data_2019740 _cell_angle_alpha 90.000 _cell_angle_beta 96.671 _cell_angle_gamma 90.000 _cell_length_a 16.7649 _cell_length_b 13.4741 _cell_length_c 21.0984 _exptl_crystal_F_000 2232.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file ov3054Isup2.hkl _[local]_cod_data_source_block I _shelx_title ' 2 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 455.33 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 207325.77 218233.91 2370.64 o 3 0 0 13225.02 17571.03 286.06 o 4 0 0 124184.67 100458.03 1433.56 o 5 0 0 6549.04 7157.96 407.71 o 6 0 0 70106.43 115321.88 33974.82 o 7 0 0 25950.33 28028.67 517.20 o 8 0 0 76145.81 65974.02 1090.77 o 9 0 0 5539.45 4599.90 325.10 o 10 0 0 18705.10 22143.23 528.03 o 11 0 0 19256.63 19568.73 650.20 o 12 0 0 9346.47 12106.39 470.01 o 13 0 0 3386.49 3008.51 348.06 o 14 0 0 7958.59 6980.41 618.14 o 15 0 0 2993.64 3166.34 476.76 o 16 0 0 2170.51 2577.79 394.56 o 17 0 0 734.34 723.36 341.95 o 18 0 0 3583.57 2946.04 598.41 o 19 0 0 1625.89 1742.64 355.10 o 20 0 0 87.32 174.26 190.70 o 2 1 0 2479.59 2390.37 104.55 o 3 1 0 71760.58 61619.96 587.21 o 4 1 0 1736.31 1627.56 115.06 o 5 1 0 86658.16 105679.92 771.90 o 6 1 0 13584.34 15643.55 3097.46 o 7 1 0 35035.69 36881.82 598.32 o 8 1 0 4038.47 3250.64 196.90 o 9 1 0 29178.89 27821.89 505.64 o 10 1 0 14204.07 14058.12 419.86 o 11 1 0 23237.50 25563.53 456.50 o 12 1 0 5167.71 5064.22 260.42 o 13 1 0 8714.30 7996.40 369.41 o 14 1 0 1500.23 1974.26 235.45 o 15 1 0 3764.57 4067.25 406.79 o 16 1 0 848.36 657.60 225.14 o 17 1 0 1541.19 1522.99 270.07 o 18 1 0 348.79 286.06 177.40 o 19 1 0 420.55 424.15 154.83 o 20 1 0 556.07 412.71 164.63 o 0 2 0 1781.41 1767.54 202.21 o 1 2 0 471.92 877.89 61.55 o 2 2 0 6508.87 5472.46 120.79 o 3 2 0 121.24 151.25 59.94 o 4 2 0 8491.15 7314.99 497.35 o 5 2 0 732.48 1213.27 100.50 o 6 2 0 13602.87 16192.05 258.23 o 7 2 0 4848.10 4899.11 153.72 o 8 2 0 5698.82 5402.49 287.11 o 9 2 0 53.01 95.35 86.29 o 10 2 0 6007.38 5429.43 261.55 o 11 2 0 278.45 187.42 113.87 o 12 2 0 2971.84 2791.51 339.42 o 13 2 0 143.49 124.94 181.17 o 14 2 0 2747.39 2525.18 274.13 o 15 2 0 10.22 58.56 116.12 o 16 2 0 386.86 381.41 201.10 o 17 2 0 25.51 30.72 138.07 o 18 2 0 168.38 269.62 127.46 o 19 2 0 45.36 31.89 127.92 o 20 2 0 1322.35 2002.39 209.56 o 1 3 0 18348.19 16347.02 268.56 o 2 3 0 5113.94 4285.66 138.93 o 3 3 0 14273.66 19693.11 260.82 o 4 3 0 356.06 358.39 68.71 o 5 3 0 23646.18 23066.72 448.09 o 6 3 0 401.19 371.54 77.09 o 7 3 0 15240.64 17983.65 364.26 o 8 3 0 15603.37 14952.55 343.44 o 9 3 0 9403.86 8420.55 245.78 o 10 3 0 3232.85 2663.27 235.09 o 11 3 0 3154.47 3420.37 220.04 o 12 3 0 4520.26 3904.70 398.48 o 13 3 0 216.97 190.70 156.82 o 14 3 0 4134.11 3983.51 413.14 