#------------------------------------------------------------------------------ #$Date: 2016-04-06 16:35:31 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181869 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/99/2019924.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2019924 _cell_angle_alpha 90.000 _cell_angle_beta 95.978 _cell_angle_gamma 90.000 _cell_length_a 21.3690 _cell_length_b 20.4890 _cell_length_c 6.7444 _exptl_crystal_F_000 1216.00 _reflns_d_resolution_high 0.7696 _cod_data_source_file qs3046Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' jo3cgr' _shelx_refln_list_code 4 _shelx_f_calc_maximum 350.91 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 3463.77 3246.28 62.24 o 8 0 0 17013.53 17093.56 316.59 o 10 0 0 2107.13 2138.16 49.24 o 12 0 0 467.84 501.68 32.45 o 14 0 0 687.98 682.27 33.06 o 16 0 0 1432.75 1427.71 70.49 o 18 0 0 7793.04 7687.70 216.86 o 20 0 0 453.67 481.18 61.29 o 22 0 0 527.65 484.01 45.97 o 24 0 0 242.86 239.78 55.36 o 26 0 0 386.38 459.00 183.73 o 5 1 0 285.59 308.59 29.46 o 7 1 0 348.77 400.55 17.09 o 9 1 0 128.32 92.95 18.42 o 11 1 0 1058.76 1046.74 24.90 o 13 1 0 652.30 659.67 26.71 o 15 1 0 2403.68 2434.24 49.79 o 17 1 0 1.37 14.64 24.61 o 19 1 0 938.28 987.77 33.09 o 21 1 0 390.38 359.92 42.32 o 23 1 0 1.22 -2.15 39.63 o 25 1 0 90.66 101.21 49.18 o 27 1 0 366.27 548.81 100.86 o 4 2 0 7058.08 6231.11 109.83 o 6 2 0 3408.15 3098.45 61.00 o 8 2 0 766.13 738.80 21.79 o 10 2 0 7283.06 7427.99 111.79 o 12 2 0 2279.36 2343.62 39.41 o 14 2 0 23.88 16.58 22.75 o 16 2 0 63.44 97.59 25.06 o 18 2 0 1720.02 1774.19 42.35 o 20 2 0 802.02 762.97 28.89 o 22 2 0 191.43 195.79 30.80 o 24 2 0 159.45 114.24 43.75 o 26 2 0 6.60 19.68 65.94 o 3 3 0 12.47 14.47 9.88 o 5 3 0 331.50 389.71 20.55 o 7 3 0 1033.79 1159.88 25.16 o 9 3 0 2989.29 2847.28 46.45 o 11 3 0 0.35 -5.58 20.70 o 13 3 0 764.73 861.47 24.34 o 15 3 0 1604.84 1611.60 52.04 o 17 3 0 2422.53 2334.47 47.95 o 19 3 0 286.64 325.17 38.14 o 21 3 0 1324.19 1330.50 61.90 o 23 3 0 32.13 39.52 26.07 o 25 3 0 2.33 36.31 82.95 o 27 3 0 0.01 42.03 80.53 o 0 4 0 38012.61 25654.59 705.21 o 2 4 0 780.57 746.93 16.80 o 4 4 0 9961.83 9404.99 174.37 o 6 4 0 20.27 27.01 13.72 o 8 4 0 40.48 -2.15 35.17 o 10 4 0 617.21 664.01 22.99 o 12 4 0 41.13 41.22 31.14 o 14 4 0 3524.54 3496.95 63.49 o 16 4 0 84.67 88.81 24.79 o 18 4 0 20.53 70.66 37.46 o 20 4 0 818.29 796.81 29.52 o 22 4 