data_2019652 _cell_angle_alpha 90.000 _cell_angle_beta 95.173 _cell_angle_gamma 90.000 _cell_length_a 10.0019 _cell_length_b 9.0293 _cell_length_c 39.2513 _exptl_crystal_F_000 1624.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file eg3166RhBICPnbdBF4sup2.hkl _cod_data_source_block RhBICPnbdBF4 #BEGIN Tags that were not found in dictionaries: _shelx_title ' ks452abs2 in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 331.24 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 -10 0 794.87 583.48 263.23 o 1 -10 0 769.11 597.50 186.09 o 2 -10 0 266.36 115.50 186.78 o 3 -10 0 1509.80 1591.42 204.35 o 4 -10 0 232.04 228.77 206.59 o 1 -9 0 606.13 495.80 166.29 o 2 -9 0 276.99 212.87 139.57 o 3 -9 0 940.62 963.05 177.52 o 4 -9 0 1333.13 1212.65 138.01 o 5 -9 0 231.11 302.94 159.55 o 6 -9 0 1736.38 1523.06 312.03 o 0 -8 0 6880.94 6791.23 255.55 o 1 -8 0 54.45 22.90 150.40 o 2 -8 0 250.35 198.39 149.99 o 3 -8 0 7.85 48.05 135.06 o 4 -8 0 345.69 421.70 171.06 o 5 -8 0 186.44 182.69 135.37 o 6 -8 0 1305.06 1414.13 140.05 o 7 -8 0 436.65 346.90 147.37 o 1 -7 0 316.11 311.98 143.09 o 2 -7 0 1666.88 1702.11 131.94 o 3 -7 0 227.59 213.01 157.34 o 4 -7 0 4024.90 4162.71 131.14 o 5 -7 0 25.22 71.28 122.87 o 6 -7 0 3686.66 3991.59 145.82 o 7 -7 0 70.48 73.96 135.65 o 8 -7 0 109.86 54.61 142.81 o 0 -6 0 2592.90 2325.16 213.87 o 1 -6 0 1022.11 913.02 121.78 o 2 -6 0 2393.86 2380.06 143.72 o 3 -6 0 1322.39 1279.60 115.26 o 4 -6 0 1260.53 1651.49 366.09 o 5 -6 0 3661.04 3621.20 144.37 o 6 -6 0 1858.32 1921.96 138.32 o 7 -6 0 527.96 366.93 138.90 o 8 -6 0 1746.56 1810.23 186.01 o 9 -6 0 226.43 170.47 156.51 o 1 -5 0 1794.00 1582.61 122.89 o 2 -5 0 400.24 343.52 107.88 o 3 -5 0 3625.12 3758.48 143.21 o 4 -5 0 2891.14 2570.93 158.94 o 5 -5 0 1898.96 2104.98 123.57 o 6 -5 0 1992.09 1708.15 147.08 o 7 -5 0 1093.76 1016.99 145.02 o 8 -5 0 769.25 801.54 140.62 o 9 -5 0 2099.14 2156.59 324.78 o 10 -5 0 408.55 284.18 178.87 o 0 -4 0 60.92 70.19 190.84 o 1 -4 0 4901.39 5225.49 172.49 o 2 -4 0 100.17 153.34 106.56 o 3 -4 0 14904.08 15845.66 180.63 o 4 -4 0 317.42 332.54 100.51 o 5 -4 0 9982.26 10872.31 325.46 o 6 -4 0 9.41 37.49 139.03 o 7 -4 0 2060.43 2278.72 143.47 o 8 -4 0 489.20 504.39 125.97 o 9 -4 0 646.65 743.68 169.59 o 10 -4 0 445.45 519.86 195.87 o 1 -3 0 30036.69 