#------------------------------------------------------------------------------ #$Date: 2016-04-06 16:33:17 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181867 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/97/2019745.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2019745 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.0760 _cell_length_b 30.5493 _cell_length_c 7.5386 _exptl_crystal_F_000 1472.00 _reflns_d_resolution_high 0.7594 _cod_data_source_file yf3075IVsup3.hkl _cod_data_source_block IV #BEGIN Tags that were not found in dictionaries: _shelx_title ' X1a in Pccn' _shelx_refln_list_code 4 _shelx_f_calc_maximum 691.35 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y+1/2, z' '-x, y+1/2, -z+1/2' 'x+1/2, -y, -z+1/2' '-x, -y, -z' 'x-1/2, y-1/2, -z' 'x, -y-1/2, z-1/2' '-x-1/2, y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5016.32 5485.27 124.84 o 4 0 0 477958.09 460034.97 15663.30 o 6 0 0 48.49 25.14 15.60 o 8 0 0 51336.73 54492.04 576.08 o 10 0 0 2354.10 2301.24 101.65 o 12 0 0 8623.43 8531.68 176.57 o 14 0 0 204.95 218.04 84.40 o 16 0 0 6972.67 7494.19 323.54 o 1 1 0 482.97 401.29 44.67 o 3 1 0 703.69 710.18 17.79 o 5 1 0 424.68 361.67 17.98 o 7 1 0 128.55 93.50 15.36 o 9 1 0 575.77 564.01 29.39 o 11 1 0 970.81 1023.91 42.36 o 13 1 0 992.93 960.91 50.46 o 15 1 0 99.59 127.87 58.40 o 17 1 0 1793.15 2011.58 193.42 o 2 2 0 1183.48 1205.62 41.58 o 4 2 0 6182.80 6654.70 142.59 o 6 2 0 669.40 657.35 26.25 o 8 2 0 6768.79 7361.68 81.26 o 10 2 0 365.42 360.84 27.82 o 12 2 0 3098.44 3156.92 69.95 o 14 2 0 31.08 32.22 35.11 o 16 2 0 801.62 713.90 92.01 o 1 3 0 1944.86 2037.80 67.71 o 3 3 0 1164.31 1095.63 23.07 o 5 3 0 4454.95 4336.57 83.94 o 7 3 0 1683.54 1671.30 38.48 o 9 3 0 1376.35 1294.70 40.39 o 11 3 0 1383.25 1383.56 47.19 o 13 3 0 37.54 -4.27 25.38 o 15 3 0 926.02 1004.47 77.76 o 17 3 0 104.70 165.29 101.99 o 0 4 0 359.32 307.75 12.84 o 2 4 0 447.89 414.00 17.68 o 4 4 0 40316.47 40596.39 925.03 o 6 4 0 3297.93 3177.57 47.18 o 8 4 0 21536.04 21749.90 328.26 o 10 4 0 35.55 32.20 17.20 o 12 4 0 9138.73 9680.28 151.14 o 14 4 0 60.70 62.97 31.08 o 16 4 0 703.01 692.23 90.54 o 1 5 0 15230.77 16345.76 439.23 o 3 5 0 15719.20 16579.65 400.05 o 5 5 0 10395.62 10681.03 235.91 o 7 5 0 4056.93 3874.74 78.27 o 9 5 0 4340.73 4437.11 75.34 o 11 5 0 512.53 414.25 41.93 o 13 5 0 739.94 771.12 55.37 o 15 5 0 438.72 477.17 61.44 o 17 5 0 48.06 35.17 84.40 o 0 6 0 22934.10 24821.69 698.05 o 2 6 0 2873.31 2927.08 81.70 o 4 6 0 2976.08 2852.20 67.68 o 6 6 0 18.82 12.65 10.50 o 8 6 0 7472.61 7471.54 173.53 o 10 6 0 190.24 203.98 23.74 o 12 6 0 2872.21 3173.99 92.25 o 14 6 0 6.07 18.94 28.20 o 16 6 0 35.34 60.73 43.38 o 1 7 0 5632.67 6102.11 130.28 o 3 7 0 15441.73 16084.36 338.64 o 5 7 0 178.31 189.41 12.33 o 7 7 0 3567.35 3419.47 96.99 o 9 7 0 74.41 98.22 18.40 o 11 7 0 450.32 387.14 41.53 o 13 7 0 2.03 