0 382.69 399.06 47.70 o 24 4 0 0.05 -24.37 77.64 o 26 4 0 106.99 16.76 69.16 o 1 5 0 4349.90 4070.49 57.83 o 3 5 0 108.35 155.02 22.51 o 5 5 0 994.97 930.04 40.04 o 7 5 0 1059.84 1045.18 24.10 o 9 5 0 722.00 753.05 23.16 o 11 5 0 1862.80 1794.69 41.72 o 13 5 0 158.96 160.33 38.55 o 15 5 0 146.70 138.95 35.17 o 17 5 0 985.60 929.27 38.70 o 19 5 0 744.44 681.44 35.95 o 21 5 0 329.08 352.81 52.37 o 23 5 0 117.58 153.81 59.48 o 25 5 0 170.29 -8.33 111.44 o 27 5 0 428.72 546.01 75.58 o 0 6 0 23217.33 22768.22 520.27 o 2 6 0 3638.74 3240.61 48.88 o 4 6 0 4219.93 4225.38 57.94 o 6 6 0 2226.73 2242.72 37.39 o 8 6 0 1590.92 1639.32 33.58 o 10 6 0 520.23 597.71 20.90 o 12 6 0 1486.58 1625.89 39.30 o 14 6 0 98.53 69.68 34.36 o 16 6 0 537.04 577.12 36.47 o 18 6 0 67.45 30.49 30.44 o 20 6 0 1443.52 1423.73 44.42 o 22 6 0 92.75 142.12 49.78 o 24 6 0 138.92 117.62 45.94 o 26 6 0 59.81 48.84 95.33 o 1 7 0 43.44 57.05 15.45 o 3 7 0 3739.14 3968.35 57.54 o 5 7 0 113.24 94.87 12.42 o 7 7 0 68.44 50.65 19.20 o 9 7 0 2817.06 3097.03 62.59 o 11 7 0 84.97 87.33 25.11 o 13 7 0 2827.05 2899.74 65.54 o 15 7 0 65.83 68.63 28.94 o 17 7 0 75.01 84.12 46.55 o 19 7 0 9.13 10.04 46.59 o 21 7 0 165.50 190.61 85.87 o 23 7 0 37.32 31.57 47.25 o 25 7 0 429.46 490.95 66.67 o 0 8 0 3329.72 3125.03 72.03 o 2 8 0 2222.35 2322.98 46.01 o 4 8 0 835.54 775.50 23.82 o 6 8 0 714.74 731.01 19.56 o 8 8 0 263.31 276.25 20.23 o 10 8 0 975.92 1084.17 29.78 o 12 8 0 1906.51 2101.47 54.50 o 14 8 0 619.64 654.10 31.85 o 16 8 0 1.84 45.67 75.36 o 18 8 0 23.38 43.08 28.76 o 20 8 0 174.78 135.25 32.03 o 22 8 0 968.23 953.81 52.29 o 24 8 0 10.81 -9.58 100.10 o 26 8 0 198.08 141.60 58.97 o 1 9 0 2166.34 2163.69 39.63 o 3 9 0 621.91 735.71 27.16 o 5 9 0 4063.61 4326.75 67.15 o 7 9 0 1955.08 1982.54 34.86 o 9 9 0 206.27 293.65 28.37 o 11 9 0 8.08 -13.41 37.34 o 13 9 0 6365.71 6051.14 114.05 o 15 9 0 193.40 256.95 29.76 o 17 9 0 768.31 741.59 37.18 o 19 9 0 116.93 69.52 70.28 o 21 9 0 749.29 841.68 59.07 o 23 9 0 197.32 147.66 71.92 o 25 9 0 82.46 163.58 62.02 o 0 10 0 7113.09 8035.49 160.67 o 2 10 0 0.98 39.24 19.51 o 4 10 0 5.96 4.36 24.05 o 6 10 0 157.98 168.71 18.66 o 8 10 0 2365.49 2262.58 44.68 o 10 10 0 1565.57 1620.17 44.09 o 12 10 0 336.51 378.41 28.63 o 14 10 0 213.12 293.21 35.23 o 16 10 0 222.14 151.79 31.02 o 18 10 0 413.19 329.08 35.11 o 20 10 0 314.11 396.15 41.74 o 22 10 0 268.13 289.36 62.37 o 24 10 0 