28708.89 234.94 o 2 -3 0 596.26 479.21 112.10 o 3 -3 0 5179.44 5435.74 140.41 o 4 -3 0 1487.53 1311.47 172.95 o 5 -3 0 1149.44 1391.52 133.58 o 6 -3 0 660.38 596.48 140.41 o 7 -3 0 545.42 716.66 145.45 o 8 -3 0 373.36 423.70 189.00 o 9 -3 0 4746.03 5455.94 858.92 o 10 -3 0 151.36 100.99 174.21 o 11 -3 0 787.62 801.60 348.70 o 0 -2 0 71672.64 63473.66 772.13 o 1 -2 0 6476.87 6068.14 289.07 o 2 -2 0 1929.44 2006.49 140.31 o 3 -2 0 5219.01 5018.59 184.74 o 4 -2 0 5062.39 6015.06 246.01 o 5 -2 0 8812.24 9826.93 628.11 o 6 -2 0 1251.31 1373.96 192.84 o 7 -2 0 715.22 766.33 188.10 o 8 -2 0 2264.70 2254.52 206.99 o 9 -2 0 1241.74 1155.99 223.17 o 10 -2 0 708.08 638.09 146.82 o 11 -2 0 368.17 439.51 155.21 o 1 -1 0 6285.77 6283.52 551.06 o 2 -1 0 22341.27 24721.11 844.56 o 3 -1 0 608.60 444.26 149.69 o 4 -1 0 22899.57 26155.90 1080.32 o 5 -1 0 1683.03 1678.21 195.89 o 6 -1 0 2312.33 2641.56 201.06 o 7 -1 0 482.33 457.69 197.74 o 8 -1 0 640.39 796.71 154.59 o 9 -1 0 672.83 587.00 139.94 o 10 -1 0 144.65 157.86 141.08 o 11 -1 0 490.04 390.22 156.11 o 1 0 0 67.68 9.65 230.62 o 2 0 0 335.18 359.16 189.71 o 3 0 0 0.02 -65.06 206.09 o 4 0 0 3146.00 3271.48 152.96 o 5 0 0 29.88 16.19 137.22 o 6 0 0 324.64 508.34 143.37 o 7 0 0 1018.54 1298.05 161.27 o 8 0 0 3860.28 4084.78 168.23 o 9 0 0 59.79 74.69 151.79 o 10 0 0 4946.64 4905.54 168.70 o 11 0 0 395.04 424.83 154.55 o 1 1 0 6380.35 6237.14 814.64 o 2 1 0 23855.96 24896.67 844.37 o 3 1 0 565.65 445.02 146.82 o 4 1 0 22703.73 23118.17 853.43 o 5 1 0 1695.29 1560.99 145.53 o 6 1 0 2617.94 2808.90 172.79 o 7 1 0 508.33 544.51 161.59 o 8 1 0 624.18 695.97 150.12 o 9 1 0 644.57 701.59 151.66 o 10 1 0 141.91 251.44 154.38 o 11 1 0 481.08 340.63 166.28 o 0 2 0 69288.12 60785.46 749.10 o 1 2 0 6427.74 6113.00 458.65 o 2 2 0 1750.49 1889.43 148.35 o 3 2 0 5076.13 4988.92 189.88 o 4 2 0 5013.83 5620.85 169.54 o 5 2 0 8689.40 8674.13 258.83 o 6 2 0 1372.05 1389.10 164.75 o 7 2 0 638.35 549.99 157.37 o 8 2 0 2157.91 2105.88 366.87 o 9 2 0 1244.82 1169.71 146.06 o 10 2 0 681.89 684.21 159.29 o 11 2 0 384.59 457.50 159.73 o 1 3 0 30408.98 29353.84 259.22 o 2 3 0 574.26 447.21 114.37 o 3 3 0 4853.12 4984.93 147.29 o 4 3 0 1480.77 1369.46 133.71 o 5 3 0 1087.15 1113.30 140.64 o 6 3 0 652.98 669.24 142.95 o 7 3 0 522.41 637.05 140.63 o 8 3 0 