data_2019894 _cell_angle_alpha 90.000 _cell_angle_beta 106.130 _cell_angle_gamma 90.000 _cell_length_a 14.7510 _cell_length_b 10.0144 _cell_length_c 16.4180 _exptl_crystal_F_000 1208.00 _reflns_d_resolution_high 0.7700 _cod_data_source_file ku3147Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' I in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 269.02 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 169.33 261.12 30.38 o 6 0 0 4.91 27.74 20.14 o 8 0 0 10540.00 9818.15 348.26 o 10 0 0 3444.17 3407.54 187.45 o 12 0 0 12566.72 13515.37 370.34 o 14 0 0 360.74 417.52 47.67 o 16 0 0 273.37 267.54 74.86 o 18 0 0 10.43 7.10 16.90 o 2 1 0 1593.21 1758.32 32.58 o 3 1 0 7022.98 6706.94 72.51 o 4 1 0 5255.62 5183.69 76.64 o 5 1 0 19913.98 19863.80 151.24 o 6 1 0 7730.48 7570.87 98.85 o 7 1 0 12179.07 12032.01 241.37 o 8 1 0 6654.32 6271.67 110.00 o 9 1 0 4292.52 4322.97 118.50 o 10 1 0 3549.38 3635.73 122.21 o 11 1 0 2.79 71.63 16.41 o 12 1 0 172.17 181.40 18.99 o 13 1 0 2156.64 2187.43 81.66 o 14 1 0 654.90 674.72 45.10 o 15 1 0 3757.94 3816.86 100.56 o 16 1 0 106.83 120.88 21.32 o 17 1 0 690.47 743.49 42.96 o 18 1 0 154.76 143.91 29.64 o 0 2 0 26.35 49.44 11.20 o 1 2 0 5.56 15.47 3.71 o 2 2 0 9651.70 9467.83 110.60 o 3 2 0 154.17 140.42 6.96 o 4 2 0 60181.95 61977.44 390.56 o 5 2 0 1712.99 1646.27 23.42 o 6 2 0 405.72 339.32 13.93 o 7 2 0 3779.92 3977.16 84.11 o 8 2 0 9842.32 9788.82 194.87 o 9 2 0 203.28 187.05 15.17 o 10 2 0 591.67 605.41 28.04 o 11 2 0 1092.61 1178.46 60.65 o 12 2 0 5694.74 5959.87 230.43 o 13 2 0 1047.75 1080.28 39.74 o 14 2 0 2443.95 2576.94 103.03 o 15 2 0 27.47 74.77 16.84 o 16 2 0 1877.90 1974.50 97.77 o 17 2 0 40.89 49.16 22.19 o 18 2 0 469.00 472.38 46.88 o 1 3 0 50993.41 52607.13 408.98 o 2 3 0 14598.04 14794.42 147.56 o 3 3 0 30.36 41.79 6.01 o 4 3 0 3686.47 3465.69 46.23 o 5 3 0 7434.15 7617.13 113.45 o 6 3 0 3608.44 3769.84 89.69 o 7 3 0 8224.13 8463.10 176.29 o 8 3 0 3281.16 3193.61 65.54 o 9 3 0 368.51 363.64 15.33 o 10 3 0 1407.66 1254.33 45.61 o 11 3 0 6479.78 6563.24 132.95 o 12 3 0 46.61 70.26 20.45 o 13 3 0 6411.14 6782.52 151.79 o 14 3 0 60.17 46.98 15.49 o 15 3 0 285.59 279.78 33.64 o 16 3 0 137.09 119.71 24.61 o 17 3 0 29.10 23.18 16.45 o 0 4 0 20798.76 20200.91 379.42 o 1 4 0 7282.58 8073.68 75.84 o 2 4 0 3630.00 3971.72 50.49 o 3 4 0 5010.96 5279.53 65.97 o 4 4 0 3533.90 3404.45 62.99 o 5 4 0 1048.82 868.08 24.49 o 6 4 0 268.21 314.61 14.71 o 7 4 0 4263.11 