2.09 26.41 o 15 7 0 132.96 124.94 38.58 o 17 7 0 62.33 21.10 57.19 o 0 8 0 383.73 327.63 21.69 o 2 8 0 62.16 48.50 11.32 o 4 8 0 1352.24 1420.62 25.12 o 6 8 0 3295.15 3695.20 124.75 o 8 8 0 1079.23 984.79 33.27 o 10 8 0 27.28 25.29 24.36 o 12 8 0 55.48 67.18 29.81 o 14 8 0 1.19 20.00 29.50 o 16 8 0 202.32 245.72 66.59 o 1 9 0 14453.90 16121.60 305.64 o 3 9 0 19854.23 22209.05 428.77 o 5 9 0 2039.15 1981.38 49.50 o 7 9 0 6833.69 7144.00 197.39 o 9 9 0 59.66 60.66 23.06 o 11 9 0 1576.68 1593.43 68.02 o 13 9 0 17.96 15.86 25.94 o 15 9 0 129.29 123.72 38.99 o 17 9 0 55.88 70.05 60.89 o 0 10 0 17875.26 18925.51 503.59 o 2 10 0 1587.76 1622.55 63.43 o 4 10 0 571.46 491.98 24.00 o 6 10 0 458.98 426.66 20.71 o 8 10 0 1208.21 1039.31 62.08 o 10 10 0 657.31 654.90 47.34 o 12 10 0 233.05 218.16 38.04 o 14 10 0 152.14 144.49 38.85 o 16 10 0 596.93 814.97 79.79 o 1 11 0 4531.30 4558.53 112.19 o 3 11 0 5621.78 6277.85 150.21 o 5 11 0 7009.54 7416.87 125.90 o 7 11 0 4524.36 4316.65 126.41 o 9 11 0 1516.53 1544.72 61.93 o 11 11 0 1076.08 1087.39 59.67 o 13 11 0 25.49 21.12 28.46 o 15 11 0 29.82 40.22 34.12 o 17 11 0 0.97 -10.77 60.58 o 0 12 0 2642.34 3067.20 114.25 o 2 12 0 453.74 434.30 18.49 o 4 12 0 1411.20 1536.18 39.63 o 6 12 0 1226.75 1277.66 39.11 o 8 12 0 1548.28 1608.73 73.60 o 10 12 0 14.70 18.40 25.67 o 12 12 0 3.55 -5.56 25.37 o 14 12 0 112.95 88.35 34.90 o 16 12 0 1.57 -4.92 40.45 o 1 13 0 3017.92 3035.02 69.72 o 3 13 0 1984.87 1848.40 78.99 o 5 13 0 3084.05 3031.17 86.13 o 7 13 0 1835.95 1703.44 47.33 o 9 13 0 643.45 636.05 46.09 o 11 13 0 520.67 478.11 45.93 o 13 13 0 34.28 35.02 29.97 o 15 13 0 57.64 43.79 36.61 o 17 13 0 3.04 -13.49 43.86 o 0 14 0 31052.92 36311.30 1283.35 o 2 14 0 373.25 371.03 19.82 o 4 14 0 27393.34 31603.75 767.58 o 6 14 0 1303.56 1359.72 45.94 o 8 14 0 2592.54 2659.12 78.08 o 10 14 0 163.32 152.26 34.12 o 12 14 0 2492.77 2600.84 90.72 o 14 14 0 2.44 -0.52 29.81 o 16 14 0 572.74 638.32 78.10 o 1 15 0 16925.87 20232.34 379.89 o 3 15 0 7408.12 8263.62 233.18 o 5 15 0 4534.69 4894.69 180.00 o 7 15 0 2593.97 2599.35 75.49 o 9 15 0 273.20 250.71 37.40 o 11 15 0 1527.44 1479.52 69.81 o 13 15 0 313.90 342.70 47.90 o 15 15 0 885.71 933.86 84.54 o 17 15 0 427.88 499.38 130.12 o 0 16 0 13939.23 16016.06 610.26 o 2 16 0 136.24 127.81 14.94 o 4 16 0 7744.05 8639.98 164.17 o 6 16 0 19.18 16.75 19.27 o 8 16 0 1469.07 1464.77 63.26 o 10 16 0 47.20 31.69 27.35 o 12 16 0 381.11 348.14 46.49 o 14 16 0 2.59 -5.40 30.90 o 16 16 0 178.26 204.87 60.07 o 1 17 0 1034.51 930.56 30.64 o 3 17 0 377.67 328.47 26.30 o 5 17 0 69.67 108.41 20.54 o 7 17 0 68.38 80.72 27.18 o 9 17 0 330.75 394.48 43.75 o 11 17 0 9.14 15.80 26.38 o 13 17 0 65.13 75.31 35.52 o 15 17 0 194.16 219.32 58.11 o 0 18 0 3937.10 3902.49 169.67 o 2 18 0 278.22 249.37 19.82 o 4 18 0 2165.40 2079.83 70.83 o 6 18 0 116.92 142.26 28.81 o 8 18 0 6505.76 6934.77 