#------------------------------------------------------------------------------ #$Date: 2016-04-06 16:30:44 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181866 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/96/2019653.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2019653 _cell_angle_alpha 90.000 _cell_angle_beta 108.265 _cell_angle_gamma 90.000 _cell_length_a 10.2285 _cell_length_b 13.9823 _cell_length_c 14.5131 _exptl_crystal_F_000 916.00 _reflns_d_resolution_high 0.7501 _cod_data_source_file eg3166RhBICPcodBF4sup3.hkl _cod_data_source_block RhBICPcodBF4 #BEGIN Tags that were not found in dictionaries: _shelx_title ' AX0388abs in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 164.33 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 -18 0 280.53 273.55 23.59 o 1 -18 0 101.84 89.92 12.69 o 2 -18 0 78.50 82.90 18.41 o 3 -18 0 112.95 126.45 16.73 o 1 -17 0 68.72 87.53 15.43 o 2 -17 0 61.40 73.90 12.93 o 3 -17 0 512.14 546.21 23.52 o 4 -17 0 496.24 570.05 26.15 o 5 -17 0 434.33 465.98 24.95 o 0 -16 0 909.70 912.81 34.66 o 1 -16 0 869.71 854.89 21.63 o 2 -16 0 688.25 703.17 20.29 o 3 -16 0 73.82 64.95 11.75 o 4 -16 0 452.40 438.78 20.55 o 5 -16 0 454.89 429.10 19.68 o 6 -16 0 906.88 956.32 27.73 o 1 -15 0 431.23 459.65 15.34 o 2 -15 0 1223.50 1265.97 22.39 o 3 -15 0 1540.11 1594.92 32.36 o 4 -15 0 1141.76 1118.05 25.80 o 5 -15 0 800.34 808.25 22.32 o 6 -15 0 34.33 46.78 9.79 o 7 -15 0 709.91 672.45 26.06 o 0 -14 0 1943.34 1965.01 55.16 o 1 -14 0 1969.97 1964.98 27.41 o 2 -14 0 568.97 595.44 14.89 o 3 -14 0 179.28 180.63 9.60 o 4 -14 0 257.45 295.14 14.26 o 5 -14 0 190.82 201.69 12.65 o 6 -14 0 1174.45 1155.15 26.25 o 7 -14 0 701.62 738.64 23.77 o 8 -14 0 614.88 601.65 27.09 o 1 -13 0 567.44 626.56 13.57 o 2 -13 0 3066.61 3031.06 37.33 o 3 -13 0 1568.43 1591.17 22.19 o 4 -13 0 554.10 537.00 15.23 o 5 -13 0 296.75 292.22 13.96 o 6 -13 0 18.10 18.11 8.37 o 7 -13 0 213.29 250.87 14.95 o 8 -13 0 249.13 254.94 19.27 o 9 -13 0 594.29 578.52 21.90 o 0 -12 0 1256.07 1327.82 33.74 o 1 -12 0 1780.79 1808.50 26.90 o 2 -12 0 452.92 427.07 10.64 o 3 -12 0 526.64 501.16 11.21 o 4 -12 0 820.12 856.41 16.24 o 5 -12 0 1270.58 1242.53 25.17 o 6 -12 0 1482.71 1496.26 28.93 o 7 -12 0 382.89 439.10 17.48 o 8 -12 0 