4142.81 78.73 o 8 4 0 12958.70 13017.08 215.17 o 9 4 0 5628.77 5716.30 130.20 o 10 4 0 712.45 731.61 41.96 o 11 4 0 1774.55 1644.83 85.60 o 12 4 0 2135.54 2267.26 63.41 o 13 4 0 215.63 188.11 32.14 o 14 4 0 36.90 73.36 16.61 o 15 4 0 0.63 37.75 17.94 o 16 4 0 293.82 275.85 48.28 o 17 4 0 198.25 124.61 49.09 o 1 5 0 158.96 169.46 8.46 o 2 5 0 458.10 437.31 28.68 o 3 5 0 14808.68 14606.76 196.44 o 4 5 0 1.71 33.46 10.78 o 5 5 0 14931.70 14235.76 174.07 o 6 5 0 821.26 823.30 28.93 o 7 5 0 3693.21 3451.18 69.26 o 8 5 0 0.06 32.42 11.84 o 9 5 0 1374.67 1401.37 43.38 o 10 5 0 0.11 45.34 11.20 o 11 5 0 656.52 584.79 47.59 o 12 5 0 53.28 101.88 15.00 o 13 5 0 121.71 100.59 19.40 o 14 5 0 24.75 49.76 15.84 o 15 5 0 3353.10 3562.40 166.13 o 16 5 0 0.12 34.67 30.73 o 0 6 0 11445.71 10651.26 322.92 o 1 6 0 5.75 28.65 7.07 o 2 6 0 1825.43 1973.72 54.49 o 3 6 0 3278.80 3270.37 78.82 o 4 6 0 4682.63 4590.67 103.84 o 5 6 0 4776.31 4618.43 69.35 o 6 6 0 45.19 44.96 6.99 o 7 6 0 4465.92 4469.59 178.43 o 8 6 0 1804.61 1743.86 67.78 o 9 6 0 2438.64 2422.83 65.27 o 10 6 0 34.08 50.62 17.48 o 11 6 0 623.33 632.00 61.95 o 12 6 0 2261.19 2258.25 82.21 o 13 6 0 83.68 57.67 21.84 o 14 6 0 2.46 13.39 52.62 o 15 6 0 4.87 49.93 37.55 o 16 6 0 283.21 312.96 49.57 o 1 7 0 15936.30 16747.39 277.40 o 2 7 0 733.64 695.52 42.56 o 3 7 0 6.96 34.59 8.35 o 4 7 0 1951.59 1891.00 62.39 o 5 7 0 1353.53 1262.41 56.37 o 6 7 0 500.59 455.34 27.76 o 7 7 0 4965.93 4850.96 104.20 o 8 7 0 2217.81 2162.60 58.88 o 9 7 0 730.59 776.74 45.51 o 10 7 0 181.30 192.32 22.19 o 11 7 0 855.01 835.64 61.06 o 12 7 0 205.55 301.62 40.06 o 13 7 0 2161.09 1958.26 124.97 o 14 7 0 145.06 91.27 28.70 o 15 7 0 187.89 140.60 35.60 o 0 8 0 2547.94 2241.69 117.42 o 1 8 0 2.30 47.74 13.06 o 2 8 0 3542.19 3594.75 77.85 o 3 8 0 6.10 41.45 10.89 o 4 8 0 2009.32 1873.78 70.88 o 5 8 0 979.34 1034.10 49.15 o 6 8 0 224.48 219.23 19.93 o 7 8 0 158.33 154.92 15.33 o 8 8 0 3667.08 3647.19 177.21 o 9 8 0 428.97 368.37 32.87 o 10 8 0 162.13 163.23 53.04 o 11 8 0 167.12 200.22 74.74 o 12 8 0 113.17 75.53 25.70 o 13 8 0 39.45 95.58 33.13 o 14 8 0 436.90 308.16 48.58 o 1 9 0 50.65 60.63 13.11 o 2 9 0 490.93 504.66 31.10 o 3 9 0 2656.10 2618.39 68.34 o 4 9 0 999.99 1012.86 50.93 o 5 9 0 2404.15 2350.08 67.24 o 6 9 0 1235.77 1122.81 43.36 o 7 9 0 1979.89 1975.88 76.37 o 8 9 0 683.91 581.06 85.23 o 9 9 0 314.98 318.93 40.38 o 10 9 0 765.63 706.81 59.86 o 11 9 0 13.35 120.70 34.84 o 12 9 0 235.55 