data_2019732 _cell_angle_alpha 90.000(5) _cell_angle_beta 111.556(6) _cell_angle_gamma 90.000(5) _cell_length_a 12.5219(8) _cell_length_b 4.2601(3) _cell_length_c 16.0008(9) _exptl_crystal_F_000 496 _reflns_d_resolution_high ? _[local]_cod_data_source_file sk3557IIasup4.hkl _[local]_cod_data_source_block IIa _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 205.24 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x+1/2, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 32316.90 29818.70 214.66 o 4 0 0 6131.29 6879.60 165.93 o 6 0 0 885.96 893.85 93.11 o 8 0 0 1019.99 1271.51 47.99 o 10 0 0 1118.44 1561.92 64.78 o 12 0 0 154.48 131.92 39.28 o 1 1 0 773.16 821.12 37.29 o 2 1 0 7544.74 8502.57 184.28 o 3 1 0 1138.51 1372.80 119.92 o 4 1 0 4307.94 5418.09 231.21 o 5 1 0 2292.91 2752.45 167.67 o 6 1 0 5780.97 6576.15 254.69 o 7 1 0 1782.99 2013.19 50.58 o 8 1 0 3134.24 3287.44 77.51 o 9 1 0 426.91 380.83 26.69 o 10 1 0 624.47 533.83 32.81 o 11 1 0 62.68 35.37 12.42 < 12 1 0 6.71 5.99 4.25 < 13 1 0 7.77 15.06 6.09 < 0 2 0 4233.67 4312.51 120.78 o 1 2 0 13291.20 13465.40 216.77 o 2 2 0 2774.21 3420.99 123.97 o 3 2 0 6796.30 8948.08 247.15 o 4 2 0 923.38 1077.53 45.65 o 5 2 0 468.86 540.98 24.47 o 6 2 0 44.90 57.99 9.47 o 7 2 0 4.54 17.81 6.66 < 8 2 0 21.82 22.48 6.47 o 9 2 0 198.19 205.50 20.71 o 10 2 0 20.90 20.24 8.36 < 11 2 0 86.87 103.09 15.45 o 12 2 0 37.46 25.56 6.24 o 1 3 0 149.96 141.94 30.80 o 2 3 0 53.41 59.53 8.70 o 3 3 0 1281.81 1483.63 83.02 o 4 3 0 15.02 22.10 9.78 < 5 3 0 2111.10 2550.40 71.32 o 6 3 0 0.03 -3.28 4.59 < 7 3 0 953.75 1204.31 43.32 o 8 3 0 65.57 74.43 13.45 o 9 3 0 308.18 293.47 23.50 o 10 3 0 0.14 -8.79 7.41 < 11 3 0 46.55 14.77 8.54 < 0 4 0 796.60 781.17 44.79 o 1 4 0 1278.84 813.77 84.59 o 2 4 0 443.79 345.25 52.80 o 3 4 0 823.66 727.81 69.30 o 4 4 0 183.43 180.58 33.73 o 5 4 0 90.82 90.29 15.53 o 6 4 0 30.21 46.98 14.45 o 7 4 0 4.16 0.64 5.46 < 8 4 0 2.18 -8.52 5.61 < -13 0 1 129.93 89.48 28.42 o -11 0 1 78.22 155.94 39.05 o -9 0 1 137.64 76.99 22.99 o -7 0 1 1649.65 1571.09 137.54 o -5 0 1 15585.00 17097.90 305.45 o -3 0 1 30646.80 28997.30 268.95 o -1 0 1 11679.80 13046.40 110.92 o 1 0 1 11299.50 14670.60 105.79 o 3 0 1 263.60 328.89 30.90 o 5 0 1 146.89 129.12 34.29 o 7 0 1 847.52 1159.70 49.12 o 9 0 1 856.53 886.13 50.72 o 11 0 1 162.15 122.48 27.02 o 13 0 1 54.07 51.33 14.73 o -13 1 1 34.43 26.05 5.66 o -12 1 1 9.51 7.27 8.00 < -11 1 1 181.80 156.63 16.82 o -10 1 1 25.43 14.20 4.95 < -9 1 1 909.33 