data_2019866 _cell_angle_alpha 90.000 _cell_angle_beta 104.129 _cell_angle_gamma 90.000 _cell_length_a 21.5898 _cell_length_b 12.3292 _cell_length_c 43.4034 _exptl_crystal_F_000 4688.00 _reflns_d_resolution_high 0.8353 _cod_data_source_file fg3327Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' skni325 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 751.97 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 146992.94 146348.80 1494.40 o 4 0 0 405074.06 385364.59 3880.53 o 6 0 0 14398.77 14820.31 341.41 o 8 0 0 166.90 449.46 53.46 o 10 0 0 5205.34 5103.16 175.37 o 12 0 0 1306.23 1781.41 166.79 o 14 0 0 408.92 720.60 60.59 o 16 0 0 1708.64 904.09 168.86 o 18 0 0 9797.39 11300.34 396.42 o 20 0 0 933.75 1409.88 142.62 o 22 0 0 112.87 153.57 50.27 o 24 0 0 662.92 709.87 87.33 o 1 1 0 147809.64 150808.58 1055.64 o 3 1 0 90431.60 82302.20 721.21 o 5 1 0 30921.98 34622.15 473.52 o 7 1 0 52616.86 42991.36 359.36 o 9 1 0 26007.21 29349.38 347.38 o 11 1 0 1872.35 1108.23 74.82 o 13 1 0 8763.14 8178.73 173.18 o 15 1 0 5808.61 5607.94 127.32 o 17 1 0 2743.26 3185.56 129.31 o 19 1 0 2311.72 2702.59 112.28 o 21 1 0 1246.80 1325.95 98.55 o 23 1 0 27.37 -1.39 29.72 o 0 2 0 2138.64 1028.92 47.45 o 2 2 0 3202.72 2328.58 45.82 o 4 2 0 2701.57 2157.94 46.14 o 6 2 0 45185.79 44495.43 415.37 o 8 2 0 12153.07 13856.96 198.66 o 10 2 0 54988.17 56054.46 548.22 o 12 2 0 8119.79 7829.26 197.15 o 14 2 0 146.97 91.54 28.16 o 16 2 0 713.41 577.20 46.82 o 18 2 0 2525.50 2023.23 97.12 o 20 2 0 145.92 116.81 41.91 o 22 2 0 589.49 694.71 60.32 o 24 2 0 390.62 358.48 40.26 o 1 3 0 76612.20 74614.97 549.78 o 3 3 0 1679.29 2146.93 54.18 o 5 3 0 2129.10 2136.18 54.06 o 7 3 0 9314.20 8856.46 143.56 o 9 3 0 4263.12 5054.25 102.16 o 11 3 0 115.03 69.27 33.02 o 13 3 0 2114.21 2447.13 95.12 o 15 3 0 3487.50 4234.86 102.43 o 17 3 0 287.08 192.07 34.55 o 19 3 0 2308.92 2814.25 97.24 o 21 3 0 26.72 -15.35 30.06 o 23 3 0 0.95 47.08 38.26 o 0 4 0 14976.30 12544.43 200.84 o 2 4 0 28083.39 25876.12 206.75 o 4 4 0 32378.35 26574.73 243.81 o 6 4 0 10652.06 11313.27 166.27 o 8 4 0 7765.76 7957.30 255.34 o 10 4 0 1657.32 2055.26 102.93 o 12 4 0 39.13 53.79 24.58 o 14 4 0 17.76 4.90 19.26 o 16 4 0 1223.32 1626.87 66.68 o 18 4 0 32.52 51.32 34.38 o 20 4 0 1080.81 1328.63 68.48 o 22 4 0 58.50 135.56 31.22 o 24 4 0 83.54 115.38 93.75 o 1 5 0 6107.27 5167.98 79.42 o 3 5 0 16891.74 18617.48 204.10 o 5 5 0 1261.48 555.72 49.55 o 7 5 0 13.17 