243.16 108.41 o 13 9 0 222.07 183.05 123.71 o 0 10 0 8227.06 8415.91 415.21 o 1 10 0 212.25 261.83 22.53 o 2 10 0 495.80 537.23 38.21 o 3 10 0 334.57 333.82 27.97 o 4 10 0 29.28 43.34 12.31 o 5 10 0 15.01 32.12 11.82 o 6 10 0 41.47 37.70 13.07 o 7 10 0 89.53 113.14 57.70 o 8 10 0 628.48 566.91 65.53 o 9 10 0 2.78 27.72 26.37 o 10 10 0 304.19 298.03 34.98 o 11 10 0 7.69 32.22 25.41 o 1 11 0 7.79 22.68 9.67 o 2 11 0 36.43 56.99 12.91 o 3 11 0 572.06 549.81 38.50 o 4 11 0 452.30 491.75 122.52 o 5 11 0 958.35 965.77 94.97 o 6 11 0 399.26 472.19 68.96 o 7 11 0 577.71 582.20 55.98 o 8 11 0 390.45 462.94 61.79 o 9 11 0 53.32 64.45 27.04 o 0 12 0 294.63 262.21 40.72 o 1 12 0 47.53 43.74 10.75 o 2 12 0 1530.25 1496.76 134.48 o 3 12 0 119.32 102.75 27.52 o 4 12 0 1228.86 1147.41 88.79 o 5 12 0 6.21 62.77 18.84 o 6 12 0 14.67 61.89 44.19 o 7 12 0 93.37 71.37 24.55 o -17 0 1 14.64 56.68 17.80 o -15 0 1 26.83 69.74 32.65 o -13 0 1 11972.90 11950.49 537.97 o -11 0 1 2431.54 2578.56 182.49 o -9 0 1 496.13 439.68 27.90 o -7 0 1 10688.31 10921.68 144.13 o -5 0 1 12652.47 13200.19 116.88 o -3 0 1 37721.52 38585.79 582.03 o 3 0 1 123.85 153.37 10.45 o 5 0 1 244.37 183.71 12.54 o 7 0 1 20726.67 20870.51 1028.70 o 9 0 1 757.76 712.92 89.87 o 11 0 1 12623.29 13120.42 542.21 o 13 0 1 7171.46 7488.88 252.66 o 15 0 1 297.35 302.32 46.58 o 17 0 1 35.95 42.32 20.83 o -18 1 1 361.36 321.77 41.81 o -17 1 1 5.13 80.54 19.05 o -16 1 1 1852.53 1936.21 72.93 o -15 1 1 431.02 435.85 59.88 o -14 1 1 143.66 207.40 24.14 o -13 1 1 7.79 32.77 13.34 o -12 1 1 1284.80 1347.92 57.19 o -11 1 1 3182.58 3209.37 77.71 o -10 1 1 740.58 714.88 29.76 o -9 1 1 10222.85 10399.31 299.43 o -8 1 1 17127.17 16725.32 324.29 o -7 1 1 6216.15 5871.68 101.88 o -6 1 1 2134.46 1819.91 34.48 o -5 1 1 2415.46 2345.01 28.78 o -4 1 1 45578.60 46730.80 405.02 o -3 1 1 5843.34 6061.54 65.50 o -2 1 1 839.51 902.97 20.95 o 2 1 1 16857.55 17166.33 138.33 o 3 1 1 36.72 66.19 8.58 o 4 1 1 10002.24 9413.91 94.95 o 5 1 1 7212.63 6931.05 76.59 o 6 1 1 2314.49 2331.49 40.22 o 7 1 1 6301.76 5951.01 89.98 o 8 1 1 16033.79 16126.61 301.91 o 9 1 1 2148.59 2032.11 84.29 o 10 1 1 308.22 284.03 19.67 o 11 1 1 49.60 64.45 22.92 o 12 1 1 2744.32 2880.87 77.58 o 13 1 1 3.82 70.61 16.06 o 14 1 1 1616.19 1652.41 66.76 o 15 1 1 159.27 120.49 25.22 o 16 1 1 1130.62 1169.90 54.80 o 17 1 1 537.27 586.74 45.05 o 18 1 1 9.78 23.28 13.98 o -18 2 1 34.25 61.77 56.51 o -17 2 1 2941.46 2908.33 112.32 o -16 