65.10 64.34 9.53 o 9 -12 0 23.01 4.35 8.74 o 1 -11 0 388.55 361.99 8.62 o 2 -11 0 2559.08 2601.24 29.63 o 3 -11 0 1089.63 1120.29 16.44 o 4 -11 0 518.97 482.12 11.29 o 5 -11 0 199.09 215.34 10.22 o 6 -11 0 491.63 527.25 14.92 o 7 -11 0 254.33 246.73 13.85 o 8 -11 0 448.23 470.46 18.68 o 9 -11 0 1654.26 1655.67 32.52 o 10 -11 0 471.04 517.39 23.44 o 0 -10 0 4825.36 4955.74 87.31 o 1 -10 0 2721.89 2794.66 29.85 o 2 -10 0 188.15 200.15 8.43 o 3 -10 0 307.39 296.44 9.06 o 4 -10 0 2253.57 2099.01 26.56 o 5 -10 0 783.87 827.75 16.32 o 6 -10 0 1050.05 1046.32 20.37 o 7 -10 0 616.25 636.75 17.43 o 8 -10 0 441.06 488.47 17.87 o 9 -10 0 71.34 99.79 11.87 o 10 -10 0 684.76 729.16 23.06 o 1 -9 0 1513.21 1388.87 17.59 o 2 -9 0 2354.17 2411.29 26.69 o 3 -9 0 2166.33 2132.59 26.44 o 4 -9 0 1883.30 1951.99 24.60 o 5 -9 0 363.26 370.16 10.02 o 6 -9 0 310.77 299.31 11.06 o 7 -9 0 44.72 43.91 7.39 o 8 -9 0 1363.72 1367.90 26.84 o 9 -9 0 1011.18 1029.37 26.72 o 10 -9 0 636.93 650.25 21.59 o 11 -9 0 151.56 153.11 15.29 o 0 -8 0 9398.92 9525.17 120.88 o 1 -8 0 1992.48 2078.99 21.96 o 2 -8 0 6610.02 6534.68 64.66 o 3 -8 0 233.50 208.69 7.01 o 4 -8 0 680.38 656.91 11.64 o 5 -8 0 1529.85 1511.40 21.36 o 6 -8 0 2360.78 2324.15 33.90 o 7 -8 0 532.49 547.31 15.13 o 8 -8 0 668.48 706.52 17.97 o 9 -8 0 85.98 90.50 11.85 o 10 -8 0 43.10 51.07 9.83 o 11 -8 0 220.23 223.87 17.63 o 1 -7 0 911.47 879.91 12.39 o 2 -7 0 2753.66 2747.96 36.06 o 3 -7 0 3823.08 3734.52 42.73 o 4 -7 0 3155.54 3095.33 34.41 o 5 -7 0 3369.46 3147.19 33.64 o 6 -7 0 3.47 8.25 5.64 o 7 -7 0 564.21 562.00 15.09 o 8 -7 0 884.45 915.77 22.09 o 9 -7 0 721.46 732.54 19.96 o 10 -7 0 252.20 234.43 13.91 o 11 -7 0 236.33 252.71 16.85 o 12 -7 0 56.04 58.10 10.49 o 0 -6 0 5548.01 5057.14 96.55 o 1 -6 0 1004.85 946.03 15.64 o 2 -6 0 2420.78 2368.58 32.16 o 3 -6 0 400.21 450.33 9.55 o 4 -6 0 2654.34 2830.57 31.20 o 5 -6 0 1681.12 1684.38 20.93 o 6 -6 0 5886.48 5857.53 67.90 o 7 -6 0 1828.28 1833.11 28.02 o 8 -6 0 153.80 184.96 10.62 o 9 -6 0 217.00 215.88 11.73 o 10 -6 0 139.83 137.77 10.35 o 11 -6 0 523.69 514.80 18.09 o 12 -6 0 191.22 200.54 18.01 o 1 -5 0 592.65 607.70 11.20 o 2 -5 0 4876.80 4741.30 63.86 o 3 -5 0 1022.76 959.04 14.97 o 4 -5 0 2873.53 2766.97 31.54 o 5 -5 0 1272.79 1275.95 17.39 