data_2019676 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.1299 _cell_length_b 13.1194 _cell_length_c 23.7966 _exptl_crystal_F_000 1924.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file sk3552Isup2.hkl _[local]_cod_data_source_block I _shelx_title ' 130903a2 in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 357.75 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 60219.34 60844.04 593.46 o 4 0 0 95128.69 96938.62 947.48 o 6 0 0 5375.50 5114.75 75.55 o 8 0 0 1187.06 1363.48 40.66 o 10 0 0 1448.90 1367.70 107.73 o 12 0 0 773.17 950.44 109.09 o 14 0 0 158.89 219.54 85.91 o 2 1 0 33871.64 34768.42 264.92 o 4 1 0 1397.84 1497.89 25.42 o 6 1 0 9547.01 10298.12 98.28 o 8 1 0 1.06 1.53 11.85 o 10 1 0 143.91 228.01 42.83 o 12 1 0 1277.45 1460.51 111.82 o 14 1 0 51.42 18.37 81.13 o 0 2 0 32617.34 32992.59 548.17 o 2 2 0 8041.90 7675.77 83.28 o 4 2 0 1270.01 1128.19 19.85 o 6 2 0 27725.27 27112.69 223.64 o 8 2 0 80.40 107.20 19.45 o 10 2 0 3938.15 4033.81 118.09 o 12 2 0 22.20 13.61 43.36 o 14 2 0 1490.53 1699.65 110.87 o 2 3 0 284.86 247.39 11.48 o 4 3 0 45746.61 45717.85 464.04 o 6 3 0 3215.44 3327.08 43.08 o 8 3 0 686.77 710.45 28.47 o 10 3 0 359.09 376.44 54.62 o 12 3 0 0.63 101.34 45.61 o 14 3 0 15.55 -60.70 77.73 o 0 4 0 50805.20 48800.95 815.44 o 2 4 0 134.57 92.54 9.92 o 4 4 0 2243.35 1724.56 68.86 o 6 4 0 1933.62 2249.67 65.04 o 8 4 0 5393.70 5150.31 94.28 o 10 4 0 476.79 499.13 46.63 o 12 4 0 3168.54 3377.23 135.68 o 14 4 0 301.82 478.48 165.68 o 2 5 0 6285.28 5354.56 70.50 o 4 5 0 3267.05 3425.28 51.73 o 6 5 0 9369.47 9707.81 163.26 o 8 5 0 3176.23 3095.46 89.50 o 10 5 0 1981.04 1948.38 68.22 o 12 5 0 1573.91 1371.79 133.63 o 0 6 0 27109.62 30606.27 535.90 o 2 6 0 58770.61 57570.08 569.29 o 4 6 0 3355.34 3264.75 52.92 o 6 6 0 11743.46 11345.64 200.45 o 8 6 0 1941.97 1946.04 76.26 o 10 6 0 18.24 9.79 40.23 o 12 6 0 16.84 -39.02 39.02 o 2 7 0 1113.62 1154.68 32.09 o 4 7 0 3616.41 3672.13 60.05 o 6 7 0 760.02 810.56 49.70 o 8 7 0 3063.15 3129.46 97.44 o 10 7 0 1425.54 1425.34 78.29 o 12 7 0 42.48 32.97 42.54 o 0 8 0 1881.95 2437.65 61.51 o 2 8 0 5195.85 4758.44 74.54 o 4 8 0 11889.07 11240.48 184.60 o 6 8 0 169.02 161.42 33.58 o 8 8 0 10312.65 10053.16 192.06 o 10 8 0 15.73 7.76 36.83 o 12 8 0 401.33 370.20 60.48 o 2 9 0 728.08 681.86 30.67 o 4 9 0 55.73 62.78 23.59 o 6 9 0 657.25 566.32 66.14 o 8 9 0 235.92 214.24 71.59 o 10 9 0 26.40 -33.33 37.83 o 12 9 0 11.81 -43.33 43.33 o 0 10 0 1411.74 1446.96 92.73 o 2 10 0 9050.28 9146.85 149.07 o 4 10 0 3803.79 4032.81 103.05 o 6 10 0 9113.89 9086.48 179.27 o 8 10 0 2312.71 2441.21 95.90 o 10 10 0 2894.83 2683.73 171.13 o 2 11 0 241.35 233.14 25.84 o 4 11 0 19562.34 19492.49 302.23 o 6 11 0 2.26 7.77 31.78 o 8 11 0 2.43 -33.55 33.55 o 10 11 0 244.84 178.99 53.65 o 0 12 0 517.22 460.41 41.43 o 2 12 0 6658.14 6407.61 137.84 o 4 12 0 5281.65 5520.41 152.04 o 6 12 0 20.25 -28.56 32.76 o 8 12 0 1305.46 1313.39 87.07 o 10 12 0 602.17 546.81 92.73 o 2 13 0 1050.59 1069.13 66.00 o 4 13 0 58.50 48.65 58.64 o 6 13 0 359.36 383.61 62.04 o 8 13 0 1075.82 1178.21 86.26 o 0 14 0 765.46 886.13 