o 15 3 0 45.34 29.59 130.20 o 16 3 0 2922.45 2699.44 364.46 o 17 3 0 359.88 339.77 178.98 o 18 3 0 1060.90 1208.96 248.95 o 19 3 0 295.02 276.19 147.87 o 20 3 0 181.83 177.93 124.69 o 0 4 0 24346.46 19953.09 444.68 o 1 4 0 489.36 519.50 64.92 o 2 4 0 28824.79 27863.02 353.59 o 3 4 0 4675.47 4549.45 176.64 o 4 4 0 86498.24 131359.45 30463.40 o 5 4 0 6482.33 5487.66 270.97 o 6 4 0 72740.16 66737.74 788.51 o 7 4 0 8216.87 12769.25 318.18 o 8 4 0 19985.04 18504.86 451.82 o 9 4 0 4065.01 4296.82 225.25 o 10 4 0 11050.28 13477.56 1424.41 o 11 4 0 1603.20 2143.77 313.46 o 12 4 0 4911.20 4657.28 415.99 o 13 4 0 2135.00 2081.30 316.19 o 14 4 0 5555.34 5180.37 428.84 o 15 4 0 1733.30 2299.79 331.28 o 16 4 0 80.48 42.74 165.64 o 17 4 0 1722.56 1870.87 430.73 o 18 4 0 223.12 266.33 141.02 o 19 4 0 524.02 443.88 186.78 o 1 5 0 64041.11 59869.59 612.63 o 2 5 0 1500.17 1390.90 102.51 o 3 5 0 58318.21 56167.13 616.88 o 4 5 0 281.12 229.79 54.88 o 5 5 0 32906.89 29411.24 482.57 o 6 5 0 4781.88 4487.36 272.55 o 7 5 0 26068.94 25796.37 499.90 o 8 5 0 804.41 888.51 167.09 o 9 5 0 18742.72 17620.44 502.92 o 10 5 0 641.83 601.70 198.22 o 11 5 0 7003.91 6618.73 478.85 o 12 5 0 104.83 154.54 145.18 o 13 5 0 5221.03 4785.25 455.39 o 14 5 0 551.45 1196.83 268.94 o 15 5 0 7496.04 6930.10 521.98 o 16 5 0 156.48 187.42 172.64 o 17 5 0 1646.68 1761.92 327.16 o 18 5 0 99.14 141.38 249.89 o 19 5 0 1785.76 2179.94 284.63 o 0 6 0 29885.55 26391.01 615.79 o 1 6 0 292.58 246.60 78.91 o 2 6 0 8488.16 12664.51 2212.97 o 3 6 0 2824.95 2888.09 194.02 o 4 6 0 3646.92 3707.79 180.38 o 5 6 0 1624.45 1897.17 154.25 o 6 6 0 3966.67 3530.08 281.16 o 7 6 0 10.02 12.46 78.56 o 8 6 0 7397.47 6512.55 309.61 o 9 6 0 632.82 535.94 175.05 o 10 6 0 7907.65 6830.94 447.44 o 11 6 0 271.71 322.22 201.63 o 12 6 0 3481.53 3917.16 416.93 o 13 6 0 411.33 457.03 203.77 o 14 6 0 7814.06 7486.76 546.13 o 15 6 0 340.51 358.39 183.22 o 16 6 0 5291.40 4971.44 498.25 o 17 6 0 317.92 279.48 187.68 o 18 6 0 2702.55 2659.99 562.25 o 19 6 0 32.74 105.22 230.16 o 1 7 0 1026.18 1315.95 132.21 o 2 7 0 1923.62 2469.27 154.01 o 3 7 0 644.00 540.86 116.49 o 4 7 0 2523.36 2525.11 179.08 o 5 7 0 1525.64 1547.51 193.49 o 6 7 0 4358.34 4290.43 255.87 o 7 7 0 32.95 28.75 99.89 o 8 7 0 4579.69 4077.11 276.25 o 9 7 0 866.64 766.10 173.21 o 10 7 0 3563.76 3624.65 400.20 o 11 7 0 5748.59 5583.01 400.65 o 12 7 0 3988.92 3490.79 435.15 o 13 7 0 5503.79 4770.88 445.23 o 14 7 0 4128.74 3692.11 411.34 o 15 7 0 1012.98 1138.67 294.28 o 16 7 0 217.66 225.12 185.85 o 17 7 0 1526.83 1686.74 336.25 o 18 7 0 221.80 200.57 151.29 o 0 8 0 14023.32 16206.51 480.44 o 1 8 0 1893.60 1881.48 184.36 o 2 8 0 3661.47 3155.16 228.60 o 3 8 0 2512.88 2767.09 162.76 o 4 8 