#------------------------------------------------------------------------------ #$Date: 2016-04-06 16:30:44 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181866 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/96/2019694.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2019694 _cell_angle_alpha 90.000 _cell_angle_beta 90.488 _cell_angle_gamma 90.000 _cell_length_a 5.3348 _cell_length_b 18.4371 _cell_length_c 16.4712 _exptl_crystal_F_000 884.00 _reflns_d_resolution_high 0.8255 _cod_data_source_file sk3554Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 271.67 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2.75 0.00 11.10 o 3 0 0 13587.22 13050.78 911.21 o 4 0 0 9572.40 8988.90 639.92 o 5 0 0 8139.80 8202.86 316.83 o 6 0 0 527.93 667.20 173.38 o 1 1 0 2258.88 2311.55 53.76 o 2 1 0 4677.95 4529.09 84.74 o 3 1 0 607.08 590.67 39.41 o 4 1 0 16.47 27.95 20.42 o 5 1 0 280.70 159.75 43.84 o 6 1 0 447.17 728.68 182.35 o 0 2 0 3865.86 3954.57 192.11 o 1 2 0 4720.43 4846.68 89.56 o 2 2 0 158.67 125.60 23.59 o 3 2 0 1499.85 1526.92 57.58 o 4 2 0 1946.23 2080.41 76.73 o 5 2 0 0.98 59.88 35.15 o 6 2 0 14.94 138.45 116.21 o 1 3 0 5151.22 5151.31 135.62 o 2 3 0 8438.76 7673.02 187.98 o 3 3 0 6016.32 5924.10 130.92 o 4 3 0 195.21 217.18 32.00 o 5 3 0 2247.56 2445.85 122.36 o 6 3 0 2390.61 2541.59 206.02 o 0 4 0 3528.08 3748.48 108.55 o 1 4 0 509.21 602.50 36.12 o 2 4 0 734.97 791.62 43.25 o 3 4 0 4746.05 4926.78 133.60 o 4 4 0 2483.74 2661.38 97.11 o 5 4 0 1287.15 1233.36 179.75 o 6 4 0 35.88 15.95 100.03 o 1 5 0 4171.24 4378.95 106.27 o 2 5 0 110.62 135.26 20.75 o 3 5 0 856.10 775.47 51.58 o 4 5 0 109.42 125.68 49.78 o 5 5 0 2.26 61.76 37.08 o 6 5 0 18.57 104.52 86.58 o 0 6 0 13855.80 14014.45 311.41 o 1 6 0 2600.31 2505.21 103.74 o 2 6 0 778.06 772.03 42.45 o 3 6 0 4982.38 5135.49 122.00 o 4 6 0 5480.71 5477.41 171.89 o 5 6 0 1310.68 1532.16 139.86 o 6 6 0 31.35 133.96 122.13 o 1 7 0 2010.04 1711.49 132.60 o 2 7 0 12147.71 12305.71 241.66 o 3 7 0 1259.10 1271.21 88.27 o 4 7 0 236.00 333.84 51.56 o 5 7 0 1757.92 1959.46 179.52 o 6 7 0 778.82 860.90 148.53 o 0 8 0 4475.41 5125.91 216.42 o 1 8 0 811.67 904.96 52.42 o 2 8 0 2.90 0.00 13.64 o 3 8 0 653.27 646.19 68.67 o 4 8 0 339.47 374.70 94.20 o 5 8 0 10.61 87.11 85.58 o 6 8 0 93.16 264.99 157.39 o 1 9 0 9483.04 9520.08 186.81 o 2 9 0 12027.18 11731.76 217.15 o 3 9 0 4063.13 3876.00 185.53 o 4 9 0 156.73 