o 6 -5 0 102.92 120.10 5.91 o 7 -5 0 734.57 746.88 17.77 o 8 -5 0 2276.05 2310.82 39.72 o 9 -5 0 325.47 347.24 12.74 o 10 -5 0 108.68 84.16 8.76 o 11 -5 0 4.83 10.01 7.61 o 12 -5 0 29.92 40.68 10.74 o 0 -4 0 26195.79 25838.22 409.49 o 1 -4 0 4160.58 4304.10 53.03 o 2 -4 0 3628.24 3676.80 45.82 o 3 -4 0 2432.85 2576.29 33.70 o 4 -4 0 1505.19 1588.00 21.09 o 5 -4 0 3160.45 3325.61 35.21 o 6 -4 0 6029.77 6297.46 67.88 o 7 -4 0 1455.97 1469.61 22.62 o 8 -4 0 79.68 84.60 6.85 o 9 -4 0 314.31 324.62 11.14 o 10 -4 0 988.87 984.65 20.49 o 11 -4 0 1405.58 1400.24 26.57 o 12 -4 0 816.09 742.15 26.39 o 1 -3 0 816.96 848.21 13.40 o 2 -3 0 5239.68 5351.49 64.51 o 3 -3 0 11034.38 11305.95 126.01 o 4 -3 0 3697.36 3994.82 50.47 o 5 -3 0 53.32 53.90 3.51 o 6 -3 0 143.83 125.84 4.99 o 7 -3 0 1258.01 1271.26 21.12 o 8 -3 0 2317.41 2337.42 29.36 o 9 -3 0 752.38 699.62 15.27 o 10 -3 0 1571.05 1589.95 27.75 o 11 -3 0 508.61 460.57 14.71 o 12 -3 0 157.69 156.74 14.92 o 0 -2 0 14144.99 14416.70 227.30 o 1 -2 0 3077.65 3180.67 42.16 o 2 -2 0 13336.30 14197.50 157.56 o 3 -2 0 1845.71 1962.56 24.98 o 4 -2 0 6810.22 6888.97 82.96 o 5 -2 0 412.44 410.48 7.62 o 6 -2 0 3219.07 3336.02 36.39 o 7 -2 0 232.53 225.47 9.12 o 8 -2 0 1406.73 1322.82 23.69 o 9 -2 0 684.88 671.25 17.19 o 10 -2 0 503.51 473.78 14.53 o 11 -2 0 1313.16 1285.99 28.75 o 12 -2 0 757.66 795.00 26.83 o 1 -1 0 11706.48 11810.13 130.49 o 2 -1 0 8755.51 9001.56 104.29 o 3 -1 0 7046.01 7396.43 89.68 o 4 -1 0 5685.89 5675.95 68.51 o 5 -1 0 904.71 898.44 12.65 o 6 -1 0 514.73 560.70 8.00 o 7 -1 0 610.43 609.21 9.52 o 8 -1 0 1654.54 1614.96 23.64 o 9 -1 0 2118.22 2024.47 27.52 o 10 -1 0 1419.39 1463.02 25.55 o 11 -1 0 420.12 414.69 15.77 o 12 -1 0 10.63 9.04 23.30 o 1 0 0 9178.35 8522.28 109.23 o 2 0 0 9618.39 9680.09 114.39 o 3 0 0 1404.77 1371.52 17.81 o 4 0 0 1717.30 1884.65 24.26 o 6 0 0 1473.61 1505.02 16.04 o 7 0 0 2941.32 2929.61 32.61 o 8 0 0 1461.68 1415.39 20.23 o 9 0 0 2.29 4.91 4.39 o 10 0 0 213.72 241.57 10.78 o 11 0 0 608.23 633.06 19.11 o 12 0 0 610.42 625.87 27.01 o 1 1 0 11827.57 11936.29 150.40 o 2 1 0 8303.35 8590.25 112.31 o 3 1 0 7320.18 7653.94 96.83 o 4 1 0 5669.92 5652.98 73.85 o 5 1 0 909.54 900.97 13.31 o 6 1 0 514.07 563.36 8.22 o 7 1 0 561.26 562.12 9.91 o 8 1 0 