379.39 369.64 130.09 o 9 3 0 4584.90 4437.26 213.73 o 10 3 0 141.05 102.29 132.19 o 11 3 0 777.99 742.28 171.73 o 0 4 0 69.85 123.90 117.32 o 1 4 0 5083.68 5452.59 114.13 o 2 4 0 108.23 197.41 108.84 o 3 4 0 14999.67 15903.09 397.66 o 4 4 0 321.80 426.95 118.80 o 5 4 0 9698.24 10713.84 308.02 o 6 4 0 9.14 -17.31 159.23 o 7 4 0 2130.82 2225.83 157.03 o 8 4 0 483.05 416.55 151.27 o 9 4 0 609.32 726.84 135.28 o 10 4 0 441.18 352.05 139.79 o 1 5 0 1752.22 1542.96 98.34 o 2 5 0 465.25 437.47 111.73 o 3 5 0 3784.17 3983.94 164.48 o 4 5 0 2878.34 2600.88 180.31 o 5 5 0 1914.56 2014.83 140.19 o 6 5 0 1929.24 1860.61 160.55 o 7 5 0 1037.85 894.56 157.99 o 8 5 0 780.91 748.44 159.51 o 9 5 0 2070.74 2096.04 183.35 o 10 5 0 439.03 236.22 140.32 o 0 6 0 2386.63 2149.65 168.92 o 1 6 0 1017.74 864.15 121.93 o 2 6 0 2332.49 2195.53 113.58 o 3 6 0 1480.50 1393.20 123.24 o 4 6 0 1229.35 1081.57 136.38 o 5 6 0 3470.60 3707.26 158.34 o 6 6 0 1796.02 1858.76 151.72 o 7 6 0 532.16 622.80 152.01 o 8 6 0 1795.72 2040.78 236.51 o 9 6 0 221.70 212.04 157.70 o 1 7 0 318.98 299.26 99.60 o 2 7 0 1583.89 1522.00 129.17 o 3 7 0 244.90 256.58 116.58 o 4 7 0 4267.23 4448.81 158.32 o 5 7 0 26.35 116.39 144.97 o 6 7 0 3720.93 4022.91 173.58 o 7 7 0 71.00 -24.05 165.29 o 8 7 0 110.94 45.44 156.55 o 0 8 0 6744.48 6707.10 201.28 o 1 8 0 56.88 13.16 105.53 o 2 8 0 356.07 333.46 106.97 o 3 8 0 10.14 39.08 133.05 o 4 8 0 384.34 355.30 116.02 o 5 8 0 195.40 173.12 150.54 o 6 8 0 1277.95 1360.55 161.86 o 7 8 0 434.66 488.27 154.03 o 1 9 0 560.40 373.47 109.76 o 2 9 0 269.45 281.46 113.06 o 3 9 0 947.98 896.57 144.21 o 4 9 0 1344.08 1225.08 149.95 o 5 9 0 223.30 177.65 151.88 o 6 9 0 1783.99 1652.07 165.14 o 0 10 0 826.90 680.41 161.85 o 1 10 0 765.75 724.27 117.90 o 2 10 0 278.76 238.61 126.54 o 3 10 0 1434.14 1600.79 126.51 o 4 10 0 238.66 147.52 142.37 o -4 -10 1 1121.47 992.30 211.57 o -3 -10 1 67.93 86.74 189.19 o -2 -10 1 1555.16 1504.13 193.72 o -1 -10 1 33.48 -4.42 179.90 o 0 -10 1 888.93 802.72 186.90 o 1 -10 1 645.77 507.23 154.28 o 2 -10 1 350.92 441.95 157.72 o 3 -10 1 479.58 471.47 195.36 o 4 -10 1 1543.92 1451.47 214.20 o -6 -9 1 1039.91 863.89 295.03 o -5 -9 1 1187.48 991.19 166.22 o -4 -9 1 369.03 348.69 153.33 o -3 -9 1 3234.36 2906.74 204.24 o -2 -9 1 39.63 137.47 169.23 o -1 -9 1 2127.81 