.90 223.10 24.13 o 5 10 0 1359.66 1251.09 59.97 o 6 10 0 2472.33 2299.42 99.47 o 7 10 0 256.04 209.07 32.64 o 8 10 0 322.40 254.79 34.72 o 9 10 0 321.65 234.51 33.53 o 10 10 0 111.42 68.80 25.99 o 11 10 0 106.43 77.75 23.59 o 1 11 0 2455.51 2412.18 89.25 o 2 11 0 4501.03 4857.06 378.59 o 3 11 0 355.37 341.22 27.33 o 4 11 0 129.07 155.77 22.19 o 5 11 0 1922.43 1859.88 81.31 o 6 11 0 1418.11 1527.64 90.78 o 7 11 0 1882.07 1822.92 98.74 o 8 11 0 613.37 542.63 95.78 o 9 11 0 115.64 92.09 27.75 o 10 11 0 51.34 8.79 23.70 o 0 12 0 9041.69 9553.49 435.23 o 1 12 0 9056.90 9683.58 324.42 o 2 12 0 507.89 480.64 31.68 o 3 12 0 411.33 349.36 60.71 o 4 12 0 2178.69 2247.84 91.89 o 5 12 0 2460.77 2402.37 99.44 o 6 12 0 2437.90 2319.63 101.62 o 7 12 0 502.31 593.75 45.83 o 8 12 0 50.19 38.09 24.81 o 9 12 0 271.14 222.29 34.93 o 10 12 0 361.85 245.58 67.68 o 1 13 0 3232.21 3391.50 122.20 o 2 13 0 4317.59 4496.28 160.92 o 3 13 0 553.50 504.53 34.21 o 4 13 0 740.51 783.81 45.47 o 5 13 0 860.02 875.01 50.89 o 6 13 0 1183.79 1178.68 63.63 o 7 13 0 1605.16 1622.69 135.66 o 8 13 0 936.77 922.66 60.45 o 9 13 0 361.29 281.59 51.28 o 10 13 0 101.56 103.19 30.01 o 0 14 0 7002.60 7626.68 368.15 o 1 14 0 4822.67 5127.64 333.23 o 2 14 0 447.82 440.70 32.82 o 3 14 0 132.78 125.25 23.52 o 4 14 0 1062.24 1163.20 58.72 o 5 14 0 693.08 690.02 45.19 o 6 14 0 300.74 265.60 34.08 o 7 14 0 183.45 210.04 34.51 o 8 14 0 152.31 128.89 33.04 o 9 14 0 21.56 -7.35 26.11 o 10 14 0 128.98 132.95 33.68 o 1 15 0 1418.28 1723.80 71.90 o 2 15 0 965.41 982.40 50.67 o 3 15 0 253.19 207.40 27.78 o 4 15 0 742.86 728.79 46.44 o 5 15 0 316.45 311.75 35.50 o 6 15 0 526.12 489.72 42.31 o 7 15 0 596.23 583.02 51.55 o 8 15 0 149.37 114.99 39.89 o 9 15 0 60.19 26.15 28.33 o 0 16 0 1423.50 1654.58 101.43 o 1 16 0 50.67 68.45 22.77 o 2 16 0 657.00 628.01 39.73 o 3 16 0 1009.90 963.71 52.41 o 4 16 0 438.29 404.75 41.71 o 5 16 0 120.49 61.90 25.20 o 6 16 0 11.82 -2.60 22.89 o 7 16 0 81.55 61.47 28.32 o 8 16 0 244.79 185.55 35.77 o 9 16 0 16.14 35.47 49.25 o 1 17 0 204.93 147.22 24.41 o 2 17 0 447.71 457.41 36.59 o 3 17 0 949.18 988.20 63.07 o 4 17 0 1029.14 1027.83 57.67 o 5 17 0 532.10 463.40 43.06 o 6 17 0 288.71 292.10 37.98 o 7 17 0 140.72 118.20 66.22 o 8 17 0 80.58 70.32 31.59 o 9 17 0 286.62 271.07 42.33 