#------------------------------------------------------------------------------ #$Date: 2016-04-06 16:34:18 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181868 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/98/2019823.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2019823 _cell_angle_alpha 99.823 _cell_angle_beta 99.061 _cell_angle_gamma 102.677 _cell_length_a 10.3522 _cell_length_b 13.0010 _cell_length_c 21.9803 _exptl_crystal_F_000 1290.00 _reflns_d_resolution_high 0.7661 _cod_data_source_file gk2624Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 13mk0503_0m in P1 New: P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 302.53 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 14277.34 16587.22 115.86 o 3 0 0 24791.74 24949.54 157.56 o 4 0 0 45.11 6.21 27.81 o 5 0 0 300.88 303.07 26.33 o 6 0 0 2281.88 2727.95 50.10 o 7 0 0 2441.02 2842.59 87.03 o 8 0 0 10421.77 9930.24 125.28 o 9 0 0 3433.45 3580.21 122.23 o 10 0 0 778.29 1005.34 94.54 o 11 0 0 5573.02 5201.49 168.72 o 12 0 0 194.05 172.77 106.80 o -13 1 0 2616.10 2778.83 175.35 o -12 1 0 4.21 -114.72 114.72 o -11 1 0 8330.19 8737.97 197.31 o -10 1 0 2003.33 1932.58 105.87 o -9 1 0 2968.85 3084.10 99.84 o -8 1 0 9317.02 9264.22 96.57 o -7 1 0 5788.95 5555.34 78.17 o -6 1 0 247.26 218.30 27.46 o -5 1 0 5344.72 5355.11 52.44 o -4 1 0 10.65 30.28 16.72 o -3 1 0 29846.80 31467.33 187.00 o -2 1 0 29172.67 28842.26 162.51 o 1 1 0 570.89 352.94 88.69 o 2 1 0 6980.68 7118.67 60.02 o 3 1 0 888.82 996.66 28.94 o 4 1 0 3467.14 3652.36 51.14 o 5 1 0 9278.66 9054.08 102.19 o 6 1 0 15285.00 14613.10 146.21 o 7 1 0 3476.80 3923.87 83.55 o 8 1 0 1946.39 2057.09 71.82 o 9 1 0 4480.90 4628.54 190.41 o 10 1 0 30.20 56.54 81.87 o 11 1 0 3152.87 3373.33 146.03 o 12 1 0 1019.76 1260.90 134.84 o -13 2 0 3970.39 4163.72 305.17 o -12 2 0 77.10 -83.87 110.40 o -11 2 0 7616.56 8015.24 183.49 o -10 2 0 5946.97 5994.51 187.06 o -9 2 0 132.72 192.10 51.66 o -8 2 0 1364.90 1440.70 45.59 o -7 2 0 451.18 479.86 34.28 o -6 2 0 160.82 113.28 20.63 o -5 2 0 12704.73 13076.41 108.90 o -4 2 0 300.48 407.16 18.43 o -3 2 0 23716.77 24213.32 147.09 o -2 2 0 17245.73 18935.34 134.35 o -1 2 0 9034.28 9068.18 90.42 o 0 2 0 14724.36 14540.87 208.63 o 1 2 0 274.15 411.85 94.40 o 2 2 0 464.89 477.65 26.86 o 3 2 0 1741.73 1777.60 36.83 o 4 2 0 1228.23 1262.60 44.36 o 5 2 0 7360.78 7695.34 105.72 o 6 2 0 17790.65 17573.49 185.57 o 7 2 0 5640.61 5900.28 116.23 o 8 2 0 5757.62 5617.81 130.78 o 9 2 0 3312.09 3461.70 131.89 o 10 2 0 2352.57 2424.16 127.49 o 11 2 0 5583.74 5570.20 201.72 o 12 2 0 330.83 516.52 128.71 o -13 3 0 4540.05 4495.45 250.09 o -12 3 0 694.87 796.91 99.65 o -11 3 0 2918.63 2800.41 122.16 o -10 3 0 4929.88 