1737.72 145.93 o 0 -9 1 414.31 221.27 164.41 o 1 -9 1 197.97 265.44 164.69 o 2 -9 1 317.11 278.04 174.17 o 3 -9 1 134.51 64.78 175.56 o 4 -9 1 792.18 872.75 158.00 o 5 -9 1 1051.67 1044.74 164.52 o 6 -9 1 580.72 437.58 199.98 o -7 -8 1 3643.94 3967.47 503.10 o -6 -8 1 336.04 308.12 144.87 o -5 -8 1 1120.37 1197.06 139.45 o -4 -8 1 298.39 182.78 140.74 o -3 -8 1 1837.97 1873.56 125.70 o -2 -8 1 65.41 4.67 153.50 o -1 -8 1 83.37 82.96 150.83 o 0 -8 1 160.24 86.15 151.62 o 1 -8 1 3023.71 3042.64 167.81 o 2 -8 1 111.69 48.72 156.03 o 3 -8 1 1600.99 1864.73 140.38 o 4 -8 1 8.46 31.65 172.09 o 5 -8 1 1326.85 1287.75 133.41 o 6 -8 1 201.84 169.13 134.96 o 7 -8 1 581.64 544.85 153.33 o -9 -7 1 1163.24 984.84 183.93 o -8 -7 1 50.40 43.67 142.45 o -7 -7 1 109.66 160.84 135.05 o -6 -7 1 192.89 166.17 138.02 o -5 -7 1 1729.25 2002.02 151.34 o -4 -7 1 265.70 365.53 116.78 o -3 -7 1 8644.56 9171.73 179.78 o -2 -7 1 63.11 34.55 146.58 o -1 -7 1 5700.17 5838.19 169.84 o 0 -7 1 209.22 227.60 115.04 o 1 -7 1 467.64 562.60 142.70 o 2 -7 1 134.30 70.72 122.78 o 3 -7 1 949.49 1180.49 173.49 o 4 -7 1 376.42 385.34 124.51 o 5 -7 1 3613.44 3955.90 141.25 o 6 -7 1 425.41 433.71 136.61 o 7 -7 1 2809.53 2886.94 166.06 o 8 -7 1 46.31 232.68 151.31 o -9 -6 1 179.17 219.12 169.87 o -8 -6 1 173.54 232.95 143.78 o -7 -6 1 3145.20 3242.83 308.76 o -6 -6 1 240.43 284.38 131.03 o -5 -6 1 3135.88 3184.63 134.94 o -4 -6 1 7518.12 7286.54 345.58 o -3 -6 1 1972.39 2152.36 142.79 o -2 -6 1 1841.95 1549.43 128.18 o -1 -6 1 330.55 202.41 142.31 o 0 -6 1 548.21 358.50 141.90 o 1 -6 1 6852.53 6696.67 178.37 o 2 -6 1 21.37 158.75 137.16 o 3 -6 1 6037.14 5723.84 138.07 o 4 -6 1 3310.15 3142.44 133.70 o 5 -6 1 1584.57 1664.72 153.40 o 6 -6 1 1985.52 1888.95 139.63 o 7 -6 1 714.96 743.95 140.64 o 8 -6 1 476.96 329.94 141.99 o 9 -6 1 1290.32 1212.05 174.96 o -10 -5 1 93.15 53.43 193.02 o -9 -5 1 1337.70 1248.43 155.11 o -8 -5 1 1252.80 1390.55 141.58 o -7 -5 1 581.35 668.22 137.03 o -6 -5 1 4210.68 4361.28 156.52 o -5 -5 1 106.77 53.67 126.75 o -4 -5 1 4215.83 4362.65 204.44 o -3 -5 1 3950.40 3786.72 467.51 o -2 -5 1 5320.63 5034.31 127.06 o -1 -5 1 364.94 110.17 115.50 o 0 -5 1 2455.80 2433.29 148.90 o 1 -5 1 383.65 261.73 116.60 o 2 -5 1 9057.17 9132.19 143.86 o 3 -5 1 563.55 516.46 119.86 o 4 -5 1 9382.22 