66.82 o 2 14 0 2491.32 2536.18 76.22 o 4 14 0 380.53 351.73 51.42 o 6 14 0 3091.24 3340.11 233.18 o 2 15 0 365.18 286.30 38.93 o 4 15 0 752.67 962.01 195.68 o 6 15 0 7.12 -15.68 55.23 o 0 16 0 1122.31 966.80 103.63 o 2 16 0 144.96 184.50 37.43 o 4 16 0 708.69 624.96 66.51 o 1 1 1 8794.10 7979.82 282.63 o 2 1 1 6408.49 6547.47 43.79 o 3 1 1 36517.95 37002.06 201.69 o 4 1 1 2624.54 2542.38 21.84 o 5 1 1 19140.79 18730.32 102.45 o 6 1 1 43.56 29.72 5.54 o 7 1 1 64.69 56.36 7.21 o 8 1 1 1026.55 1072.78 19.93 o 9 1 1 2115.33 2117.90 40.93 o 10 1 1 54.58 79.62 21.85 o 11 1 1 994.23 1170.94 63.38 o 12 1 1 738.67 766.18 50.41 o 13 1 1 469.58 520.59 49.31 o 14 1 1 101.95 105.59 49.23 o 0 2 1 29792.98 30460.38 358.69 o 1 2 1 4888.25 4870.16 38.92 o 2 2 1 1118.92 1143.93 17.59 o 3 2 1 16673.98 17028.58 110.70 o 4 2 1 652.81 728.79 11.44 o 5 2 1 6946.74 7398.38 51.57 o 6 2 1 23.92 27.95 5.77 o 7 2 1 1.40 0.59 6.36 o 8 2 1 1576.67 1558.11 25.88 o 9 2 1 1621.71 1654.41 31.04 o 10 2 1 881.60 915.41 36.89 o 11 2 1 0.16 5.03 27.73 o 12 2 1 36.95 13.98 31.31 o 13 2 1 119.53 168.33 39.15 o 14 2 1 136.63 171.41 44.25 o 1 3 1 5172.58 4854.78 41.39 o 2 3 1 7265.08 7003.11 56.42 o 3 3 1 679.71 556.90 16.83 o 4 3 1 1367.68 1355.79 25.47 o 5 3 1 10159.85 10311.93 77.49 o 6 3 1 287.87 229.98 11.52 o 7 3 1 1866.97 1845.19 29.73 o 8 3 1 73.67 75.94 10.93 o 9 3 1 2626.12 2625.63 39.14 o 10 3 1 221.90 179.23 20.22 o 11 3 1 4017.25 4301.95 93.03 o 12 3 1 45.93 82.53 33.39 o 13 3 1 2012.74 2219.55 139.62 o 14 3 1 17.03 28.59 64.56 o 0 4 1 2267.78 2207.07 68.18 o 1 4 1 986.30 952.89 15.86 o 2 4 1 104.89 111.95 9.86 o 3 4 1 7157.89 6962.18 67.67 o 4 4 1 0.61 -6.61 6.61 o 5 4 1 68.91 64.68 8.95 o 6 4 1 228.87 247.61 19.39 o 7 4 1 980.57 1048.02 42.29 o 8 4 1 2474.73 2582.65 48.89 o 9 4 1 105.46 79.41 15.35 o 10 4 1 81.60 50.97 21.28 o 11 4 1 882.96 856.19 38.34 o 12 4 1 527.10 569.11 47.04 o 13 4 1 133.28 213.33 40.82 o 14 4 1 193.22 249.52 47.20 o 1 5 1 4575.10 4167.28 41.30 o 2 5 1 637.58 666.10 21.85 o 3 5 1 10521.85 9869.11 81.46 o 4 5 1 8331.07 8119.35 80.30 o 5 5 1 6816.11 6757.96 71.95 o 6 5 1 657.62 652.18 29.67 o 7 5 1 1372.62 1263.29 39.92 o 8 5 1 423.33 406.30 34.64 o 9 5 1 924.23 916.41 41.80 o 10 5 1 2991.04 2937.96 64.57 o 11 5 1 14.92 10.61 30.11 o 12 5 1 1.17 60.87 51.52 o 13 5 1 489.13 548.17 97.50 o 0 6 1 23989.29 25264.46 318.19 o 1 6 1 998.65 1061.52 30.29 o 2 6 1 25186.91 26142.37 193.05 o 3 6 1 128.17 138.10 9.79 o 4 6 1 1681.87 1919.83 26.91 o 5 6 1 678.71 691.90 29.31 o 6 6 1 1894.77 1988.19 46.72 o 7 6 1 2029.58 1968.76 50.24 o 8 6 1 1333.00 1279.88 45.97 o 9 6 1 710.62 709.11 50.58 o 10 6 1 19.78 14.76 29.52 o 11 6 1 522.48 561.63 61.21 o 12 6 1 29.72 55.03 31.26 o 13 6 1 27.25 22.76 55.83 o 1 7 1 11058.54 11383.65 96.03 o 2 7 1 669.42 991.42 21.18 o 3 7 1 7341.77 7172.91 67.62 o 4 7 1 214.89 220.27 14.74 o 5 7 1 677.12 607.89 48.53 o 6 7 1 53.75 30.46 20.14 o 7 7 1 5748.38 5674.10 89.46 o 8 7 1 979.60 958.46 44.20 o 9 7 1 662.47 721.56 42.07 o 10 7 1 8.77 22.78 25.87 o 11 7 1 677.04 681.29 45.85 o 12 7 1 3.82 -28.75 28.75 o 13 7 1 344.81 356.44 