4845.51 122.17 o -9 3 0 195.33 169.15 49.79 o -8 3 0 143.34 90.05 30.03 o -7 3 0 1083.16 1085.15 52.29 o -6 3 0 5.98 -19.76 19.76 o -5 3 0 32975.25 32791.47 233.04 o -4 3 0 18329.86 17780.09 124.74 o -3 3 0 4293.55 4269.82 52.36 o -2 3 0 33779.42 34429.29 194.86 o -1 3 0 22875.17 24942.79 157.50 o 0 3 0 2448.81 2610.73 41.03 o 1 3 0 5064.22 6875.14 109.40 o 2 3 0 1932.58 2201.82 48.26 o 3 3 0 11607.72 11016.22 103.15 o 4 3 0 9778.03 9476.25 101.93 o 5 3 0 2033.91 2153.53 70.38 o 6 3 0 13882.24 13624.77 187.30 o 7 3 0 1044.15 1054.88 76.63 o 8 3 0 6635.96 6415.15 153.93 o 9 3 0 2908.14 3070.58 123.61 o 10 3 0 746.76 943.28 107.41 o 11 3 0 6535.31 6541.49 233.11 o 12 3 0 2626.02 2728.39 175.07 o -13 4 0 4540.54 4579.43 369.39 o -12 4 0 4273.29 4607.98 186.71 o -11 4 0 95.77 64.63 63.62 o -10 4 0 425.79 414.38 56.91 o -9 4 0 64.88 -44.18 44.18 o -8 4 0 1595.79 1629.98 39.49 o -7 4 0 4448.42 4435.70 64.93 o -6 4 0 196.24 286.07 27.84 o -5 4 0 32860.39 31366.19 271.82 o -4 4 0 25473.27 24715.63 199.37 o -3 4 0 1039.72 1143.81 28.01 o -2 4 0 5330.04 5212.52 46.21 o -1 4 0 6366.63 6837.67 59.46 o 0 4 0 1179.49 1267.04 30.37 o 1 4 0 4558.45 4551.04 51.19 o 2 4 0 687.38 1239.71 141.09 o 3 4 0 1402.48 1425.10 56.37 o 4 4 0 19789.64 18734.53 250.85 o 5 4 0 1789.65 2148.54 57.26 o 6 4 0 8643.22 8590.22 149.54 o 7 4 0 820.63 934.63 78.08 o 8 4 0 7563.92 8308.34 169.66 o 9 4 0 6711.76 6873.37 179.44 o 10 4 0 582.07 670.74 116.00 o 11 4 0 1140.50 1101.46 141.81 o -13 5 0 994.34 951.82 260.17 o -12 5 0 1214.38 1325.65 176.72 o -11 5 0 81.78 -73.79 73.79 o -10 5 0 1518.47 1690.83 122.51 o -9 5 0 3189.88 3031.59 70.53 o -8 5 0 3412.21 3362.44 124.17 o -7 5 0 20527.03 20039.97 208.44 o -6 5 0 7691.42 7750.62 95.56 o -5 5 0 6555.05 6594.66 84.99 o -4 5 0 13325.56 13314.77 112.73 o -3 5 0 806.43 1026.99 27.14 o -2 5 0 12130.12 12390.59 89.11 o -1 5 0 5924.57 6323.53 64.21 o 0 5 0 4781.93 4895.78 61.47 o 1 5 0 25570.88 25236.79 190.81 o 2 5 0 32641.15 32803.27 291.50 o 3 5 0 173.66 251.68 42.67 o 4 5 0 7531.95 7648.70 117.14 o 5 5 0 1983.08 2096.09 85.53 o 6 5 0 6071.77 5911.99 104.28 o 7 5 0 302.19 410.67 71.30 o 8 5 0 4184.93 4320.47 134.64 o 9 5 0 8531.74 8612.45 205.22 o 10 5 0 1439.29 1432.83 235.69 o 11 5 0 228.83 168.84 131.23 o -13 6 0 166.75 117.62 232.98 o -12 6 0 789.32 506.63 159.88 o -11 6 0 82.83 -146.73 146.73 o -10 6 0 4043.91 3902.37 148.69 o -9 6 0 10722.04 10525.04 189.21 o -8 6 0 681.15 698.48 38.55 o -7 6 0 36900.20 35751.99 396.63 o -6 6 0 18694.18 17982.71 209.59 o -5 6 0 62.40 96.04 24.89 o -4 6 0 8714.13 9221.77 93.74 o -3 6 0 297.38 243.71 23.32 o -2 6 0 14355.35 15119.94 113.95 o -1 6 0 9684.04 9236.14 125.62 o 0 6 0 330.89 461.25 38.50 o 1 6 0 19243.40 