9279.00 263.10 o 5 -5 1 546.72 496.33 118.28 o 6 -5 1 1372.71 1321.93 130.18 o 7 -5 1 1142.83 1097.49 132.33 o 8 -5 1 2032.07 2018.58 217.04 o 9 -5 1 558.10 547.88 146.09 o 10 -5 1 1081.91 910.63 191.06 o -11 -4 1 130.63 199.73 199.58 o -10 -4 1 3064.30 3197.66 568.08 o -9 -4 1 294.74 375.70 167.38 o -8 -4 1 684.73 775.55 135.14 o -7 -4 1 175.77 198.56 129.08 o -6 -4 1 227.99 267.01 139.61 o -5 -4 1 258.31 258.58 129.72 o -4 -4 1 3596.33 3738.03 121.53 o -3 -4 1 261.80 263.15 110.58 o -2 -4 1 16211.05 16324.55 173.56 o -1 -4 1 15.60 68.48 112.62 o 0 -4 1 11164.81 11383.58 206.67 o 1 -4 1 208.58 249.31 139.57 o 2 -4 1 3256.91 3308.59 119.99 o 3 -4 1 180.37 173.58 109.53 o 4 -4 1 8206.58 9039.03 189.02 o 5 -4 1 182.78 221.62 130.45 o 6 -4 1 490.38 535.28 135.20 o 7 -4 1 301.85 419.95 131.16 o 8 -4 1 4625.89 4911.27 366.93 o 9 -4 1 444.00 372.06 169.65 o 10 -4 1 194.80 124.96 175.51 o -11 -3 1 98.39 -21.80 187.35 o -10 -3 1 702.46 826.48 318.37 o -9 -3 1 587.00 483.96 167.71 o -8 -3 1 3317.52 3424.85 221.27 o -7 -3 1 192.83 126.33 143.12 o -6 -3 1 5881.28 6193.86 203.10 o -5 -3 1 182.29 264.27 119.35 o -4 -3 1 9925.50 11103.88 226.85 o -3 -3 1 1762.25 1670.47 129.15 o -2 -3 1 81.22 137.51 108.71 o -1 -3 1 1848.66 1854.60 115.99 o 0 -3 1 7649.64 7228.74 198.92 o 1 -3 1 1398.32 1256.86 115.99 o 2 -3 1 3163.12 2851.26 122.30 o 3 -3 1 1057.14 1040.90 119.80 o 4 -3 1 18810.59 20683.75 232.07 o 5 -3 1 329.31 305.50 131.49 o 6 -3 1 356.35 595.56 144.29 o 7 -3 1 182.36 245.15 144.07 o 8 -3 1 1597.24 1920.97 170.20 o 9 -3 1 546.12 535.46 169.64 o 10 -3 1 2359.29 2739.05 562.88 o 11 -3 1 101.77 120.69 184.71 o -11 -2 1 69.08 8.49 162.23 o -10 -2 1 1813.81 1795.58 181.62 o -9 -2 1 591.87 525.13 197.21 o -8 -2 1 925.55 952.88 194.89 o -7 -2 1 2337.70 2555.95 204.53 o -6 -2 1 739.13 1120.12 269.70 o -5 -2 1 4939.48 5007.91 351.29 o -4 -2 1 6071.22 6490.13 437.40 o -3 -2 1 133.40 129.48 116.60 o -2 -2 1 5362.20 5116.13 192.34 o -1 -2 1 4140.62 4235.47 170.50 o 0 -2 1 41012.75 37582.49 556.48 o 1 -2 1 27456.31 25220.43 578.77 o 2 -2 1 7988.09 7752.11 199.97 o 3 -2 1 9751.99 9459.64 448.96 o 4 -2 1 8886.32 9110.05 618.43 o 5 -2 1 2889.49 3119.82 172.38 o 6 -2 1 2304.43 2480.06 219.07 o 7 -2 1 912.61 1113.22 196.29 o 8 -2 1 1075.36 1228.40 194.77 o 9 -2 1 1355.33 1123.20 205.30 