134.32 o 0 8 1 9190.89 10015.50 125.87 o 1 8 1 331.40 384.64 16.27 o 2 8 1 1.09 -2.48 12.13 o 3 8 1 1251.78 1249.21 25.19 o 4 8 1 279.37 271.80 22.21 o 5 8 1 240.48 242.90 32.48 o 6 8 1 98.91 78.45 24.41 o 7 8 1 5143.26 5103.68 86.99 o 8 8 1 377.73 342.16 32.08 o 9 8 1 10.55 5.51 25.39 o 10 8 1 227.92 247.02 52.75 o 11 8 1 91.92 88.41 44.81 o 12 8 1 0.16 -29.99 29.99 o 1 9 1 4626.10 4666.54 54.31 o 2 9 1 1317.06 1366.95 28.54 o 3 9 1 7616.27 7547.00 85.49 o 4 9 1 90.84 60.98 18.50 o 5 9 1 1392.54 1338.47 43.88 o 6 9 1 123.69 98.38 22.56 o 7 9 1 5180.55 4919.52 88.25 o 8 9 1 4.41 8.68 23.08 o 9 9 1 1171.09 1150.72 53.52 o 10 9 1 137.68 115.91 32.50 o 11 9 1 452.49 455.90 44.13 o 12 9 1 44.11 -1.01 33.74 o 0 10 1 893.19 872.71 31.21 o 1 10 1 918.52 964.10 34.15 o 2 10 1 3660.63 3690.26 49.69 o 3 10 1 1.85 -2.29 15.74 o 4 10 1 200.07 264.14 25.22 o 5 10 1 787.18 799.94 38.78 o 6 10 1 15.22 38.89 21.74 o 7 10 1 39.68 21.62 23.23 o 8 10 1 7.66 -12.09 23.88 o 9 10 1 33.77 17.17 26.39 o 10 10 1 23.32 -33.09 36.02 o 11 10 1 415.00 316.81 42.97 o 1 11 1 1316.73 1355.87 29.95 o 2 11 1 9.00 32.33 15.04 o 3 11 1 44.13 36.81 24.99 o 4 11 1 2395.05 2401.22 89.16 o 5 11 1 30.13 28.75 21.85 o 6 11 1 574.44 540.00 38.20 o 7 11 1 2558.21 2620.06 71.84 o 8 11 1 0.02 12.74 26.50 o 9 11 1 723.80 715.98 48.54 o 10 11 1 599.10 568.63 48.14 o 11 11 1 1690.90 1655.43 137.72 o 0 12 1 1910.73 1833.56 48.81 o 1 12 1 221.54 193.99 16.02 o 2 12 1 53.35 16.12 19.70 o 3 12 1 41.19 59.40 22.16 o 4 12 1 2709.34 2864.64 90.93 o 5 12 1 23.44 41.52 23.68 o 6 12 1 47.52 34.70 25.83 o 7 12 1 129.65 169.85 31.83 o 8 12 1 26.04 39.82 29.67 o 9 12 1 21.66 30.86 31.95 o 10 12 1 235.84 291.99 99.54 o 1 13 1 4776.04 4621.59 69.32 o 2 13 1 644.32 650.85 35.55 o 3 13 1 661.38 753.37 41.91 o 4 13 1 1817.64 1684.54 88.43 o 5 13 1 3297.03 3229.69 78.11 o 6 13 1 631.61 581.69 57.47 o 7 13 1 2105.93 2186.24 73.00 o 8 13 1 30.13 49.55 41.73 o 9 13 1 1413.36 1235.62 93.39 o 0 14 1 40.22 28.70 24.66 o 1 14 1 266.00 252.39 25.63 o 2 14 1 49.50 29.16 18.83 o 3 14 1 187.40 230.36 30.95 o 4 14 1 194.18 187.09 34.84 o 5 14 1 0.02 -14.55 25.52 o 6 14 1 101.46 114.00 32.04 o 7 14 1 214.66 140.06 35.23 o 1 15 1 3891.39 4076.10 69.57 o 2 15 1 6.75 22.11 20.52 o 3 15 1 2206.06 2184.56 60.42 o 4 15 1 125.57 143.07 31.81 o 5 15 1 1420.61 1468.22 66.02 o 6 15 1 61.27 53.89 33.47 o 0 16 1 432.15 435.37 70.23 o 1 16 1 81.79 41.94 27.70 o 2 16 1 74.92 43.36 22.78 o 3 16 1 52.02 63.07 24.62 o 4 16 1 72.78 29.04 27.47 o 1 0 2 9279.52 8761.99 258.48 o 2 0 2 47488.49 48923.32 343.64 o 3 0 2 34618.77 35387.95 250.56 o 4 0 2 3700.58 3585.86 47.67 o 5 0 2 2152.22 2252.68 29.98 o 6 0 2 6493.34 6370.54 62.67 o 7 0 2 8643.35 9296.67 86.12 o 8 0 2 5848.86 5897.21 64.96 o 9 0 2 1624.57 1784.09 58.93 o 10 0 2 459.03 484.52 40.59 o 11 0 2 313.89 204.83 51.82 o 12 0 2 1402.93 1615.33 94.97 o 13 0 2 76.07 134.81 77.04 o 14 0 2 756.33 951.09 86.29 o 1 1 2 2700.29 2664.94 23.46 o 2 1 2 233.41 230.46 6.59 o 3 1 2 458.31 518.16 12.59 o 4 1 2 31.94 26.48 4.64 o 5 1 2 408.07 525.80 10.94 o 6 1 2 342.59 373.52 11.88 o 7 1 2 135.85 149.53 