#------------------------------------------------------------------------------ #$Date: 2016-04-06 16:34:18 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181868 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/98/2019874.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2019874 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.1930 _cell_length_b 23.9240 _cell_length_c 7.2840 _exptl_crystal_F_000 983.47 _reflns_d_resolution_high 0.7108 _cod_data_source_file yf3078Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' aouatef_mgtetra R = New: P21212' _shelx_refln_list_code 4 _shelx_f_calc_maximum 348.97 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'x+1/2, -y+1/2, -z' '-x+1/2, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2106.98 2257.12 18.39 o 4 0 0 4649.31 4836.73 33.34 o 6 0 0 15022.34 15632.41 217.29 o 8 0 0 3566.77 3560.08 48.90 o 10 0 0 801.74 841.73 27.84 o 12 0 0 34.01 37.19 22.68 o 14 0 0 220.63 222.28 38.01 o 2 1 0 703.73 801.69 15.12 o 3 1 0 22179.18 21833.34 67.67 o 4 1 0 308.23 302.06 15.60 o 5 1 0 9742.72 10002.59 124.35 o 6 1 0 64.38 70.81 4.66 o 7 1 0 586.88 617.26 12.53 o 8 1 0 93.80 83.26 7.80 o 9 1 0 370.34 371.85 12.95 o 10 1 0 875.29 850.16 19.83 o 11 1 0 959.89 970.59 40.12 o 12 1 0 35.75 38.84 20.58 o 13 1 0 55.98 66.72 18.85 o 14 1 0 104.09 114.84 22.68 o 2 2 0 1059.47 1061.67 18.99 o 3 2 0 5304.60 5178.09 21.20 o 4 2 0 4586.82 4593.19 27.24 o 5 2 0 371.21 307.21 7.76 o 6 2 0 0.19 1.97 4.71 o 7 2 0 398.81 400.28 10.34 o 8 2 0 0.00 8.86 5.67 o 9 2 0 1183.88 1150.03 23.52 o 10 2 0 180.70 210.28 11.13 o 11 2 0 138.68 164.80 20.85 o 12 2 0 28.22 38.79 16.73 o 13 2 0 86.59 92.82 20.00 o 14 2 0 86.43 148.16 55.33 o 1 3 0 205.07 190.36 5.49 o 2 3 0 2399.30 2511.27 18.67 o 3 3 0 4754.83 4585.28 26.04 o 4 3 0 3215.23 3613.76 35.38 o 5 3 0 848.39 847.23 12.39 o 6 3 0 0.19 5.25 4.10 o 7 3 0 2390.36 2269.62 23.80 o 8 3 0 12.29 -1.40 7.79 o 9 3 0 506.11 455.41 15.64 o 10 3 0 758.50 714.45 21.40 o 11 3 0 272.95 271.92 27.57 o 12 3 0 465.31 439.73 31.27 o 13 3 0 98.97 118.51 21.39 o 14 3 0 25.90 22.67 27.18 o 0 4 0 1979.77 1820.58 24.89 o 1 4 0 1874.03 2158.11 14.40 o 2 4 0 392.23 373.47 6.82 o 3 4 0 7880.92 7657.42 28.12 o 4 4 0 249.13 271.77 6.49 o 5 4 0 11678.56 11992.36 42.27 o 6 4 0 15.12 17.90 3.96 o 7 4 0 941.18 967.84 19.34 o 8 4 0 469.69 470.85 22.23 o 9 4 0 3023.64 2964.40 37.52 o 10 4 0 772.02 727.63 20.32 o 11 4 0 654.58 676.43 48.17 o 12 4 0 0.05 1.81 15.74 o 13 4 0 175.42 206.04 28.54 o 14 4 0 6.10 8.53 21.19 o 1 