458.03 63.49 o 9 5 0 3164.56 2775.09 114.63 o 11 5 0 1457.57 1418.29 52.60 o 13 5 0 557.42 450.91 30.04 o 15 5 0 8735.07 7059.04 124.48 o 17 5 0 139.84 129.04 31.57 o 19 5 0 163.61 189.59 48.52 o 21 5 0 1.85 -29.54 29.54 o 23 5 0 210.77 425.36 30.95 o 0 6 0 5745.52 4717.84 174.02 o 2 6 0 1674.39 1857.30 75.16 o 4 6 0 779.85 871.99 66.47 o 6 6 0 291.17 50.65 32.11 o 8 6 0 367.97 138.14 38.97 o 10 6 0 1115.14 1095.34 36.55 o 12 6 0 3104.57 2469.72 70.31 o 14 6 0 2438.51 2076.61 69.92 o 16 6 0 1009.17 1455.36 52.24 o 18 6 0 70.38 60.14 30.82 o 20 6 0 210.24 244.17 29.67 o 22 6 0 6.37 51.18 21.45 o 1 7 0 2361.83 2716.81 102.89 o 3 7 0 734.01 609.19 62.46 o 5 7 0 30.93 38.69 29.39 o 7 7 0 4370.94 5602.76 74.06 o 9 7 0 8487.12 8622.55 95.79 o 11 7 0 1726.18 2529.04 55.82 o 13 7 0 6575.14 5907.35 107.98 o 15 7 0 2509.41 2494.82 72.05 o 17 7 0 2076.97 1785.16 65.77 o 19 7 0 1138.81 967.98 42.51 o 21 7 0 0.13 10.70 25.46 o 0 8 0 9398.09 8462.79 190.14 o 2 8 0 6615.66 8439.65 109.67 o 4 8 0 80.30 126.57 16.74 o 6 8 0 4595.24 4584.78 61.53 o 8 8 0 753.72 797.21 30.66 o 10 8 0 5940.97 6558.06 99.68 o 12 8 0 2995.19 3645.21 71.21 o 14 8 0 2594.40 2551.91 64.63 o 16 8 0 2995.04 3990.58 82.19 o 18 8 0 224.99 596.91 35.39 o 20 8 0 195.42 266.76 27.81 o 1 9 0 25.26 39.52 28.33 o 3 9 0 9478.44 10261.06 104.33 o 5 9 0 9351.90 8946.08 97.77 o 7 9 0 2950.57 2891.69 56.50 o 9 9 0 614.04 686.79 36.22 o 11 9 0 2704.99 3686.13 77.44 o 13 9 0 5931.31 5668.96 101.27 o 15 9 0 1460.30 1166.65 54.73 o 17 9 0 90.55 146.75 36.86 o 19 9 0 111.16 196.32 33.91 o 0 10 0 29987.78 34498.10 599.84 o 2 10 0 4417.78 4308.50 98.89 o 4 10 0 5323.36 4473.88 94.59 o 6 10 0 9.16 220.99 32.91 o 8 10 0 382.47 342.56 28.07 o 10 10 0 20.90 123.13 24.85 o 12 10 0 813.29 1540.75 59.16 o 14 10 0 23.33 88.79 27.13 o 16 10 0 616.12 561.11 46.64 o 18 10 0 18.36 84.23 40.44 o 1 11 0 1232.25 1718.07 57.13 o 3 11 0 327.30 404.95 37.47 o 5 11 0 1.17 9.74 30.45 o 7 11 0 206.97 259.06 34.88 o 9 11 0 73.46 148.76 40.26 o 11 11 0 1.59 120.52 32.25 o 13 11 0 61.58 271.04 30.57 o 15 11 0 223.58 440.52 40.10 o 0 12 0 4299.88 3779.48 112.96 o 2 12 0 163.58 173.85 25.52 o 4 12 0 84.92 259.14 37.44 o 6 12 0 533.60 683.29 46.37 o 8 12 0 1314.62 1128.87 75.02 o 10 12 0 614.12 694.98 52.68 o 12 12 0 70.97 148.88 27.95 o 14 12 0 0.43 92.17 38.15 o 1 13 0 5.62 184.22 33.65 o 3 13 0 38.77 59.87 31.76 o 5 13 0 633.65 555.95 47.78 o 7 13 0 27.12 -0.85 36.13 o 9 13 0 28.49 