2 1 96.06 129.32 23.07 o -15 2 1 3705.01 3890.79 101.33 o -14 2 1 134.81 143.37 15.69 o -13 2 1 1102.92 1149.45 38.62 o -12 2 1 26.45 86.90 17.55 o -11 2 1 1040.84 1090.54 71.08 o -10 2 1 2196.82 2138.98 70.51 o -9 2 1 2779.31 2694.64 72.90 o -8 2 1 2169.76 2178.87 79.30 o -7 2 1 367.75 307.57 13.29 o -6 2 1 1701.74 1674.33 31.67 o -5 2 1 35711.21 35083.68 449.58 o -4 2 1 3223.67 3451.93 45.30 o -3 2 1 16101.03 15950.77 95.83 o -2 2 1 35090.91 36830.53 304.74 o -1 2 1 3005.59 3163.43 35.36 o 0 2 1 3587.55 3588.98 46.53 o 1 2 1 114.10 137.17 6.59 o 2 2 1 759.93 686.48 16.83 o 3 2 1 4001.68 3960.36 52.25 o 4 2 1 955.51 900.07 22.36 o 5 2 1 12561.39 12414.88 113.79 o 6 2 1 4153.71 4068.68 66.61 o 7 2 1 15578.29 15363.12 158.00 o 8 2 1 36.55 61.50 8.13 o 9 2 1 1666.92 1774.63 86.22 o 10 2 1 2597.71 2493.43 71.90 o 11 2 1 330.51 365.78 30.71 o 12 2 1 117.03 146.06 17.83 o 13 2 1 11.71 52.98 26.10 o 14 2 1 75.95 91.73 22.68 o 15 2 1 5361.01 6131.81 129.09 o 16 2 1 231.85 194.16 39.34 o 17 2 1 363.62 353.10 31.19 o -18 3 1 8.76 7.81 19.61 o -17 3 1 0.20 97.57 35.16 o -16 3 1 13.57 36.78 11.49 o -15 3 1 12.40 48.02 14.52 o -14 3 1 373.07 377.11 30.26 o -13 3 1 930.20 942.95 38.68 o -12 3 1 14958.45 14784.27 585.87 o -11 3 1 315.54 321.23 26.94 o -10 3 1 774.43 743.44 28.15 o -9 3 1 1401.34 1309.63 43.68 o -8 3 1 8745.68 8864.02 200.38 o -7 3 1 3495.04 3811.30 72.21 o -6 3 1 1097.03 1154.67 26.08 o -5 3 1 3421.11 3454.41 44.75 o -4 3 1 1850.38 1759.47 30.59 o -3 3 1 12533.82 13081.29 137.81 o -2 3 1 3163.70 3176.60 36.61 o -1 3 1 558.83 697.14 12.24 o 0 3 1 67545.94 68885.50 601.37 o 1 3 1 20.77 35.56 8.32 o 2 3 1 77.65 70.76 4.48 o 3 3 1 433.63 385.95 15.15 o 4 3 1 2155.38 2044.45 30.12 o 5 3 1 1909.91 1720.90 26.18 o 6 3 1 351.49 321.07 22.67 o 7 3 1 2649.81 2672.87 70.78 o 8 3 1 2161.64 2116.88 60.94 o 9 3 1 600.64 603.55 25.38 o 10 3 1 8022.45 7753.71 200.39 o 11 3 1 90.33 102.27 18.77 o 12 3 1 10292.08 10881.73 252.66 o 13 3 1 113.88 137.13 21.89 o 14 3 1 61.46 72.04 20.68 o 15 3 1 274.32 338.91 45.13 o 16 3 1 0.48 49.84 18.65 o 17 3 1 139.43 106.02 23.32 o -17 4 1 16.28 55.58 23.53 o -16 4 1 1.11 9.77 19.92 o -15 4 1 956.81 896.09 61.54 o -14 4 1 119.97 109.28 17.96 o -13 4 1 5333.78 5222.83 215.11 o -12 4 1 1129.88 1043.97 34.43 o -11 4 1 1603.18 1610.62 47.07 o -10 4 1 1471.43 1366.28 46.68 o -9 4 1 2623.03 2585.96 66.74 o -8 4 1 6483.10 6489.81 110.78 o -7 4 1 4269.48 4261.68 80.52 o -6 4 1 6089.77 6110.92 