data_2019678 _cell_angle_alpha 90.000 _cell_angle_beta 108.061 _cell_angle_gamma 90.000 _cell_length_a 13.8034 _cell_length_b 14.2545 _cell_length_c 14.9313 _exptl_crystal_F_000 1310.00 _reflns_d_resolution_high 0.7700 _cod_data_source_file sk3552IIIsup4.hkl _cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_title ' 110419a2013 in Pn' _shelx_refln_list_code 4 _shelx_f_calc_maximum 283.75 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' 'x+1/2, -y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 -19 394.69 339.21 58.84 o 5 0 -19 123.76 160.95 43.27 o 7 0 -19 1784.34 2003.26 110.76 o 3 1 -19 29.50 26.83 32.02 o 4 1 -19 495.88 477.26 45.89 o 5 1 -19 193.96 162.12 32.08 o 6 1 -19 168.50 243.59 37.64 o 7 1 -19 12.21 21.55 23.27 o 8 1 -19 336.07 323.64 56.25 o 3 2 -19 108.07 134.13 43.27 o 4 2 -19 10.98 12.11 35.48 o 5 2 -19 355.23 356.52 58.84 o 6 2 -19 53.92 64.04 39.81 o 7 2 -19 277.72 396.33 60.57 o 8 2 -19 97.16 102.98 43.27 o 4 3 -19 130.00 113.36 42.40 o 5 3 -19 79.09 168.74 47.59 o 6 3 -19 257.98 286.43 53.65 o 7 3 -19 8.73 23.36 34.61 o 0 0 -18 36.86 -20.77 32.88 o 2 0 -18 22.48 51.06 32.88 o 4 0 -18 26.06 -6.92 31.15 o 6 0 -18 651.16 623.05 70.96 o 8 0 -18 837.91 719.10 77.88 o 10 0 -18 1612.96 1832.79 104.71 o 0 1 -18 58.78 42.07 27.51 o 1 1 -18 417.36 433.98 43.39 o 2 1 -18 565.08 539.72 112.49 o 3 1 -18 15.89 37.52 22.89 o 4 1 -18 18.15 24.81 22.79 o 5 1 -18 204.10 189.16 32.41 o 6 1 -18 10.57 -11.21 20.49 o 7 1 -18 844.65 1095.79 113.79 o 8 1 -18 207.15 211.96 71.39 o 9 1 -18 731.80 695.46 52.93 o 10 1 -18 31.91 34.29 27.69 o 11 1 -18 579.31 665.45 78.75 o 0 2 -18 100.75 81.76 27.22 o 1 2 -18 2.30 25.05 23.23 o 2 2 -18 224.13 197.05 70.53 o 3 2 -18 167.03 135.60 50.19 o 4 2 -18 121.85 112.49 27.51 o 5 2 -18 285.74 277.82 35.70 o 6 2 -18 604.56 590.50 48.62 o 7 2 -18 4.28 3.03 25.09 o 8 2 -18 230.10 225.02 35.47 o 9 2 -18 117.05 110.48 29.96 o 10 2 -18 703.62 778.09 57.43 o 11 2 -18 287.77 265.66 53.65 o 0 3 -18 56.05 48.46 34.61 o 1 3 -18 266.48 346.64 41.22 o 2 3 -18 3.34 27.69 34.61 o 3 3 -18 148.64 134.87 28.68 o 4 3 -18 87.46 82.59 26.74 o 5 3 -18 497.79 459.62 61.01 o 6 3 -18 2.09 -20.56 20.56 o 7 3 -18 111.67 88.88 26.74 o 8 3 -18 18.73 5.16 22.54 o 9 3 -18 17.28 17.97 22.54 o 10 3 -18 175.08 184.98 33.92 o 0 4 -18 48.89 43.84 22.79 o 1 4 -18 7.52 -2.68 25.53 o 2 4 -18 194.45 216.37 34.86 o 3 4 -18 71.14 58.41 25.09 o 4 4 -18 267.59 240.54 34.57 o 5 4 -18 7.30 19.90 23.55 o 6 4 -18 346.84 428.63 43.72 o 7 4 -18 93.92 86.81 26.90 o 8 4 -18 220.01 186.37 33.50 o 9 4 -18 113.90 121.13 32.45 o 10 