961.59 42.57 o -8 1 1 466.67 517.46 25.83 o -7 1 1 1416.48 1629.78 52.52 o -6 1 1 1372.87 1481.63 149.30 o -5 1 1 3536.98 4433.76 265.11 o -4 1 1 21.55 32.04 53.61 < -3 1 1 779.04 820.03 159.79 o -2 1 1 1294.19 1538.76 74.23 o -1 1 1 2088.23 2440.53 41.54 o 0 1 1 1490.07 1542.42 122.27 o 1 1 1 15068.20 16160.60 252.15 o 2 1 1 8910.15 10437.80 267.51 o 3 1 1 16301.40 19395.40 256.14 o 4 1 1 2308.78 2850.36 141.73 o 5 1 1 7740.59 8519.05 255.69 o 6 1 1 550.51 589.99 31.25 o 7 1 1 1905.74 2036.69 57.35 o 8 1 1 532.50 456.47 30.27 o 9 1 1 35.31 12.89 7.64 < 10 1 1 71.07 46.59 11.46 o 11 1 1 23.85 19.60 6.41 o 12 1 1 13.15 12.62 6.38 < 13 1 1 14.53 18.27 5.94 o -13 2 1 13.41 13.50 10.18 < -12 2 1 1.08 8.75 4.96 < -11 2 1 21.66 30.86 7.87 o -10 2 1 50.72 50.86 10.54 o -9 2 1 40.37 36.11 8.82 o -8 2 1 40.53 31.94 6.85 o -7 2 1 458.54 497.74 23.68 o -6 2 1 2943.77 3460.37 67.28 o -5 2 1 1354.85 1753.07 51.04 o -4 2 1 5142.04 5532.07 122.46 o -3 2 1 4422.47 5494.44 186.90 o -2 2 1 5168.20 6061.74 189.65 o -1 2 1 2573.23 2654.41 116.74 o 0 2 1 6366.62 6619.19 149.83 o 1 2 1 581.96 626.17 52.35 o 2 2 1 2467.32 2787.74 132.63 o 3 2 1 2.41 -0.43 10.43 < 4 2 1 6.18 6.35 5.12 < 5 2 1 45.52 49.24 8.58 o 6 2 1 194.68 237.90 16.31 o 7 2 1 437.76 486.12 26.33 o 8 2 1 39.53 46.34 10.07 o 9 2 1 188.42 192.07 16.89 o 10 2 1 244.38 228.97 19.06 o 11 2 1 37.73 20.27 6.58 o 12 2 1 50.23 14.89 7.37 < -11 3 1 0.88 -16.52 6.11 < -10 3 1 158.12 146.57 16.43 o -9 3 1 7.87 10.60 6.56 < -8 3 1 653.22 806.86 41.14 o -7 3 1 0.14 -5.24 5.24 < -6 3 1 787.13 921.74 40.24 o -5 3 1 17.78 31.89 12.23 < -4 3 1 342.76 390.49 49.76 o -3 3 1 4.00 2.54 18.87 < -2 3 1 136.58 130.21 15.50 o -1 3 1 17.32 23.13 22.59 < 0 3 1 1935.22 2041.83 71.29 o 1 3 1 38.63 34.76 14.84 < 2 3 1 4055.48 4913.89 143.15 o 3 3 1 4.69 3.25 5.52 < 4 3 1 3463.91 4338.73 107.21 o 5 3 1 0.28 9.11 9.07 < 6 3 1 1171.49 1384.15 52.07 o 7 3 1 1.29 3.88 5.65 < 8 3 1 119.71 89.26 11.62 o 9 3 1 13.03 11.45 6.74 < 10 3 1 11.50 10.06 6.46 < -8 4 1 35.18 22.07 7.25 o -7 4 1 93.20 97.92 15.04 o -6 4 1 248.37 246.38 33.47 o -5 4 1 329.09 294.11 79.48 o -4 4 1 840.33 773.66 79.24 o -3 4 1 493.01 289.27 52.02 o -2 4 1 1527.02 892.49 101.75 o -1 4 1 382.13 333.57 83.41 o 0 4 1 789.54 835.43 49.29 o 1 4 1 183.50 139.52 31.29 o 2 4 1 210.75 209.81 36.32 o 3 4 1 2.21 11.70 10.84 < 4 4 1 2.36 0.25 9.07 < 5 4 1 18.81 34.59 9.79 o 6 4 1 156.93 128.27 17.82 o 7 4 1 32.59 31.22 9.84 o 8 4 1 107.22 34.38 16.15 < -14 0 2 2.08 -19.25 12.75 < -12 0 2 271.92 238.22 31.40 o -10 0 2 1585.82 1435.14 96.54 o -8 0 2 2467.93 2727.58 108.87 o -6 0 2 7165.90 7994.01 237.28 o -4 0 2 27787.60 26727.50 314.41 o -2 0 2 1146.64 1062.43 43.78 o 0 0 2 276.31 251.99 25.04 o 2 0 2 1230.45 1436.19 60.15 o 4 0 2 18471.90 22001.70 379.25 o 6 0 2 6131.98 6479.03 180.53 o 8 0 2 1896.14 1180.17 95.68 o 10 0 2 344.20 158.50 34.64 o 12 0 2 31.01 23.41 11.67 < -14 1 2 41.24 24.54 11.78 < -13 1 2 15.28 16.42 5.62 < -12 1 2 318.56 327.73 28.86 o -11 1 2 178.81 167.04 21.03 o -10 1 2 345.66 394.52 26.72 o -9 1 2 121.22 135.09 13.96 o -8 1 2 809.77 970.29 41.22 o -7 1 2 72.35 76.83 6.65 o -6 1 2 1.20 -39.19 72.31 < -5 1 2 166.09 353.94 211.97 < -4 1 2 5353.23 4674.36 444.67 o -3 1 2 5093.17 5367.98 314.43 o -2 1 2 40586.60 42125.00 655.00 o -1 1 2 9870.01 10670.80 115.90 o 0 1 2 20135.60 22356.30 347.84 o 1 1 2 6917.27 6656.99 214.18 o 2 1 2 13411.10 12953.80 281.45 o 3 1 2 3759.91 4306.73 126.19 o 4 1 2 4649.10 5220.08 179.03 o 5 1 2 164.33 123.66 32.16 o 6 1 2 39.72 23.23 5.97 o 7 1 2 15.32 -17.12 7.35 < 8 1 2 111.58 129.13 17.09 o 9 1 2 28.67 17.91 9.41 < 10 1 2 55.28 56.28 11.02 o 11 1 2 12.96 -2.59 6.79 < 12 1 2 43.24 41.39 7.92 o -13 2 2 0.01 5.77 3.84 < -12 2 2 0.07 -0.75 4.33 < -11 2 2 140.08 123.82 14.98 o -10 2 2 5.34 14.42 7.46 < -9 2 2 546.70 587.53 30.35 o -8 2 2 438.85 485.45 24.21 o -7 2 2 2551.00 2924.80 80.21 o -6 2 2 927.19 1068.41 34.72 o -5 2 2 4166.24 4708.87 75.74 o -4 2 2 1810.51 2050.50 103.79 o -3 2 2 4461.87 4859.03 172.49 o -2 2 2 4136.10 4786.67 157.60 o -1 2 2 3299.98 3488.57 99.88 o 0 2 2 301.97 326.75 22.16 o 1 2 2 13.46 25.00 14.94 < 2 2 2 128.98 121.98 34.26 o 3 2 2 926.90 1007.60 54.11 o 4 2 2 715.57 865.15 33.76 o 5 2 2 2121.04 2453.03 61.38 o 6 2 2 807.75 879.59 31.31 o 7 2 2 1676.13 1805.62 44.53 o 8 2 2 616.87 553.81 40.59 o 9 2 2 439.39 355.35 26.63 o 10 2 2 31.61 15.62 8.62 < 11 2 2 139.16 78.03 12.33 o 12 2 2 1.24 -6.01 5.18 < -11 3 2 165.07 152.24 14.87 o -10 3 2 13.33 11.65 6.29 < -9 3 2 381.33 444.56 35.45 o -8 3 2 24.87 40.01 12.88 o -7 3 2 212.89 274.49 34.10 o -6 3 2 0.46 -2.84 12.35 < -5 3 2 139.83 144.57 51.13 < -4 3 2 107.49 154.53 55.14 < -3 3 2 1688.37 1828.85 52.10 o -2 3 2 55.09 61.79 10.44 o -1 3 2 5560.32 6137.48 113.69 o 0 3 2 8.05 -0.80 10.26 < 1 3 2 7151.95 8203.98 133.11 o 2 3 2 14.81 10.30 8.37 < 3 3 2 3661.06 4579.25 120.62 o 4 3 2 30.98 59.68 14.55 o 5 3 2 829.52 1056.58 54.11 o 6 3 2 43.84 43.64 9.20 o 7 3 2 80.91 72.21 10.55 o 8 3 2 2.90 -8.57 5.91 < 9 3 2 9.99 20.86 8.63 < 10 3 2 8.93 4.67 5.18 < -9 4 2 54.61 53.59 12.18 o -8 4 2 102.61 126.43 17.76 o -7 4 2 419.96 397.52 40.51 o -6 4 2 177.13 141.32 28.23 o -5 4 2 766.93 73.72 78.50 < -4 4 2 305.03 62.62 145.70 < -3 4 2 848.24 572.12 192.61 < -2 4 2 134.91 89.05 89.52 < -1 4 2 571.87 470.33 132.14 o 0 4 2 9.69 2.01 4.74 < 1 4 2 1.05 10.91 12.96 < 2 4 2 4.57 23.61 14.35 < 3 4 2 318.65 297.14 34.82 o 4 4 2 97.86 113.19 21.40 o 5 4 2 351.88 352.53 29.86 o 6 4 2 103.61 110.10 16.54 o 7 4 2 237.58 140.99 19.36 o -13 0 3 20.55 27.17 11.45 < -11 0 3 213.29 180.60 21.48 o -9 0 3 2376.18 2448.82 112.93 o -7 0 3 8126.69 9283.02 291.23 o -5 0 3 9291.59 9956.93 220.87 o -3 0 3 7938.21 7881.49 154.70 o -1 0 3 2185.89 2433.29 63.98 o 1 0 3 15188.50 13097.40 335.70 o 3 0 3 13834.40 16019.80 310.64 o 5 0 3 12645.10 11198.90 394.11 o 7 0 3 982.21 475.90 48.58 o 9 0 3 305.36 93.99 31.70 < 11 0 3 0.33 2.43 5.08 < -14 1 3 15.90 19.88 5.64 o -13 1 3 80.80 84.75 11.30 o -12 1 3 230.73 235.90 20.40 o -11 1 3 96.14 135.71 17.42 o -10 1 3 139.08 162.01 19.55 o -9 1 3 2.58 -7.07 6.98 < -8 1 3 300.85 245.82 18.51 o -7 1 3 584.42 632.15 24.77 o -6 1 3 233.13 269.34 225.13 < -5 1 3 7609.94 9015.91 545.55 o -4 1 3 3077.74 3438.75 242.20 o -3 1 3 7266.67 8442.54 276.09 o -2 1 3 17693.00 18485.20 187.32 o -1 1 3 13821.30 14633.80 166.05 o 0 1 3 4143.68 4218.00 69.58 o 1 1 3 7580.32 7173.95 214.46 o 2 1 3 2215.40 1967.39 110.90 o 3 1 3 3635.31 3602.06 156.97 o 4 1 3 1616.01 1810.34 107.54 o 5 1 3 34.31 25.40 6.22 o 6 1 3 16.27 6.10 5.30 < 7 1 3 300.86 235.99 23.30 o 8 1 3 161.14 134.29 16.57 o 9 1 3 213.20 201.15 17.93 o 10 1 3 57.99 46.57 8.91 o 11 1 3 77.80 69.37 8.88 o 12 1 3 20.60 23.53 6.09 o -13 2 3 5.62 -7.37 5.37 < -12 2 3 9.32 15.88 6.38 < -11 2 3 44.63 47.52 10.09 o -10 2 3 749.67 844.57 34.59 o -9 2 3 137.74 160.20 18.22 o -8 2 3 1246.88 1367.97 46.40 o -7 2 3 1046.42 1146.21 113.47 o -6 2 3 3306.51 3740.98 50.87 o -5 2 3 907.94 976.68 41.10 o -4 2 3 5075.90 5826.51 139.64 o -3 2 3 22.71 38.58 17.73 < -2 2 3 688.61 734.51 80.83 o -1 2 3 304.82 302.79 26.62 o 0 2 3 2036.07 1928.90 95.41 o 1 2 3 1047.37 859.38 92.26 o 2 2 3 4440.29 4254.00 230.38 o 3 2 3 1235.31 1227.38 51.71 o 4 2 3 3769.07 4306.47 69.68 o 5 2 3 821.36 828.58 28.05 o 6 2 3 2779.68 2708.98 59.50 o 7 2 3 52.46 32.87 8.51 o 8 2 3 564.30 376.84 38.52 o 9 2 3 10.50 -13.66 9.35 < 10 2 3 6.43 5.57 8.22 < 11 2 3 4.68 3.95 4.10 < -11 3 3 3.18 6.12 4.22 < -10 3 3 48.57 59.32 13.27 o -9 3 3 