8.59 o 8 1 2 620.40 642.70 16.67 o 9 1 2 3329.75 3352.60 45.23 o 10 1 2 9.65 -7.35 17.51 o 11 1 2 63.97 97.22 38.77 o 12 1 2 0.02 25.77 45.07 o 13 1 2 229.25 290.72 54.99 o 14 1 2 30.11 30.62 42.73 o 0 2 2 35838.06 36063.34 349.22 o 1 2 2 2283.58 2391.83 22.91 o 2 2 2 44288.02 44256.17 308.00 o 3 2 2 103.98 147.40 7.46 o 4 2 2 259.32 170.45 8.92 o 5 2 2 34848.00 36552.29 217.63 o 6 2 2 642.44 494.20 11.88 o 7 2 2 759.68 872.17 17.37 o 8 2 2 1311.18 1285.21 23.85 o 9 2 2 1313.39 1312.06 30.42 o 10 2 2 5134.02 5138.53 66.75 o 11 2 2 774.43 777.12 48.23 o 12 2 2 435.50 317.65 39.90 o 13 2 2 4.54 45.82 35.92 o 14 2 2 1233.89 1463.62 74.10 o 1 3 2 430.64 425.05 10.71 o 2 3 2 2831.06 2907.93 28.75 o 3 3 2 38205.35 38241.45 296.73 o 4 3 2 72.22 63.28 7.98 o 5 3 2 2932.10 3268.57 36.59 o 6 3 2 2725.44 2650.20 36.52 o 7 3 2 2996.31 3330.66 64.62 o 8 3 2 18.05 9.48 11.21 o 9 3 2 1235.21 1293.98 36.59 o 10 3 2 133.64 127.39 18.72 o 11 3 2 1920.81 2026.83 92.90 o 12 3 2 124.28 171.10 35.48 o 13 3 2 286.58 279.87 41.87 o 14 3 2 58.05 -10.13 40.01 o 0 4 2 137.12 188.41 21.27 o 1 4 2 1046.88 1087.30 17.79 o 2 4 2 1401.90 1167.29 17.70 o 3 4 2 4455.35 4196.62 62.51 o 4 4 2 4545.08 4272.33 49.93 o 5 4 2 544.95 580.57 32.49 o 6 4 2 676.81 515.21 19.91 o 7 4 2 713.15 781.69 23.76 o 8 4 2 4175.40 4170.36 54.62 o 9 4 2 83.57 106.10 15.83 o 10 4 2 876.30 953.79 36.94 o 11 4 2 1689.52 1731.77 55.78 o 12 4 2 2076.32 2339.09 78.55 o 13 4 2 12.59 0.23 35.90 o 14 4 2 1445.28 1546.43 140.45 o 1 5 2 492.99 511.44 13.56 o 2 5 2 297.31 228.88 10.38 o 3 5 2 512.29 486.71 13.35 o 4 5 2 3339.37 3387.27 44.31 o 5 5 2 1952.67 2201.62 35.65 o 6 5 2 2233.23 2371.43 48.71 o 7 5 2 8.06 25.97 15.10 o 8 5 2 23.31 2.19 17.74 o 9 5 2 1164.07 1187.55 58.89 o 10 5 2 41.80 22.25 20.76 o 11 5 2 992.35 1045.72 60.03 o 12 5 2 1784.93 1977.78 109.87 o 13 5 2 358.46 310.90 65.55 o 0 6 2 3472.53 3295.99 80.64 o 1 6 2 6979.99 7073.06 64.23 o 2 6 2 249.87 134.28 10.27 o 3 6 2 823.97 743.80 17.54 o 4 6 2 1496.02 1209.83 36.36 o 5 6 2 2850.82 2970.44 54.36 o 6 6 2 6053.16 5747.28 95.26 o 7 6 2 3525.57 3468.29 66.25 o 8 6 2 4993.18 4982.57 99.98 o 9 6 2 206.18 177.01 27.20 o 10 6 2 4451.47 4364.16 100.38 o 11 6 2 177.18 196.97 29.25 o 12 6 2 1287.67 1404.63 72.57 o 13 6 2 526.75 446.99 73.28 o 1 7 2 1746.66 1919.28 29.12 o 2 7 2 210.71 234.55 12.60 o 3 7 2 17.54 17.58 8.04 o 4 7 2 45.66 39.53 10.45 o 5 7 2 197.48 204.13 20.54 o 6 7 2 20.77 8.94 19.29 o 7 7 2 3019.61 3069.35 64.30 o 8 7 2 199.80 165.11 25.33 o 9 7 2 1459.14 1511.83 54.32 o 10 7 2 289.21 261.49 32.97 o 11 7 2 47.66 22.38 25.74 o 12 7 2 223.89 181.50 56.49 o 13 7 2 37.23 151.36 92.73 o 0 8 2 17828.62 17644.29 199.30 o 1 8 2 51.28 38.66 9.03 o 2 8 2 4162.43 4012.29 61.08 o 3 8 2 112.40 91.29 10.63 o 4 8 2 11382.37 10980.86 129.16 o 5 8 2 8249.13 8156.09 107.71 o 6 8 2 7324.24 7291.64 103.57 o 7 8 2 1522.24 1592.80 51.16 o 8 8 2 1817.15 1955.87 58.60 o 9 8 2 0.97 -22.73 22.73 o 10 8 2 341.59 369.52 37.94 o 11 8 2 41.14 31.46 29.33 o 12 8 2 341.88 266.01 66.33 o 1 9 2 669.56 660.43 21.14 o 2 9 2 52.53 70.06 11.01 o 3 9 2 39.84 55.12 