147.71 o 10 18 0 693.66 734.32 58.68 o 12 18 0 641.59 637.40 56.65 o 14 18 0 18.04 17.91 35.63 o 16 18 0 99.67 132.03 73.07 o 1 19 0 1170.35 1072.90 56.40 o 3 19 0 1781.92 1763.67 78.25 o 5 19 0 2614.06 2701.29 77.22 o 7 19 0 1169.16 1195.80 58.72 o 9 19 0 4976.13 5210.83 147.71 o 11 19 0 1113.84 1158.53 67.91 o 13 19 0 1523.05 1611.51 82.98 o 15 19 0 696.30 799.15 85.84 o 0 20 0 11086.84 10908.86 463.34 o 2 20 0 145.67 116.80 21.29 o 4 20 0 10733.21 11162.25 301.04 o 6 20 0 34.46 32.22 24.50 o 8 20 0 13760.81 14861.64 365.52 o 10 20 0 57.78 39.92 29.25 o 12 20 0 3127.88 3286.95 110.20 o 14 20 0 47.72 42.73 45.99 o 1 21 0 432.95 406.23 26.92 o 3 21 0 67.07 73.81 20.72 o 5 21 0 303.20 236.50 35.29 o 7 21 0 1474.18 1516.19 67.68 o 9 21 0 2936.44 3111.46 124.36 o 11 21 0 728.57 747.78 60.64 o 13 21 0 1012.01 1175.35 116.24 o 15 21 0 39.41 84.40 101.99 o 0 22 0 3059.89 3023.35 83.71 o 2 22 0 11.07 8.36 18.69 o 4 22 0 3663.44 3562.31 104.81 o 6 22 0 266.49 261.83 37.99 o 8 22 0 208.66 192.68 36.61 o 10 22 0 144.87 116.01 35.94 o 12 22 0 31.70 42.61 31.85 o 14 22 0 3.57 11.74 47.85 o 1 23 0 300.97 247.13 29.09 o 3 23 0 681.80 620.50 39.62 o 5 23 0 447.35 446.02 44.08 o 7 23 0 1991.91 1983.69 77.93 o 9 23 0 197.08 166.17 36.61 o 11 23 0 853.72 888.61 67.99 o 13 23 0 349.74 353.10 61.82 o 0 24 0 18071.64 19304.37 1404.94 o 2 24 0 16.10 -8.98 18.72 o 4 24 0 12038.37 12559.81 257.93 o 6 24 0 1696.10 1734.92 72.70 o 8 24 0 721.20 691.26 56.10 o 10 24 0 457.10 447.25 52.53 o 12 24 0 804.50 791.04 68.54 o 14 24 0 412.79 281.34 119.57 o 1 25 0 345.71 302.53 37.78 o 3 25 0 40.89 53.13 28.20 o 5 25 0 11.96 9.05 24.90 o 7 25 0 274.65 236.64 40.16 o 9 25 0 1595.52 1588.40 78.11 o 11 25 0 297.44 234.12 45.46 o 13 25 0 788.19 738.95 84.95 o 0 26 0 2.03 30.48 37.05 o 2 26 0 101.37 125.90 31.58 o 4 26 0 336.40 336.47 42.04 o 6 26 0 47.73 61.05 30.22 o 8 26 0 279.20 239.63 42.73 o 10 26 0 127.95 106.81 37.50 o 12 26 0 0.73 -1.07 33.71 o 1 27 0 15090.19 15539.60 508.61 o 3 27 0 10835.34 10722.70 310.65 o 5 27 0 7849.41 8099.21 263.44 o 7 27 0 3803.89 3883.81 132.99 o 9 27 0 1484.90 1477.78 90.40 o 11 27 0 1748.31 1790.16 103.98 o 0 28 0 239.71 164.32 49.55 o 2 28 0 5.42 13.91 29.61 o 4 28 0 151.24 110.07 28.87 o 6 28 0 536.51 564.88 55.06 o 8 28 0 1068.91 1103.03 70.49 o 10 28 0 19.52 -0.12 30.58 o 12 28 0 428.06 400.65 142.43 o 1 29 0 151.79 188.59 41.93 o 3 29 0 718.76 862.50 71.18 o 5 29 0 70.23 81.72 31.18 o 7 29 0 122.08 142.47 38.99 o 9 29 0 19.99 22.37 30.58 o 11 29 0 12.12 0.34 37.45 o 0 30 0 4.58 -34.55 34.55 o 2 30 0 109.27 114.02 38.47 o 4 30 0 361.72 388.30 49.50 o 6 30 0 169.35 213.97 43.18 o 8 30 0 1133.63 1206.80 75.78 o 10 30 0 16.17 36.67 38.02 o 1 31 0 591.39 648.08 66.18 o 3 31 0 2125.85 2211.01 151.45 o 5 31 0 78.43 64.41 32.86 o 7 31 0 1581.62 1573.69 98.47 o 9 31 0 298.46 248.08 51.96 o 11 31 0 511.73 611.91 137.15 o 0 