3.87 11.19 6.47 < -8 3 3 48.61 75.93 23.06 o -7 3 3 24.30 13.70 24.60 < -6 3 3 720.02 806.79 37.90 o -5 3 3 5.17 3.69 25.10 < -4 3 3 2626.67 3105.08 113.44 o -3 3 3 5.48 5.90 11.77 < -2 3 3 5004.69 5696.32 106.20 o -1 3 3 17.08 13.10 9.29 < 0 3 3 5056.37 5600.75 108.42 o 1 3 3 12.35 11.37 8.42 < 2 3 3 1749.45 2002.10 72.16 o 3 3 3 32.84 38.89 12.12 o 4 3 3 153.21 157.58 25.83 o 5 3 3 27.15 14.66 11.13 < 6 3 3 3.30 10.61 8.59 < 7 3 3 10.98 -0.28 6.71 < 8 3 3 90.45 60.00 10.94 o 9 3 3 4.02 6.71 5.74 < 10 3 3 82.09 62.85 6.93 o -9 4 3 29.38 35.81 7.88 o -8 4 3 291.30 343.62 27.68 o -7 4 3 62.73 49.90 14.34 o -6 4 3 469.05 327.45 48.12 o -5 4 3 51.03 45.46 33.19 < -4 4 3 208.39 149.04 79.96 < -3 4 3 22.74 26.38 40.48 < -2 4 3 6.39 9.71 40.68 < -1 4 3 11.69 19.66 17.62 < 0 4 3 197.87 231.42 30.71 o 1 4 3 96.44 88.41 21.23 o 2 4 3 798.18 802.63 55.11 o 3 4 3 126.33 110.62 20.50 o 4 4 3 485.73 490.35 42.49 o 5 4 3 127.67 87.55 15.46 o 6 4 3 169.15 103.68 15.71 o 7 4 3 37.51 20.72 11.32 < -14 0 4 40.04 31.91 10.01 o -12 0 4 106.45 96.48 22.10 o -10 0 4 1321.82 1474.74 68.31 o -8 0 4 2104.54 2236.79 52.93 o -6 0 4 144.95 183.01 35.75 o -4 0 4 3965.47 4343.59 137.61 o -2 0 4 3087.57 3599.57 89.91 o 0 0 4 26669.90 23514.70 242.05 o 2 0 4 10897.00 9267.15 202.67 o 4 0 4 2243.31 1508.58 135.84 o 6 0 4 1792.70 1398.61 73.27 o 8 0 4 15.32 -0.71 8.13 < 10 0 4 1.40 2.44 5.03 < 12 0 4 15.69 25.57 4.68 o -14 1 4 6.95 13.21 5.49 < -13 1 4 10.41 0.52 5.02 < -12 1 4 3.03 5.55 4.51 < -11 1 4 23.84 33.21 8.10 o -10 1 4 63.43 48.77 7.79 o -9 1 4 110.71 74.86 12.59 o -8 1 4 1560.83 1606.15 37.41 o -7 1 4 1189.92 1132.10 31.89 o -6 1 4 4879.28 5912.49 384.36 o -5 1 4 1847.35 2233.69 183.80 o -4 1 4 10461.80 11352.30 319.26 o -3 1 4 2757.84 2828.39 89.57 o -2 1 4 7505.50 7790.03 81.13 o -1 1 4 3450.56 3854.65 91.57 o 0 1 4 7390.70 8109.84 198.50 o 1 1 4 388.37 317.81 45.15 o 2 1 4 807.26 703.81 61.20 o 3 1 4 8.13 -6.90 22.46 < 4 1 4 1644.68 1811.15 111.76 o 5 1 4 459.49 441.98 19.26 o 6 1 4 1280.22 1094.80 45.59 o 7 1 4 371.88 325.62 25.91 o 8 1 4 656.85 693.30 36.18 o 9 1 4 142.89 118.23 11.62 o 10 1 4 129.32 130.68 12.26 o 11 1 4 63.83 50.92 7.17 o 12 1 4 8.04 5.75 4.31 < -13 2 4 88.28 73.12 12.44 o -12 2 4 110.09 122.65 15.12 o -11 2 4 319.77 367.53 26.22 o -10 2 4 215.60 267.05 22.04 o -9 2 4 960.23 1095.74 34.06 o -8 2 4 246.86 283.83 59.61 o -7 2 4 407.26 349.86 35.02 o -6 2 4 179.38 187.41 19.26 o -5 2 4 2.86 8.42 4.09 < -4 2 4 983.51 1054.36 51.00 o -3 2 4 