data_2019848 _cell_angle_alpha 103.601 _cell_angle_beta 90.867 _cell_angle_gamma 108.240 _cell_length_a 9.7935 _cell_length_b 11.2141 _cell_length_c 19.5696 _exptl_crystal_F_000 760.00 _reflns_d_resolution_high 0.8393 _[local]_cod_data_source_file lx2294Isup2.hkl _[local]_cod_data_source_block I _shelx_title ' S965B IN P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 175.01 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 487.72 451.80 26.85 o 2 0 0 8.64 24.57 14.07 o 3 0 0 1684.72 1750.30 80.55 o 4 0 0 1919.26 1913.34 71.85 o 5 0 0 56.55 66.08 29.26 o 6 0 0 193.17 118.34 38.19 o 7 0 0 512.95 535.63 69.57 o 8 0 0 100.57 69.30 43.28 o 9 0 0 330.69 485.39 76.56 o 10 0 0 29.22 83.94 72.52 o 11 0 0 56.68 71.29 74.37 o -11 1 0 10.22 36.72 67.74 o -10 1 0 151.21 151.49 58.25 o -9 1 0 26.14 25.08 42.49 o -8 1 0 56.85 31.36 41.12 o -7 1 0 1600.76 1479.40 90.16 o -6 1 0 19.21 0.64 32.56 o -5 1 0 16.11 44.53 25.47 o -4 1 0 744.61 775.15 47.90 o -3 1 0 275.20 276.94 31.42 o -2 1 0 509.93 490.29 28.31 o -1 1 0 15.93 24.66 7.50 o 1 1 0 555.13 639.56 63.50 o 2 1 0 2404.88 2498.01 147.63 o 3 1 0 489.28 477.16 27.62 o 4 1 0 2562.66 2633.97 234.70 o 5 1 0 805.04 858.12 98.06 o 6 1 0 718.79 729.62 68.87 o 7 1 0 815.07 962.81 80.27 o 8 1 0 42.58 70.59 44.30 o 9 1 0 494.48 568.80 81.67 o 10 1 0 2.06 58.02 63.57 o -11 2 0 2.93 2.93 58.48 o -10 2 0 26.39 41.02 44.84 o -9 2 0 47.80 90.74 45.17 o -8 2 0 6.84 8.13 37.51 o -7 2 0 769.25 884.62 78.80 o -6 2 0 375.26 379.12 74.22 o -5 2 0 127.65 101.23 29.87 o -4 2 0 311.74 367.55 58.33 o -3 2 0 323.16 390.93 33.11 o -2 2 0 11877.98 12100.96 154.69 o -1 2 0 2163.97 2290.66 48.05 o 0 2 0 911.17 950.35 48.45 o 1 2 0 5004.21 5008.22 127.92 o 2 2 0 86.33 70.09 19.98 o 3 2 0 514.97 535.09 32.27 o 4 2 0 68.20 98.36 21.06 o 5 2 0 59.35 41.69 20.49 o 6 2 0 85.23 114.19 42.06 o 7 2 0 929.08 953.03 102.30 o 8 2 0 87.84 59.43 43.27 o 9 2 0 16.35 7.25 58.64 o 10 2 0 13.69 16.97 67.28 o -11 3 0 62.08 95.07 52.55 o -10 3 0 10.40 7.14 44.75 o -9 3 0 750.54 771.35 87.95 o -8 3 0 300.29 308.14 59.71 o -7 3 0 216.52 171.56 45.79 o -6 3 0 709.58 707.08 59.26 o -5 3 0 117.31 75.41 32.64 o -4 3 0 29.23 12.04 18.40 o -3 3 0 233.33 260.15 31.27 o -2 3 0 4802.07 4834.24 87.05 o -1 3 0 115.64 107.56 21.12 o 0 3 0 4292.00 4094.44 115.88 o 1 3 0 2518.94 2432.13 104.62 o 2 3 0 98.36 118.50 38.73 o 3 3 0 861.19 820.26 48.83 o 4 3 0 149.37 102.23 26.47 o 5 3 0 731.30 780.79 48.94 o 6 3 0 44.42 7.04 34.38 o 7 3 0 