19797.18 171.36 o 2 6 0 3170.69 2888.79 62.79 o 3 6 0 4345.43 4698.77 81.54 o 4 6 0 8013.96 8057.23 121.17 o 5 6 0 773.48 759.43 59.46 o 6 6 0 8380.38 8621.21 140.05 o 7 6 0 9488.21 9588.73 205.66 o 8 6 0 103.08 142.64 81.31 o 9 6 0 1237.44 1362.34 133.39 o 10 6 0 836.72 770.13 155.39 o -13 7 0 44.66 -122.16 187.32 o -12 7 0 1893.56 1679.07 182.56 o -11 7 0 201.60 129.16 97.63 o -10 7 0 8308.48 7971.16 198.11 o -9 7 0 5129.66 5144.75 156.27 o -8 7 0 800.18 861.96 120.45 o -7 7 0 3273.23 3111.81 107.54 o -6 7 0 988.55 1075.75 45.14 o -5 7 0 3539.92 3269.94 55.95 o -4 7 0 12307.00 12597.33 121.85 o -3 7 0 616.24 755.28 34.92 o -2 7 0 11399.30 10996.25 105.27 o -1 7 0 11997.59 11619.89 135.07 o 0 7 0 5320.26 4740.20 71.02 o 1 7 0 889.62 949.12 38.65 o 2 7 0 742.63 648.07 39.53 o 3 7 0 1289.38 1240.69 59.83 o 4 7 0 7609.53 7601.04 132.35 o 5 7 0 192.09 176.69 70.20 o 6 7 0 3378.61 3346.81 138.14 o 7 7 0 7326.85 7329.72 166.33 o 8 7 0 804.20 870.48 111.57 o 9 7 0 537.83 438.07 110.89 o 10 7 0 1563.49 1611.99 184.71 o -12 8 0 4176.45 4449.54 249.76 o -11 8 0 1858.07 1850.49 128.81 o -10 8 0 2204.02 2137.28 133.11 o -9 8 0 5119.68 4914.95 146.81 o -8 8 0 3568.21 3563.33 134.30 o -7 8 0 4944.60 4904.71 83.43 o -6 8 0 204.63 282.69 43.63 o -5 8 0 509.06 456.40 38.25 o -4 8 0 14149.95 13669.43 136.76 o -3 8 0 8789.28 9141.39 101.20 o -2 8 0 143.72 186.19 34.70 o -1 8 0 16785.09 16320.52 160.79 o 0 8 0 7427.87 7769.54 132.52 o 1 8 0 5309.79 5548.06 104.42 o 2 8 0 6220.14 6415.12 96.00 o 3 8 0 1855.80 2009.00 100.72 o 4 8 0 14854.56 14284.18 193.01 o 5 8 0 10556.98 10648.82 176.77 o 6 8 0 27.69 83.46 87.95 o 7 8 0 3883.56 3503.35 153.99 o 8 8 0 3286.15 3040.28 189.16 o 9 8 0 282.85 274.12 131.54 o -12 9 0 3282.95 3098.58 216.95 o -11 9 0 6554.25 6739.74 210.59 o -10 9 0 1522.84 1383.72 115.92 o -9 9 0 344.91 201.84 85.73 o -8 9 0 1780.90 1544.89 120.72 o -7 9 0 2189.26 2222.44 65.89 o -6 9 0 3449.30 3247.54 65.20 o -5 9 0 452.15 488.52 32.94 o -4 9 0 6252.60 6304.52 84.76 o -3 9 0 19224.38 18186.63 177.90 o -2 9 0 2628.84 2660.56 67.63 o -1 9 0 4752.62 4812.07 87.82 o 0 9 0 1278.64 1287.51 61.05 o 1 9 0 6503.89 6663.14 151.93 o 2 9 0 8380.45 8147.14 156.57 o 3 9 0 577.61 465.45 75.22 o 4 9 0 9378.50 9374.97 186.68 o 5 9 0 3077.33 2986.33 118.09 o 6 9 0 589.71 569.22 102.56 o 7 9 0 738.92 673.71 113.05 o 8 9 0 1118.93 1089.27 157.34 o 9 9 0 573.28 915.00 336.12 o -12 10 0 1624.27 1768.48 194.34 o -11 10 0 5221.40 5149.79 191.45 o -10 10 0 592.35 514.26 108.41 o -9 10 0 1052.42 1070.10 121.07 o -8 10 0 1384.84 1545.24 127.91 o -7 10 0 1843.46 1749.81 47.79 o -6 10 0 6836.95 6759.88 125.20 o -5 10 0 7672.80 7527.39 121.42 o -4 10 0 691.91 764.78 44.06 o -3 10 0 5573.56 