data_2019843 _cell_angle_alpha 90.000 _cell_angle_beta 105.133 _cell_angle_gamma 90.000 _cell_length_a 18.0348 _cell_length_b 5.9874 _cell_length_c 16.2362 _exptl_crystal_F_000 704.00 _reflns_d_resolution_high 0.8402 _cod_data_source_file lf3007Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' SM1805_a.res in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 180.93 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 25.39 15.53 1.34 o 2 0 0 2907.90 2992.00 80.86 o 3 0 0 8124.51 8073.64 193.73 o 4 0 0 6955.11 6092.89 189.61 o 5 0 0 28007.69 23082.77 711.92 o 6 0 0 31.18 23.66 1.15 o 7 0 0 16517.91 16426.00 359.43 o 8 0 0 490.38 616.91 12.41 o 9 0 0 1659.20 1575.14 29.59 o 10 0 0 4402.09 4813.46 86.99 o 11 0 0 173.20 195.71 5.31 o 12 0 0 2200.85 2453.54 83.29 o 13 0 0 504.23 528.76 12.10 o 14 0 0 1301.06 1271.16 13.97 o 15 0 0 1672.81 1645.57 20.16 o 16 0 0 18.67 14.11 0.67 o 17 0 0 37.09 44.58 1.08 o 18 0 0 635.26 640.99 7.54 o 19 0 0 886.60 932.03 10.02 o 20 0 0 0.65 0.76 0.25 o 1 1 0 9672.91 8893.79 216.45 o 2 1 0 5131.05 4196.31 131.75 o 3 1 0 2435.59 2182.40 77.17 o 4 1 0 5938.94 6066.28 189.94 o 5 1 0 101.75 127.02 8.77 o 6 1 0 1253.15 1192.52 17.36 o 7 1 0 1800.60 1833.75 21.99 o 8 1 0 1582.08 1649.30 20.02 o 9 1 0 2573.92 2626.45 34.05 o 10 1 0 588.01 606.00 11.68 o 11 1 0 1618.24 1661.55 27.26 o 12 1 0 14.75 21.86 1.15 o 13 1 0 97.38 99.36 2.88 o 14 1 0 3176.28 3074.46 24.27 o 15 1 0 210.83 221.30 2.37 o 16 1 0 942.18 943.48 8.53 o 17 1 0 11.05 10.75 0.43 o 18 1 0 51.09 53.42 0.87 o 19 1 0 55.20 49.48 0.77 o 20 1 0 153.17 148.09 1.47 o 0 2 0 1216.04 1133.97 56.27 o 1 2 0 78.56 73.46 1.27 o 2 2 0 437.36 473.25 7.02 o 3 2 0 1819.39 1674.76 30.37 o 4 2 0 1.17 0.53 0.30 o 5 2 0 1008.05 951.12 15.62 o 6 2 0 886.05 950.13 15.78 o 7 2 0 314.53 272.04 6.54 o 8 2 0 2088.88 2235.72 35.91 o 9 2 0 44.87 60.36 1.61 o 10 2 0 586.83 575.76 9.71 o 11 2 0 2.13 4.99 1.10 o 12 2 0 2.02 2.43 0.59 o 13 2 0 554.86 518.86 4.90 o 14 2 0 541.90 543.66 4.91 o 15 2 0 95.84 102.64 1.45 o 16 2 0 261.51 245.55 2.71 o 17 2 0 2.68 2.08 0.31 o 18 2 0 248.39 229.23 2.86 o 19 2 0 95.94 110.09 1.65 o 1 3 0 607.18 643.03 8.73 o 2 3 0 1979.38 1990.80 25.53 o 3 3 0 82.92 143.83 2.51 o 4 3 0 2540.45 2682.60 34.13 o 5 3 0 882.18 