5 0 675.06 691.44 9.90 o 2 5 0 4859.81 4883.30 23.61 o 3 5 0 8348.61 8466.17 31.10 o 4 5 0 51.58 61.05 4.11 o 5 5 0 220.48 287.67 9.81 o 6 5 0 943.98 935.88 19.54 o 7 5 0 2705.85 2646.88 31.76 o 8 5 0 1359.18 1332.15 34.44 o 9 5 0 25.47 19.81 11.51 o 10 5 0 817.16 792.09 28.96 o 11 5 0 9.45 15.26 19.70 o 12 5 0 268.26 248.99 25.05 o 13 5 0 0.71 6.60 15.96 o 14 5 0 331.23 398.51 33.30 o 0 6 0 3372.08 3627.69 43.09 o 1 6 0 4374.57 4553.85 21.81 o 2 6 0 17227.63 17287.00 46.56 o 3 6 0 325.01 307.12 8.74 o 4 6 0 23233.91 22687.62 177.44 o 5 6 0 666.86 652.39 10.91 o 6 6 0 2115.66 2174.14 20.57 o 7 6 0 168.50 157.60 9.50 o 8 6 0 1089.36 1037.18 22.05 o 9 6 0 100.47 115.19 10.76 o 10 6 0 1864.28 1805.42 43.13 o 11 6 0 171.47 176.99 28.78 o 12 6 0 205.22 223.08 33.55 o 13 6 0 7.76 52.41 46.60 o 14 6 0 157.48 158.68 25.32 o 1 7 0 15015.28 15655.27 140.35 o 2 7 0 547.90 608.93 8.93 o 3 7 0 6067.57 6870.72 58.48 o 4 7 0 1.28 3.45 3.36 o 5 7 0 116.83 139.26 7.06 o 6 7 0 116.57 115.51 6.51 o 7 7 0 2264.28 2230.46 30.44 o 8 7 0 2103.17 1994.70 43.49 o 9 7 0 1146.36 1164.25 24.87 o 10 7 0 714.27 709.96 28.50 o 11 7 0 13.09 23.18 20.14 o 12 7 0 42.21 33.38 22.48 o 13 7 0 416.32 345.44 30.62 o 14 7 0 14.64 59.45 20.04 o 0 8 0 25855.39 25249.45 129.73 o 1 8 0 2160.37 2198.76 40.25 o 2 8 0 352.82 342.12 7.31 o 3 8 0 277.06 328.69 8.42 o 4 8 0 2945.01 2914.62 22.43 o 5 8 0 1197.95 1331.99 20.68 o 6 8 0 66.99 49.69 6.59 o 7 8 0 410.53 434.31 14.75 o 8 8 0 645.98 649.35 18.46 o 9 8 0 230.41 217.78 18.87 o 10 8 0 1.42 18.42 10.55 o 11 8 0 0.01 34.51 21.39 o 12 8 0 75.61 85.61 26.49 o 13 8 0 179.52 163.94 34.32 o 1 9 0 254.36 312.85 7.47 o 2 9 0 1885.34 2185.45 17.78 o 3 9 0 11039.33 11341.54 46.67 o 4 9 0 2538.90 2585.26 21.93 o 5 9 0 2057.32 2027.26 32.78 o 6 9 0 337.14 408.34 12.79 o 7 9 0 82.85 65.17 10.69 o 8 9 0 140.35 175.66 12.03 o 9 9 0 54.10 78.22 9.01 o 10 9 0 436.88 417.16 27.92 o 11 9 0 302.48 241.23 32.71 o 12 9 0 127.75 103.38 28.12 o 13 9 0 37.96 98.54 29.85 o 0 10 0 3273.84 3227.82 38.28 o 1 10 0 10178.09 10829.40 41.62 o 2 10 0 166.06 172.22 6.70 o 3 10 0 183.06 302.13 8.72 o 4 10 0 0.11 3.53 4.07 o 5 10 0 1076.14 1146.85 16.16 o 6 10 0 1167.35 1110.49 16.68 o 7 10 0 121.07 133.92 15.07 o 8 10 0 70.62 91.49 9.22 o 9 10 0 1301.49 1278.14 27.56 o 10 10 0 62.21 43.88 16.66 o 11 10 0 4.27 39.03 22.08 o 12 10 0 12.86 -2.43 21.22 o 13 10 0 286.28 252.47 37.47 o 1 11 0 1028.29 883.73 24.49 o 2 11 0 3058.42 3061.40 24.73 o 3 11 0 772.37 878.90 16.29 o 4 11 0 1560.79 1634.25 25.90 