5598.56 107.48 o -2 10 0 14.70 -13.17 38.38 o -1 10 0 4177.48 4151.48 89.05 o 0 10 0 2476.64 2329.40 109.80 o 1 10 0 3389.38 3311.02 134.34 o 2 10 0 12297.27 12044.61 217.98 o 3 10 0 7324.61 8014.04 186.15 o 4 10 0 884.23 866.61 107.18 o 5 10 0 4598.36 4473.18 179.26 o 6 10 0 44.98 -108.16 108.16 o 7 10 0 3947.25 3843.12 211.51 o 8 10 0 669.52 644.96 144.70 o -11 11 0 1392.10 1200.86 165.68 o -10 11 0 67.63 107.80 107.90 o -9 11 0 2569.74 2585.20 185.08 o -8 11 0 4842.73 4878.09 291.84 o -7 11 0 1051.70 1089.42 60.64 o -6 11 0 10727.22 10398.86 180.77 o -5 11 0 10212.12 10138.84 165.49 o -4 11 0 50.88 83.77 67.32 o -3 11 0 508.51 436.20 59.11 o -2 11 0 1823.14 1932.35 90.13 o -1 11 0 4322.09 4353.80 156.57 o 0 11 0 8807.00 8703.41 195.86 o 1 11 0 4.73 -41.75 84.75 o 2 11 0 11666.31 11383.65 221.85 o 3 11 0 4405.58 4033.09 155.70 o 4 11 0 391.30 313.55 103.04 o 5 11 0 1824.69 1697.19 178.85 o 6 11 0 349.77 509.67 146.05 o 7 11 0 4811.90 4972.68 246.04 o -11 12 0 1685.74 1864.28 191.35 o -10 12 0 133.35 74.94 118.59 o -9 12 0 4225.41 4473.65 215.10 o -8 12 0 7170.74 7466.33 252.29 o -7 12 0 392.48 357.61 63.42 o -6 12 0 3295.27 3341.06 117.02 o -5 12 0 2503.61 2470.89 106.46 o -4 12 0 485.06 480.14 75.32 o -3 12 0 7012.11 6738.28 159.90 o -2 12 0 2165.44 2234.42 98.43 o -1 12 0 5115.25 4911.42 145.68 o 0 12 0 18442.75 17642.47 277.70 o 1 12 0 3094.38 3352.79 151.50 o 2 12 0 409.62 433.49 109.69 o 3 12 0 1802.84 1836.74 172.43 o 4 12 0 221.57 259.99 133.24 o 5 12 0 2339.96 2361.10 187.60 o 6 12 0 211.94 346.04 136.64 o -10 13 0 583.92 1012.79 147.32 o -9 13 0 1766.44 1884.20 156.43 o -8 13 0 5295.67 5034.22 222.16 o -7 13 0 1592.99 1727.61 94.65 o -6 13 0 237.92 264.74 73.92 o -5 13 0 698.79 595.75 84.21 o -4 13 0 593.16 675.38 89.81 o -3 13 0 4667.20 4563.35 147.78 o -2 13 0 4388.90 4254.96 157.10 o -1 13 0 68.04 176.51 79.89 o 0 13 0 5827.18 5626.16 189.29 o 1 13 0 2642.25 3071.67 178.60 o 2 13 0 1295.31 1265.42 151.47 o 3 13 0 4461.30 4401.82 365.21 o 4 13 0 3.24 211.86 148.24 o 5 13 0 2454.31 2789.56 184.38 o -9 14 0 95.96 -60.17 132.26 o -8 14 0 949.67 726.68 187.16 o -7 14 0 366.81 277.20 78.06 o -6 14 0 1304.42 1514.71 195.94 o -5 14 0 4209.65 4166.53 157.51 o -4 14 0 247.68 143.32 96.96 o -3 14 0 3724.86 3592.87 156.17 o -2 14 0 10231.92 10266.56 240.82 o -1 14 0 3681.16 3570.94 165.23 o 0 14 0 1220.97 1441.80 158.21 o 1 14 0 1754.51 1774.08 131.06 o 2 14 0 1746.72 2045.77 157.33 o 3 14 0 3314.61 3627.99 290.70 o 4 14 0 96.10 110.36 150.92 o -8 15 0 490.65 250.17 201.03 o -7 15 0 1144.30 1287.02 203.79 o -6 15 0 138.67 74.08 126.40 o -5 15 0 4876.79 4576.41 179.02 o -4 15 0 2914.55 2927.92 186.37 o -3 15 0 1638.33 1608.38 158.22 o -2 15 0 3747.24 3771.09 