401.73 132.02 o 5 9 0 3054.77 3015.18 232.82 o 0 10 0 4202.02 3886.63 159.30 o 1 10 0 14436.18 14358.16 256.34 o 2 10 0 544.87 406.13 55.01 o 3 10 0 3937.16 3923.93 160.73 o 4 10 0 3729.18 4044.85 375.28 o 5 10 0 345.59 401.28 142.11 o 1 11 0 37.17 22.98 20.87 o 2 11 0 801.42 905.42 106.71 o 3 11 0 562.10 458.80 83.86 o 4 11 0 323.04 233.89 113.09 o 5 11 0 3.10 13.25 59.99 o 0 12 0 1534.47 1412.97 105.38 o 1 12 0 6120.57 5908.90 154.37 o 2 12 0 941.15 840.32 107.69 o 3 12 0 517.10 601.20 78.39 o 4 12 0 3018.69 2653.01 213.27 o 5 12 0 403.49 337.17 110.20 o 1 13 0 3673.97 3560.65 184.66 o 2 13 0 8938.38 8441.13 323.31 o 3 13 0 2038.23 1959.99 126.85 o 4 13 0 12.23 2.70 61.19 o 5 13 0 795.41 711.32 144.77 o 0 14 0 2132.22 2235.20 186.01 o 1 14 0 653.15 668.00 76.43 o 2 14 0 638.91 516.79 115.71 o 3 14 0 123.59 136.24 47.79 o 4 14 0 363.90 234.33 93.03 o 1 15 0 2325.87 2432.05 131.51 o 2 15 0 3612.79 2479.37 610.93 o 3 15 0 1996.07 1926.19 183.67 o 4 15 0 320.60 272.13 149.78 o 0 16 0 986.07 1026.52 168.29 o 1 16 0 1752.90 2129.99 203.95 o 2 16 0 23.33 6.11 40.08 o 3 16 0 1034.66 1353.99 163.37 o 4 16 0 1088.59 1315.59 385.79 o 1 17 0 1209.63 1269.77 110.97 o 2 17 0 325.49 357.91 73.46 o 3 17 0 303.53 395.95 108.62 o 4 17 0 9.92 116.96 79.12 o 0 18 0 1054.71 891.52 174.89 o 1 18 0 1046.55 1217.91 112.35 o 2 18 0 0.53 91.67 82.42 o 3 18 0 446.87 495.86 132.60 o 1 19 0 3017.15 3121.92 209.17 o 2 19 0 3065.43 3136.43 228.28 o 3 19 0 745.40 737.78 145.89 o 0 20 0 908.61 1355.28 225.10 o 1 20 0 964.21 1016.69 139.91 o 2 20 0 18.81 91.32 85.22 o 1 21 0 95.52 122.35 68.71 o 2 21 0 355.82 281.06 142.68 o 0 22 0 2286.66 2360.21 302.00 o 1 22 0 486.01 510.68 179.84 o -6 1 1 27.91 226.74 169.40 o -5 1 1 746.12 856.96 93.59 o -4 1 1 4069.20 4159.25 109.52 o -3 1 1 2182.86 2077.98 65.09 o -2 1 1 10.62 6.58 8.70 o -1 1 1 11356.85 11297.81 151.36 o 0 1 1 32333.97 31008.09 451.58 o 1 1 1 168.42 195.16 18.90 o 2 1 1 288.64 357.96 28.35 o 3 1 1 9527.50 9569.62 230.67 o 4 1 1 8420.12 8287.71 201.00 o 5 1 1 2213.52 2093.53 100.45 o -6 2 1 1498.81 1742.28 180.06 o -5 2 1 1200.87 1194.42 92.25 o -4 2 1 14.18 41.31 21.16 o -3 2 1 1407.45 1397.30 59.25 o -2 2 1 25175.81 25106.86 295.01 o -1 2 1 20601.31 20703.63 277.38 o 0 2 1 759.31 790.24 21.48 o 1 2 1 8208.84 7854.30 113.33 o 2 2 1 14934.63 14584.64 209.12 o 3 2 1 6945.36 7351.95 148.29 o 4 2 1 94.38 80.79 23.16 o 5 2 1 2123.30 2161.97 