0 5924.86 5302.46 241.07 o 5 8 0 3438.20 3751.60 233.89 o 6 8 0 3343.15 3462.58 265.39 o 7 8 0 3610.42 3889.69 252.23 o 8 8 0 637.69 706.92 213.90 o 9 8 0 2230.49 2125.62 302.22 o 10 8 0 59.85 72.62 129.55 o 11 8 0 2478.29 2415.62 334.22 o 12 8 0 11.27 18.62 148.31 o 13 8 0 1807.44 1993.61 382.58 o 14 8 0 336.18 381.41 197.97 o 15 8 0 180.65 215.54 187.23 o 16 8 0 263.15 182.47 180.17 o 17 8 0 106.37 104.48 192.80 o 18 8 0 47.44 91.18 171.86 o 1 9 0 8048.64 7664.31 282.07 o 2 9 0 473.07 411.00 132.09 o 3 9 0 3195.72 2960.67 237.30 o 4 9 0 0.17 -4.97 83.51 o 5 9 0 4220.08 4065.75 250.88 o 6 9 0 575.46 628.01 146.74 o 7 9 0 4138.60 3737.22 442.90 o 8 9 0 192.84 153.92 135.63 o 9 9 0 4558.01 4192.19 407.43 o 10 9 0 0.55 -6.58 132.45 o 11 9 0 1654.87 1821.55 289.61 o 12 9 0 38.35 23.07 153.39 o 13 9 0 1735.74 1729.48 316.46 o 14 9 0 0.29 -0.07 163.80 o 15 9 0 681.17 647.21 255.46 o 16 9 0 209.03 217.01 174.55 o 17 9 0 211.85 195.62 188.28 o 0 10 0 4065.85 4165.89 398.48 o 1 10 0 263.86 273.30 101.69 o 2 10 0 5215.13 4413.61 254.98 o 3 10 0 9.77 11.31 74.77 o 4 10 0 2902.17 2809.65 255.32 o 5 10 0 77.77 47.61 84.76 o 6 10 0 3938.38 3793.54 277.87 o 7 10 0 851.24 817.07 260.40 o 8 10 0 6276.60 5424.82 481.00 o 9 10 0 879.50 700.34 248.06 o 10 10 0 5451.20 5229.12 475.24 o 11 10 0 535.11 591.84 181.50 o 12 10 0 1738.32 2193.09 323.01 o 13 10 0 645.34 618.14 233.75 o 14 10 0 2752.73 2860.55 447.90 o 15 10 0 471.06 483.33 239.95 o 16 10 0 2329.94 2663.27 371.16 o 1 11 0 5177.62 5067.27 297.79 o 2 11 0 0.34 -5.02 93.08 o 3 11 0 1574.15 1624.70 181.75 o 4 11 0 144.62 127.31 109.53 o 5 11 0 646.02 561.83 172.99 o 6 11 0 391.61 384.70 164.37 o 7 11 0 2964.02 3283.98 364.22 o 8 11 0 1472.34 1757.47 318.52 o 9 11 0 2515.96 2526.63 355.63 o 10 11 0 2425.51 3004.99 341.67 o 11 11 0 1502.67 1481.50 296.32 o 12 11 0 1245.67 1891.88 300.20 o 13 11 0 1846.57 1453.32 387.06 o 14 11 0 959.14 851.59 241.44 o 15 11 0 2256.66 2288.44 368.88 o 0 12 0 700.79 835.15 235.56 o 1 12 0 68.04 100.73 114.44 o 2 12 0 1423.01 1900.46 208.20 o 3 12 0 235.21 196.56 114.65 o 4 12 0 1500.47 1499.32 228.56 o 5 12 0 582.71 453.74 161.52 o 6 12 0 1086.87 1805.11 273.30 o 7 12 0 274.75 219.78 183.87 o 8 12 0 1204.93 1322.23 335.38 o 9 12 0 457.28 397.85 189.44 o 10 12 0 1906.57 2104.31 313.56 o 11 12 0 234.70 263.04 195.19 o 12 12 0 1251.43 1868.10 275.84 o 13 12 0 110.63 147.96 191.50 o 14 12 0 781.48 634.58 194.51 o 1 13 0 412.75 396.57 172.47 o 2 13 0 491.21 450.45 138.09 o 3 13 0 900.98 1086.87 196.11 o 4 13 0 63.21 108.50 146.81 o 5 13 0 305.82 335.38 174.60 o 6 13 0 58.22 82.20 197.62 o 7 13 0 174.41 118.37 199.91 o 8 13 0 397.20 315.65 228.31 o 9 13 0 256.26 235.26 235.98 o 10 13 0 25.07 26.30 154.31 o 