62.02 32.59 o 11 13 0 68.24 17.53 35.81 o 0 14 0 40.58 171.38 44.07 o 2 14 0 22.84 1.14 28.25 o 4 14 0 449.48 514.31 142.34 o 6 14 0 59.65 54.35 34.40 o -25 1 1 96.16 316.34 60.50 o -23 1 1 130.59 122.83 33.61 o -21 1 1 1016.24 1006.74 87.69 o -19 1 1 811.22 680.76 64.27 o -17 1 1 1694.09 1275.90 84.86 o -15 1 1 1041.78 1521.91 60.81 o -13 1 1 538.84 507.30 73.97 o -11 1 1 1511.02 1527.83 84.52 o -9 1 1 1511.22 1444.75 64.19 o -7 1 1 2214.42 1901.22 51.54 o -5 1 1 31698.57 27457.23 243.92 o -3 1 1 100184.66 85895.05 1253.04 o -1 1 1 17606.44 13201.88 254.47 o 1 1 1 14243.64 17729.81 188.42 o 3 1 1 11048.50 8509.23 119.95 o 5 1 1 4761.87 5729.62 96.79 o 7 1 1 14664.49 14588.75 158.76 o 9 1 1 121.52 130.56 33.83 o 11 1 1 24570.37 23683.06 419.90 o 13 1 1 328.44 346.58 41.45 o 15 1 1 2858.27 2473.04 97.66 o 17 1 1 759.44 627.48 74.66 o 19 1 1 1742.87 974.35 91.29 o 21 1 1 356.92 347.23 48.18 o 23 1 1 96.87 104.29 27.37 o -24 2 1 1222.17 1291.03 67.18 o -22 2 1 75.23 59.54 34.63 o -20 2 1 512.59 461.90 54.25 o -18 2 1 1695.55 1707.76 77.07 o -16 2 1 6975.89 6777.85 129.20 o -14 2 1 604.86 275.71 29.22 o -12 2 1 1149.17 1125.19 83.12 o -10 2 1 555.28 637.17 55.73 o -8 2 1 8292.76 9298.80 157.05 o -6 2 1 110725.35 117887.59 807.52 o -4 2 1 23335.62 23243.67 173.70 o -2 2 1 177.57 547.19 24.70 o 0 2 1 8049.54 9836.83 322.26 o 2 2 1 2842.60 2562.45 47.41 o 4 2 1 91367.98 83516.02 697.22 o 6 2 1 48572.82 45563.47 393.92 o 8 2 1 127.79 215.66 26.84 o 10 2 1 726.75 1356.74 79.93 o 12 2 1 2975.31 2274.50 131.64 o 14 2 1 1472.18 1371.52 56.94 o 16 2 1 3215.91 3337.61 102.83 o 18 2 1 67.84 24.10 39.07 o 20 2 1 773.26 820.98 84.69 o 22 2 1 2149.96 2486.89 101.34 o 24 2 1 37.51 152.97 26.45 o -23 3 1 1135.28 1605.96 64.34 o -21 3 1 553.34 554.53 47.52 o -19 3 1 75.17 231.10 39.43 o -17 3 1 2.71 106.95 33.24 o -15 3 1 10144.14 9651.80 171.79 o -13 3 1 3501.93 3399.26 99.55 o -11 3 1 5454.23 5188.24 136.18 o -9 3 1 27146.71 29019.51 373.27 o -7 3 1 244.64 263.05 34.46 o -5 3 1 16121.35 19227.39 175.17 o -3 3 1 50769.92 52214.00 355.37 o -1 3 1 1789.44 775.65 29.01 o 1 3 1 65097.51 61455.01 437.82 o 3 3 1 22224.72 21574.26 190.69 o 5 3 1 9943.19 8298.84 125.05 o 7 3 1 31911.14 31779.16 258.73 o 9 3 1 3463.54 2914.54 78.10 o 11 3 1 817.88 517.04 56.58 o 13 3 1 410.10 213.76 28.03 o 15 3 1 1439.52 1063.20 55.05 o 17 3 1 21.51 43.95 29.81 o 19 3 1 1948.64 2029.25 84.52 o 21 3 1 574.46 732.21 52.78 o 23 3 1 171.06 104.71 