o 5 11 0 66.62 82.35 5.96 o 6 11 0 1198.34 1185.15 17.69 o 7 11 0 89.97 106.55 9.64 o 8 11 0 1943.69 1845.71 32.15 o 9 11 0 64.66 52.19 8.70 o 10 11 0 29.89 54.46 13.57 o 11 11 0 88.40 83.42 24.94 o 12 11 0 121.39 181.28 32.26 o 13 11 0 31.04 74.67 27.70 o 0 12 0 11091.49 10979.92 79.78 o 1 12 0 2218.59 2350.58 29.23 o 2 12 0 12850.56 13279.17 94.61 o 3 12 0 3023.48 3223.86 31.35 o 4 12 0 259.34 271.27 9.50 o 5 12 0 6867.55 6970.53 58.09 o 6 12 0 141.95 153.16 10.37 o 7 12 0 2.66 3.29 6.76 o 8 12 0 2991.58 2867.21 40.76 o 9 12 0 1026.83 1029.64 26.34 o 10 12 0 219.51 255.78 32.16 o 11 12 0 495.13 506.77 43.59 o 12 12 0 19.63 24.93 23.54 o 13 12 0 10.64 3.05 23.26 o 1 13 0 2476.46 2398.24 22.42 o 2 13 0 4009.61 4122.32 40.77 o 3 13 0 856.41 868.68 17.24 o 4 13 0 399.62 403.17 11.53 o 5 13 0 5310.86 5524.17 37.76 o 6 13 0 4396.24 4224.59 51.73 o 7 13 0 2153.54 2111.08 30.63 o 8 13 0 115.34 124.14 10.83 o 9 13 0 19.10 30.65 13.28 o 10 13 0 658.41 718.01 48.37 o 11 13 0 785.16 739.46 51.89 o 12 13 0 0.09 10.82 21.27 o 13 13 0 597.95 589.91 52.41 o 0 14 0 48.12 36.77 8.55 o 1 14 0 128.03 123.12 13.65 o 2 14 0 860.62 922.48 21.38 o 3 14 0 0.82 13.12 7.50 o 4 14 0 2933.42 2857.36 33.10 o 5 14 0 58.60 51.42 5.96 o 6 14 0 41.04 59.02 7.38 o 7 14 0 1192.26 1154.00 22.68 o 8 14 0 179.48 182.94 12.77 o 9 14 0 1006.84 956.91 52.11 o 10 14 0 59.43 115.21 26.36 o 11 14 0 0.71 13.48 21.13 o 12 14 0 38.79 62.19 26.64 o 13 14 0 281.99 294.39 40.08 o 1 15 0 1791.21 1720.62 19.02 o 2 15 0 613.58 609.00 19.82 o 3 15 0 193.83 190.83 8.80 o 4 15 0 1272.36 1295.70 23.20 o 5 15 0 0.10 19.96 5.92 o 6 15 0 1273.98 1261.23 28.28 o 7 15 0 618.87 596.99 17.16 o 8 15 0 147.50 162.88 15.12 o 9 15 0 536.42 523.60 40.69 o 10 15 0 2.32 25.47 20.21 o 11 15 0 180.16 214.62 32.88 o 12 15 0 1.46 21.39 22.77 o 0 16 0 1220.11 1296.91 31.85 o 1 16 0 3359.50 3547.02 32.56 o 2 16 0 1592.48 1604.84 20.96 o 3 16 0 75.72 88.35 7.18 o 4 16 0 70.05 58.94 7.56 o 5 16 0 1154.18 1102.44 20.91 o 6 16 0 604.03 578.49 19.22 o 7 16 0 669.62 605.21 39.94 o 8 16 0 798.87 710.09 27.99 o 9 16 0 98.59 131.11 25.40 o 10 16 0 781.11 760.49 50.71 o 11 16 0 0.59 50.51 23.19 o 12 16 0 61.43 63.54 26.46 o 1 17 0 155.02 167.28 7.45 o 2 17 0 41.70 28.16 5.18 o 3 17 0 490.61 444.40 12.72 o 4 17 0 23.94 29.65 6.98 o 5 17 0 0.93 25.94 7.64 o 6 17 0 23.89 17.91 9.31 o 7 17 0 0.33 20.68 17.67 o 8 17 0 97.39 120.09 25.10 o 9 17 0 12.15 36.12 19.27 o 10 17 0 76.68 106.89 26.42 o 11 17 0 216.01 298.12 37.54 o 12 17 0 91.98 159.28 31.44 o 0 