143.71 o 6 2 1 887.40 960.82 141.35 o -6 3 1 0.02 0.00 59.24 o -5 3 1 201.88 268.94 64.21 o -4 3 1 324.28 358.52 39.17 o -3 3 1 528.55 483.11 35.72 o -2 3 1 4240.11 4499.68 94.10 o -1 3 1 149.92 152.13 21.56 o 0 3 1 1455.69 1524.56 46.85 o 1 3 1 10.92 11.84 7.80 o 2 3 1 932.42 998.87 42.08 o 3 3 1 442.28 445.15 35.66 o 4 3 1 2.48 3.02 19.12 o 5 3 1 103.17 144.94 47.27 o 6 3 1 9.75 42.40 72.99 o -6 4 1 1530.66 1686.58 179.38 o -5 4 1 1899.80 1952.19 116.71 o -4 4 1 0.37 35.14 30.37 o -3 4 1 4603.06 4698.79 102.47 o -2 4 1 3348.22 3041.64 74.35 o -1 4 1 16464.91 16320.35 325.15 o 0 4 1 4614.03 4822.10 114.00 o 1 4 1 12733.24 13248.62 181.69 o 2 4 1 12505.52 12587.73 219.90 o 3 4 1 354.73 354.38 36.09 o 4 4 1 99.34 96.23 26.56 o 5 4 1 2576.44 2532.16 149.42 o 6 4 1 1483.05 1717.37 180.22 o -6 5 1 16.94 107.18 71.50 o -5 5 1 4648.29 4227.04 164.44 o -4 5 1 11311.35 11331.90 259.14 o -3 5 1 4969.79 4723.99 114.58 o -2 5 1 570.27 577.05 35.03 o -1 5 1 15293.11 14441.79 307.40 o 0 5 1 32621.00 30607.51 1379.28 o 1 5 1 3568.41 3521.91 75.30 o 2 5 1 100.04 123.95 20.59 o 3 5 1 5806.09 6025.51 134.62 o 4 5 1 5597.02 5683.83 224.57 o 5 5 1 1255.09 1380.28 122.15 o 6 5 1 135.36 159.86 113.68 o -6 6 1 202.89 60.43 90.41 o -5 6 1 259.03 241.33 67.12 o -4 6 1 196.62 177.66 42.47 o -3 6 1 105.52 144.04 45.50 o -2 6 1 312.38 297.63 40.98 o -1 6 1 389.33 457.10 30.40 o 0 6 1 5977.98 6376.10 126.00 o 1 6 1 150.48 150.33 20.60 o 2 6 1 2717.53 2720.36 82.44 o 3 6 1 1227.07 1361.68 87.68 o 4 6 1 119.01 128.49 32.45 o 5 6 1 259.84 313.58 82.08 o 6 6 1 126.08 183.82 80.09 o -6 7 1 0.96 0.00 94.94 o -5 7 1 581.69 476.78 83.93 o -4 7 1 1178.91 1205.55 128.56 o -3 7 1 177.99 108.35 53.37 o -2 7 1 6.00 11.62 12.24 o -1 7 1 3814.40 3849.00 92.24 o 0 7 1 2683.07 2757.01 80.27 o 1 7 1 1948.27 1908.52 64.81 o 2 7 1 8.94 0.00 12.15 o 3 7 1 123.86 145.51 27.54 o 4 7 1 1149.66 1064.56 83.57 o 5 7 1 162.96 149.02 59.61 o 6 7 1 32.56 182.85 84.36 o -6 8 1 1443.98 1596.06 192.37 o -5 8 1 1897.54 2151.28 257.96 o -4 8 1 36.10 113.46 42.91 o -3 8 1 4840.67 4910.55 172.28 o -2 8 1 13757.00 13973.62 263.52 o -1 8 1 6731.61 6770.82 195.29 o 0 8 1 1930.73 2118.66 73.79 o 1 8 1 14936.73 15224.01 252.85 o 2 8 1 16930.58 16767.60 277.95 o 3 8 1 3995.43 4208.06 216.18 o 4 8 1 168.39 177.85 44.59 o 5 8 1 1624.26 1798.76 146.50 o 6 8 1 1983.91 2199.27 216.56 o -5 9 1 789.16 778.34 167.89 o -4 9 1 1705.11 1659.02 