202.44 o -1 15 0 68.37 16.67 120.02 o 0 15 0 2909.60 2934.31 216.67 o 1 15 0 1708.30 1661.81 179.26 o 2 15 0 1793.69 1990.57 171.43 o -6 16 0 6.39 -212.76 239.58 o -5 16 0 3194.19 3140.71 280.48 o -4 16 0 7655.04 8108.69 372.55 o -3 16 0 49.73 124.32 131.06 o -2 16 0 4554.97 4402.60 442.93 o -1 16 0 38.43 17.39 144.95 o 0 16 0 4210.95 3667.66 217.98 o 0 -16 1 729.07 828.97 291.26 o 1 -16 1 3402.64 3437.06 286.00 o 2 -16 1 382.99 388.97 147.95 o 3 -16 1 2404.51 2339.54 183.43 o 4 -16 1 590.63 254.59 188.67 o 5 -16 1 817.10 620.30 188.92 o 6 -16 1 2593.72 2424.01 219.25 o 7 -16 1 1032.32 1112.11 366.21 o -2 -15 1 2900.72 2685.59 452.54 o -1 -15 1 1231.26 1174.50 167.17 o 0 -15 1 963.25 1084.39 173.25 o 1 -15 1 2654.55 2413.09 254.41 o 2 -15 1 535.90 588.71 140.60 o 3 -15 1 6412.83 6533.94 215.33 o 4 -15 1 7139.96 7022.23 215.80 o 5 -15 1 54.14 -81.81 130.52 o 6 -15 1 4269.80 4483.98 174.67 o 7 -15 1 1681.83 1535.66 152.38 o 8 -15 1 277.20 293.70 306.60 o -4 -14 1 4099.75 3852.52 272.82 o -3 -14 1 284.26 463.67 150.43 o -2 -14 1 2073.76 2377.44 182.49 o -1 -14 1 2440.61 2435.42 174.81 o 0 -14 1 928.30 487.30 135.63 o 1 -14 1 5331.48 4855.75 178.52 o 2 -14 1 699.79 612.09 97.20 o 3 -14 1 2788.56 2739.30 134.70 o 4 -14 1 6141.55 6066.00 168.73 o 5 -14 1 891.30 880.29 96.57 o 6 -14 1 1071.30 1096.78 96.35 o 7 -14 1 1100.82 1011.86 90.78 o 8 -14 1 1168.25 953.93 150.42 o 9 -14 1 6141.64 6250.84 437.06 o -5 -13 1 770.43 689.89 157.97 o -4 -13 1 4761.25 4535.18 187.16 o -3 -13 1 209.56 116.10 118.10 o -2 -13 1 921.53 951.53 201.24 o -1 -13 1 2037.84 2029.72 138.10 o 0 -13 1 150.88 312.62 93.70 o 1 -13 1 8218.94 7877.39 156.63 o 2 -13 1 5885.00 6204.35 166.06 o 3 -13 1 471.19 550.50 87.09 o 4 -13 1 6108.75 5922.76 157.82 o 5 -13 1 320.41 322.80 88.33 o 6 -13 1 2726.32 2229.62 107.09 o 7 -13 1 1632.52 1542.14 89.93 o 8 -13 1 454.65 503.33 139.25 o 9 -13 1 5028.69 5174.64 293.52 o 10 -13 1 2820.79 2635.35 212.53 o -6 -12 1 1792.18 1804.59 184.03 o -5 -12 1 217.41 252.02 124.07 o -4 -12 1 4481.92 4389.71 175.56 o -3 -12 1 303.74 370.22 103.70 o -2 -12 1 743.84 802.14 104.72 o -1 -12 1 8962.19 8716.62 214.79 o 0 -12 1 1258.04 1393.69 112.68 o 1 -12 1 4000.04 3806.78 110.04 o 2 -12 1 14284.36 14283.15 194.18 o 3 -12 1 878.94 979.70 88.71 o 4 -12 1 5317.52 5059.74 139.74 o 5 -12 1 139.69 120.18 67.85 o 6 -12 1 6726.47 6651.42 150.82 o 7 -12 1 4597.82 4774.14 138.49 o 8 -12 1 382.44 493.38 133.19 o 9 -12 1 2091.40 2133.93 212.89 o 10 -12 1 3066.35 3395.19 181.63 o 11 -12 1 541.37 367.79 155.67 o -7 -11 1 911.13 607.76 157.45 o -6 -11 1 4401.45 4512.92 200.18 o -5 -11 1 65.13 -110.03 110.03 o -4 -11 1 2621.50 2395.06 139.72 o 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