18 0 2635.07 2630.40 30.59 o 1 18 0 206.96 218.60 8.44 o 2 18 0 253.37 256.84 9.17 o 3 18 0 360.64 294.11 11.04 o 4 18 0 422.13 414.11 22.13 o 5 18 0 165.46 161.21 24.52 o 6 18 0 900.90 874.76 27.46 o 7 18 0 271.34 232.25 28.89 o 8 18 0 578.78 537.82 40.95 o 9 18 0 395.50 391.51 37.65 o 10 18 0 58.29 88.01 26.13 o 11 18 0 37.57 51.89 25.10 o 12 18 0 9.09 23.89 24.36 o 1 19 0 2436.21 2304.74 26.30 o 2 19 0 370.83 380.17 17.13 o 3 19 0 502.49 556.28 21.56 o 4 19 0 433.58 439.32 22.23 o 5 19 0 6735.43 6074.45 112.87 o 6 19 0 793.72 766.94 44.97 o 7 19 0 40.46 64.03 21.60 o 8 19 0 8.74 31.04 20.05 o 9 19 0 445.53 451.45 40.62 o 10 19 0 18.22 -0.75 20.07 o 11 19 0 104.62 84.77 27.00 o 0 20 0 283.06 299.79 27.49 o 1 20 0 168.01 208.45 17.31 o 2 20 0 152.53 147.09 12.83 o 3 20 0 144.76 149.17 12.96 o 4 20 0 1099.79 1059.38 33.61 o 5 20 0 1137.26 1118.12 51.62 o 6 20 0 81.45 91.21 22.63 o 7 20 0 152.82 212.69 29.64 o 8 20 0 132.27 173.77 28.95 o 9 20 0 486.22 519.26 44.15 o 10 20 0 283.49 276.91 36.38 o 11 20 0 44.08 19.93 23.65 o 1 21 0 208.45 188.51 16.79 o 2 21 0 2281.08 2166.54 47.57 o 3 21 0 86.00 107.19 15.48 o 4 21 0 125.96 107.37 21.43 o 5 21 0 3739.98 3602.96 91.79 o 6 21 0 45.75 22.43 19.60 o 7 21 0 36.88 48.65 20.56 o 8 21 0 9.37 51.92 23.43 o 9 21 0 145.73 120.96 28.09 o 10 21 0 24.44 27.09 23.51 o 11 21 0 546.07 616.75 51.40 o 0 22 0 236.38 256.92 26.82 o 1 22 0 5.85 15.21 11.65 o 2 22 0 720.82 694.11 29.11 o 3 22 0 102.11 121.12 31.52 o 4 22 0 361.61 376.75 32.97 o 5 22 0 64.31 131.87 24.10 o 6 22 0 880.74 794.73 47.93 o 7 22 0 2.37 17.00 20.33 o 8 22 0 33.16 43.33 22.78 o 9 22 0 5.78 46.88 23.67 o 10 22 0 149.59 134.07 31.20 o 1 23 0 714.89 719.63 41.76 o 2 23 0 184.76 189.51 55.98 o 3 23 0 48.16 61.43 19.40 o 4 23 0 161.83 180.00 26.31 o 5 23 0 7.11 24.22 19.21 o 6 23 0 47.94 65.46 22.70 o 7 23 0 99.69 70.99 23.50 o 8 23 0 3.80 32.37 22.04 o 9 23 0 171.19 160.17 31.62 o 10 23 0 72.49 84.66 28.93 o 0 24 0 117.09 151.89 23.71 o 1 24 0 13.56 45.97 24.83 o 2 24 0 1257.40 1241.42 39.69 o 3 24 0 1.28 16.33 12.91 o 4 24 0 175.15 164.06 26.24 o 5 24 0 15.73 34.98 20.17 o 6 24 0 0.61 10.15 18.28 o 7 24 0 7.77 18.37 20.67 o 8 24 0 3.26 6.81 21.30 o 9 24 0 0.59 -15.25 21.21 o 10 24 0 644.10 748.93 56.47 o 1 25 0 791.85 770.10 32.30 o 2 25 0 607.80 611.74 29.71 o 3 25 0 100.66 95.83 26.02 o 4 25 0 21.35 54.13 21.88 o 5 25 0 189.59 243.05 31.87 o 6 25 0 2.23 1.70 17.95 o 7 25 0 839.33 752.04 51.08 o 8 25 0 25.87 65.98 25.16 o 9 25 0 329.72 387.81 42.23 o 0 26 0 218.37 246.16 