998.33 16.28 o 6 3 0 1100.14 1143.48 21.82 o 7 3 0 536.50 579.54 14.94 o 8 3 0 414.18 395.02 11.17 o 9 3 0 947.81 934.14 32.94 o 10 3 0 142.65 146.72 8.32 o 11 3 0 1530.65 1519.04 18.53 o 12 3 0 425.77 414.25 6.10 o 13 3 0 2.30 2.91 0.53 o 14 3 0 31.15 28.38 1.34 o 15 3 0 1.20 3.06 0.53 o 16 3 0 3.12 2.88 0.54 o 17 3 0 14.35 17.87 0.95 o 18 3 0 1.74 2.87 0.44 o 0 4 0 1566.13 1572.64 29.44 o 1 4 0 4.04 11.40 1.04 o 2 4 0 165.40 168.49 3.14 o 3 4 0 201.90 180.83 3.02 o 4 4 0 354.50 348.59 5.47 o 5 4 0 3100.05 3030.38 84.20 o 6 4 0 160.34 173.24 3.80 o 7 4 0 394.76 370.55 5.31 o 8 4 0 111.65 123.37 2.85 o 9 4 0 10.18 16.23 1.05 o 10 4 0 1276.41 1190.08 19.41 o 11 4 0 413.86 453.72 8.58 o 12 4 0 234.38 243.03 4.94 o 13 4 0 343.77 349.72 10.71 o 14 4 0 83.08 73.68 2.06 o 15 4 0 615.00 568.56 9.65 o 16 4 0 0.28 1.00 0.44 o 17 4 0 63.60 66.52 1.85 o 1 5 0 834.99 778.92 6.85 o 2 5 0 112.28 113.41 1.59 o 3 5 0 985.28 919.14 7.92 o 4 5 0 390.47 372.72 3.78 o 5 5 0 338.08 314.31 3.58 o 6 5 0 795.19 756.40 8.48 o 7 5 0 206.08 205.53 3.15 o 8 5 0 71.98 73.21 2.55 o 9 5 0 500.55 513.16 17.75 o 10 5 0 13.78 9.78 0.95 o 11 5 0 23.03 18.61 1.21 o 12 5 0 28.42 26.69 1.32 o 13 5 0 363.29 349.60 7.22 o 14 5 0 128.42 124.51 2.93 o 0 6 0 219.93 212.06 3.47 o 1 6 0 126.26 132.92 1.92 o 2 6 0 448.91 448.80 5.00 o 3 6 0 1.86 4.93 0.40 o 4 6 0 17.32 16.05 0.62 o 5 6 0 100.33 90.72 1.59 o 6 6 0 1.72 2.97 0.48 o 7 6 0 32.89 28.35 1.07 o 8 6 0 0.23 0.89 0.58 o 9 6 0 134.25 125.62 3.98 o 10 6 0 13.85 17.33 1.28 o 11 6 0 73.31 66.29 2.35 o 1 7 0 6.43 5.16 0.28 o 2 7 0 20.51 25.96 0.55 o 3 7 0 3.31 5.45 0.32 o -20 1 1 96.78 88.20 1.07 o -19 1 1 17.53 19.33 0.53 o -18 1 1 147.33 151.10 1.73 o -17 1 1 4.61 3.29 0.34 o -16 1 1 90.61 85.17 1.10 o -15 1 1 1566.15 1523.32 11.37 o -14 1 1 342.49 318.57 2.87 o -13 1 1 548.35 602.22 10.40 o -12 1 1 66.22 70.84 2.16 o -11 1 1 770.68 827.92 11.87 o -10 1 1 137.06 118.58 2.68 o -9 1 1 16.33 10.63 1.06 o -8 1 1 63.29 77.57 1.55 o -7 1 1 1367.33 1438.07 20.07 o -6 1 1 829.43 869.97 12.84 o -5 1 1 0.14 -0.27 0.27 o -4 1 1 1403.88 1372.81 40.59 o -3 1 1 1207.70 1139.75 35.93 o -2 1 1 2717.52 2740.09 64.20 o -1 1 1 68.64 68.31 5.08 o 0 1 1 15000.92 14374.75 541.58 o 1 1 1 3748.68 3525.93 82.45 o 2 1 1 