32 0 285.85 207.49 87.92 o 2 32 0 232.93 309.50 54.75 o 4 32 0 939.80 992.85 81.88 o 6 32 0 24.68 13.97 32.14 o 8 32 0 130.45 141.58 45.80 o 10 32 0 46.54 19.30 55.91 o 1 33 0 512.76 488.93 82.06 o 3 33 0 593.14 619.50 70.83 o 5 33 0 528.31 660.98 73.49 o 7 33 0 606.83 587.89 65.16 o 9 33 0 319.68 348.92 66.76 o 0 34 0 1904.15 1571.99 165.29 o 2 34 0 41.20 73.91 41.25 o 4 34 0 1633.91 1778.00 104.79 o 6 34 0 345.24 349.13 64.14 o 8 34 0 520.08 494.67 73.49 o 1 35 0 464.65 406.92 116.05 o 3 35 0 131.41 140.03 46.45 o 5 35 0 1390.56 1569.34 101.25 o 7 35 0 417.58 466.61 91.91 o 0 36 0 2787.25 2412.49 200.45 o 2 36 0 261.19 236.73 66.82 o 4 36 0 1284.97 1346.99 98.71 o 6 36 0 98.35 131.88 69.63 o 1 37 0 63.47 39.97 50.93 o 3 37 0 37.63 39.69 50.64 o 5 37 0 313.92 312.99 85.55 o 0 38 0 4150.42 4213.06 281.34 o 2 38 0 104.60 147.64 68.08 o 4 38 0 2037.66 2430.67 160.26 o 1 1 1 18438.05 19738.48 487.30 o 2 1 1 39982.77 45159.46 1153.52 o 3 1 1 20349.74 22447.36 673.39 o 4 1 1 5342.72 5562.05 176.47 o 5 1 1 5542.43 5949.15 168.74 o 6 1 1 8241.54 8913.21 218.34 o 7 1 1 2458.20 2590.19 51.70 o 8 1 1 700.15 721.49 21.36 o 9 1 1 3208.36 3249.99 60.76 o 10 1 1 2271.47 2234.27 46.54 o 11 1 1 271.29 266.71 19.52 o 12 1 1 117.74 112.73 19.62 o 13 1 1 1955.42 1959.55 50.07 o 14 1 1 1646.55 1556.91 59.61 o 15 1 1 87.16 87.92 55.91 o 16 1 1 311.18 352.68 78.30 o 17 1 1 649.04 737.10 101.96 o 18 1 1 600.16 576.87 105.66 o 1 2 1 2790.25 2747.09 65.54 o 2 2 1 3180.85 3407.17 84.13 o 3 2 1 50417.56 55770.86 1510.66 o 4 2 1 16699.17 18175.45 467.79 o 5 2 1 288.21 281.53 10.80 o 6 2 1 4703.87 4758.13 118.93 o 7 2 1 1353.48 1342.11 33.82 o 8 2 1 1402.58 1451.34 29.25 o 9 2 1 2097.23 2087.78 34.97 o 10 2 1 586.13 547.50 22.57 o 11 2 1 199.83 195.25 19.55 o 12 2 1 0.33 9.76 14.66 o 13 2 1 80.51 52.22 19.52 o 14 2 1 8.28 0.80 21.91 o 15 2 1 14.41 9.13 36.23 o 16 2 1 24.19 22.08 53.42 o 17 2 1 69.03 68.22 62.02 o 18 2 1 34.06 73.03 74.48 o 1 3 1 1015.69 964.04 22.33 o 2 3 1 182.90 190.91 8.24 o 3 3 1 4411.83 4624.15 143.33 o 4 3 1 20247.58 21736.05 579.43 o 5 3 1 522.92 518.04 13.95 o 6 3 1 6818.76 7239.02 186.74 o 7 3 1 0.08 5.56 8.29 o 8 3 1 5206.58 5398.05 92.23 o 9 3 1 0.92 5.39 10.13 o 10 3 1 2941.11 2983.74 43.35 o 11 3 1 124.40 137.48 18.36 o 12 3 1 13.97 5.15 15.21 o 13 3 1 194.17 174.39 27.35 o 14 3 1 59.63 35.65 24.52 o 15 3 1 52.86 28.66 32.67 o 16 3 1 115.49 127.75 60.89 o 17 3 1 5.73 14.98 57.03 o 18 3 1 7.21 -56.07 65.86 o 1 4 1 36.30 31.71 4.37 o 2 4 1 1184.03 1050.00 26.36 o 3 4 1 8555.75 9063.03 229.02 o 4 4 1 5321.58 5557.63 148.65 o 5 4 1 158.64 134.14 8.43 o 6 4 1 386.02 385.65 13.78 o 7 4 1 111.48 124.45 10.89 o 8 4 1 274.42 272.34 14.40 o 9 4 1 154.69 121.15 13.78 o 10 4 1 24.06 26.82 13.28 o 11 4 1 66.12 54.64 15.38 o 12 4 1 53.88 46.65 15.79 o 13 4 1 36.05 36.27 19.68 o 14 4 1 17.14 21.95 24.06 o 15 4 1 73.89 96.97 32.42 o 