13.36 o 4 9 2 1256.00 1308.12 40.85 o 5 9 2 701.89 622.37 57.83 o 6 9 2 2269.77 2316.28 58.58 o 7 9 2 1036.31 1005.02 45.00 o 8 9 2 726.37 740.37 43.07 o 9 9 2 45.41 0.90 26.06 o 10 9 2 408.76 338.20 39.02 o 11 9 2 728.40 672.90 50.00 o 12 9 2 28.21 16.19 41.92 o 0 10 2 2287.86 2250.65 47.34 o 1 10 2 336.67 328.87 16.68 o 2 10 2 2097.95 2046.35 38.99 o 3 10 2 18.81 0.86 15.45 o 4 10 2 2315.53 2233.29 54.86 o 5 10 2 298.67 270.19 26.66 o 6 10 2 4465.13 4373.09 83.23 o 7 10 2 228.14 210.12 29.22 o 8 10 2 1392.24 1439.45 58.65 o 9 10 2 344.56 323.95 36.31 o 10 10 2 896.14 876.55 53.25 o 11 10 2 63.34 42.16 34.24 o 1 11 2 296.92 315.88 17.87 o 2 11 2 230.94 268.56 21.09 o 3 11 2 2463.41 2521.08 58.62 o 4 11 2 949.53 929.34 42.67 o 5 11 2 37.42 69.38 34.05 o 6 11 2 9.51 6.74 22.88 o 7 11 2 68.80 -7.49 23.24 o 8 11 2 210.55 197.16 34.44 o 9 11 2 9.33 -9.90 33.26 o 10 11 2 3.36 19.32 34.25 o 0 12 2 787.68 801.31 36.09 o 1 12 2 6.63 0.52 12.75 o 2 12 2 26.55 24.20 19.72 o 3 12 2 548.43 558.48 34.92 o 4 12 2 3051.07 3140.01 113.57 o 5 12 2 216.62 257.56 31.45 o 6 12 2 1804.87 1749.33 88.77 o 7 12 2 310.72 299.01 36.15 o 8 12 2 1287.74 1318.74 60.72 o 9 12 2 103.86 65.58 32.60 o 10 12 2 760.33 762.26 103.63 o 1 13 2 501.52 476.39 24.26 o 2 13 2 847.93 840.03 38.18 o 3 13 2 24.13 13.36 22.08 o 4 13 2 2048.40 2112.66 63.35 o 5 13 2 1080.02 1024.68 51.00 o 6 13 2 260.54 258.04 34.47 o 7 13 2 5.06 -28.03 28.03 o 8 13 2 98.40 50.91 38.84 o 0 14 2 2494.52 2596.52 74.32 o 1 14 2 25.28 26.05 18.29 o 2 14 2 2457.64 2779.25 61.64 o 3 14 2 1.37 25.80 21.67 o 4 14 2 2050.04 2171.05 66.55 o 5 14 2 233.24 253.47 34.85 o 6 14 2 809.51 784.20 50.69 o 7 14 2 1595.36 1670.03 85.22 o 1 15 2 88.40 101.22 24.94 o 2 15 2 0.28 -18.66 18.66 o 3 15 2 35.16 20.33 25.92 o 4 15 2 1.06 -10.72 26.74 o 5 15 2 64.33 51.50 30.34 o 6 15 2 25.65 35.12 32.97 o 0 16 2 3494.23 3506.04 207.27 o 1 16 2 68.41 20.62 35.03 o 2 16 2 1501.08 1614.30 51.10 o 3 16 2 1.17 -17.83 22.18 o 4 16 2 1298.24 1388.99 86.54 o 1 1 3 8244.59 8245.10 57.79 o 2 1 3 1583.68 1652.87 15.79 o 3 1 3 22037.75 22137.75 140.85 o 4 1 3 5517.95 5625.27 40.99 o 5 1 3 9042.98 9202.63 59.12 o 6 1 3 19.88 22.69 5.53 o 7 1 3 14213.96 14536.92 87.06 o 8 1 3 1944.40 2074.60 28.73 o 9 1 3 324.38 319.29 20.57 o 10 1 3 662.57 721.73 33.25 o 11 1 3 301.60 357.88 42.12 o 12 1 3 171.86 232.64 36.95 o 13 1 3 427.57 535.74 62.59 o 14 1 3 356.92 294.59 46.36 o 0 2 3 977.45 963.78 18.79 o 1 2 3 181.70 187.75 12.91 o 2 2 3 207.11 210.17 7.96 o 3 2 3 2.15 0.55 4.99 o 4 2 3 14.97 25.33 6.26 o 5 2 3 6315.31 6402.80 49.17 o 6 2 3 2770.90 2634.07 27.64 o 7 2 3 2386.71 2596.01 28.69 o 8 2 3 504.39 561.89 19.64 o 9 2 3 2553.98 2614.94 55.60 o 10 2 3 57.71 75.51 18.09 o 11 2 3 842.93 900.79 44.18 o 12 2 3 369.42 413.33 43.01 o 13 2 3 3.20 -16.28 34.38 o 14 2 3 395.79 455.22 59.62 o 1 3 3 9261.39 8636.82 68.20 o 2 3 3 2651.66 2700.95 28.01 o 3 3 3 10456.62 9905.57 82.06 o 4 3 3 2481.34 2633.22 31.31 o 5 3 3 10818.30 10321.73 78.67 o 6 3 3 108.63 143.77 10.77 o 7 3 3 6221.83 6207.62 61.08 o 8 3 3 2465.07 2647.73 47.93 o 9 3 3 179.76 180.37 16.84 o 10 