102.97 127.16 5.49 o 3 1 1 7371.23 6680.86 435.81 o 4 1 1 0.38 0.33 0.47 o 5 1 1 3152.55 3287.65 51.35 o 6 1 1 316.63 311.97 4.39 o 7 1 1 113.27 113.63 2.03 o 8 1 1 6427.80 7153.16 83.89 o 9 1 1 213.91 226.96 3.75 o 10 1 1 170.15 174.22 4.00 o 11 1 1 28.13 38.81 1.47 o 12 1 1 15.46 21.93 1.18 o 13 1 1 273.24 274.83 3.22 o 14 1 1 156.96 161.24 1.77 o 15 1 1 46.44 55.87 0.91 o 16 1 1 101.47 91.69 1.23 o 17 1 1 12.44 12.43 0.47 o 18 1 1 2.64 1.80 0.24 o 19 1 1 19.34 21.96 0.56 o 20 1 1 51.68 49.19 0.70 o -20 2 1 131.89 120.52 4.44 o -19 2 1 105.69 103.98 1.52 o -18 2 1 15.49 17.21 0.57 o -17 2 1 268.82 258.09 2.80 o -16 2 1 16.32 18.72 0.61 o -15 2 1 158.08 163.70 1.99 o -14 2 1 1538.32 1463.07 13.05 o -13 2 1 959.61 977.60 8.63 o -12 2 1 319.31 321.22 7.75 o -11 2 1 0.08 0.43 0.48 o -10 2 1 34.16 49.48 1.88 o -9 2 1 101.77 119.80 7.98 o -8 2 1 114.80 142.03 3.50 o -7 2 1 13.83 18.63 1.35 o -6 2 1 826.91 910.90 15.16 o -5 2 1 62.88 55.03 1.26 o -3 2 1 1867.52 1802.09 22.93 o -2 2 1 1623.52 1538.28 21.51 o -1 2 1 488.17 509.80 7.19 o 0 2 1 41.01 47.71 1.28 o 1 2 1 251.31 264.60 3.75 o 2 2 1 122.48 144.12 2.86 o 3 2 1 746.24 756.65 10.95 o 4 2 1 118.31 124.02 2.80 o 5 2 1 1518.49 1558.54 25.02 o 6 2 1 79.22 99.65 3.23 o 7 2 1 131.99 157.92 3.44 o 8 2 1 671.98 695.93 10.82 o 9 2 1 0.16 0.33 0.28 o 10 2 1 5.30 7.10 0.71 o 11 2 1 0.68 1.11 0.47 o 12 2 1 145.04 140.35 2.28 o 13 2 1 979.12 937.60 8.33 o 14 2 1 60.98 58.00 0.93 o 15 2 1 177.80 161.91 2.00 o 16 2 1 396.31 384.61 3.97 o 17 2 1 301.28 289.28 3.35 o 18 2 1 20.81 18.43 0.61 o 19 2 1 33.77 29.18 0.67 o -19 3 1 175.00 167.94 4.47 o -18 3 1 29.14 32.03 1.15 o -17 3 1 237.47 229.85 4.36 o -16 3 1 2.46 4.68 0.63 o -15 3 1 0.37 0.98 0.77 o -14 3 1 834.53 864.92 11.75 o -13 3 1 788.68 775.22 10.61 o -12 3 1 815.37 760.55 10.39 o -11 3 1 333.77 299.87 4.39 o -10 3 1 350.87 358.96 14.97 o -9 3 1 804.74 751.51 26.95 o -8 3 1 367.24 342.65 13.97 o -7 3 1 2173.58 2238.59 50.45 o -6 3 1 475.07 536.39 11.00 o -5 3 1 38.16 32.79 1.14 o -4 3 1 305.92 323.91 5.58 o -3 3 1 3420.64 3664.19 42.92 o -2 3 1 744.69 765.48 10.31 o -1 3 1 20.57 29.43 0.93 o 0 3 1 1587.99 1725.33 22.25 o 1 3 1 0.84 2.02 0.32 o 2 3 1 962.17 1103.35 15.94 o 3 3 1 33.08 42.43 1.08 o 4 3 1 14.10 25.61 