16 4 1 19.10 15.41 39.33 o 17 4 1 11.55 -11.72 55.91 o 18 4 1 45.61 43.39 73.33 o 1 5 1 96.60 100.96 6.68 o 2 5 1 6083.99 6686.68 154.64 o 3 5 1 599.16 589.17 16.24 o 4 5 1 1389.65 1373.91 39.09 o 5 5 1 22.83 14.57 5.78 o 6 5 1 175.53 193.98 10.76 o 7 5 1 278.28 275.58 13.05 o 8 5 1 278.25 296.85 14.57 o 9 5 1 1.35 -0.03 9.42 o 10 5 1 0.12 -1.23 11.19 o 11 5 1 74.66 70.00 16.11 o 12 5 1 9.36 14.66 16.90 o 13 5 1 0.35 -4.44 17.99 o 14 5 1 40.69 14.68 22.20 o 15 5 1 36.03 50.14 26.90 o 16 5 1 18.39 15.39 38.77 o 17 5 1 0.09 2.74 54.92 o 18 5 1 55.53 104.70 87.92 o 1 6 1 407.51 355.20 10.81 o 2 6 1 2686.94 2654.87 51.74 o 3 6 1 2366.82 2476.40 60.67 o 4 6 1 825.44 859.28 26.52 o 5 6 1 2104.09 2102.74 45.08 o 6 6 1 1048.28 1076.64 20.21 o 7 6 1 4773.21 4757.78 94.23 o 8 6 1 4.70 12.42 8.57 o 9 6 1 437.04 405.92 19.38 o 10 6 1 101.29 91.98 15.24 o 11 6 1 946.18 869.72 34.74 o 12 6 1 139.44 97.66 21.89 o 13 6 1 6.23 1.72 18.34 o 14 6 1 4.36 -12.92 23.06 o 15 6 1 354.69 312.41 38.86 o 16 6 1 35.73 14.86 30.47 o 17 6 1 1.15 41.20 49.22 o 18 6 1 11.56 -3.52 98.47 o 1 7 1 518.68 470.87 11.98 o 2 7 1 302.11 285.28 9.81 o 3 7 1 71.34 54.76 7.03 o 4 7 1 986.25 903.72 27.89 o 5 7 1 1399.54 1367.85 33.65 o 6 7 1 85.62 77.48 8.83 o 7 7 1 365.83 338.11 14.13 o 8 7 1 220.58 223.41 13.42 o 9 7 1 399.51 381.61 19.91 o 10 7 1 21.95 26.39 13.17 o 11 7 1 156.85 149.58 21.50 o 12 7 1 47.76 45.62 19.92 o 13 7 1 0.29 -7.40 18.06 o 14 7 1 98.17 77.83 25.39 o 15 7 1 12.79 20.46 25.43 o 16 7 1 32.91 16.51 30.30 o 17 7 1 7.75 1.25 45.28 o 18 7 1 5.91 -3.52 91.44 o 1 8 1 3391.36 3325.34 58.51 o 2 8 1 2612.00 2696.88 61.83 o 3 8 1 1798.77 1774.73 37.71 o 4 8 1 2340.77 2427.12 50.25 o 5 8 1 127.29 100.18 9.29 o 6 8 1 389.92 321.06 12.67 o 7 8 1 962.68 1000.82 26.45 o 8 8 1 253.90 252.22 16.04 o 9 8 1 105.45 118.25 15.29 o 10 8 1 229.13 180.02 21.35 o 11 8 1 403.48 414.72 30.37 o 12 8 1 141.82 132.04 23.43 o 13 8 1 11.08 -3.80 19.51 o 14 8 1 277.00 252.46 32.73 o 15 8 1 148.04 138.85 32.56 o 16 8 1 87.26 100.90 34.91 o 17 8 1 8.11 -37.27 37.27 o 18 8 1 148.67 135.39 77.09 o 1 9 1 90.43 69.24 6.75 o 2 9 1 1134.32 1019.50 16.25 o 3 9 1 190.32 207.69 10.37 o 4 9 1 633.97 580.08 17.45 o 5 9 1 303.20 294.35 13.07 o 6 9 1 223.78 207.40 12.57 o 7 9 1 149.73 139.58 12.62 o 8 9 1 74.02 49.00 12.62 o 9 9 1 55.55 31.79 14.29 o 10 9 1 304.38 313.57 24.27 o 11 9 1 83.45 63.33 20.60 o 12 9 1 375.42 379.42 30.97 o 13 9 1 25.02 17.66 21.52 o 14 9 1 23.70 16.70 22.32 o 15 9 1 35.03 14.18 26.66 o 16 9 1 7.34 -3.35 31.07 o 17 9 1 1.77 -15.17 32.51 o 1 10 1 430.83 406.63 11.67 o 2 10 1 118.40 112.87 7.80 o 3 10 1 221.60 223.96 11.16 o 4 10 1 516.58 519.37 19.27 o 5 10 1 744.88 741.99 21.03 o 6 10 1 5.10 1.66 7.30 o 7 10 1 689.18 670.19 23.05 o 8 10 1 201.53 194.29 17.08 o 9 10 1 633.37 650.44 28.84 o 10 10 1 17.04 14.81 17.32 o 11 10 1 22.41 4.96 18.22 o 12 10 1 36.54 33.56 