157.64 o -3 9 1 2996.67 3144.61 139.54 o -2 9 1 861.06 1109.48 81.38 o -1 9 1 4736.78 5036.53 122.25 o 0 9 1 13480.16 13789.52 242.41 o 1 9 1 2959.66 2874.41 90.74 o 2 9 1 7.25 3.27 16.79 o 3 9 1 4285.37 4155.17 270.23 o 4 9 1 2006.08 2209.57 265.42 o 5 9 1 469.42 829.47 196.34 o -5 10 1 533.68 708.26 129.35 o -4 10 1 28.21 0.00 65.89 o -3 10 1 2123.92 2077.87 142.65 o -2 10 1 2598.10 2548.06 118.20 o -1 10 1 5532.63 5508.15 135.32 o 0 10 1 0.54 11.20 17.46 o 1 10 1 1170.11 1269.04 75.08 o 2 10 1 2115.11 2180.10 106.42 o 3 10 1 2336.09 2199.73 166.26 o 4 10 1 19.54 106.74 126.29 o 5 10 1 742.20 643.54 130.71 o -5 11 1 583.52 687.36 202.15 o -4 11 1 3749.73 3473.03 320.08 o -3 11 1 3681.59 3189.52 353.06 o -2 11 1 4.55 16.71 26.82 o -1 11 1 3069.98 3011.88 100.42 o 0 11 1 6435.27 6359.95 237.77 o 1 11 1 12082.92 11905.57 271.21 o 2 11 1 1305.56 1290.98 90.91 o 3 11 1 4131.16 3981.89 267.54 o 4 11 1 4183.90 4393.45 251.73 o 5 11 1 728.40 793.33 138.57 o -5 12 1 156.35 120.43 79.69 o -4 12 1 9.49 15.05 75.86 o -3 12 1 1588.26 1214.17 145.06 o -2 12 1 949.28 986.65 87.96 o -1 12 1 816.94 798.37 77.35 o 0 12 1 12.91 54.36 23.50 o 1 12 1 1116.16 1077.81 77.80 o 2 12 1 3910.85 4046.26 159.69 o 3 12 1 197.11 206.03 50.49 o 4 12 1 136.55 73.72 77.72 o 5 12 1 244.54 372.01 255.88 o -5 13 1 119.45 74.64 73.08 o -4 13 1 240.34 207.60 82.79 o -3 13 1 1035.67 866.68 106.51 o -2 13 1 4.70 50.53 34.74 o -1 13 1 620.60 616.43 74.33 o 0 13 1 873.70 1024.58 69.16 o 1 13 1 1309.64 1329.42 77.06 o 2 13 1 118.60 28.94 61.49 o 3 13 1 757.69 564.87 108.59 o 4 13 1 265.73 212.47 83.51 o 5 13 1 14.32 12.29 56.06 o -4 14 1 11.67 12.92 58.55 o -3 14 1 1612.79 1355.87 192.53 o -2 14 1 7546.71 7671.57 276.14 o -1 14 1 511.85 424.35 74.86 o 0 14 1 755.61 722.84 62.42 o 1 14 1 4471.42 4420.87 172.02 o 2 14 1 2120.20 2208.19 130.15 o 3 14 1 2719.37 2627.56 203.58 o 4 14 1 501.54 315.17 156.17 o 5 14 1 1341.37 1566.54 272.16 o -4 15 1 1525.71 1260.90 390.67 o -3 15 1 2274.81 1932.45 198.91 o -2 15 1 16.38 0.00 38.55 o -1 15 1 2474.56 2641.35 140.88 o 0 15 1 2066.83 2148.43 119.90 o 1 15 1 1743.39 1781.86 228.24 o 2 15 1 121.49 125.20 46.98 o 3 15 1 982.01 1130.11 148.76 o 4 15 1 1099.04 1023.11 162.72 o -4 16 1 146.42 128.07 80.97 o -3 16 1 169.55 251.22 84.97 o -2 16 1 133.02 79.14 44.81 o -1 16 1 862.57 888.75 105.14 o 0 16 1 184.53 187.01 46.20 o 1 16 1 50.47 32.65 37.27 o 2 16 1 32.65 11.27 45.87 