28.96 o 1 26 0 190.93 164.04 18.64 o 2 26 0 20.72 16.12 16.17 o 3 26 0 146.25 160.09 19.94 o 4 26 0 248.64 282.99 33.44 o 5 26 0 90.30 81.47 24.42 o 6 26 0 200.90 193.55 30.62 o 7 26 0 72.68 119.77 27.09 o 8 26 0 121.38 103.57 26.99 o 9 26 0 33.70 74.08 27.37 o 1 27 0 44.06 49.91 20.85 o 2 27 0 0.10 13.86 18.61 o 3 27 0 172.28 206.43 30.38 o 4 27 0 12.64 8.81 18.95 o 5 27 0 6.75 15.34 19.66 o 6 27 0 45.21 59.16 24.15 o 7 27 0 0.92 22.23 22.29 o 8 27 0 47.98 115.80 29.25 o 0 28 0 37.72 44.74 21.00 o 1 28 0 1.09 17.17 15.11 o 2 28 0 84.61 58.37 25.93 o 3 28 0 28.06 39.26 21.28 o 4 28 0 52.20 81.96 24.98 o 5 28 0 78.22 82.69 25.16 o 6 28 0 21.32 10.66 20.84 o 7 28 0 344.54 407.37 42.49 o 1 29 0 54.17 49.35 14.99 o 2 29 0 27.58 48.33 15.77 o 3 29 0 2.83 -9.26 19.67 o 4 29 0 129.24 175.33 30.34 o 5 29 0 124.23 137.67 29.01 o 6 29 0 33.63 38.52 22.33 o 7 29 0 9.40 -27.34 23.31 o 0 30 0 24.30 54.30 22.39 o 1 30 0 18.00 40.06 15.46 o 2 30 0 104.30 155.26 19.90 o 3 30 0 25.45 50.53 22.91 o 4 30 0 47.67 87.57 25.76 o 5 30 0 47.26 40.99 23.49 o 6 30 0 2.56 -2.21 21.74 o 1 31 0 180.12 224.54 23.23 o 2 31 0 14.49 48.23 16.59 o 3 31 0 225.26 212.02 32.69 o 4 31 0 17.64 14.59 21.76 o 5 31 0 152.91 233.47 35.58 o 0 32 0 369.97 378.17 40.30 o 1 32 0 191.24 222.45 23.99 o 2 32 0 105.25 154.03 35.05 o 3 32 0 17.05 38.29 22.99 o 4 32 0 0.06 6.88 21.53 o 1 33 0 261.01 345.59 48.48 o 2 33 0 9.51 27.35 16.37 o 1 0 1 138.44 138.19 3.53 o 2 0 1 956.31 990.55 11.48 o 3 0 1 45.32 28.39 4.35 o 4 0 1 310.20 253.84 5.92 o 5 0 1 777.72 891.85 11.75 o 6 0 1 333.69 355.83 8.63 o 7 0 1 70.02 73.81 6.70 o 8 0 1 78.15 88.10 7.62 o 9 0 1 104.70 107.22 9.19 o 10 0 1 3071.70 2972.88 46.72 o 11 0 1 2.90 30.25 14.98 o 12 0 1 124.41 138.50 20.60 o 13 0 1 73.50 82.54 20.27 o 14 0 1 140.53 178.76 25.27 o -14 1 1 126.85 109.33 22.56 o -13 1 1 77.54 76.83 19.17 o -12 1 1 14.73 45.59 19.40 o -11 1 1 73.25 68.52 26.75 o -10 1 1 93.48 92.22 11.52 o -9 1 1 169.69 174.31 9.24 o -8 1 1 270.45 268.87 10.14 o -7 1 1 1804.15 1836.25 21.10 o -6 1 1 1383.90 1472.59 20.40 o -5 1 1 1491.41 1574.93 27.13 o -4 1 1 569.38 586.10 12.98 o -3 1 1 157.13 133.83 8.39 o -2 1 1 724.74 773.20 11.78 o -1 1 1 5727.07 5917.53 41.66 o 0 1 1 25.11 29.72 2.18 o 1 1 1 5731.34 5931.31 23.84 o 2 1 1 723.78 781.21 8.90 o 3 1 1 155.87 151.69 6.33 o 4 1 1 571.66 601.34 9.18 o 5 1 1 1494.09 1650.60 17.73 o 6 1 1 1382.68 1496.96 25.73 o 7 1 1 1810.09 1839.64 37.33 o 8 1 1 268.93 277.00 11.55 o 9 1 1 173.00 163.13 13.02 o 10 1 1 93.95 76.95 10.85 