308.05 387.46 66.71 o 8 3 0 23.11 73.56 45.82 o 9 3 0 2.29 45.37 74.37 o -11 4 0 9.96 10.00 41.96 o -10 4 0 5.05 -23.41 36.91 o -9 4 0 576.50 542.73 75.82 o -8 4 0 176.15 167.30 49.50 o -7 4 0 1349.18 1302.03 84.89 o -6 4 0 1113.79 962.26 68.07 o -5 4 0 376.25 306.94 44.12 o -4 4 0 156.19 121.19 29.46 o -3 4 0 4130.13 4167.65 134.55 o -2 4 0 4645.71 4829.57 98.43 o -1 4 0 28.49 28.10 17.11 o 0 4 0 4797.12 4728.47 144.89 o 1 4 0 2982.02 2987.31 129.15 o 2 4 0 297.66 287.16 60.95 o 3 4 0 783.44 720.82 52.54 o 4 4 0 98.26 115.44 30.83 o 5 4 0 1313.22 1186.90 129.61 o 6 4 0 416.06 493.31 109.86 o 7 4 0 65.82 81.32 65.42 o 8 4 0 55.19 6.33 58.79 o 9 4 0 33.66 -15.43 58.64 o -11 5 0 2.42 18.32 43.71 o -10 5 0 163.53 170.07 55.30 o -9 5 0 740.65 775.58 88.25 o -8 5 0 13.54 28.62 53.39 o -7 5 0 729.62 689.35 75.32 o -6 5 0 1.27 -26.56 24.38 o -5 5 0 8.09 12.49 23.54 o -4 5 0 393.90 363.91 47.22 o -3 5 0 3309.99 3630.00 101.61 o -2 5 0 1665.06 1871.96 71.89 o -1 5 0 19.32 11.64 21.45 o 0 5 0 494.30 400.26 64.50 o 1 5 0 1188.83 1065.93 90.73 o 2 5 0 799.73 735.72 86.87 o 3 5 0 365.87 401.68 51.38 o 4 5 0 422.21 437.21 111.87 o 5 5 0 1018.19 1076.26 131.77 o 6 5 0 288.38 294.10 91.50 o 7 5 0 113.84 165.72 84.10 o 8 5 0 5.31 42.90 70.05 o -11 6 0 20.36 14.20 72.83 o -10 6 0 33.97 32.85 41.41 o -9 6 0 327.09 367.16 107.01 o -8 6 0 1.10 28.69 36.28 o 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8 0 2.83 28.39 69.75 o -9 8 0 126.37 241.48 93.51 o -8 8 0 83.52 95.82 74.22 o -7 8 0 264.33 217.64 52.71 o -6 8 0 912.56 992.69 82.72 o -5 8 0 13.58 7.54 31.88 o -4 8 0 1125.34 1199.50 80.96 o -3 8 0 45.28 25.62 31.65 o -2 8 0 1571.97 1531.23 89.82 o -1 8 0 1011.73 858.42 78.71 o 0 8 0 55.22 35.49 45.83 o 1 8 0 455.12 530.80 100.14 o 2 8 0 7.91 19.16 34.70 o 3 8 0 214.16 257.07 84.87 o 4 8 0 12.03 52.46 62.18 o 5 8 0 172.24 245.03 94.12 o 6 8 0 8.12 -7.10 61.10 o -10 9 0 74.29 2.31 72.68 o -9 9 0 199.86 217.26 100.14 o -8 9 0 116.42 229.14 97.06 o -7 9 0 83.29 106.93 75.61 o -6 9 0 80.77 164.49 80.70 o -5 9 0 6.29 -5.73 34.33 o -4 9 0 51.59 47.22 38.07 o -3 9 0 480.72 494.51 89.80 o -2 9 0 3001.07 2945.06 129.16 o -1 9 0 158.79 166.79 49.63 o 0 9 0 153.90 70.52 54.31 o 1 9 0 545.15 445.32 99.06 o 2 9 0 50.16 3.86 48.30 o 3 9 0 12.57 66.04 62.80 o 4 9 0 12.82 38.27 62.49 o 5 9 0 103.03 91.50 77.92 o -9 10 0 129.81 85.79 84.25 o -8 10 0 160.63 123.75 89.80 o -7 10 0 11.94 20.99 67.28 o 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