o 3 16 1 1.91 0.00 53.01 o 4 16 1 12.39 0.00 64.13 o -4 17 1 1114.23 1195.52 183.04 o -3 17 1 1289.50 1457.56 179.68 o -2 17 1 15.88 1.34 42.30 o -1 17 1 2988.51 3143.95 179.64 o 0 17 1 4964.98 5306.44 402.36 o 1 17 1 3530.96 3714.78 226.82 o 2 17 1 1.06 50.32 54.98 o 3 17 1 1123.33 1211.13 201.82 o 4 17 1 1978.01 1496.13 199.05 o -3 18 1 1322.47 1205.77 168.24 o -2 18 1 2906.44 2824.65 168.49 o -1 18 1 1734.74 1961.20 138.45 o 0 18 1 144.44 0.00 46.24 o 1 18 1 3234.35 3419.08 170.86 o 2 18 1 2854.60 3243.57 239.66 o 3 18 1 1266.64 1062.50 163.70 o -3 19 1 5.20 132.89 123.74 o -2 19 1 0.00 99.82 58.33 o -1 19 1 48.55 76.60 50.44 o 0 19 1 0.78 0.00 53.91 o 1 19 1 27.57 123.90 62.08 o 2 19 1 20.44 60.68 123.17 o 3 19 1 1.64 0.00 88.34 o -2 20 1 2314.48 1960.73 195.39 o -1 20 1 1211.22 1219.23 170.19 o 0 20 1 0.06 127.65 279.98 o 1 20 1 886.88 858.38 192.75 o 2 20 1 1384.08 1446.92 245.40 o -2 21 1 66.98 241.66 112.80 o -1 21 1 721.39 697.85 193.68 o 0 21 1 1257.62 1430.24 166.83 o 1 21 1 518.59 556.01 168.00 o 2 21 1 29.19 87.30 91.39 o -1 22 1 100.20 63.05 110.54 o 0 22 1 2.32 0.00 85.76 o 1 22 1 83.45 327.75 124.89 o -6 0 2 0.71 0.00 106.96 o -5 0 2 1593.39 1475.29 205.38 o -4 0 2 10173.35 10135.36 260.09 o -3 0 2 6039.03 5916.14 164.23 o -2 0 2 309.34 330.65 33.73 o -1 0 2 73805.89 68122.91 3937.40 o 0 0 2 30679.58 30021.88 902.89 o 1 0 2 33275.74 31226.31 717.31 o 2 0 2 632.87 627.76 45.37 o 3 0 2 25673.62 26413.08 474.21 o 4 0 2 15348.51 15286.12 609.78 o 5 0 2 224.07 330.46 111.05 o -6 1 2 18.17 0.00 65.12 o -5 1 2 1962.47 1979.78 271.37 o -4 1 2 789.64 861.66 75.33 o -3 1 2 1251.20 1282.34 51.59 o -2 1 2 4558.17 4589.46 84.28 o -1 1 2 5069.67 5116.35 82.99 o 0 1 2 478.79 448.37 19.42 o 1 1 2 22380.41 22372.20 267.43 o 2 1 2 2068.02 1940.80 64.63 o 3 1 2 307.66 291.58 36.83 o 4 1 2 78.16 145.49 29.40 o 5 1 2 360.76 392.77 48.47 o -6 2 2 114.47 4.47 200.18 o -5 2 2 276.82 265.95 61.26 o -4 2 2 79.78 35.53 22.96 o -3 2 2 686.09 771.53 42.58 o -2 2 2 3503.52 3748.35 74.42 o -1 2 2 1585.23 1604.52 40.84 o 0 2 2 8635.24 8550.52 112.54 o 1 2 2 2.30 0.00 5.74 o 2 2 2 403.93 473.78 35.00 o 3 2 2 2925.95 3020.24 89.71 o 4 2 2 4193.56 4280.93 124.93 o 5 2 2 367.05 276.21 84.56 o 6 2 2 598.11 336.36 131.35 o -6 3 2 1891.00 1841.37 185.20 o -5 3 2 2010.40 2092.49 139.46 o -4 3 2 2.64 0.00 27.18 o -3 3 2 1794.31 1752.54 64.22 o -2 3 2 26000.63 25371.42 349.71 o -1 3 2 