o 11 1 1 72.90 85.85 18.01 o 12 1 1 14.87 30.83 31.58 o 13 1 1 78.13 79.96 19.67 o 14 1 1 127.24 160.62 24.93 o -14 2 1 631.36 670.91 40.63 o -13 2 1 0.03 24.52 16.64 o -12 2 1 225.77 199.27 24.76 o -11 2 1 66.18 69.86 21.22 o -10 2 1 879.78 848.79 26.20 o -9 2 1 127.92 131.79 8.26 o -8 2 1 753.66 786.34 23.74 o -7 2 1 1261.93 1294.24 17.46 o -6 2 1 675.11 650.76 11.55 o -5 2 1 2251.87 2272.52 48.01 o -4 2 1 1400.83 1514.79 20.25 o -3 2 1 86.07 81.30 5.94 o -2 2 1 3586.55 3723.56 31.22 o -1 2 1 2149.42 2180.65 11.21 o 0 2 1 5608.44 5597.80 20.75 o 1 2 1 2150.69 2191.18 13.99 o 2 2 1 3580.33 3675.86 18.38 o 3 2 1 85.89 71.97 5.14 o 4 2 1 1402.20 1535.54 14.81 o 5 2 1 2256.31 2357.50 19.98 o 6 2 1 669.83 631.98 16.41 o 7 2 1 1262.23 1280.58 17.56 o 8 2 1 756.68 778.58 18.37 o 9 2 1 129.44 137.60 10.21 o 10 2 1 878.77 833.02 42.39 o 11 2 1 66.85 86.87 17.89 o 12 2 1 225.67 177.67 22.31 o 13 2 1 0.03 18.94 17.09 o 14 2 1 630.72 667.33 40.54 o -14 3 1 209.57 214.52 26.57 o -13 3 1 5.20 28.81 16.84 o -12 3 1 18.78 30.97 15.84 o -11 3 1 542.17 507.80 30.37 o -10 3 1 1960.14 1905.35 38.34 o -9 3 1 946.06 939.90 29.33 o -8 3 1 1288.64 1182.10 20.52 o -7 3 1 1233.22 1189.46 16.68 o -6 3 1 3808.55 3882.49 29.04 o -5 3 1 1108.56 958.73 11.50 o -4 3 1 1194.92 1263.62 20.04 o -3 3 1 1001.39 943.70 12.79 o -2 3 1 37.49 35.31 3.91 o -1 3 1 3520.76 3509.11 17.77 o 0 3 1 16.66 22.19 2.17 o 1 3 1 3519.70 3475.73 14.30 o 2 3 1 34.92 34.41 3.66 o 3 3 1 1004.41 930.02 13.24 o 4 3 1 1197.37 1292.57 17.02 o 5 3 1 1103.25 971.35 14.62 o 6 3 1 3802.23 3938.61 28.64 o 7 3 1 1238.66 1193.48 22.13 o 8 3 1 1287.91 1191.56 21.05 o 9 3 1 941.77 980.92 22.17 o 10 3 1 1962.74 1945.11 44.42 o 11 3 1 544.50 536.07 44.56 o 12 3 1 17.81 2.88 14.73 o 13 3 1 5.90 11.42 16.59 o 14 3 1 208.84 294.08 42.96 o -14 4 1 32.57 116.39 28.78 o -13 4 1 29.97 0.82 22.99 o -12 4 1 101.61 109.49 19.87 o -11 4 1 167.39 154.96 22.54 o -10 4 1 391.94 358.73 21.37 o -9 4 1 133.97 119.33 16.07 o -8 4 1 740.44 737.91 16.52 o -7 4 1 105.94 108.81 6.89 o -6 4 1 936.68 971.58 19.09 o -5 4 1 3919.97 3855.50 67.80 o -4 4 1 1507.46 1546.14 18.98 o -3 4 1 517.03 491.43 14.86 o -2 4 1 1302.38 1297.00 11.95 o -1 4 1 146.51 151.75 5.50 o 0 4 1 221.32 206.58 4.56 o 1 4 1 149.32 162.51 4.80 o 2 4 1 1306.31 1281.04 10.10 o 3 4 1 512.21 480.14 11.38 o 4 4 1 1511.33 1595.69 19.17 o 5 4 1 3919.06 3949.69 45.78 o 6 4 1 936.71 981.06 18.05 o 7 4 1 105.69 115.91 6.92 o 8 4 1 745.38 760.77 17.17 o 9 4 1 129.63 126.35 9.90 o 10 4 1 391.63 341.20 