73.87 o -5 4 1 13479.05 13101.99 163.47 o -3 4 1 6305.27 6587.07 84.92 o -2 4 1 144.18 118.03 7.19 o -1 4 1 5053.24 4803.37 59.91 o 0 4 1 882.26 843.29 19.95 o 1 4 1 3865.94 3802.37 48.57 o 2 4 1 2223.92 2196.89 30.19 o 3 4 1 12682.39 13119.73 152.90 o 4 4 1 6698.54 6715.72 71.73 o 5 4 1 3493.88 3307.37 66.36 o 6 4 1 4980.44 4925.03 100.50 o 7 4 1 9362.06 9094.91 117.80 o 8 4 1 6029.04 5968.42 134.66 o 9 4 1 237.01 240.00 15.00 o 10 4 1 73.40 76.04 10.98 o 11 4 1 1828.81 1951.60 56.25 o 12 4 1 2.20 40.07 13.93 o 13 4 1 2141.60 2084.38 73.66 o 14 4 1 500.21 402.10 37.68 o 15 4 1 890.60 897.95 58.45 o 16 4 1 89.59 57.98 27.76 o 17 4 1 14.28 71.39 27.03 o -17 5 1 4.69 36.26 22.11 o -16 5 1 2438.22 2440.08 124.17 o -15 5 1 139.58 96.09 28.91 o -14 5 1 608.21 695.73 63.44 o -13 5 1 22.79 44.28 21.06 o -12 5 1 387.50 391.45 26.52 o -11 5 1 22.72 74.15 19.38 o -10 5 1 1259.83 1202.86 58.78 o -9 5 1 3.72 15.76 5.95 o -8 5 1 3390.52 3449.41 67.37 o -7 5 1 280.94 290.09 13.94 o -6 5 1 8815.58 8566.68 111.52 o -5 5 1 442.62 543.55 19.45 o -4 5 1 17247.76 16441.74 308.98 o -3 5 1 100.52 157.21 14.83 o -2 5 1 9203.13 9209.03 164.87 o -1 5 1 217.63 324.95 12.52 o 0 5 1 7894.12 7998.76 97.45 o 1 5 1 1521.34 1592.52 29.97 o 2 5 1 10688.89 10342.28 122.57 o 3 5 1 1368.16 1442.64 31.58 o 4 5 1 9045.92 8978.01 97.47 o 5 5 1 82.75 66.80 8.41 o 6 5 1 9.09 15.50 5.83 o 7 5 1 229.47 215.53 17.07 o 8 5 1 5944.05 5954.64 213.22 o 9 5 1 695.22 644.46 41.52 o 10 5 1 285.51 371.85 36.35 o 11 5 1 35.54 51.86 15.02 o 12 5 1 380.21 380.88 36.09 o 13 5 1 28.13 45.32 16.74 o 14 5 1 2461.28 2342.56 105.49 o 15 5 1 25.21 71.08 34.92 o 16 5 1 1489.83 1368.30 107.58 o -16 6 1 1.65 60.14 44.43 o -15 6 1 462.33 377.03 43.84 o -14 6 1 78.63 61.88 23.82 o -13 6 1 2680.04 2838.32 114.53 o -12 6 1 260.47 223.64 25.25 o -11 6 1 828.22 711.22 55.15 o -10 6 1 1654.94 1548.46 43.26 o -9 6 1 2300.40 2122.84 50.66 o -8 6 1 3716.51 3570.56 70.14 o -7 6 1 6990.25 6807.79 153.33 o -6 6 1 2475.28 2419.60 98.84 o -5 6 1 4236.53 4015.78 92.99 o -4 6 1 1027.52 1029.30 28.14 o -3 6 1 231.48 228.33 13.21 o -2 6 1 249.52 218.62 24.63 o -1 6 1 13681.19 14138.74 179.54 o 0 6 1 6.19 30.77 7.13 o 1 6 1 4815.91 4839.11 91.67 o 2 6 1 1917.21 1725.96 55.33 o 3 6 1 3681.64 3659.83 71.81 o 4 6 1 3730.17 3572.10 70.40 o 5 6 1 1588.80 1509.02 40.34 o 6 6 1 5159.77 5035.00 154.06 o 7 6 1 7983.73 7870.89 204.32 o 8 6 1 2729.04 2797.28 61.74 o 9 6 1 763.94 792.44 78.01 o 10 6 1 