0.81 o 5 3 1 908.76 1026.61 16.74 o 6 3 1 102.85 109.04 2.32 o 7 3 1 76.52 72.32 2.15 o 8 3 1 223.34 222.84 5.21 o 9 3 1 525.12 519.54 9.44 o 10 3 1 119.70 111.26 3.96 o 11 3 1 540.67 501.18 6.29 o 12 3 1 76.74 72.77 1.55 o 13 3 1 6.15 6.18 0.54 o 14 3 1 70.94 75.85 1.56 o 15 3 1 37.29 38.50 1.12 o 16 3 1 133.47 136.03 3.77 o 17 3 1 1.07 1.05 0.41 o 18 3 1 44.74 48.57 1.99 o -17 4 1 0.00 0.22 0.38 o -16 4 1 0.32 1.55 0.58 o -15 4 1 251.15 260.27 7.25 o -14 4 1 182.68 173.56 3.73 o -13 4 1 136.56 127.33 3.27 o -12 4 1 117.02 109.12 2.77 o -11 4 1 2542.53 2325.75 58.28 o -10 4 1 561.26 569.78 11.51 o -9 4 1 289.35 299.57 5.95 o -8 4 1 815.67 786.36 12.10 o -7 4 1 59.09 71.72 2.28 o -6 4 1 311.88 324.99 7.23 o -5 4 1 0.01 0.59 0.82 o -4 4 1 2574.42 2585.74 84.60 o -3 4 1 1.01 5.23 0.52 o -2 4 1 169.63 219.12 3.50 o -1 4 1 288.11 363.24 5.23 o 0 4 1 133.66 158.09 2.75 o 1 4 1 127.99 164.60 2.84 o 2 4 1 453.07 465.62 6.43 o 3 4 1 0.42 1.11 0.37 o 4 4 1 524.46 560.39 7.63 o 5 4 1 151.74 179.92 3.62 o 6 4 1 44.28 47.17 1.52 o 7 4 1 126.05 129.73 2.18 o 8 4 1 327.13 300.02 4.87 o 9 4 1 11.99 20.64 1.21 o 10 4 1 416.33 397.69 7.35 o 11 4 1 954.03 951.39 15.79 o 12 4 1 429.34 438.87 7.94 o 13 4 1 148.69 165.33 3.60 o 14 4 1 177.33 185.28 3.81 o 15 4 1 0.26 0.81 0.44 o 16 4 1 20.33 26.36 1.49 o -15 5 1 0.70 0.67 0.67 o -14 5 1 3.28 2.15 0.51 o -13 5 1 10.99 12.01 1.34 o -12 5 1 0.74 3.81 0.90 o -11 5 1 28.47 39.60 1.71 o -10 5 1 252.68 244.99 5.61 o -9 5 1 0.28 0.45 0.62 o -8 5 1 31.48 23.93 1.30 o -7 5 1 12.61 14.17 0.76 o -6 5 1 21.13 24.44 1.10 o -5 5 1 316.99 333.49 5.18 o -4 5 1 322.02 319.93 3.49 o -3 5 1 39.58 47.14 0.93 o -2 5 1 334.61 321.57 3.28 o -1 5 1 838.62 825.77 7.72 o 0 5 1 14.94 11.76 0.52 o 1 5 1 9.32 8.81 0.44 o 2 5 1 37.66 43.73 0.84 o 3 5 1 143.52 151.58 1.70 o 4 5 1 34.82 41.25 0.89 o 5 5 1 149.34 165.20 2.30 o 6 5 1 185.61 175.47 2.39 o 7 5 1 61.85 57.76 1.49 o 8 5 1 0.69 1.24 0.62 o 9 5 1 0.31 6.65 2.00 o 10 5 1 195.66 192.92 6.00 o 11 5 1 0.46 0.50 0.71 o 12 5 1 96.37 91.16 3.41 o 13 5 1 217.48 198.58 5.89 o 14 5 1 47.65 45.26 1.88 o -11 6 1 6.47 7.32 0.80 o -10 6 1 10.34 8.07 1.04 o -9 6 1 260.96 259.48 6.94 o -8 6 1 54.97 45.74 1.26 o -7 6 1 86.09 86.38 1.79 o -6 6 1 45.51 50.13 1.15 o -5 6 1 117.66 112.61 1.99 o -4 6 1 15.49 22.08 0.79 o -3 6 1 95.57 108.25 1.69 o -2 6 1 247.25 260.35 3.18 o -1 6 1 187.02 170.30 2.20 o 0 6 1 205.95 198.99 2.42 o 1 6 1 5.76 7.93 0.48 o 2 6 1 193.18 176.28 2.35 o 3 6 1 211.03 221.24 2.65 o 4 6 1 25.46 24.44 0.73 o 5 6 1 15.35 16.97 0.71 o 6 6 1 50.89 45.35 1.29 o 7 6 1 7.15 6.42 0.63 o 8 6 1 1.59 0.76 0.48 o 9 6 1 1.47 1.50 0.71 o 10 6 1 8.10 7.33 0.94 o -4 7 1 139.48 149.26 2.46 o -3 7 1 11.61 15.97 0.52 o -2 7 1 299.53 323.75 3.51 o -1 7 1 27.21 31.14 0.63 o 0 7 1 293.14 317.13 3.18 o 1 7 1 43.12 43.83 0.70 o 2 7 1 224.94 233.69 2.79 o 3 7 1 24.13 23.34 0.67 o -21 0 2 235.79 227.26 2.85 o -20 0 2 234.08 232.61 2.97 o -19 0 2 841.85 838.49 9.64 o -18 0 2 11.73 11.58 0.56 o -17 0 2 381.67 368.14 5.92 o -16 0 2 247.25 256.30 3.64 o -15 0 2 4362.27 4314.49 47.54 o -14 0 2 612.45 574.86 7.60 o -13 0 2 616.61 603.85 16.39 o -12 0 2 913.95 955.07 23.92 o -11 0 2 774.63 796.03 16.15 o -10 0 2 57.37 44.58 1.90 o -9 0 2 651.71 588.61 18.30 o -8 0 2 216.27 193.78 4.64 o -7 0 2 56.01 32.31 1.28 o -6 0 2 346.31 325.15 8.14 o -5 0 2 4465.12 4507.62 140.30 o -4 0 2 5022.70 5008.30 133.20 o -3 0 2 3714.37 3217.94 136.06 o -2 0 2 1159.46 1149.24 38.25 o -1 0 2 7069.42 6554.85 380.58 o 0 0 2 2417.82 2478.11 95.12 o 1 0 2 122.97 131.62 9.53 o 2 0 2 48.44 48.85 6.34 o 3 0 2 19025.77 18301.92 536.42 o 4 0 2 221.45 231.18 6.98 o 5 0 2 4433.14 4852.30 200.67 o 6 0 2 2921.63 2958.37 53.51 o 7 0 2 1611.33 1642.11 43.77 o 8 0 2 6601.37 7570.10 163.36 o 9 0 2 91.60 60.99 2.41 o 10 0 2 519.09 570.20 12.34 o 11 0 2 246.38 220.71 6.10 o 12 0 2 1535.28 1578.59 31.01 o 13 0 2 42.42 30.07 0.85 o 14 0 2 142.85 143.42 2.10 o 15 0 2 0.53 2.60 0.38 o 16 0 2 1750.46 1732.99 22.34 o 17 0 2 5.40 8.62 0.58 o 18 0 2 76.91 94.84 1.68 o 19 0 2 539.06 527.20 6.59 o 20 0 2 11.41 14.38 0.51 o -20 1 2 11.53 11.77 0.38 o -19 1 2 26.92 23.17 0.68 o -18 1 2 324.95 329.61 3.31 o -17 1 2 415.48 414.26 3.77 o -16 1 2 527.93 526.20 4.51 o -15 1 2 973.61 992.13 8.29 o -14 1 2 901.69 879.46 7.36 o -13 1 2 2.12 2.07 0.56 o -12 1 2 217.66 238.40 4.83 o -11 1 2 157.01 132.79 3.06 o -10 1 2 1966.88 2099.72 30.25 o -9 1 2 545.69 515.58 9.78 o -8 1 2 38.03 28.77 0.87 o -7 1 2 1113.91 1160.53 15.51 o -6 1 2 1.82 8.00 