o 0 18 0 948.81 1011.10 78.33 o 1 18 0 386.13 417.22 34.68 o 2 18 0 1372.40 1403.56 69.38 o 3 18 0 2701.34 2940.98 117.23 o 4 18 0 148.66 148.23 28.27 o 5 18 0 13.84 3.08 33.45 o 6 18 0 162.77 163.21 32.06 o 7 18 0 9.82 -15.04 25.50 o 8 18 0 49.60 56.61 30.06 o 1 19 0 16.28 14.54 20.89 o 2 19 0 670.60 719.77 47.94 o 3 19 0 362.06 503.98 41.02 o 4 19 0 1577.14 1627.34 79.37 o 5 19 0 516.89 485.47 43.81 o 6 19 0 495.30 523.45 54.55 o 7 19 0 210.73 257.16 40.95 o 8 19 0 146.16 134.26 34.79 o 0 20 0 486.07 585.44 61.70 o 1 20 0 6.79 -20.85 20.85 o 2 20 0 477.58 472.27 57.81 o 3 20 0 2268.56 2440.54 105.71 o 4 20 0 115.83 115.25 29.49 o 5 20 0 7.16 -19.97 25.46 o 6 20 0 50.53 41.73 27.38 o 7 20 0 13.34 -24.64 25.85 o 1 21 0 70.82 47.27 26.16 o 2 21 0 404.05 446.84 43.05 o 3 21 0 76.13 139.65 31.39 o 4 21 0 555.33 572.42 48.38 o 5 21 0 28.15 27.53 26.05 o 6 21 0 48.66 42.48 29.46 o 7 21 0 4.35 18.52 29.21 o 0 22 0 58.56 86.95 43.45 o 1 22 0 89.64 108.62 29.87 o 2 22 0 33.96 39.25 30.43 o 3 22 0 58.34 62.75 26.86 o 4 22 0 83.34 73.54 28.78 o 5 22 0 69.98 51.64 29.99 o 6 22 0 11.20 -8.36 26.85 o 1 23 0 102.41 110.49 30.84 o 2 23 0 258.50 282.53 43.89 o 3 23 0 0.37 -24.57 24.57 o 4 23 0 85.83 91.87 31.39 o 5 23 0 69.89 39.23 35.85 o 0 24 0 664.59 706.74 76.90 o 1 24 0 641.53 782.00 58.62 o 2 24 0 130.59 133.31 34.12 o 3 24 0 5.53 1.19 27.29 o 4 24 0 115.12 156.72 36.46 o 5 24 0 72.02 58.79 31.31 o 1 25 0 116.74 206.78 49.70 o 2 25 0 393.11 452.72 51.32 o 3 25 0 59.12 52.73 30.01 o 0 26 0 141.60 120.88 51.34 o 1 26 0 222.25 270.50 44.81 o 2 26 0 126.04 109.95 36.70 o -7 -22 1 10.44 -22.62 34.29 o -6 -22 1 80.96 90.36 45.00 o -5 -22 1 39.23 29.38 36.98 o -4 -22 1 28.45 39.08 38.48 o -7 -21 1 162.88 140.57 47.28 o -6 -21 1 110.38 134.11 46.80 o -5 -21 1 19.84 61.88 38.24 o -4 -21 1 332.68 297.24 55.23 o -3 -21 1 156.40 66.37 39.38 o -8 -20 1 12.65 66.25 43.21 o -7 -20 1 344.12 320.34 61.22 o -6 -20 1 797.13 827.68 85.69 o -5 -20 1 535.42 516.44 67.98 o -4 -20 1 811.71 829.06 80.49 o -3 -20 1 101.39 108.49 38.90 o -2 -20 1 120.54 83.78 37.46 o -8 -19 1 55.89 81.09 45.54 o -7 -19 1 319.46 325.72 62.66 o -6 -19 1 105.66 99.76 42.73 o -5 -19 1 122.07 147.39 44.40 o -4 -19 1 1120.11 1016.54 89.94 o -3 -19 1 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