20.19 o 11 4 1 167.41 138.96 28.72 o 12 4 1 102.32 108.83 28.14 o 13 4 1 31.29 58.86 18.94 o 14 4 1 33.10 31.34 42.05 o -14 5 1 59.05 88.61 20.38 o -13 5 1 21.90 13.79 16.42 o -12 5 1 44.07 44.38 31.47 o -11 5 1 203.70 183.52 21.21 o -10 5 1 343.70 378.00 21.84 o -9 5 1 151.99 140.82 8.85 o -8 5 1 83.70 79.50 6.99 o -7 5 1 253.47 272.75 8.83 o -6 5 1 283.25 338.72 8.94 o -5 5 1 1663.10 1680.84 18.43 o -4 5 1 273.14 290.54 7.29 o -3 5 1 675.54 660.70 16.48 o -2 5 1 172.69 165.70 5.34 o -1 5 1 229.53 251.21 5.75 o 0 5 1 524.02 543.41 8.33 o 1 5 1 230.01 258.06 5.61 o 2 5 1 175.72 170.32 4.79 o 3 5 1 668.26 628.76 8.84 o 4 5 1 272.16 277.42 6.17 o 5 5 1 1660.47 1725.72 22.01 o 6 5 1 282.32 329.06 9.57 o 7 5 1 253.77 246.13 10.22 o 8 5 1 85.16 89.40 8.63 o 9 5 1 152.20 153.82 10.69 o 10 5 1 341.78 331.75 20.81 o 11 5 1 200.84 228.66 32.61 o 12 5 1 45.14 74.04 25.98 o 13 5 1 21.36 41.42 18.08 o 14 5 1 58.27 60.74 20.65 o -14 6 1 785.04 809.72 43.89 o -13 6 1 162.30 222.99 25.68 o -12 6 1 416.68 423.32 30.21 o -11 6 1 187.00 171.96 28.02 o -10 6 1 362.34 337.08 21.28 o -9 6 1 1290.09 1234.24 22.60 o -8 6 1 198.99 180.03 11.19 o -7 6 1 196.40 197.95 7.94 o -6 6 1 2655.58 2693.79 24.36 o -5 6 1 393.46 379.09 9.20 o -4 6 1 2639.31 2856.70 31.70 o -3 6 1 67.05 82.85 7.15 o -2 6 1 398.42 377.55 8.69 o -1 6 1 134.54 128.88 6.24 o 0 6 1 6.66 7.24 3.66 o 1 6 1 135.76 142.31 5.96 o 2 6 1 391.71 373.53 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26.98 o -6 22 2 493.48 511.99 35.39 o -5 22 2 129.32 134.30 21.53 o -4 22 2 262.02 248.89 19.78 o -3 22 2 313.15 316.18 48.55 o -2 22 2 437.62 416.84 22.82 o -1 22 2 54.63 97.59 22.52 o 0 22 2 280.24 269.13 14.49 o 1 22 2 54.13 49.39 19.62 o 2 22 2 438.67 376.54 20.45 o 3 22 2 315.21 316.45 19.29 o 4 22 2 261.60 251.16 18.15 o 5 22 2 131.27 123.39 26.92 o 6 22 2 489.23 462.57 41.90 o 7 22 2 26.88 24.27 23.72 o 8 22 2 66.14 91.64 28.30 o 9 22 2 22.14 61.32 27.08 o 10 22 2 153.66 259.28 39.76 o -5 23 2 155.40 211.84 25.09 o -4 23 2 20.66 25.52 12.54 o -3 23 2 458.69 429.86 56.91 o -2 23 2 78.27 70.47 13.33 o -1 23 2 547.49 558.99 26.16 o 0 23 2 116.26 113.32 11.25 o 1 23 2 545.58 581.76 20.30 o 2 23 2 78.28 56.77 22.82 o 3 23 2 453.30 442.63 39.08 o 4 23 2 20.44 58.71 23.55 o 5 23 2 157.27 141.28 27.92 o 6 23 2 135.82 161.07 30.00 o 7 23 2 111.78 102.66 28.31 o 8 23 2 41.22 38.66 25.05 o 9 23 2 36.05 -9.33 23.62 o 10 23 2 51.77 29.60 27.23 o -4 24 2 48.25 42.31 13.46 o -3 24 2 87.26 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