5032.11 4926.65 117.53 o 0 3 2 57.90 53.43 10.14 o 1 3 2 1322.76 1241.99 36.10 o 2 3 2 12347.31 11943.72 183.08 o 3 3 2 6786.08 6615.81 139.42 o 4 3 2 55.73 49.88 26.02 o 5 3 2 3776.82 3876.16 154.93 o 6 3 2 1452.33 1125.24 155.26 o -6 4 2 231.59 196.19 123.01 o -5 4 2 3457.95 3364.91 198.59 o -4 4 2 3258.54 3320.01 211.84 o -3 4 2 248.93 201.14 27.69 o -2 4 2 630.73 605.71 35.56 o -1 4 2 2225.91 2230.15 76.19 o 0 4 2 17603.45 18528.57 256.81 o 1 4 2 1181.08 1162.38 38.33 o 2 4 2 54.94 39.01 13.84 o 3 4 2 3872.98 3887.67 103.14 o 4 4 2 1801.60 1906.39 82.92 o 5 4 2 207.26 182.32 56.31 o 6 4 2 176.51 368.61 81.13 o -6 5 2 162.80 286.27 95.95 o -5 5 2 3.40 0.00 35.46 o -4 5 2 269.02 320.64 60.72 o -3 5 2 222.13 209.54 27.31 o -2 5 2 48.71 16.42 19.39 o -1 5 2 4.03 12.52 14.05 o 0 5 2 10829.27 11328.63 182.05 o 1 5 2 15.41 4.50 8.95 o 2 5 2 10.18 10.75 12.26 o 3 5 2 137.83 173.33 27.95 o 4 5 2 139.18 114.01 36.14 o 5 5 2 238.91 171.25 63.39 o 6 5 2 16.84 38.91 56.51 o -6 6 2 4.23 119.59 81.27 o -5 6 2 2769.45 2737.09 191.50 o -4 6 2 6956.62 7011.21 228.10 o -3 6 2 4781.40 4780.66 164.55 o -2 6 2 2.71 7.96 19.69 o -1 6 2 16515.14 16613.67 358.36 o 0 6 2 25129.78 23676.35 576.41 o 1 6 2 5067.44 5039.31 100.52 o 2 6 2 3.67 0.00 11.43 o 3 6 2 3978.24 4160.85 110.63 o 4 6 2 4984.49 4889.09 159.44 o 5 6 2 1107.45 1397.85 127.33 o 6 6 2 0.23 79.20 61.58 o -6 7 2 916.57 865.66 153.94 o -5 7 2 1864.89 1815.28 137.19 o -4 7 2 59.55 53.82 36.08 o -3 7 2 3970.16 4088.96 154.13 o -2 7 2 16832.00 16738.52 337.76 o -1 7 2 10004.95 10184.41 401.94 o 0 7 2 4379.41 4945.59 132.09 o 1 7 2 7572.34 7386.59 147.50 o 2 7 2 7475.97 7099.00 167.87 o 3 7 2 1149.02 1195.48 60.89 o 4 7 2 44.83 8.44 49.26 o 5 7 2 505.41 652.49 98.19 o 6 7 2 1408.40 1617.76 256.92 o -6 8 2 6.56 51.39 70.45 o -5 8 2 230.87 231.34 76.91 o -4 8 2 122.84 105.08 62.71 o -3 8 2 73.46 83.53 33.16 o -2 8 2 7.06 0.74 20.83 o -1 8 2 1716.10 1867.24 101.23 o 0 8 2 0.41 0.00 13.24 o 1 8 2 32.17 33.82 16.84 o 2 8 2 450.31 499.03 39.42 o 3 8 2 518.89 571.40 57.56 o 4 8 2 4.62 126.88 52.57 o 5 8 2 0.36 26.41 57.00 o -5 9 2 121.39 157.07 63.95 o -4 9 2 113.10 128.92 44.27 o -3 9 2 4743.93 4653.51 174.71 o -2 9 2 6888.06 6935.95 249.81 o -1 9 2 10673.70 10882.65 200.56 o 0 9 2 2540.70 2700.82 88.40 o 1 9 2 10564.84 10516.22 202.98 o 2 9 2 15182.19 15747.22 360.14 o 3 9 2 3070.99 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