3 3 185.48 190.09 24.04 o 11 3 3 319.95 352.10 36.65 o 12 3 3 0.03 27.66 31.95 o 13 3 3 639.64 673.40 52.26 o 14 3 3 2.32 -12.93 54.15 o 0 4 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19 369.85 362.56 41.64 o 11 3 19 125.21 160.64 50.77 o 0 4 19 9738.46 9312.25 140.89 o 1 4 19 1674.52 1646.26 49.73 o 2 4 19 306.42 380.04 26.96 o 3 4 19 148.12 117.48 16.97 o 4 4 19 263.59 234.04 23.63 o 5 4 19 0.85 3.66 17.06 o 6 4 19 122.53 79.13 19.70 o 7 4 19 61.19 64.63 21.85 o 8 4 19 476.09 502.33 36.13 o 9 4 19 12.66 27.50 27.10 o 10 4 19 130.83 101.84 33.07 o 1 5 19 4962.52 4919.53 74.85 o 2 5 19 126.03 137.74 18.48 o 3 5 19 3706.04 3654.19 78.33 o 4 5 19 645.14 677.65 50.39 o 5 5 19 6489.60 6524.53 113.22 o 6 5 19 372.35 413.63 40.54 o 7 5 19 2595.64 2629.25 64.44 o 8 5 19 3.00 -4.31 19.58 o 9 5 19 1188.44 1163.47 62.05 o 10 5 19 49.22 63.44 31.07 o 0 6 19 3189.83 3079.86 100.09 o 1 6 19 888.39 867.98 36.05 o 2 6 19 875.99 936.08 37.04 o 3 6 19 88.40 137.70 24.14 o 4 6 19 144.23 164.16 25.11 o 5 6 19 236.64 302.56 37.57 o 6 6 19 1099.10 1092.02 63.57 o 7 6 19 11.79 10.77 29.72 o 8 6 19 23.32 30.32 25.92 o 9 6 19 96.48 89.66 31.49 o 10 6 19 6.23 43.64 79.77 o 1 7 19 2094.21 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34.86 o 1 11 19 1263.66 1496.68 73.22 o 2 11 19 5.26 24.38 24.41 o 3 11 19 3153.21 3005.42 109.04 o 4 11 19 182.71 202.29 44.89 o 5 11 19 529.99 526.52 61.69 o 6 11 19 86.15 59.32 39.95 o 0 12 19 1522.80 1812.24 132.27 o 1 12 19 134.51 66.38 34.28 o 2 12 19 247.46 310.29 34.42 o 3 12 19 0.05 -21.52 25.40 o 4 12 19 70.78 108.85 43.67 o 5 12 19 98.65 61.36 58.64 o 1 13 19 12.50 34.92 33.69 o 2 13 19 31.66 92.56 80.31 o 0 0 20 22.04 16.14 16.90 o 1 0 20 995.36 1094.46 64.80 o 2 0 20 1203.22 1147.20 46.55 o 3 0 20 9437.15 9094.49 142.16 o 4 0 20 6699.86 6642.03 118.68 o 5 0 20 376.16 435.43 37.49 o 6 0 20 69.35 89.22 28.86 o 7 0 20 508.32 518.65 46.83 o 8 0 20 3964.51 4133.69 121.63 o 9 0 20 8.99 5.65 33.78 o 10 0 20 1152.26 1300.56 75.65 o 11 0 20 3.88 102.27 79.09 o 1 1 20 1593.93 1697.20 37.55 o 2 1 20 153.37 172.13 17.21 o 3 1 20 307.20 345.74 33.03 o 4 1 20 1295.96 1275.52 37.11 o 5 1 20 761.83 756.20 32.84 o 6 1 20 101.16 106.08 20.36 o 7 1 20 47.31 39.36 24.02 o 8 1 20 216.13 206.69 27.17 o 9 1 20 30.82 -1.49 22.96 o 10 1 20 47.46 24.21 26.19 o 0 2 20 49.78 54.43 13.95 o 1 2 20 30.53 43.78 12.82 o 2 2 20 2057.33 1907.11 41.21 o 3 2 20 334.13 383.36 24.38 o 4 2 20 3681.72 3580.42 64.38 o 5 2 20 204.85 311.60 34.29 o 6 2 20 3679.60 3751.93 77.64 o 7 2 20 41.10 67.15 21.09 o 8 2 20 1385.25 1383.78 53.92 o 9 2 20 70.89 22.08 28.12 o 10 2 20 1111.69 1173.43 74.52 o 1 3 20 4657.18 4371.32 62.88 o 2 3 20 30.90 34.36 13.20 o 3 3 20 536.91 537.43 27.33 o 4 3 20 1282.70 1211.34 37.12 o 5 3 20 1612.49 1499.60 47.50 o 6 3 20 4.08 -17.56 17.56 o 7 3 20 443.41 497.14 31.69 o 8 3 20 317.73 250.56 31.31 o 9 3 20 17.49 -33.26 33.26 o 10 3 20 9.63 27.51 29.50 o 0 4 20 8082.33 7663.09 125.91 o 1 4 20 0.99 -10.87 12.83 o 2 4 20 1756.89 1731.77 50.46 o 3 4 20 272.84 250.56 21.46 o 4 4 20 4446.50 4421.38 75.91 o 5 4 20 26.54 10.60 18.51 o 