1693.29 1657.55 22.66 o 9 1 0 2238.44 2124.41 27.71 o 10 1 0 1442.16 1428.57 25.13 o 11 1 0 430.43 424.79 14.81 o 12 1 0 11.05 4.48 9.30 o 0 2 0 14590.64 14737.69 334.83 o 1 2 0 3125.09 3272.15 43.10 o 2 2 0 13485.12 14421.50 169.22 o 3 2 0 1804.48 1909.85 26.82 o 4 2 0 6781.63 6848.92 89.43 o 5 2 0 407.44 392.34 8.00 o 6 2 0 3127.77 3161.52 33.08 o 7 2 0 233.50 220.73 6.95 o 8 2 0 1502.06 1434.07 20.19 o 9 2 0 677.57 659.94 12.87 o 10 2 0 457.63 437.03 19.38 o 11 2 0 1281.16 1278.36 26.03 o 12 2 0 776.02 809.77 36.45 o 1 3 0 730.86 784.09 13.18 o 2 3 0 5063.05 5210.42 76.74 o 3 3 0 11144.61 11347.57 146.13 o 4 3 0 3822.54 4134.02 54.44 o 5 3 0 66.61 76.72 4.76 o 6 3 0 142.20 135.50 4.80 o 7 3 0 1233.42 1199.47 18.87 o 8 3 0 2294.15 2308.44 28.23 o 9 3 0 776.88 742.31 13.17 o 10 3 0 1655.40 1676.00 27.93 o 11 3 0 537.68 512.88 16.57 o 12 3 0 155.81 137.84 14.47 o 0 4 0 27004.29 26599.65 473.46 o 1 4 0 4006.03 4219.27 70.53 o 2 4 0 3582.72 3598.16 54.47 o 3 4 0 2460.66 2604.28 40.04 o 4 4 0 1532.03 1633.47 26.73 o 5 4 0 3158.18 3265.17 42.17 o 6 4 0 6100.63 6297.43 69.00 o 7 4 0 1493.59 1507.51 23.50 o 8 4 0 84.66 79.65 6.06 o 9 4 0 319.05 326.10 9.44 o 10 4 0 997.30 1026.06 19.21 o 11 4 0 1431.59 1453.69 26.68 o 12 4 0 822.93 800.59 26.92 o 1 5 0 633.20 659.16 14.84 o 2 5 0 4828.88 4705.76 78.54 o 3 5 0 887.34 832.57 17.19 o 4 5 0 2732.71 2650.67 39.21 o 5 5 0 1302.48 1287.88 18.77 o 6 5 0 100.48 113.11 5.45 o 7 5 0 674.88 681.61 13.81 o 8 5 0 2236.55 2277.05 31.63 o 9 5 0 368.01 410.13 10.99 o 10 5 0 92.76 92.37 7.60 o 11 5 0 1.73 -5.96 5.96 o 12 5 0 28.60 35.34 14.87 o 0 6 0 5363.37 5031.12 117.63 o 1 6 0 970.55 916.97 20.46 o 2 6 0 2379.39 2371.26 37.89 o 3 6 0 390.27 428.17 12.47 o 4 6 0 2644.74 2800.68 37.37 o 5 6 0 1708.84 1713.11 23.67 o 6 6 0 5789.61 5808.84 69.45 o 7 6 0 1824.63 1831.67 24.98 o 8 6 0 149.70 167.88 8.31 o 9 6 0 216.93 216.71 9.56 o 10 6 0 137.66 145.40 9.85 o 11 6 0 547.98 529.83 17.45 o 12 6 0 221.36 224.48 14.10 o 1 7 0 917.67 895.44 14.37 o 2 7 0 2725.97 2675.05 42.95 o 3 7 0 3883.61 3883.52 57.31 o 4 7 0 3134.78 3087.72 41.32 o 5 7 0 3367.71 3178.37 42.55 o 6 7 0 4.03 3.09 5.20 o 7 7 0 586.42 586.53 13.34 o 8 7 0 952.01 963.11 20.89 o 9 7 0 668.52 650.59 17.65 o 10 7 0 242.21 261.83 13.76 o 11 