3411.00 3473.82 144.29 o -2 2 4 1450.10 1516.26 68.23 o -1 2 4 7229.81 7595.53 179.66 o 0 2 4 1492.19 1749.74 94.98 o 1 2 4 9202.35 9082.44 277.17 o 2 2 4 2889.93 2800.01 94.08 o 3 2 4 5122.34 4795.04 94.13 o 4 2 4 921.16 989.59 36.22 o 5 2 4 1182.85 1115.22 37.40 o 6 2 4 87.21 71.16 9.98 o 7 2 4 139.32 106.77 13.88 o 8 2 4 0.61 -9.90 8.17 < 9 2 4 1.84 -1.36 6.61 < 10 2 4 2.92 10.35 4.66 < 11 2 4 32.31 35.37 6.54 o -12 3 4 9.21 2.33 4.92 < -11 3 4 21.14 14.15 5.54 < -10 3 4 4.44 8.64 7.43 < -9 3 4 342.01 444.77 33.81 o -8 3 4 15.32 10.59 16.42 < -7 3 4 1415.00 1762.74 57.92 o -6 3 4 22.47 24.73 19.54 < -5 3 4 3620.34 4524.63 159.90 o -4 3 4 187.96 222.33 34.77 o -3 3 4 5395.83 6437.19 164.93 o -2 3 4 11.53 16.29 8.95 < -1 3 4 2249.21 2445.54 68.81 o 0 3 4 1.13 -0.84 6.60 < 1 3 4 65.22 67.50 16.56 o 2 3 4 3.69 -13.30 8.19 < 3 3 4 242.15 230.18 27.15 o 4 3 4 73.98 81.19 12.25 o 5 3 4 814.86 768.85 34.06 o 6 3 4 49.14 44.64 11.56 o 7 3 4 671.34 437.54 24.59 o 8 3 4 13.95 6.79 5.30 < 9 3 4 197.76 164.72 14.37 o -9 4 4 125.55 123.45 13.43 o -8 4 4 31.44 28.24 7.04 o -7 4 4 71.64 102.00 20.98 o -6 4 4 0.21 1.19 12.82 < -5 4 4 9.88 12.16 13.96 < -4 4 4 89.53 72.57 22.93 o -3 4 4 267.00 281.46 76.17 o -2 4 4 224.70 135.86 54.53 < -1 4 4 1122.65 1389.73 74.50 o 0 4 4 477.72 593.82 53.62 o 1 4 4 1025.13 1274.27 86.42 o 2 4 4 371.24 378.87 37.78 o 3 4 4 710.29 771.61 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166.47 o 4 1 5 1704.74 1631.81 47.84 o 5 1 5 1845.80 1788.30 42.50 o 6 1 5 696.91 649.81 30.44 o 7 1 5 892.66 795.31 32.31 o 8 1 5 115.25 87.18 12.64 o 9 1 5 243.36 244.03 20.81 o 10 1 5 6.95 9.41 3.79 < 11 1 5 19.96 15.11 3.80 o -13 2 5 7.99 8.09 6.30 < -12 2 5 157.14 201.94 19.14 o -11 2 5 103.79 102.77 12.66 o -10 2 5 92.23 116.56 15.88 o -9 2 5 143.52 138.72 16.65 o -8 2 5 28.55 21.57 8.77 < -7 2 5 2.05 -15.15 8.50 < -6 2 5 1402.03 1553.41 50.24 o -5 2 5 41.80 55.00 10.97 o -4 2 5 5355.34 6067.51 103.66 o -3 2 5 1141.59 1141.59 69.37 o -2 2 5 9386.80 9865.55 205.53 o -1 2 5 3696.21 3914.65 134.39 o 0 2 5 7311.79 8038.35 152.98 o 1 2 5 3880.32 3980.80 127.11 o 2 2 5 4499.40 4295.17 104.97 o 3 2 5 622.33 577.75 31.31 o 4 2 5 608.79 540.83 30.20 o 5 2 5 25.05 8.00 4.99 < 6 2 5 4.96 -0.56 4.64 < 7 2 5 1.31 2.70 6.17 < 8 2 5 26.74 22.58 8.07 < 9 2 5 61.36 77.35 8.25 o 10 2 5 42.67 52.62 6.67 o -12 3 5 43.35 39.39 10.78 o -11 3 5 1.36 1.53 5.36 < -10 3 5 317.47 366.54 22.82 o -9 3 5 9.68 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