0.53 o -5 1 2 4699.69 4470.45 71.06 o -4 1 2 3.09 2.33 1.00 o -3 1 2 23.65 14.97 1.33 o -2 1 2 10321.75 8072.62 249.16 o -1 1 2 870.15 819.34 20.45 o 0 1 2 376.02 354.96 11.64 o 1 1 2 1058.33 842.31 26.95 o 2 1 2 1098.59 1102.27 24.58 o 3 1 2 4404.88 3507.30 180.48 o 4 1 2 48.99 55.25 1.87 o 5 1 2 5373.76 5266.54 200.53 o 6 1 2 6.16 3.23 0.70 o 7 1 2 3020.26 3306.24 43.57 o 8 1 2 3539.28 3745.59 44.45 o 9 1 2 147.99 186.20 3.30 o 10 1 2 1650.14 1652.10 22.40 o 11 1 2 132.56 166.38 6.17 o 12 1 2 1460.21 1526.29 22.49 o 13 1 2 3705.37 3615.71 26.71 o 14 1 2 26.73 25.12 0.60 o 15 1 2 259.63 293.51 2.77 o 16 1 2 37.67 31.93 0.68 o 17 1 2 1416.71 1397.09 11.49 o 18 1 2 145.73 150.97 1.58 o 19 1 2 257.65 243.87 2.25 o -20 2 2 141.00 150.89 2.07 o -19 2 2 100.18 97.10 1.39 o -18 2 2 556.27 567.37 5.72 o -17 2 2 234.10 249.42 2.87 o -16 2 2 289.54 299.08 3.47 o -15 2 2 16.86 16.82 0.55 o -14 2 2 648.87 626.23 6.19 o -13 2 2 162.01 149.86 1.83 o -12 2 2 97.35 86.45 3.00 o -11 2 2 69.70 54.52 2.10 o -10 2 2 599.05 608.58 12.53 o -9 2 2 268.91 332.01 10.31 o -8 2 2 172.31 157.97 5.67 o -7 2 2 1769.79 1712.64 46.49 o -6 2 2 1067.18 1146.59 32.11 o -5 2 2 28.64 55.21 1.32 o -4 2 2 317.20 289.25 3.96 o -3 2 2 518.78 432.62 5.91 o -2 2 2 2201.16 2221.58 28.21 o -1 2 2 83.44 69.87 1.33 o 0 2 2 4.19 5.18 0.75 o 1 2 2 536.57 561.50 7.47 o 2 2 2 928.25 885.71 13.73 o 3 2 2 3298.66 3565.70 43.51 o 4 2 2 38.58 33.44 1.41 o 5 2 2 1673.31 1739.07 22.46 o 6 2 2 13.83 17.08 1.86 o 7 2 2 1189.19 1117.21 25.49 o 8 2 2 140.29 152.18 3.74 o 9 2 2 1918.44 1995.24 29.00 o 10 2 2 17.17 24.97 1.59 o 11 2 2 453.85 493.00 8.68 o 12 2 2 2260.31 2169.20 17.27 o 13 2 2 1468.67 1480.75 12.78 o 14 2 2 839.66 816.54 7.51 o 15 2 2 127.18 131.97 1.80 o 16 2 2 186.50 190.69 2.31 o 17 2 2 194.27 191.17 2.38 o 18 2 2 262.63 238.95 2.91 o 19 2 2 776.41 737.70 11.85 o -19 3 2 89.15 89.25 1.91 o -18 3 2 145.73 155.17 2.87 o -17 3 2 224.50 238.95 4.07 o -16 3 2 398.47 411.55 7.31 o -15 3 2 1.72 2.50 0.49 o -14 3 2 90.20 97.18 2.19 o -13 3 2 727.04 742.94 11.13 o -12 3 2 118.12 127.03 2.48 o -11 3 2 946.31 946.14 11.93 o -10 3 2 42.42 60.22 4.66 o -9 3 2 948.75 925.15 32.27 o -8 3 2 23.11 21.29 2.66 o -7 3 2 390.07 345.01 9.38 o -6 3 2 359.51 350.43 