24.88 o -24 4 1 65.14 20.63 26.07 o -22 4 1 189.38 90.01 33.10 o -20 4 1 813.43 990.12 60.11 o -18 4 1 1484.99 1618.62 87.89 o -16 4 1 2272.68 2854.96 85.61 o -14 4 1 158.93 140.98 24.64 o -12 4 1 24.82 -13.94 23.90 o -10 4 1 7.91 7.57 43.76 o -8 4 1 3608.76 4107.16 144.31 o -6 4 1 28325.92 25286.49 261.12 o -4 4 1 25002.79 25379.09 238.75 o -2 4 1 12735.16 15020.89 149.29 o 0 4 1 9906.77 10404.07 126.71 o 2 4 1 40391.82 42819.20 289.21 o 4 4 1 39942.95 38826.48 311.80 o 6 4 1 41114.03 47971.09 458.93 o 8 4 1 2356.04 3360.13 98.26 o 10 4 1 26.52 265.96 46.97 o 12 4 1 24.52 13.13 22.15 o 14 4 1 89.75 138.26 24.36 o 16 4 1 98.11 214.21 34.18 o 18 4 1 2.98 87.32 39.92 o 20 4 1 93.40 230.90 37.22 o 22 4 1 315.44 287.75 34.22 o -23 5 1 59.96 21.73 18.71 o -21 5 1 4.83 6.37 27.33 o -19 5 1 42.93 73.15 30.79 o -17 5 1 6535.20 5539.39 122.01 o -15 5 1 927.12 1019.66 46.89 o -13 5 1 79.30 114.22 23.17 o -11 5 1 256.55 202.30 26.19 o -9 5 1 1881.71 2602.56 108.33 o -7 5 1 4122.66 4274.99 193.60 o -5 5 1 5479.30 7063.36 130.59 o -3 5 1 3197.87 3863.06 88.21 o -1 5 1 493.32 341.51 21.94 o 1 5 1 33458.74 34510.98 248.03 o 3 5 1 5531.64 5023.40 174.06 o 5 5 1 3707.78 4112.92 123.16 o 7 5 1 1554.68 1593.95 110.91 o 9 5 1 45.31 -1.36 28.74 o 11 5 1 1629.30 1782.99 50.61 o 13 5 1 631.59 1027.33 41.39 o 15 5 1 2045.77 3114.35 84.90 o 17 5 1 259.90 98.18 30.01 o 19 5 1 180.42 278.53 39.45 o 21 5 1 584.17 603.99 46.08 o 23 5 1 17.48 -13.92 26.23 o -22 6 1 253.36 262.21 27.42 o -20 6 1 351.29 288.50 32.70 o -18 6 1 151.00 33.78 25.41 o -16 6 1 1.10 2.40 21.49 o -14 6 1 6215.22 5436.60 110.57 o -12 6 1 131.77 418.18 31.02 o -10 6 1 237.53 54.67 18.70 o -8 6 1 208.13 140.99 35.47 o -6 6 1 1093.86 569.77 54.71 o -4 6 1 26973.48 31554.19 474.66 o -2 6 1 30516.72 33402.80 415.54 o 0 6 1 6178.55 5047.12 106.57 o 2 6 1 574.51 1898.64 76.58 o 4 6 1 33972.20 34074.34 412.21 o 6 6 1 23733.96 28023.99 477.92 o 8 6 1 879.21 1650.55 89.13 o 10 6 1 3272.41 3590.10 66.88 o 12 6 1 556.34 287.46 30.72 o 14 6 1 383.31 554.12 44.00 o 16 6 1 4456.04 3621.98 92.67 o 18 6 1 2095.81 2020.34 76.99 o 20 6 1 24.69 47.47 24.57 o 22 6 1 88.57 218.32 27.51 o -21 7 1 17.82 22.37 24.92 o -19 7 1 34.00 14.98 21.32 o -17 7 1 3568.14 3532.74 83.58 o -15 7 1 776.48 765.78 44.14 o -13 7 1 37.61 19.24 21.66 o -11 7 1 279.58 160.28 22.63 o -9 7 1 567.15 535.10 29.52 o -7 7 1 425.82 1031.58 34.10 o -5 7 1 4136.68 5228.65 121.75 o -3 7 1 306.81 196.21 