18.94 o 13 10 1 49.19 48.18 23.18 o 14 10 1 3.58 -9.89 20.66 o 15 10 1 12.36 -1.86 23.36 o 16 10 1 1.96 -17.20 29.44 o 17 10 1 11.72 6.86 35.74 o 1 11 1 34.40 37.81 7.11 o 2 11 1 8393.75 9866.76 165.00 o 3 11 1 45.23 49.34 8.15 o 4 11 1 785.59 802.73 18.13 o 5 11 1 6.96 1.17 8.17 o 6 11 1 891.84 939.63 24.55 o 7 11 1 11.83 8.38 9.91 o 8 11 1 127.96 109.33 16.63 o 9 11 1 3.31 12.24 13.77 o 10 11 1 244.97 213.59 25.15 o 11 11 1 0.64 11.49 17.86 o 12 11 1 77.25 78.75 21.45 o 13 11 1 18.59 5.82 20.75 o 14 11 1 168.00 141.84 29.29 o 15 11 1 2.21 3.97 23.06 o 16 11 1 73.52 63.05 35.54 o 17 11 1 4.45 4.34 36.90 o 1 12 1 3290.77 3526.11 69.79 o 2 12 1 0.01 -5.05 6.15 o 3 12 1 14.46 15.83 7.31 o 4 12 1 8.10 10.81 7.84 o 5 12 1 600.69 556.71 19.61 o 6 12 1 64.26 56.15 10.75 o 7 12 1 2571.85 2615.82 59.15 o 8 12 1 163.03 151.03 18.89 o 9 12 1 136.40 96.44 17.86 o 10 12 1 7.88 17.53 17.38 o 11 12 1 181.65 134.07 22.84 o 12 12 1 1.12 -2.88 18.26 o 13 12 1 62.66 50.99 24.44 o 14 12 1 0.03 -10.54 21.94 o 15 12 1 182.24 164.29 32.59 o 16 12 1 3.66 -21.10 31.76 o 17 12 1 1.14 -24.46 36.07 o 1 13 1 18.78 19.24 7.53 o 2 13 1 915.23 884.83 16.92 o 3 13 1 2474.22 2859.94 58.71 o 4 13 1 94.53 68.23 9.38 o 5 13 1 488.90 457.10 16.38 o 6 13 1 13.24 3.59 10.18 o 7 13 1 740.97 815.50 28.81 o 8 13 1 241.24 249.97 21.14 o 9 13 1 16.54 32.45 17.30 o 10 13 1 7.81 -1.48 17.49 o 11 13 1 114.07 101.43 21.96 o 12 13 1 143.28 141.45 25.12 o 13 13 1 184.05 186.32 30.52 o 14 13 1 0.31 -8.88 22.47 o 15 13 1 45.69 29.93 26.67 o 16 13 1 71.73 59.18 33.71 o 17 13 1 209.97 189.90 74.60 o 1 14 1 5733.00 6673.04 153.22 o 2 14 1 850.61 819.94 17.33 o 3 14 1 3050.87 3630.80 74.26 o 4 14 1 193.20 217.68 13.08 o 5 14 1 2103.51 2390.46 44.84 o 6 14 1 1.23 12.14 11.47 o 7 14 1 1780.16 1927.95 41.55 o 8 14 1 261.00 262.25 22.31 o 9 14 1 45.65 49.88 18.72 o 10 14 1 9.11 -2.40 16.70 o 11 14 1 1701.04 1725.20 51.99 o 12 14 1 34.47 29.19 20.92 o 13 14 1 33.30 20.26 23.42 o 14 14 1 0.11 6.75 22.74 o 15 14 1 418.01 392.17 41.85 o 16 14 1 3.80 -10.60 29.83 o 17 14 1 23.97 24.62 105.50 o 1 15 1 2.67 0.47 7.83 o 2 15 1 125.73 118.47 9.68 o 3 15 1 637.86 674.22 19.79 o 4 15 1 99.97 95.22 10.91 o 5 15 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215.87 34.96 o 5 31 2 47.30 48.08 27.00 o 6 31 2 47.19 27.64 26.79 o 7 31 2 336.65 361.32 40.40 o 8 31 2 112.70 111.05 30.97 o 9 31 2 92.28 126.33 34.13 o 10 31 2 32.34 42.12 43.65 o 0 32 2 825.80 694.49 72.18 o 1 32 2 194.73 223.09 35.61 o 2 32 2 138.18 124.48 35.41 o 3 32 2 181.28 173.04 36.65 o 4 32 2 1545.81 1539.30 65.81 o 5 32 2 120.11 106.36 29.94 o 6 32 2 1.17 16.07 26.06 o 7 32 2 139.89 107.91 31.45 o 8 32 2 331.92 330.69 42.79 o 9 32 2 17.17 36.26 37.09 o 0 33 2 50.36 89.42 41.84 o 1 33 2 225.04 204.12 35.36 o 2 33 2 12.47 22.99 28.45 o 3 33 2 298.99 261.23 41.79 o 4 33 2 87.99 77.55 33.32 o 5 33 2 156.78 150.89 38.43 