16.30 o -5 3 2 568.64 603.64 14.84 o -4 3 2 198.58 142.12 3.09 o -3 3 2 1739.02 1953.48 23.26 o -2 3 2 1536.63 1515.72 18.18 o -1 3 2 261.32 298.46 4.12 o 0 3 2 202.21 233.39 3.39 o 1 3 2 614.23 802.73 9.98 o 2 3 2 54.39 71.38 1.39 o 3 3 2 26.40 12.79 0.59 o 4 3 2 11.38 7.71 0.69 o 5 3 2 607.88 634.09 10.81 o 6 3 2 19.56 20.27 0.95 o 7 3 2 16.32 20.41 1.09 o 8 3 2 454.38 426.35 9.10 o 9 3 2 256.50 254.83 5.41 o 10 3 2 375.70 351.76 4.03 o 11 3 2 565.36 546.31 5.89 o 12 3 2 1205.17 1191.08 14.10 o 13 3 2 12.94 12.62 0.66 o 14 3 2 4.84 4.88 0.51 o 15 3 2 17.34 18.99 0.82 o 16 3 2 152.37 152.35 2.57 o 17 3 2 374.35 384.78 6.57 o 18 3 2 582.70 546.81 12.58 o -17 4 2 375.83 372.26 7.36 o -16 4 2 114.93 111.50 2.44 o -15 4 2 6.44 5.70 0.91 o -14 4 2 1000.31 920.88 19.33 o -13 4 2 11.79 7.44 0.73 o -12 4 2 331.98 338.61 6.30 o -11 4 2 18.07 21.15 1.21 o -10 4 2 541.20 530.11 11.02 o -9 4 2 393.44 391.95 6.83 o -8 4 2 108.75 109.74 2.30 o -7 4 2 922.65 921.01 17.85 o -6 4 2 56.59 61.76 2.21 o -5 4 2 1916.31 1823.97 26.11 o -4 4 2 715.20 686.70 9.69 o -3 4 2 286.06 246.12 4.07 o -2 4 2 18.99 18.43 0.87 o -1 4 2 7.90 7.90 0.89 o 0 4 2 412.51 407.25 5.73 o 1 4 2 121.03 121.92 2.32 o 2 4 2 1089.00 1037.92 13.08 o 3 4 2 262.79 277.07 4.82 o 4 4 2 1224.70 1283.71 18.96 o 5 4 2 162.96 152.49 3.23 o 6 4 2 333.44 326.27 4.62 o 7 4 2 1092.25 1018.01 10.74 o 8 4 2 43.10 40.43 1.09 o 9 4 2 264.95 281.20 4.47 o 10 4 2 1.02 0.78 0.72 o 11 4 2 851.57 831.10 13.97 o 12 4 2 170.85 161.26 3.60 o 13 4 2 356.31 367.73 6.72 o 14 4 2 506.52 499.42 8.60 o 15 4 2 0.05 0.44 0.44 o 16 4 2 276.74 276.42 5.63 o -15 5 2 406.59 363.72 9.65 o -14 5 2 47.39 52.51 1.66 o -13 5 2 10.55 9.13 0.88 o -12 5 2 20.33 23.20 1.32 o -11 5 2 10.26 12.40 1.12 o -10 5 2 99.47 102.16 3.46 o -9 5 2 184.10 188.30 3.61 o -8 5 2 49.35 46.23 1.16 o -7 5 2 67.24 58.14 1.12 o -6 5 2 666.55 632.63 6.51 o -5 5 2 621.56 625.84 6.13 o -4 5 2 107.84 107.26 1.49 o -3 5 2 834.85 797.79 6.91 o -2 5 2 1023.39 999.20 8.81 o -1 5 2 12.36 9.68 0.45 o 0 5 2 379.21 390.52 3.86 o 1 5 2 204.45 185.02 2.01 o 2 5 2 271.19 268.60 2.61 o 3 5 2 1282.56 1188.01 10.33 o 4 5 2 248.60 229.12 2.80 o 5 5 2 105.06 95.34 1.57 o 6 5 2 9.49 11.37 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