43.62 o -1 7 1 2435.86 1839.27 85.93 o 1 7 1 3567.34 3072.67 109.11 o 3 7 1 2311.76 3966.18 120.54 o 5 7 1 6488.83 7364.92 200.62 o 7 7 1 5.26 172.60 20.88 o 9 7 1 278.20 24.42 15.82 o 11 7 1 86.54 75.36 20.05 o 13 7 1 1254.84 1725.58 56.96 o 15 7 1 130.41 141.66 28.70 o 17 7 1 259.56 460.34 35.67 o 19 7 1 193.58 246.41 37.28 o 21 7 1 212.48 207.53 27.82 o -20 8 1 678.45 794.27 59.47 o -18 8 1 133.83 62.13 22.34 o -16 8 1 505.35 689.04 36.38 o -14 8 1 5618.35 4805.23 82.21 o -12 8 1 2492.35 2133.01 63.63 o -10 8 1 96.61 82.14 21.01 o -8 8 1 311.37 377.74 25.91 o -6 8 1 1386.83 1385.13 36.44 o -4 8 1 202.38 112.62 16.64 o -2 8 1 1565.52 1762.04 55.24 o 0 8 1 445.50 599.90 35.27 o 2 8 1 91.53 173.92 21.85 o 4 8 1 2460.50 3075.74 50.46 o 6 8 1 4236.32 4895.13 66.12 o 8 8 1 0.37 81.94 17.77 o 10 8 1 1904.20 2148.23 53.78 o 12 8 1 654.05 656.12 34.15 o 14 8 1 374.84 545.53 35.38 o 16 8 1 1256.72 1308.94 49.73 o 18 8 1 193.51 254.80 32.99 o 20 8 1 38.56 -10.64 25.13 o -19 9 1 28.81 47.93 30.05 o -17 9 1 229.89 12.02 33.96 o -15 9 1 638.14 781.00 47.62 o -13 9 1 364.55 225.66 30.06 o -11 9 1 2189.52 2091.84 63.21 o -9 9 1 3416.06 3412.36 70.42 o -7 9 1 8667.27 9819.75 158.99 o -5 9 1 1755.57 2534.92 55.71 o -3 9 1 500.23 923.27 33.09 o -1 9 1 1703.59 1117.83 45.18 o 1 9 1 13.04 85.22 26.16 o 3 9 1 117.94 245.83 23.51 o 5 9 1 1691.64 1241.90 50.92 o 7 9 1 3777.93 4856.66 82.95 o 9 9 1 4902.97 3200.17 64.11 o 11 9 1 3779.74 4141.95 82.37 o 13 9 1 7308.87 8403.52 130.37 o 15 9 1 239.15 275.22 32.27 o 17 9 1 103.57 45.11 24.16 o 19 9 1 23.57 140.75 28.14 o -18 10 1 395.51 152.63 40.54 o -16 10 1 174.46 20.12 25.40 o -14 10 1 698.89 595.19 38.05 o -12 10 1 1486.10 1367.84 51.82 o -10 10 1 54.01 138.99 22.20 o -8 10 1 2443.64 2209.79 60.80 o -6 10 1 3309.78 3384.95 74.34 o -4 10 1 411.11 316.21 34.16 o -2 10 1 40.20 30.75 25.10 o 0 10 1 155.11 429.48 44.70 o 2 10 1 837.82 411.58 41.66 o 4 10 1 6433.75 6452.55 112.58 o 6 10 1 10305.63 10567.18 191.19 o 8 10 1 610.39 452.40 32.85 o 10 10 1 4991.92 5104.35 96.09 o 12 10 1 1646.14 1823.30 68.20 o 14 10 1 154.16 183.19 30.74 o 16 10 1 276.74 239.74 35.29 o 18 10 1 5.60 2.35 30.08 o -15 11 1 538.35 527.35 42.80 o -13 11 1 5.31 19.99 24.13 o -11 11 1 3841.94 4029.59 113.54 o -9 11 1 1023.75 989.50 48.78 o -7 11 1 104.17 114.71 31.16 o -5 11 1 9.71 19.23 28.16 o -3 11 1 3054.33 4072.71 133.21 o -1 11 1 0.75 112.98 29.35 o 1 11 1 5126.62 5087.08 89.16 o 3 11 1 142.02 