5.24 -56.12 113.90 o 1 11 0 843.81 1023.94 39.54 o 3 11 0 2629.14 2975.93 49.78 o 5 11 0 324.35 315.86 22.69 o 7 11 0 1653.07 1753.43 41.75 o 9 11 0 884.51 856.89 29.92 o 11 11 0 18.03 26.82 26.89 o 13 11 0 44.03 -8.42 48.79 o 15 11 0 759.49 728.33 54.15 o 17 11 0 208.65 193.69 29.14 o 19 11 0 9.79 59.41 40.56 o 21 11 0 44.96 179.60 59.97 o 23 11 0 160.22 164.95 62.37 o 25 11 0 7.02 -23.30 214.83 o 0 12 0 246.08 269.88 42.24 o 2 12 0 354.59 319.79 32.73 o 4 12 0 468.08 536.45 23.33 o 6 12 0 1827.53 1736.39 46.38 o 8 12 0 1067.65 1145.69 33.03 o 10 12 0 920.41 990.41 41.07 o 12 12 0 1922.68 1930.23 44.00 o 14 12 0 33.17 24.72 27.95 o 16 12 0 0.05 -6.93 50.77 o 18 12 0 8.22 7.29 42.04 o 20 12 0 298.66 329.69 50.87 o 22 12 0 4.00 24.65 182.32 o 24 12 0 34.34 -10.20 87.52 o 1 13 0 63.75 59.16 19.93 o 3 13 0 11.53 45.15 26.94 o 5 13 0 14.74 22.10 24.69 o 7 13 0 1551.61 1692.19 46.44 o 9 13 0 1008.23 1118.39 30.68 o 11 13 0 5133.25 5307.30 87.46 o 13 13 0 483.56 469.25 52.27 o 15 13 0 822.84 803.76 39.54 o 17 13 0 50.54 106.04 34.99 o 19 13 0 96.77 156.83 53.47 o 21 13 0 64.93 201.74 64.47 o 23 13 0 2.83 -52.32 111.61 o 0 14 0 251.02 276.29 35.20 o 2 14 0 159.34 201.87 22.46 o 4 14 0 42.17 -2.34 18.92 o 6 14 0 30.32 22.37 31.09 o 8 14 0 5669.98 5678.74 84.40 o 10 14 0 5225.61 5157.38 83.32 o 12 14 0 9.59 -17.47 43.21 o 14 14 0 3589.61 3407.86 66.44 o 16 14 0 495.33 456.14 57.65 o 18 14 0 128.65 126.37 55.35 o 20 14 0 133.24 91.24 87.66 o 22 14 0 715.12 809.37 173.40 o 1 15 0 839.19 911.40 31.16 o 3 15 0 1474.57 1533.67 46.99 o 5 15 0 1694.27 1707.79 43.71 o 7 15 0 3190.03 3081.69 56.75 o 9 15 0 0.79 -20.78 30.25 o 11 15 0 1403.40 1353.37 38.57 o 13 15 0 6.68 26.86 42.67 o 15 15 0 0.85 -50.78 50.78 o 17 15 0 149.74 190.89 29.89 o 19 15 0 87.66 73.93 69.26 o 21 15 0 145.47 133.51 78.70 o 0 16 0 1319.16 1362.45 52.86 o 2 16 0 59.84 64.71 25.15 o 4 16 0 1245.69 1387.70 38.65 o 6 16 0 1655.01 1744.94 41.87 o 8 16 0 7773.67 7727.26 118.35 o 10 16 0 5701.93 5755.63 102.23 o 12 16 0 576.87 465.92 37.13 o 14 16 0 126.76 146.33 34.74 o 16 16 0 252.63 325.75 99.77 o 18 16 0 146.68 178.52 51.69 o 20 16 0 551.71 703.02 84.22 o 22 16 0 12.30 -65.63 105.41 o 1 17 0 223.81 278.16 29.86 o 3 17 0 761.86 788.91 29.89 o 5 17 0 186.26 190.87 23.25 o 7 17 0 26.95 18.07 21.54 o 9 17 0 2720.33 2586.34 61.30 o 11 17 0 4.28 73.12 46.14 o 13 17 0 114.15 16.04 36.82 o 15 17 0 44.85 18.80 33.73 o 