o 6 33 2 63.00 81.53 33.41 o 7 33 2 255.55 236.62 42.06 o 8 33 2 100.79 125.56 35.56 o 9 33 2 38.10 107.33 63.37 o 0 34 2 910.72 910.30 83.02 o 1 34 2 110.48 114.06 36.94 o 2 34 2 0.03 -3.98 30.03 o 3 34 2 74.27 119.29 36.31 o 4 34 2 932.12 1039.42 70.27 o 5 34 2 60.28 52.99 33.89 o 6 34 2 15.65 45.74 37.07 o 7 34 2 5.81 11.30 33.83 o 8 34 2 405.40 507.38 94.40 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32.98 8.35 31.26 o 17 7 3 5.24 -10.87 43.87 o 1 8 3 1932.66 1936.60 42.53 o 2 8 3 1358.62 1557.37 39.50 o 3 8 3 4.20 15.04 7.47 o 4 8 3 1051.26 1109.44 29.87 o 5 8 3 1394.36 1521.41 38.53 o 6 8 3 193.77 214.90 16.18 o 7 8 3 458.67 470.95 21.73 o 8 8 3 6.20 4.37 12.81 o 9 8 3 71.55 84.28 18.34 o 10 8 3 100.29 73.09 19.18 o 11 8 3 64.32 49.99 19.04 o 12 8 3 502.64 524.13 39.88 o 13 8 3 29.89 23.90 22.61 o 14 8 3 330.54 347.92 39.95 o 15 8 3 326.48 283.47 40.82 o 16 8 3 316.69 322.96 43.76 o 1 9 3 29.35 12.29 8.33 o 2 9 3 421.66 459.54 16.14 o 3 9 3 437.78 435.51 15.41 o 4 9 3 65.97 68.77 9.09 o 5 9 3 90.03 63.51 10.38 o 6 9 3 359.86 362.20 19.27 o 7 9 3 61.06 51.20 13.94 o 8 9 3 160.63 168.09 19.02 o 9 9 3 73.40 77.80 18.01 o 10 9 3 72.66 69.28 18.55 o 11 9 3 367.31 380.07 31.42 o 12 9 3 301.65 302.69 30.63 o 13 9 3 116.24 124.45 28.39 o 14 9 3 1.10 -7.79 23.79 o 15 9 3 234.12 230.06 38.16 o 16 9 3 2.12 -7.24 29.90 o 1 10 3 1108.60 1184.47 25.62 o 2 10 3 2948.82 3388.04 57.24 o 3 10 3 371.51 367.68 14.61 o 4 10 3 509.34 504.66 18.12 o 5 10 3 294.79 286.14 17.49 o 6 10 3 1448.93 1644.57 52.56 o 7 10 3 1046.55 938.65 30.50 o 8 10 3 7.16 -0.23 13.47 o 9 10 3 1516.15 1490.37 40.30 o 10 10 3 60.58 61.09 19.75 o 11 10 3 11.70 0.08 16.95 o 12 10 3 17.68 23.36 20.10 o 13 10 3 262.96 230.09 35.53 o 14 10 3 15.19 17.85 26.03 o 15 10 3 64.75 56.72 31.30 o 16 10 3 0.01 -12.68 31.11 o 1 11 3 462.31 458.59 16.84 o 2 11 3 230.10 203.13 12.99 o 3 11 3 157.86 162.11 11.66 o 4 11 3 39.00 24.58 9.00 o 5 11 3 25.97 28.92 10.64 o 6 11 3 0.02 -10.44 11.45 o 7 11 3 375.31 370.07 23.12 o 8 11 3 1.82 -0.40 14.09 o 9 11 3 14.52 17.60 17.18 o 10 11 3 3.35 5.49 17.03 o 11 11 3 210.46 208.77 26.38 o 12 11 3 4.23 -6.46 19.29 o 13 11 3 40.52 32.71 22.85 o 14 11 3 13.05 21.54 26.25 o 15 11 3 156.53 178.69 37.44 o 16 11 3 10.10 -1.21 34.77 o 1 12 3 166.33 136.33 12.09 o 2 12 3 835.45 942.45 22.43 o 3 12 3 193.60 183.80 12.57 o 4 12 3 356.56 364.10 16.98 o 5 12 3 861.14 850.94 27.85 o 6 12 3 41.39 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217.90 45.28 o 2 16 8 20.26 42.11 33.82 o 3 16 8 283.42 335.07 51.68 o 4 16 8 147.17 122.69 41.49 o 5 16 8 66.57 54.02 37.74 o 6 16 8 71.68 110.76 46.59 o 7 16 8 416.21 538.45 79.13 o 0 17 8 362.19 366.67 81.61 o 1 17 8 110.84 124.28 39.26 o 2 17 8 0.63 -2.77 33.28 o 3 17 8 0.01 10.78 35.05 o 4 17 8 51.73 36.51 35.79 o 5 17 8 45.46 66.63 54.77 o 6 17 8 39.00 0.20 45.98 o 7 17 8 114.56 107.17 71.82 o 