o 10 -2 1 385.04 445.92 148.75 o 11 -2 1 258.80 60.64 161.22 o -11 -1 1 1452.94 1491.57 204.99 o -10 -1 1 195.81 147.21 156.01 o -9 -1 1 534.42 548.35 160.54 o -8 -1 1 641.34 494.16 166.40 o -7 -1 1 282.15 396.08 206.78 o -6 -1 1 2634.25 2599.46 185.94 o -5 -1 1 802.78 881.78 173.71 o -4 -1 1 1587.44 1601.80 184.00 o -3 -1 1 6693.06 7284.98 193.49 o -2 -1 1 5949.55 5751.58 221.94 o -1 -1 1 62541.89 61881.81 1980.53 o 0 -1 1 4258.61 3000.60 244.64 o 1 -1 1 8498.39 8009.81 227.15 o 2 -1 1 454.40 873.08 190.01 o 3 -1 1 775.69 1011.11 144.46 o 4 -1 1 3932.74 4095.67 307.81 o 5 -1 1 11555.99 12745.89 239.81 o 6 -1 1 1249.14 1255.05 199.25 o 7 -1 1 2068.90 2281.89 226.20 o 8 -1 1 556.66 535.24 175.53 o 9 -1 1 1657.19 1693.35 149.02 o 10 -1 1 343.30 365.15 144.91 o 11 -1 1 99.83 58.17 153.56 o -11 0 1 553.79 496.28 160.21 o -10 0 1 251.57 320.79 145.86 o -9 0 1 3330.03 3381.82 176.61 o -8 0 1 223.85 225.01 153.35 o -7 0 1 13851.76 14158.89 341.38 o -6 0 1 110.42 52.58 141.26 o -5 0 1 4647.31 4259.13 158.92 o -4 0 1 218.54 351.44 174.77 o -3 0 1 4198.10 4521.91 283.35 o -2 0 1 34.98 64.91 193.59 o -1 0 1 344.60 516.82 295.44 o 1 0 1 68767.37 62191.73 736.04 o 2 0 1 4.41 24.15 180.17 o 3 0 1 8495.71 8524.33 280.74 o 4 0 1 748.14 842.25 152.14 o 5 0 1 4350.41 4697.41 160.05 o 6 0 1 31.53 -46.39 160.61 o 7 0 1 1279.17 1443.94 153.21 o 8 0 1 37.11 202.22 159.75 o 9 0 1 3.54 197.23 147.89 o 10 0 1 208.26 238.11 146.69 o 11 0 1 1756.27 1861.69 168.73 o -11 1 1 1509.39 1800.01 167.96 o -10 1 1 189.74 149.41 143.52 o -9 1 1 505.85 545.69 154.29 o -8 1 1 604.48 445.07 172.45 o -7 1 1 255.28 216.85 165.70 o -6 1 1 2667.45 2353.20 207.47 o -5 1 1 810.86 670.30 130.88 o -4 1 1 1600.71 1380.57 158.80 o -3 1 1 6443.09 6534.24 191.66 o -2 1 1 5960.32 5698.16 464.43 o -1 1 1 63400.28 62726.12 2537.77 o 1 1 1 8290.55 7735.85 288.59 o 2 1 1 340.20 996.38 319.46 o 3 1 1 786.30 990.47 156.71 o 4 1 1 3892.41 3440.85 159.71 o 5 1 1 11346.39 10913.20 277.28 o 6 1 1 1283.33 1325.83 171.62 o 7 1 1 1971.99 2155.75 170.01 o 8 1 1 518.28 707.06 156.47 o 9 1 1 1674.47 1637.92 150.42 o 10 1 1 321.07 315.50 146.60 o 11 1 1 105.27 73.17 164.15 o -11 2 1 77.38 138.63 155.33 o -10 2 1 1740.63 1576.56 234.45 o -9 2 1 582.06 531.51 150.24 o -8 2 1 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