17 17 0 104.74 133.66 77.51 o 19 17 0 0.08 -21.20 219.82 o 21 17 0 0.94 -33.95 151.63 o 0 18 0 4137.45 4107.07 110.64 o 2 18 0 302.27 268.54 31.52 o 4 18 0 355.17 315.93 31.42 o 6 18 0 560.77 520.01 46.39 o 8 18 0 636.85 595.44 44.62 o 10 18 0 337.51 287.87 45.31 o 12 18 0 515.02 452.53 98.56 o 14 18 0 0.00 33.97 67.30 o 16 18 0 16.60 -18.88 44.94 o 18 18 0 5.55 89.06 58.40 o 20 18 0 94.40 126.87 86.35 o 1 19 0 322.93 258.86 27.09 o 3 19 0 110.85 127.72 21.35 o 5 19 0 120.17 122.49 33.77 o 7 19 0 669.78 615.10 31.88 o 9 19 0 178.93 164.37 25.75 o 11 19 0 45.97 0.15 22.76 o 13 19 0 0.30 -50.16 66.41 o 15 19 0 248.82 192.03 44.42 o 17 19 0 14.34 65.46 63.02 o 19 19 0 6.62 36.67 62.39 o 0 20 0 1356.53 1303.77 72.47 o 2 20 0 83.86 148.49 31.52 o 4 20 0 3.11 19.38 24.05 o 6 20 0 500.49 456.65 37.61 o 8 20 0 609.07 587.32 66.29 o 10 20 0 355.67 373.59 30.59 o 12 20 0 0.15 28.53 39.02 o 14 20 0 56.40 63.51 54.35 o 16 20 0 99.49 177.31 102.26 o 18 20 0 10.49 -112.00 137.27 o 1 21 0 8.40 25.68 27.64 o 3 21 0 27.02 51.15 34.29 o 5 21 0 875.04 814.43 61.72 o 7 21 0 203.18 239.15 46.52 o 9 21 0 14.70 -21.55 45.81 o 11 21 0 293.19 308.10 51.41 o 13 21 0 4.51 40.65 45.04 o 15 21 0 188.32 172.82 127.46 o 0 22 0 64.59 22.90 41.65 o 2 22 0 4.26 53.25 42.84 o 4 22 0 11.20 104.14 39.11 o 6 22 0 4.59 -38.22 42.59 o 8 22 0 61.69 31.37 34.92 o 10 22 0 0.68 -55.68 88.91 o 12 22 0 116.24 87.01 63.80 o 14 22 0 148.70 74.44 152.41 o 1 23 0 63.98 44.11 33.20 o 3 23 0 12.31 14.64 48.97 o 5 23 0 7.18 -9.97 34.47 o 7 23 0 241.73 390.30 72.32 o 9 23 0 217.44 268.47 67.55 o 11 23 0 107.13 43.61 91.60 o 13 23 0 240.42 327.14 79.71 o 0 24 0 1.72 70.35 118.54 o 2 24 0 5.45 -30.76 80.97 o 4 24 0 215.08 219.96 48.22 o 6 24 0 0.47 25.01 39.48 o 8 24 0 817.15 801.70 82.32 o 10 24 0 10.85 0.80 71.30 o 1 25 0 48.04 119.94 49.08 o 3 25 0 122.24 175.12 61.59 o 5 25 0 99.78 69.44 49.82 o 7 25 0 390.89 534.17 110.38 o 9 25 0 7.12 -22.52 69.60 o 0 26 0 0.05 78.98 60.14 o 2 26 0 4.21 36.49 62.22 o 4 26 0 279.11 251.97 64.34 o -27 1 1 80.76 47.93 60.41 o -25 1 1 25.65 35.62 44.36 o -23 1 1 4.47 -8.03 34.19 o -21 1 1 102.66 86.17 27.16 o -19 1 1 548.18 598.00 33.08 o -17 1 1 516.11 608.38 28.09 o -15 1 1 11.08 -15.22 28.83 o -13 1 1 324.17 383.51 19.66 o -11 1 1 65.34 79.19 17.71 o -9 1 1 3274.35 3047.76 46.55 o -7 1 1 2882.14 2848.68 43.82 o -5 1 1 5482.17 5347.80 74.72 o -3 1 1 2142.58 2120.92 45.49 o 3 1 