118.41 27.83 o 5 11 1 548.26 778.58 49.01 o 7 11 1 1707.73 1446.12 95.44 o 9 11 1 3894.39 3866.02 109.30 o 11 11 1 391.13 447.13 38.49 o 13 11 1 1016.59 779.85 39.46 o 15 11 1 535.53 627.28 68.53 o -14 12 1 750.03 1003.20 79.74 o -12 12 1 1.96 4.98 30.37 o -10 12 1 879.10 912.69 66.09 o -8 12 1 1085.45 1148.01 59.24 o -6 12 1 1925.52 1938.26 105.32 o -4 12 1 0.71 64.51 27.78 o -2 12 1 489.35 511.24 42.14 o 0 12 1 217.60 432.62 34.88 o 2 12 1 215.24 491.93 32.21 o 4 12 1 817.59 1135.30 59.06 o 6 12 1 1629.67 2493.31 82.21 o 8 12 1 225.34 91.09 27.66 o 10 12 1 81.85 121.37 33.72 o 12 12 1 752.87 623.56 36.18 o 14 12 1 95.76 -51.34 65.69 o -11 13 1 371.32 367.08 33.06 o -9 13 1 111.82 184.16 30.08 o -7 13 1 46.23 -10.35 39.72 o -5 13 1 543.37 432.83 43.21 o -3 13 1 403.21 329.21 36.84 o -1 13 1 329.83 396.20 36.05 o 1 13 1 1254.45 1044.97 55.63 o 3 13 1 27.80 16.36 32.63 o 5 13 1 0.06 -26.60 26.60 o 7 13 1 533.32 448.49 56.94 o 9 13 1 200.92 124.73 23.84 o 11 13 1 25.59 9.01 24.83 o -6 14 1 4.32 63.54 49.41 o -4 14 1 806.71 783.72 98.68 o -2 14 1 0.49 95.73 120.77 o 0 14 1 391.83 397.22 41.45 o 2 14 1 8.19 68.11 34.01 o 4 14 1 4.31 46.14 73.80 o 6 14 1 0.43 60.47 98.34 o -24 0 2 80.27 60.88 35.38 o -22 0 2 1711.21 1689.46 146.75 o -20 0 2 7885.88 7694.61 323.92 o -18 0 2 3166.17 2789.69 194.57 o -16 0 2 1570.26 1052.38 75.04 o -14 0 2 13708.24 14947.32 270.10 o -12 0 2 58565.37 55002.54 725.27 o -10 0 2 1739.69 2757.50 128.60 o -8 0 2 67872.25 70409.23 1024.15 o -6 0 2 87208.48 89987.82 1136.80 o -4 0 2 5995.10 5848.59 163.67 o -2 0 2 476485.97 441183.31 4309.38 o 2 0 2 99261.71 107897.80 1135.88 o 4 0 2 3722.31 2846.89 83.24 o 6 0 2 174451.39 150291.91 973.31 o 8 0 2 2499.98 1096.24 104.23 o 10 0 2 1260.86 1773.19 148.60 o 12 0 2 4703.75 4244.36 256.96 o 14 0 2 9877.71 10140.09 272.01 o 16 0 2 9161.19 10132.03 289.76 o 18 0 2 3369.52 3701.70 229.46 o 20 0 2 277.90 383.98 87.26 o 22 0 2 243.49 347.54 55.75 o 24 0 2 267.98 218.05 58.42 o -25 1 2 58.69 59.65 55.96 o -23 1 2 1095.17 1230.62 71.03 o -21 1 2 12.74 98.28 51.73 o -19 1 2 5342.30 5373.77 192.56 o -17 1 2 3476.97 3087.04 126.36 o -15 1 2 342.73 79.23 24.42 o -13 1 2 748.80 608.19 62.48 o -11 1 2 5379.89 6121.94 163.89 o -9 1 2 27638.03 29801.06 354.99 o -7 1 2 3.45 48.54 31.39 o -5 1 2 215275.72 197363.59 3033.15 o -3 1 2 2402.24 1341.01 51.57 o -1 1 2 294305.53 316998.31 4429.43 o 1 1 2 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