7 0 240.02 245.34 16.03 o 12 7 0 54.71 80.48 13.87 o 0 8 0 9250.57 9067.88 148.56 o 1 8 0 1811.94 1913.14 23.64 o 2 8 0 6733.40 6699.01 71.99 o 3 8 0 233.92 209.09 8.95 o 4 8 0 611.48 601.74 14.70 o 5 8 0 1580.62 1589.46 35.49 o 6 8 0 2421.74 2324.69 39.69 o 7 8 0 521.80 552.86 16.58 o 8 8 0 656.81 732.75 19.66 o 9 8 0 83.92 73.14 12.03 o 10 8 0 37.12 44.72 8.34 o 11 8 0 195.15 202.22 15.59 o 1 9 0 1428.65 1323.07 17.96 o 2 9 0 2301.90 2350.98 27.78 o 3 9 0 2226.09 2246.40 26.33 o 4 9 0 1880.17 1970.93 29.35 o 5 9 0 410.41 434.20 13.64 o 6 9 0 319.49 298.38 14.45 o 7 9 0 55.63 48.89 8.01 o 8 9 0 1363.83 1361.34 29.24 o 9 9 0 989.06 958.95 26.46 o 10 9 0 608.37 631.24 24.42 o 11 9 0 155.66 170.34 27.22 o 0 10 0 4929.67 4970.63 74.70 o 1 10 0 2713.58 2825.77 32.58 o 2 10 0 212.10 225.29 7.70 o 3 10 0 317.10 309.25 9.19 o 4 10 0 2274.59 2114.22 36.74 o 5 10 0 887.71 933.62 21.63 o 6 10 0 1077.54 1067.09 24.95 o 7 10 0 660.88 638.00 20.57 o 8 10 0 444.54 455.64 16.62 o 9 10 0 71.02 77.23 10.51 o 10 10 0 676.44 677.52 23.51 o 1 11 0 409.45 396.28 10.15 o 2 11 0 2453.38 2492.69 30.74 o 3 11 0 1005.01 1022.50 16.64 o 4 11 0 466.97 455.77 11.71 o 5 11 0 207.71 225.17 12.26 o 6 11 0 487.43 483.08 17.04 o 7 11 0 247.40 249.98 13.48 o 8 11 0 451.52 451.10 17.33 o 9 11 0 1660.70 1604.26 34.24 o 10 11 0 457.50 470.74 21.09 o 0 12 0 1262.08 1325.77 27.80 o 1 12 0 1685.73 1732.26 23.87 o 2 12 0 403.89 378.91 10.55 o 3 12 0 543.30 510.99 11.69 o 4 12 0 787.65 825.59 16.73 o 5 12 0 1260.13 1149.40 29.78 o 6 12 0 1464.75 1468.25 31.14 o 7 12 0 347.41 343.97 16.29 o 8 12 0 69.16 64.46 9.82 o 9 12 0 23.45 26.62 13.18 o 1 13 0 577.89 604.38 13.02 o 2 13 0 3093.98 3162.30 37.43 o 3 13 0 1603.01 1627.68 23.09 o 4 13 0 518.13 533.39 17.74 o 5 13 0 283.70 243.25 15.66 o 6 13 0 17.79 22.88 8.67 o 7 13 0 188.33 204.86 13.82 o 8 13 0 239.89 222.69 14.71 o 9 13 0 578.69 568.88 21.37 o 0 14 0 1861.11 1888.18 37.66 o 1 14 0 1993.94 2010.23 27.37 o 2 14 0 541.77 585.31 15.07 o 3 14 0 180.12 170.83 11.20 o 4 14 0 269.43 275.39 14.74 o 5 14 0 163.56 165.61 12.85 o 6 14 0 1163.69 1155.01 28.74 o 7 14 0 727.05 759.81 23.59 o 8 14 0 619.23 563.99 21.76 o 1 15 0 433.25 467.86 13.30 o 2 15 0 1239.26 1238.73 23.40 o 3 15 0 1547.19 1598.13 31.23 o 4 15 0 1090.52 