1 4765.40 4429.66 63.16 o 5 1 1 1120.43 1175.80 23.77 o 7 1 1 10130.10 9404.95 119.27 o 9 1 1 1800.05 1720.89 30.62 o 11 1 1 893.18 967.04 22.74 o 13 1 1 554.48 622.74 22.06 o 15 1 1 357.21 367.18 35.13 o 17 1 1 470.97 576.87 26.76 o 19 1 1 1369.49 1311.82 42.92 o 21 1 1 8.01 20.31 21.69 o 23 1 1 179.50 168.54 29.12 o 25 1 1 74.93 48.80 72.93 o 27 1 1 67.41 147.58 74.84 o -26 2 1 62.20 37.56 57.81 o -24 2 1 356.97 413.27 42.76 o -22 2 1 234.61 246.25 36.37 o -20 2 1 2583.68 2704.10 53.91 o -18 2 1 9.02 -13.07 41.06 o -16 2 1 1.35 6.39 20.16 o -14 2 1 118.61 118.77 21.93 o -12 2 1 9.06 -4.48 19.29 o -10 2 1 283.52 241.40 16.37 o -8 2 1 2831.55 2525.04 48.21 o -6 2 1 1144.81 1082.80 24.88 o -4 2 1 1230.96 1327.59 26.15 o -2 2 1 37523.91 29880.35 1078.61 o 2 2 1 2454.80 2379.29 40.08 o 4 2 1 2.67 39.10 14.61 o 6 2 1 62.19 109.58 12.99 o 8 2 1 1359.86 1084.82 21.44 o 10 2 1 2663.96 2579.64 52.63 o 12 2 1 1031.74 934.19 22.72 o 14 2 1 445.30 401.21 22.17 o 16 2 1 511.57 489.69 28.77 o 18 2 1 3318.58 3157.94 58.90 o 20 2 1 149.60 122.00 23.20 o 22 2 1 739.13 725.99 32.75 o 24 2 1 11.44 43.30 40.72 o 26 2 1 70.20 114.32 83.99 o -27 3 1 140.34 162.39 100.21 o -25 3 1 100.72 55.16 45.71 o -23 3 1 46.02 42.12 50.74 o -21 3 1 308.70 241.11 37.88 o -19 3 1 2870.39 2876.62 55.83 o -17 3 1 944.57 891.16 26.98 o -15 3 1 2214.15 2095.53 38.36 o -13 3 1 179.09 153.21 19.36 o -11 3 1 834.99 888.64 22.75 o -9 3 1 142.83 176.31 17.00 o -7 3 1 18248.48 17575.53 237.19 o -5 3 1 2137.68 2225.45 36.47 o -3 3 1 22175.69 20200.14 445.88 o -1 3 1 3966.23 3633.88 51.39 o 1 3 1 36361.39 30567.85 644.36 o 3 3 1 3.81 18.61 20.54 o 5 3 1 27603.96 25238.18 394.83 o 7 3 1 1136.47 938.33 23.58 o 9 3 1 2180.66 2261.28 35.57 o 11 3 1 1323.90 1258.20 24.44 o 13 3 1 319.11 267.84 20.77 o 15 3 1 531.56 520.39 21.34 o 17 3 1 4261.52 4121.28 74.54 o 19 3 1 2055.03 1870.86 43.32 o 21 3 1 280.23 258.40 24.83 o 23 3 1 71.46 115.91 55.10 o 25 3 1 20.68 40.16 45.61 o -26 4 1 390.10 473.23 106.48 o -24 4 1 0.24 -22.44 58.17 o -22 4 1 2136.15 2152.02 56.13 o -20 4 1 3951.14 3864.20 62.44 o -18 4 1 213.89 264.40 26.19 o -16 4 1 2.08 21.50 34.32 o -14 4 1 0.02 -20.55 37.08 o -12 4 1 733.31 686.34 22.13 o -10 4 1 4664.93 5058.72 70.88 o -8 4 1 2304.18 2309.11 35.86 o -6 4 1 1850.85 1718.40 32.91 o -4 4 1 18797.96 17669.15 273.18 o -2 4 1 9554.98 8893.26 134.89 o 0 4 1 6446.13 6011.32 100.86 o 2 4 1 2930.78 2734.22 