11 13 0 314.59 242.09 134.88 o 12 13 0 9.74 72.34 171.68 o 0 14 0 805.27 1122.72 401.14 o 1 14 0 123.19 110.67 127.94 o 2 14 0 805.86 802.64 178.03 o 3 14 0 517.57 402.99 133.26 o 4 14 0 27.51 105.22 132.09 o 5 14 0 755.38 797.32 258.04 o 6 14 0 10.68 30.69 159.15 o 7 14 0 631.52 601.70 274.62 o 8 14 0 9.20 13.15 234.95 o 9 14 0 705.13 644.45 303.82 o 10 14 0 91.81 138.10 252.62 o 11 14 0 332.54 322.22 183.10 o 1 15 0 265.06 230.16 153.23 o 2 15 0 22.47 72.34 127.97 o 3 15 0 394.02 354.76 200.26 o 4 15 0 67.66 93.92 166.41 o 5 15 0 547.27 489.91 208.26 o 6 15 0 52.08 85.49 170.40 o 7 15 0 230.12 213.72 271.06 o 8 15 0 619.18 848.65 290.72 o 0 16 0 2897.41 3102.35 466.21 o 1 16 0 0.02 53.52 123.30 o 2 16 0 2251.66 2442.98 337.37 o 3 16 0 14.01 20.98 153.41 o 4 16 0 1548.80 1765.65 366.86 o 5 16 0 19.64 36.17 172.37 o -20 1 1 979.92 789.12 219.59 o -19 1 1 583.61 565.53 211.57 o -18 1 1 4519.08 3579.49 449.25 o -17 1 1 43.24 34.26 175.67 o -16 1 1 5144.26 4373.03 523.05 o -15 1 1 0.08 12.52 135.07 o -14 1 1 9996.89 9091.30 391.18 o -13 1 1 1361.61 1754.01 160.90 o -12 1 1 12881.17 14499.94 931.63 o -11 1 1 253.41 263.04 122.00 o -10 1 1 12630.13 16820.54 371.58 o -9 1 1 4389.41 3597.06 243.55 o -8 1 1 21652.67 17858.85 520.14 o -7 1 1 18076.85 22408.14 296.76 o -6 1 1 42044.44 40331.67 501.28 o -5 1 1 2931.84 3090.71 172.09 o -4 1 1 56420.16 54250.08 616.35 o -3 1 1 17006.06 20888.62 234.33 o -2 1 1 27029.54 26777.58 297.30 o -1 1 1 22756.28 22553.24 226.45 o 1 1 1 3919.03 3904.32 130.14 o 2 1 1 4661.03 4218.49 116.18 o 3 1 1 9839.65 12182.01 290.22 o 4 1 1 10887.97 14362.08 230.28 o 5 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17981.09 609.02 o -13 3 1 565.38 568.82 201.63 o -12 3 1 20413.36 23765.33 692.18 o -11 3 1 3451.36 3753.20 265.35 o -10 3 1 26858.38 22296.86 560.41 o -9 3 1 4603.57 3743.20 232.30 o -8 3 1 34439.09 32941.48 557.94 o -7 3 1 3119.88 3044.16 219.25 o -6 3 1 78697.03 88152.25 13320.76 o -5 3 1 7009.85 6139.07 234.75 o -4 3 1 29971.24 33963.01 475.91 o -3 3 1 10050.33 17275.11 227.89 o -2 3 1 18274.43 16262.05 312.91 o -1 3 1 11187.71 11069.44 1218.84 o 0 3 1 40453.19 39523.59 378.89 o 1 3 1 4591.17 4073.82 138.21 o 2 3 1 45670.60 46518.52 450.20 o 3 3 1 18677.75 22541.96 309.99 o 4 3 1 37026.82 32621.50 456.00 o 5 3 1 13161.51 11845.04 346.66 o 6 3 1 5557.04 5789.16 268.54 o 7 3 1 10199.37 9051.67 251.67 o 8 3 1 9472.55 12153.18 1154.55 o 9 3 1 124.67 108.50 96.28 o 10 3 1 3833.90 3348.70 240.11 o 11 3 1 30.62 67.45 124.03 o 12 3 1 8017.26 7203.99 417.54 o 13 3 1 89.20 72.34 201.63 o 14 3 1 2294.31 2258.85 352.27 o 15 3 1 1.59 78.91 107.21 o 16 3 1 503.99 483.33 196.15 o 17 3 1 107.62 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