4 -18 355.01 386.81 57.98 o 1 5 -18 53.87 63.53 24.45 o 2 5 -18 53.73 28.71 24.78 o 3 5 -18 46.02 15.36 24.38 o 4 5 -18 79.92 48.72 22.94 o 5 5 -18 2.27 12.75 22.94 o 6 5 -18 148.78 110.26 29.06 o 7 5 -18 235.36 219.32 33.86 o 8 5 -18 160.66 162.14 32.22 o 9 5 -18 75.32 99.51 38.94 o 3 6 -18 31.07 12.11 29.42 o 4 6 -18 13.34 14.71 32.88 o 5 6 -18 9.69 -28.56 28.56 o 6 6 -18 277.76 187.78 51.06 o 7 6 -18 18.04 8.65 37.21 o -3 0 -17 83.82 70.96 38.07 o -1 0 -17 80.19 70.96 38.07 o 1 0 -17 557.55 538.24 63.17 o 3 0 -17 177.73 167.88 41.54 o 5 0 -17 388.02 308.93 48.46 o 7 0 -17 620.05 461.23 60.57 o 9 0 -17 75.45 64.04 34.61 o 11 0 -17 285.25 325.37 60.57 o -3 1 -17 39.12 20.94 23.50 o -2 1 -17 31.77 12.22 18.97 o -1 1 -17 42.07 24.36 18.31 o 0 1 -17 673.77 622.56 110.76 o 1 1 -17 882.97 796.58 55.37 o 2 1 -17 153.34 67.81 24.66 o 3 1 -17 96.88 84.37 25.70 o 4 1 -17 62.74 77.44 24.12 o 5 1 -17 44.34 51.20 23.55 o 6 1 -17 458.96 457.74 43.13 o 7 1 -17 8.12 -19.88 19.88 o 8 1 -17 507.71 579.86 47.12 o 9 1 -17 5.32 -9.95 19.55 o 10 1 -17 634.45 737.72 53.23 o 11 1 -17 205.08 247.72 57.98 o 12 1 -17 194.91 242.23 38.53 o -3 2 -17 95.61 116.82 41.54 o -2 2 -17 55.98 54.89 20.69 o -1 2 -17 144.67 159.58 24.27 o 0 2 -17 173.86 215.40 26.10 o 1 2 -17 403.27 393.05 78.75 o 2 2 -17 13.65 23.97 22.50 o 3 2 -17 85.05 87.07 26.00 o 4 2 -17 86.17 92.20 26.57 o 5 2 -17 212.72 249.84 33.59 o 6 2 -17 87.69 114.15 34.18 o 7 2 -17 139.31 194.49 64.90 o 8 2 -17 0.12 3.70 19.47 o 9 2 -17 829.81 944.37 90.43 o 10 2 -17 326.40 388.52 43.13 o 11 2 -17 644.13 735.74 71.39 o 12 2 -17 28.23 11.15 28.56 o -2 3 -17 129.02 135.01 23.95 o -1 3 -17 86.26 80.58 22.44 o 0 3 -17 334.50 294.41 29.14 o 1 3 -17 160.28 157.94 22.98 o 2 3 -17 287.18 291.17 35.79 o 3 3 -17 19.17 25.74 20.56 o 4 3 -17 240.54 198.56 46.73 o 5 3 -17 137.73 184.74 29.96 o 6 3 -17 90.08 86.26 45.86 o 7 3 -17 7.97 17.73 21.72 o 8 3 -17 293.98 335.04 38.15 o 9 3 -17 269.84 207.70 32.27 o 10 3 -17 404.01 402.99 42.17 o 11 3 -17 75.27 112.06 30.59 o 12 3 -17 119.34 160.94 61.44 o -2 4 -17 2.67 6.90 22.94 o -1 4 -17 372.66 361.21 51.28 o 0 4 -17 82.16 63.57 20.71 o 1 4 -17 165.49 210.94 25.33 o 2 4 -17 5.60 1.10 17.74 o 3 4 -17 409.18 409.40 40.52 o 4 4 -17 30.35 50.74 23.84 o 5 4 -17 294.42 285.17 58.41 o 6 4 -17 180.09 169.39 47.16 o 7 4 -17 214.55 234.36 33.65 o 8 4 -17 75.11 113.14 28.74 o 9 4 -17 275.77 385.89 41.22 o 10 4 -17 286.15 347.59 40.26 o 11 4 -17 288.66 303.58 39.43 o 12 4 -17 546.10 592.76 72.69 o -1 5 -17 165.12 164.01 25.91 o 0 5 -17 39.51 32.97 21.03 o 1 5 -17 5.83 -15.89 15.89 o 2 5 -17 173.52 204.09 28.12 o 3 5 -17 45.83 59.22 18.97 o 4 5 -17 314.61 319.36 36.92 o 5 5 -17 190.67 147.01 28.45 o 6 5 -17 292.07 290.47 36.92 o 7 5 -17 2.59 8.33 21.10 o 8 5 -17 473.15 541.25 49.32 o 9 5 -17 13.50 59.77 25.35 o 10 5 -17 133.16 131.10 31.51 o 11 5 -17 266.03 276.50 38.24 o -1 6 -17 64.89 50.74 29.02 o 0 6 -17 21.35 7.99 22.28 o 1 6 -17 52.46 54.44 41.97 o 2 6 -17 7.67 -1.30 19.58 o 3 6 -17 14.17 34.44 45.86 o 4 6 -17 194.85 206.82 47.59 o 6 6 -17 55.19 35.48 33.75 o 7 6 -17 89.30 66.63 36.34 o 8 6 -17 21.27 72.69 38.07 o 9 6 -17 654.05 627.37 70.96 o 10 6 -17 16.52 32.88 40.67 o 0 7 -17 43.36 82.86 28.45 o 1 7 -17 2.79 16.35 23.23 o 2 7 -17 213.51 233.83 36.04 o 3 7 -17 161.76 197.27 30.90 o 4 7 -17 494.68 434.91 42.17 o 5 7 -17 40.89 41.54 34.61 o 6 7 -17 23.75 5.19 32.88 o 7 7 -17 50.81 49.32 39.81 o 8 7 -17 302.38 314.12 52.79 o 9 7 -17 197.51 162.68 49.32 o 2 8 -17 10.00 -19.82 19.82 o 3 8 -17 162.89 126.10 29.98 o 4 8 -17 132.13 113.21 28.45 o 5 8 -17 117.55 161.96 31.51 o 6 8 -17 28.11 0.00 34.61 o 7 8 -17 246.35 276.91 51.92 o 8 8 -17 40.99 10.38 36.34 o -4 0 -16 27.76 43.27 32.88 o -2 0 -16 549.70 484.59 57.98 o 0 0 -16 296.87 327.10 51.06 o 2 0 -16 1647.91 1469.35 88.26 o 4 0 -16 75.36 94.32 33.75 o 6 0 -16 691.78 580.64 63.17 o 8 0 -16 85.60 170.47 40.67 o 10 0 -16 323.95 221.53 45.86 o 12 0 -16 18.61 49.32 37.21 o -4 1 -16 23.15 23.21 36.78 o -3 1 -16 174.46 178.26 30.58 o -2 1 -16 36.24 -16.27 46.73 o -1 1 -16 881.45 708.85 39.91 o 0 1 -16 211.46 165.31 22.44 o 1 1 -16 306.57 335.76 37.31 o 2 1 -16 1183.74 1045.10 53.65 o 3 1 -16 59.49 68.57 22.42 o 4 1 -16 98.40 108.92 24.51 o 5 1 -16 90.98 64.63 27.69 o 6 1 -16 9.11 18.69 21.31 o 7 1 -16 1213.52 1292.08 56.60 o 8 1 -16 0.03 20.28 20.44 o 9 1 -16 555.67 541.45 64.90 o 10 1 -16 66.54 113.51 41.10 o 11 1 -16 126.62 167.16 53.22 o 12 1 -16 4.13 34.87 24.45 o 13 1 -16 298.50 311.01 45.86 o 14 1 -16 0.82 39.81 44.13 o -4 2 -16 92.69 106.55 29.29 o -3 2 -16 10.93 -4.33 23.25 o -2 2 -16 148.37 147.97 40.67 o -1 2 -16 146.67 90.50 20.90 o 0 2 -16 819.09 782.93 53.08 o 1 2 -16 30.35 9.77 15.82 o 2 2 -16 94.41 100.53 26.12 o 3 2 -16 238.67 163.11 28.74 o 4 2 -16 229.28 254.57 32.89 o 5 2 -16 233.75 273.29 41.97 o 6 2 -16 50.04 63.03 33.75 o 7 2 -16 35.48 17.46 20.16 o 8 2 -16 935.28 961.94 51.57 o 9 2 -16 41.06 12.90 20.49 o 10 2 -16 532.47 599.37 91.29 o 11 2 -16 9.84 24.02 22.42 o 12 2 -16 47.79 42.16 26.83 o 13 2 -16 8.68 -24.12 24.12 o 14 2 -16 244.90 249.22 55.38 o -4 3 -16 0.43 -18.70 18.70 o -3 3 -16 194.48 193.84 44.13 o -2 3 -16 273.74 259.89 42.83 o -1 3 -16 343.79 363.00 37.02 o 0 3 -16 219.17 166.32 23.81 o 1 3 -16 108.62 129.09 30.15 o 2 3 -16 268.10 290.35 26.30 o 3 3 -16 55.87 118.07 26.23 o 4 3 -16 219.12 225.18 30.72 o 5 3 -16 63.42 51.63 21.80 o 6 3 -16 38.04 51.52 22.79 o 7 3 -16 298.30 327.83 43.70 o 8 3 -16 9.01 14.72 18.48 o 9 3 -16 367.24 420.56 47.59 o 10 3 -16 38.17 44.83 28.56 o 11 3 -16 231.43 301.31 37.70 o 12 3 -16 75.04 52.62 25.96 o 13 3 -16 266.51 341.57 42.36 o -4 4 -16 371.62 348.73 57.98 o -3 4 -16 75.59 46.73 39.81 o -2 4 -16 117.35 118.39 21.88 o -1 4 -16 10.69 -12.04 16.89 o 0 4 -16 52.77 76.29 19.40 o 1 4 -16 55.45 46.41 18.23 o 2 4 -16 297.84 325.83 28.17 o 3 4 -16 27.67 52.04 17.29 o 4 4 -16 238.62 264.70 33.02 o 5 4 -16 116.04 109.40 24.89 o 6 4 -16 154.08 247.19 33.02 o 7 4 -16 54.85 27.51 21.31 o 8 4 -16 195.90 191.50 29.85 o 9 4 -16 105.72 147.20 28.45 o 10 4 -16 433.15 543.00 45.78 o 11 4 -16 322.90 314.64 37.31 o 12 4 -16 1796.30 1790.49 72.51 o 13 4 -16 149.21 188.96 35.48 o -3 5 -16 407.66 389.40 58.84 o -2 5 -16 163.46 124.02 22.98 o -1 5 -16 24.35 34.86 18.15 o 0 5 -16 7.80 34.64 17.86 o 1 5 -16 144.00 122.21 21.83 o 2 5 -16 120.60 74.30 19.43 o 3 5 -16 501.29 501.38 42.71 o 4 5 -16 600.81 583.98 64.48 o 5 5 -16 427.19 477.47 41.27 o 6 5 -16 41.55 7.85 22.00 o 7 5 -16 365.50 394.77 39.03 o 8 5 -16 16.96 -5.77 20.16 o 9 5 -16 431.21 427.09 40.69 o 10 5 -16 303.01 265.60 34.86 o 11 5 -16 534.16 513.62 47.16 o 12 5 -16 215.99 236.73 76.15 o 13 5 -16 19.79 -18.17 35.48 o -3 6 -16 7.40 5.88 25.09 o -2 6 -16 127.71 108.77 22.08 o -1 6 -16 15.00 5.19 17.80 o 0 6 -16 228.05 186.37 24.95 o 1 6 -16 15.32 44.87 17.70 o 2 6 -16 354.17 373.56 29.95 o 3 6 -16 46.79 30.60 17.52 o 4 6 -16 330.33 349.55 45.88 o 5 6 -16 73.26 61.76 18.89 o 6 6 -16 598.04 597.10 46.31 o 7 6 -16 10.09 16.44 31.15 o 8 6 -16 395.53 347.87 55.38 o 9 6 -16 159.46 196.43 46.73 o 10 6 -16 310.08 327.10 57.11 o 11 6 -16 167.56 207.68 51.92 o 12 6 -16 102.59 63.17 38.94 o -2 7 -16 119.79 77.15 46.30 o -1 7 -16 39.96 34.50 24.16 o 0 7 -16 50.49 76.73 27.22 o 1 7 -16 150.70 111.18 44.13 o 2 7 -16 50.01 43.68 23.50 o 3 7 -16 413.89 525.64 43.33 o 4 7 -16 20.75 16.79 20.78 o 5 7 -16 105.23 100.64 25.78 o 6 7 -16 62.45 38.76 22.65 o 7 7 -16 393.84 398.92 58.84 o 8 7 -16 27.64 -28.56 28.56 o 9 7 -16 283.54 244.03 49.32 o 10 7 -16 65.03 65.77 37.21 o 11 7 -16 708.43 780.54 79.61 o -1 8 -16 65.47 62.30 27.22 o 0 8 -16 75.04 69.97 25.96 o 1 8 -16 42.53 43.70 25.09 o 2 8 -16 90.91 94.08 43.70 o 3 8 -16 20.32 26.85 21.18 o 4 8 -16 25.50 52.76 42.40 o 5 8 -16 7.47 12.55 21.42 o 6 8 -16 272.12 278.57 34.86 o 7 8 -16 266.74 306.33 53.65 o 8 8 -16 277.34 326.23 55.38 o 9 8 -16 21.71 12.11 32.88 o 10 8 -16 274.22 277.77 52.79 o 0 9 -16 24.93 24.10 24.73 o 1 9 -16 105.01 98.65 28.15 o 2 9 -16 18.68 -9.66 32.88 o 3 9 -16 39.65 63.62 24.73 o 4 9 -16 8.32 28.05 24.66 o 5 9 -16 359.49 457.45 42.22 o 6 9 -16 238.63 287.21 36.47 o 7 9 -16 527.79 585.29 47.35 o 8 9 -16 42.01 39.81 32.88 o 9 9 -16 101.78 181.72 49.32 o 2 10 -16 92.18 101.11 28.48 o 3 10 -16 97.58 115.23 54.08 o 4 10 -16 133.38 129.43 28.41 o 5 10 -16 171.51 199.68 33.24 o 6 10 -16 153.78 146.90 32.02 o 7 10 -16 116.94 119.15 28.45 o -5 0 -15 189.79 257.87 51.06 o -3 0 -15 233.75 211.14 44.13 o -1 0 -15 108.04 100.92 24.02 o 1 0 -15 1516.90 1420.60 54.56 o 3 0 -15 555.69 507.95 57.11 o 5 0 -15 3371.10 3360.12 125.47 o 7 0 -15 300.01 322.77 48.46 o 9 0 -15 386.22 566.80 63.17 o 11 0 -15 1463.75 1377.62 84.80 o 13 0 -15 29.14 45.86 39.81 o -6 1 -15 42.51 91.23 28.74 o -5 1 -15 167.05 115.23 29.45 o -4 1 -15 137.56 209.72 30.79 o -3 1 -15 2.58 0.19 55.38 o -2 1 -15 610.14 686.99 45.27 o -1 1 -15 3.49 -0.81 12.97 o 0 1 -15 946.04 922.06 32.29 o 1 1 -15 835.37 745.33 34.27 o 2 1 -15 67.87 39.79 14.99 o 3 1 -15 183.11 176.55 54.08 o 4 1 -15 1276.01 1288.25 54.09 o 5 1 -15 19.54 44.71 24.23 o 6 1 -15 1164.89 1159.46 52.00 o 7 1 -15 119.90 102.17 23.84 o 8 1 -15 1051.34 1029.46 51.09 o 9 1 -15 201.67 161.36 45.43 o 10 1 -15 541.35 479.56 42.52 o 11 1 -15 57.06 63.52 24.12 o 12 1 -15 270.51 335.04 40.37 o 13 1 -15 6.17 -5.69 23.16 o 14 1 -15 474.57 528.04 124.61 o -6 2 -15 325.95 315.50 40.37 o -5 2 -15 200.06 204.33 33.24 o -4 2 -15 430.40 467.74 42.10 o -3 2 -15 237.79 265.10 32.12 o -2 2 -15 2.39 -1.73 19.71 o -1 2 -15 1137.31 1100.23 36.46 o 0 2 -15 17.68 -12.17 13.28 o 1 2 -15 152.51 162.95 21.56 o 2 2 -15 37.06 44.26 16.14 o 3 2 -15 122.45 121.99 24.48 o 4 2 -15 0.46 15.91 17.43 o 5 2 -15 212.80 178.34 41.10 o 6 2 -15 23.53 13.41 18.36 o 7 2 -15 131.39 159.54 27.35 o 8 2 -15 524.48 488.34 39.43 o 9 2 -15 1037.77 1042.27 91.73 o 10 2 -15 63.68 30.23 22.28 o 11 2 -15 212.16 318.91 37.33 o 12 2 -15 19.21 7.84 28.99 o 13 2 -15 312.69 370.48 65.33 o 14 2 -15 11.26 -15.26 23.16 o -6 3 -15 117.72 164.15 34.20 o -5 3 -15 21.80 29.71 24.45 o -4 3 -15 206.61 234.79 33.92 o -3 3 -15 246.66 291.44 34.73 o -2 3 -15 147.99 164.80 57.55 o -1 3 -15 47.15 36.96 17.65 o 0 3 -15 169.28 140.34 20.38 o 1 3 -15 24.05 29.19 15.62 o 2 3 -15 220.28 183.22 22.40 o 3 3 -15 52.89 63.22 16.71 o 4 3 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