50.35 o 4 4 1 3.76 20.16 18.14 o 6 4 1 61.45 46.15 22.02 o 8 4 1 17722.48 18829.03 239.57 o 10 4 1 1092.72 1296.69 26.99 o 12 4 1 1519.17 1646.28 38.28 o 14 4 1 591.70 588.02 27.37 o 16 4 1 304.44 313.50 30.04 o 18 4 1 2915.33 2831.63 57.37 o 20 4 1 1966.56 1932.31 51.25 o 22 4 1 21.76 52.73 62.84 o 24 4 1 173.86 266.74 41.27 o 26 4 1 81.78 95.76 62.51 o -27 5 1 15.83 10.45 92.87 o -25 5 1 172.08 185.38 100.22 o -23 5 1 90.14 136.77 42.03 o -21 5 1 24.76 71.01 35.20 o -19 5 1 176.35 141.65 37.92 o -17 5 1 3029.95 3142.76 60.37 o -15 5 1 488.28 487.98 24.61 o -13 5 1 5484.39 5678.28 93.31 o -11 5 1 5307.02 5460.95 74.43 o -9 5 1 142.57 72.04 26.17 o -7 5 1 218.38 242.80 16.55 o -5 5 1 4398.07 4553.18 67.84 o -3 5 1 2536.70 2230.40 44.73 o -1 5 1 6276.86 5929.65 90.86 o 1 5 1 1207.91 1058.50 25.19 o 3 5 1 532.19 497.40 18.54 o 5 5 1 8.18 2.95 14.03 o 7 5 1 715.61 815.94 24.25 o 9 5 1 171.04 153.34 18.48 o 11 5 1 1482.84 1505.92 33.59 o 13 5 1 1095.78 1129.81 30.58 o 15 5 1 269.85 303.94 29.00 o 17 5 1 1269.34 1229.95 69.95 o 19 5 1 298.81 280.64 29.72 o 21 5 1 229.47 252.57 35.29 o 23 5 1 204.31 239.48 45.82 o 25 5 1 0.97 17.40 83.84 o -26 6 1 4.80 46.90 106.97 o -24 6 1 568.06 625.35 49.32 o -22 6 1 26.88 16.55 33.64 o -20 6 1 2830.23 2767.07 62.45 o -18 6 1 1366.51 1320.51 58.95 o -16 6 1 165.59 170.44 22.48 o -14 6 1 441.70 429.26 28.89 o -12 6 1 2016.45 1887.68 36.92 o -10 6 1 8378.18 8938.98 118.14 o -8 6 1 2996.17 2929.16 48.85 o -6 6 1 34.77 -5.70 17.84 o -4 6 1 1605.19 1617.76 42.90 o -2 6 1 1119.25 1244.71 26.80 o 0 6 1 3850.57 4122.35 60.86 o 2 6 1 1865.45 1854.67 32.40 o 4 6 1 36.69 37.72 17.06 o 6 6 1 8734.46 8382.89 118.38 o 8 6 1 15879.64 17019.63 234.29 o 10 6 1 2276.18 2264.03 44.15 o 12 6 1 475.55 499.45 25.71 o 14 6 1 45.84 64.44 24.71 o 16 6 1 24.87 11.41 25.12 o 18 6 1 2724.60 2435.79 88.51 o 20 6 1 465.14 488.22 80.96 o 22 6 1 104.26 42.23 43.25 o 24 6 1 104.89 99.23 46.55 o 26 6 1 250.10 332.02 72.68 o -25 7 1 166.82 314.86 83.09 o -23 7 1 217.90 256.66 43.95 o -21 7 1 46.85 58.70 38.71 o -19 7 1 711.44 716.86 35.50 o -17 7 1 2607.72 2551.69 55.21 o -15 7 1 2906.07 2772.22 61.15 o -13 7 1 245.62 233.39 15.49 o -11 7 1 3264.08 3208.53 58.55 o -9 7 1 2853.03 2917.03 46.82 o -7 7 1 3678.11 3831.80 66.19 o -5 7 1 318.70 370.87 18.29 o -3 7 1 931.62 921.49 23.81 o -1 7 1 787.37 774.93 21.80 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