1099.08 27.76 o 5 15 0 813.35 795.05 24.45 o 6 15 0 34.49 53.72 10.75 o 7 15 0 668.24 611.37 23.07 o 0 16 0 963.47 1016.02 29.09 o 1 16 0 873.62 885.80 21.07 o 2 16 0 699.49 739.38 18.99 o 3 16 0 78.82 91.45 13.40 o 4 16 0 439.45 433.73 17.61 o 5 16 0 466.81 458.38 19.54 o 6 16 0 908.01 930.59 27.52 o 1 17 0 58.87 77.89 9.22 o 2 17 0 57.54 79.11 9.54 o 3 17 0 526.71 539.35 22.32 o 4 17 0 497.98 524.29 22.22 o 5 17 0 458.08 470.01 21.48 o 0 18 0 245.24 232.41 17.70 o 1 18 0 127.49 117.65 11.25 o 2 18 0 85.83 99.05 11.87 o 3 18 0 110.01 99.30 11.67 o -3 -18 1 567.41 561.19 27.34 o -2 -18 1 188.52 217.22 19.01 o -1 -18 1 37.05 45.44 11.69 o 0 -18 1 91.37 107.11 12.75 o 1 -18 1 109.51 127.00 14.04 o 2 -18 1 91.53 91.42 15.78 o 3 -18 1 321.36 331.47 28.93 o -5 -17 1 839.56 845.06 30.74 o -4 -17 1 314.63 328.37 18.27 o -3 -17 1 36.85 35.40 11.29 o -2 -17 1 824.63 843.11 27.65 o -1 -17 1 313.50 343.60 17.21 o 0 -17 1 350.86 382.98 18.10 o 1 -17 1 299.25 270.78 19.29 o 2 -17 1 385.14 381.02 20.10 o 3 -17 1 102.46 96.74 14.30 o 4 -17 1 99.68 85.06 14.40 o 5 -17 1 431.27 425.13 25.82 o -6 -16 1 98.82 95.80 14.21 o -5 -16 1 607.53 635.37 23.93 o -4 -16 1 1348.20 1390.11 30.19 o -3 -16 1 1485.03 1456.29 30.73 o -2 -16 1 280.70 277.14 12.76 o -1 -16 1 121.83 137.97 12.73 o 0 -16 1 14.46 26.63 8.92 o 1 -16 1 154.22 164.50 11.92 o 2 -16 1 202.94 216.89 13.03 o 3 -16 1 906.63 907.09 26.99 o 4 -16 1 840.76 844.40 28.77 o 5 -16 1 653.15 645.38 27.10 o 6 -16 1 21.77 14.13 10.34 o -7 -15 1 236.37 221.13 17.84 o -6 -15 1 641.27 659.12 20.51 o -5 -15 1 501.74 520.13 18.45 o -4 -15 1 141.22 157.97 11.93 o -3 -15 1 292.25 298.28 13.33 o -2 -15 1 171.28 174.13 9.78 o -1 -15 1 1127.23 1169.36 23.20 o 0 -15 1 1886.52 1869.09 32.85 o 1 -15 1 769.12 797.53 19.37 o 2 -15 1 186.03 152.66 10.51 o 3 -15 1 275.79 290.89 13.84 o 4 -15 1 704.94 697.03 23.18 o 5 -15 1 591.02 625.06 19.92 o 6 -15 1 1049.19 1139.69 29.59 o 7 -15 1 490.37 454.67 22.90 o -8 -14 1 211.47 209.79 17.25 o -7 -14 1 229.62 278.36 14.81 o -6 -14 1 56.23 40.55 9.17 o -5 -14 1 755.00 778.67 20.71 o -4 -14 1 1065.47 1069.49 24.02 o -3 -14 1 1431.87 1421.67 30.41 o -2 -14 1 1388.13 1463.55 23.59 o -1 -14 1 798.98 785.59 15.27 o 0 -14 1 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