6 4 20 1546.06 1603.40 51.55 o 7 4 20 374.85 323.78 31.46 o 8 4 20 1025.48 1005.02 47.25 o 9 4 20 169.01 171.51 33.45 o 10 4 20 721.78 770.25 54.15 o 1 5 20 445.47 555.57 48.33 o 2 5 20 536.59 533.41 30.44 o 3 5 20 138.85 168.96 24.90 o 4 5 20 1.10 -18.06 18.06 o 5 5 20 19.76 -3.09 18.37 o 6 5 20 1091.86 1024.29 53.98 o 7 5 20 496.90 515.25 70.46 o 8 5 20 588.28 551.25 38.23 o 9 5 20 18.07 -19.46 31.10 o 10 5 20 387.00 348.90 57.97 o 0 6 20 17.48 42.43 24.57 o 1 6 20 41.72 39.84 15.94 o 2 6 20 845.16 912.07 37.43 o 3 6 20 259.35 252.18 29.24 o 4 6 20 198.01 213.43 28.75 o 5 6 20 484.09 435.94 37.87 o 6 6 20 4824.74 4751.86 109.73 o 7 6 20 914.87 933.05 61.01 o 8 6 20 1557.47 1438.77 70.47 o 9 6 20 183.17 172.78 37.12 o 1 7 20 27.72 17.83 15.56 o 2 7 20 596.60 588.68 56.09 o 3 7 20 666.31 628.42 40.02 o 4 7 20 634.57 730.54 51.03 o 5 7 20 160.26 155.17 27.79 o 6 7 20 861.06 889.42 49.86 o 7 7 20 22.18 14.47 29.17 o 8 7 20 14.73 21.34 29.63 o 9 7 20 11.89 -12.27 51.82 o 0 8 20 7106.50 6940.79 225.00 o 1 8 20 23.03 -1.30 30.36 o 2 8 20 1923.72 1847.07 84.83 o 3 8 20 6.53 38.08 24.41 o 4 8 20 1338.18 1406.09 55.62 o 5 8 20 57.36 58.30 25.34 o 6 8 20 347.47 398.39 37.63 o 7 8 20 69.21 68.05 31.41 o 8 8 20 356.99 348.96 45.64 o 1 9 20 158.87 164.77 28.15 o 2 9 20 7.34 30.74 26.30 o 3 9 20 467.32 476.16 44.35 o 4 9 20 260.10 217.21 35.36 o 5 9 20 47.14 70.40 25.11 o 6 9 20 60.47 36.66 40.14 o 7 9 20 28.36 38.66 33.63 o 0 10 20 1652.94 1902.24 130.91 o 1 10 20 17.84 13.35 21.50 o 2 10 20 2598.80 2768.17 84.46 o 3 10 20 139.06 192.81 35.08 o 4 10 20 220.97 242.25 38.82 o 5 10 20 6.66 -9.92 28.47 o 6 10 20 927.63 1012.33 67.36 o 1 11 20 125.64 157.66 41.58 o 2 11 20 1.84 -1.40 22.91 o 3 11 20 0.22 43.99 29.60 o 4 11 20 115.01 162.31 36.73 o 5 11 20 24.85 78.73 41.94 o 0 12 20 805.88 873.16 110.45 o 1 12 20 65.46 127.54 38.08 o 2 12 20 1183.55 1218.89 84.44 o 3 12 20 2.39 2.75 29.26 o 4 12 20 396.07 227.72 69.54 o 1 1 21 147.42 188.17 17.53 o 2 1 21 720.93 760.67 30.59 o 3 1 21 1435.20 1349.35 41.87 o 4 1 21 978.78 1019.26 42.69 o 5 1 21 580.53 604.29 31.04 o 6 1 21 3644.43 3704.99 74.04 o 7 1 21 3734.79 3710.92 76.90 o 8 1 21 152.10 173.63 29.47 o 9 1 21 2490.04 2571.33 71.22 o 10 1 21 49.58 107.67 29.54 o 0 2 21 1344.61 1250.31 46.85 o 1 2 21 97.86 124.89 15.97 o 2 2 21 1269.76 1247.34 35.46 o 3 2 21 1036.76 1022.05 34.48 o 4 2 21 42.60 35.75 15.25 o 5 2 21 1153.92 1145.42 43.69 o 6 2 21 70.59 74.32 21.84 o 7 2 21 132.06 127.81 29.56 o 8 2 21 11.23 12.77 24.65 o 9 2 21 17.29 13.71 26.67 o 10 2 21 4.22 88.12 46.45 o 1 3 21 777.34 864.83 31.63 o 2 3 21 6.21 13.24 13.68 o 3 3 21 1819.55 1888.92 43.58 o 4 3 21 242.74 285.26 26.35 o 5 3 21 1049.73 1081.54 59.75 o 6 3 21 100.88 97.96 22.97 o 7 3 21 2091.77 2091.87 59.28 o 8 3 21 329.67 282.12 37.13 o 9 3 21 3134.66 3199.90 88.17 o 10 3 21 400.36 411.84 61.51 o 0 4 21 260.71 287.32 38.86 o 1 4 21 158.67 167.32 19.64 o 2 4 21 503.25 490.96 30.41 o 3 4 21 175.84 206.42 20.77 o 4 4 21 7.94 -7.53 16.69 o 5 4 21 114.49 86.57 22.62 o 6 4 21 195.93 189.36 31.93 o 7 4 21 177.70 156.63 27.62 o 8 4 21 3.61 36.95 34.10 