263.59 324.05 31.12 o 11 6 1 2180.78 2191.65 110.76 o 12 6 1 28.76 27.38 24.16 o 13 6 1 1262.89 1312.10 54.35 o 14 6 1 46.33 88.90 31.37 o 15 6 1 905.07 921.59 62.54 o 16 6 1 308.63 186.80 59.91 o -15 7 1 0.22 18.49 19.53 o -14 7 1 522.65 530.27 67.72 o -13 7 1 74.95 106.73 31.43 o -12 7 1 3268.69 3411.34 135.91 o -11 7 1 142.16 244.37 39.30 o -10 7 1 101.15 110.25 19.56 o -9 7 1 1705.22 1621.62 75.09 o -8 7 1 4972.66 4823.44 133.10 o -7 7 1 339.09 301.41 27.12 o -6 7 1 53.32 39.49 5.66 o -5 7 1 2045.08 1914.86 82.61 o -4 7 1 3.01 21.45 5.94 o -3 7 1 5.36 18.79 6.20 o -2 7 1 3908.46 3964.86 108.03 o -1 7 1 22.82 52.32 17.07 o 0 7 1 20479.77 20994.29 326.77 o 1 7 1 1617.45 1561.87 48.08 o 2 7 1 337.43 341.35 23.33 o 3 7 1 1225.29 1139.82 36.37 o 4 7 1 1501.47 1481.99 50.39 o 5 7 1 1398.80 1407.23 47.98 o 6 7 1 1291.02 1090.97 51.47 o 7 7 1 853.78 803.46 43.40 o 8 7 1 2603.90 2544.99 65.74 o 9 7 1 635.69 582.10 44.67 o 10 7 1 946.93 803.64 59.10 o 11 7 1 15.17 54.99 16.32 o 12 7 1 3472.59 3434.86 126.50 o 13 7 1 51.94 36.49 22.54 o 14 7 1 19.34 35.69 46.70 o 15 7 1 1.88 54.05 28.04 o -14 8 1 18.41 30.88 21.05 o -13 8 1 131.03 124.26 34.93 o -12 8 1 556.71 638.02 60.23 o -11 8 1 39.00 63.58 25.34 o -10 8 1 582.04 496.04 112.89 o -9 8 1 795.90 727.69 53.96 o -8 8 1 837.66 846.04 75.78 o -7 8 1 455.39 459.98 30.09 o -6 8 1 321.23 243.52 45.28 o -5 8 1 8590.63 8410.61 173.65 o -4 8 1 183.38 152.34 21.19 o -3 8 1 4318.81 4423.35 92.11 o -2 8 1 12.89 53.01 17.17 o -1 8 1 954.38 990.10 55.72 o 0 8 1 382.08 400.29 25.99 o 1 8 1 105.78 100.91 15.33 o 2 8 1 273.44 301.62 25.98 o 3 8 1 2899.50 3080.21 67.84 o 4 8 1 436.28 447.19 27.78 o 5 8 1 3325.34 3364.48 75.98 o 6 8 1 15.42 23.99 8.43 o 7 8 1 4320.56 4366.26 242.09 o 8 8 1 364.61 373.93 39.10 o 9 8 1 337.01 396.19 33.35 o 10 8 1 222.39 194.56 54.74 o 11 8 1 25.47 42.27 26.61 o 12 8 1 5.05 44.87 64.40 o 13 8 1 63.78 72.95 49.33 o 14 8 1 4.29 51.50 21.96 o -13 9 1 254.10 328.68 54.28 o -12 9 1 486.57 499.32 102.67 o -11 9 1 487.56 496.58 63.83 o -10 9 1 25.63 74.35 27.53 o -9 9 1 630.05 631.30 55.79 o -8 9 1 2784.56 2634.94 117.73 o -7 9 1 1190.71 1100.17 44.73 o -6 9 1 1061.94 1088.30 66.70 o -5 9 1 1129.82 1116.25 41.44 o -4 9 1 2468.61 2395.93 63.53 o -3 9 1 66.59 88.16 13.75 o -2 9 1 43.75 73.37 14.04 o -1 9 1 1.92 28.76 14.40 o 0 9 1 1916.29 1949.24 54.98 o 1 9 1 518.62 490.91 30.88 o 2 9 1 1449.22 1381.68 45.50 o 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