0 18 8 3.24 28.28 56.52 o 1 18 8 190.97 183.00 49.74 o 2 18 8 0.86 4.40 33.81 o 3 18 8 102.38 78.48 40.25 o 4 18 8 220.93 336.38 58.67 o 5 18 8 548.71 716.41 87.52 o 6 18 8 318.68 344.00 87.04 o 7 18 8 339.01 422.01 140.67 o 0 19 8 958.74 1015.44 117.63 o 1 19 8 44.60 23.81 41.58 o 2 19 8 38.81 32.07 41.66 o 3 19 8 72.44 57.73 43.61 o 4 19 8 873.37 1090.55 98.65 o 5 19 8 36.48 13.77 59.53 o 0 20 8 20.77 -7.03 73.85 o 1 20 8 4.46 2.40 47.32 o 2 20 8 1.69 6.71 53.08 o 3 20 8 0.49 -42.20 73.85 o 4 20 8 111.51 140.96 75.81 o 5 20 8 267.17 309.47 126.60 o 0 21 8 450.60 597.85 140.67 o 1 21 8 11.57 38.38 57.03 o 2 21 8 10.92 80.89 84.40 o 3 21 8 141.95 161.77 101.99 o 4 21 8 748.09 985.27 116.80 o 0 22 8 394.52 597.85 144.19 o 1 22 8 3.38 -56.27 77.37 o 2 22 8 15.51 52.75 98.47 o 3 22 8 2.69 -38.68 87.92 o 2 23 8 3.11 42.20 98.47 o 1 1 9 160.40 186.12 41.59 o 2 1 9 745.20 866.00 62.31 o 3 1 9 20.92 31.76 35.55 o 4 1 9 19.37 29.88 34.69 o 5 1 9 178.08 166.85 44.13 o 6 1 9 244.06 274.66 86.61 o 7 1 9 5.14 -1.99 65.86 o 1 2 9 196.63 203.36 42.05 o 2 2 9 53.83 89.72 37.79 o 3 2 9 234.66 175.94 42.67 o 4 2 9 287.74 322.04 49.24 o 5 2 9 157.31 212.34 46.23 o 6 2 9 5.29 1.08 52.48 o 7 2 9 28.36 49.23 105.50 o 1 3 9 9.53 11.82 32.74 o 2 3 9 42.04 51.61 35.53 o 3 3 9 71.32 87.72 37.73 o 4 3 9 5.61 -0.30 33.66 o 5 3 9 14.45 -10.68 36.18 o 6 3 9 63.90 138.70 62.24 o 1 4 9 43.05 37.47 35.00 o 2 4 9 520.49 591.27 55.92 o 3 4 9 119.05 89.90 37.31 o 4 4 9 67.79 45.49 36.75 o 5 4 9 9.26 2.63 46.73 o 6 4 9 455.82 603.67 83.86 o 1 5 9 98.52 117.19 38.43 o 2 5 9 26.20 46.00 38.45 o 3 5 9 41.97 45.36 35.40 o 4 5 9 12.62 11.37 34.65 o 5 5 9 27.38 26.53 46.50 o 6 5 9 93.71 123.09 116.05 o 1 6 9 176.49 194.22 41.47 o 2 6 9 220.72 199.53 42.22 o 3 6 9 30.44 24.50 35.70 o 4 6 9 102.78 104.50 40.20 o 5 6 9 27.63 65.12 69.49 o 6 6 9 233.01 267.27 133.64 o 1 7 9 66.63 124.90 38.91 o 2 7 9 208.62 216.77 43.75 o 3 7 9 0.00 40.82 38.41 o 4 7 9 13.85 18.93 35.38 o 5 7 9 158.01 214.52 123.09 o 6 7 9 186.97 214.52 112.54 o 1 8 9 48.19 57.57 35.85 o 2 8 9 229.34 261.11 46.35 o 3 8 9 15.57 12.04 34.55 o 4 8 9 0.94 -4.41 45.25 o 5 8 9 26.30 -3.52 105.50 o 1 9 9 127.58 171.50 42.25 o 2 9 9 81.98 126.40 40.67 o 3 9 9 0.54 -13.26 34.43 o 4 9 9 1.40 7.03 94.95 o 5 9 9 107.29 144.19 116.05 o 1 10 9 1.66 11.56 33.84 o 2 10 9 63.47 72.97 38.85 o 3 10 9 136.52 189.44 56.23 o 5 10 9 47.36 91.44 116.05 o 1 11 9 7.24 -2.36 40.84 o 2 11 9 278.66 359.88 64.88 o 3 11 9 13.94 13.53 64.08 o 4 11 9 20.30 80.89 109.02 o 1 12 9 162.60 177.46 55.96 o 2 12 9 72.71 107.77 72.57 o 3 12 9 7.09 -14.51 68.35 o 4 12 9 5.90 -7.03 101.99 o 1 13 9 58.00 129.67 76.97 o 2 13 9 244.89 225.88 86.93 o 3 13 9 88.80 142.43 77.09 o 4 13 9 0.25 -56.27 98.47 o 1 14 9 103.46 84.40 101.99 o 2 14 9 0.41 63.30 98.47 o 1 15 9 100.20 101.99 98.47 o 2 15 9 623.51 640.05 151.22 o 2 16 9 272.67 348.16 130.12 o