o 9 4 21 5.73 25.17 47.42 o 10 4 21 45.72 42.26 44.83 o 1 5 21 4970.34 5093.88 99.60 o 2 5 21 147.62 118.81 19.24 o 3 5 21 1262.63 1201.93 50.35 o 4 5 21 93.32 105.29 24.91 o 5 5 21 1552.24 1450.54 68.69 o 6 5 21 26.08 20.21 21.84 o 7 5 21 1065.66 1008.65 65.34 o 8 5 21 1.51 25.14 23.39 o 9 5 21 664.01 790.40 119.45 o 0 6 21 83.07 67.15 29.70 o 1 6 21 89.14 76.51 18.24 o 2 6 21 509.84 464.79 35.77 o 3 6 21 535.79 543.27 46.21 o 4 6 21 1899.40 1682.14 58.25 o 5 6 21 1569.69 1386.02 69.48 o 6 6 21 2.61 -5.88 27.01 o 7 6 21 137.11 119.42 28.41 o 8 6 21 424.79 417.87 49.64 o 9 6 21 0.73 -4.09 50.45 o 1 7 21 3748.80 3653.44 78.78 o 2 7 21 41.82 48.92 21.98 o 3 7 21 698.61 725.02 46.06 o 4 7 21 209.85 218.22 35.36 o 5 7 21 2221.70 2286.59 67.91 o 6 7 21 17.53 8.12 23.17 o 7 7 21 511.63 602.85 45.08 o 8 7 21 210.90 158.49 65.49 o 0 8 21 98.39 83.44 32.40 o 1 8 21 89.83 145.91 30.61 o 2 8 21 8.20 14.75 24.00 o 3 8 21 447.46 478.13 42.51 o 4 8 21 29.00 69.99 25.98 o 5 8 21 52.43 42.75 26.22 o 6 8 21 259.23 223.50 32.80 o 7 8 21 22.48 27.16 36.67 o 8 8 21 473.08 451.36 85.91 o 1 9 21 2946.86 3038.82 86.12 o 2 9 21 58.36 81.74 29.42 o 3 9 21 1531.76 1547.35 67.31 o 4 9 21 30.56 23.75 24.33 o 5 9 21 1689.81 1717.99 109.98 o 6 9 21 0.90 2.16 28.43 o 7 9 21 843.92 905.59 67.77 o 0 10 21 27.89 62.73 61.36 o 1 10 21 71.18 54.92 27.48 o 2 10 21 32.79 81.53 31.30 o 3 10 21 1.30 -12.15 27.09 o 4 10 21 18.03 9.85 37.85 o 5 10 21 44.36 6.73 26.89 o 6 10 21 7.46 -11.91 38.16 o 1 11 21 54.64 57.21 33.55 o 2 11 21 6.14 15.97 28.60 o 3 11 21 491.02 464.34 48.26 o 4 11 21 25.94 -0.09 30.30 o 5 11 21 680.54 845.44 106.36 o 0 12 21 1381.93 1335.50 86.72 o 1 12 21 0.03 37.54 53.52 o 2 12 21 786.03 870.03 76.54 o 0 0 22 702.39 764.99 81.82 o 1 0 22 1670.62 1609.02 55.23 o 2 0 22 9626.76 9517.64 150.32 o 3 0 22 7418.66 7363.48 128.96 o 4 0 22 7956.70 7603.29 134.09 o 5 0 22 2001.65 1844.20 66.30 o 6 0 22 6431.50 6375.95 207.27 o 7 0 22 7.73 -10.26 43.64 o 8 0 22 3447.21 3375.29 101.14 o 9 0 22 225.44 226.68 45.37 o 10 0 22 202.93 169.51 54.32 o 1 1 22 61.15 64.45 14.38 o 2 1 22 168.71 208.81 19.30 o 3 1 22 7.47 26.93 21.29 o 4 1 22 336.44 395.29 26.32 o 5 1 22 1944.89 1898.03 53.55 o 6 1 22 202.52 252.20 27.93 o 7 1 22 462.93 504.79 42.41 o 8 1 22 266.64 239.38 37.59 o 9 1 22 84.81 92.98 31.45 o 10 1 22 190.16 155.42 45.29 o 0 2 22 118.75 138.06 23.44 o 1 2 22 110.61 131.40 18.22 o 2 2 22 624.52 746.98 32.45 o 3 2 22 235.45 280.48 22.52 o 4 2 22 283.34 270.32 23.33 o 5 2 22 8.04 -9.28 17.79 o 6 2 22 3863.46 3961.28 77.91 o 7 2 22 80.82 110.53 29.50 o 8 2 22 1364.83 1606.20 67.72 o 9 2 22 132.89 143.67 35.07 o 10 2 22 1902.65 2046.25 109.87 o 1 3 22 156.15 160.16 20.47 o 2 3 22 814.61 828.31 39.03 o 3 3 22 858.22 911.79 36.01 o 4 3 22 441.59 472.09 32.03 o 5 3 22 36.85 32.40 20.07 o 6 3 22 200.43 187.29 27.30 o 7 3 22 466.38 492.63 42.72 o 8 3 22 79.52 89.13 32.29 o 9 3 22 12.77 91.69 39.81 o 0 4 22 632.86 705.03 56.40 o 1 4 22 0.03 24.42 14.83 o 2 4 22 1978.41 2031.87 53.99 o 3 4 22 583.05 558.30 32.12 o 4 4 22 2906.51 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