#------------------------------------------------------------------------------ #$Date: 2016-04-06 16:35:31 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181869 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/99/2019931.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2019931 _cell_angle_alpha 90.000 _cell_angle_beta 110.369 _cell_angle_gamma 90.000 _cell_length_a 6.4000 _cell_length_b 3.6140 _cell_length_c 14.4530 _exptl_crystal_F_000 272.00 _reflns_d_resolution_high 0.7435 _cod_data_source_file yp3086_295sup3.hkl _cod_data_source_block yzq295 #BEGIN Tags that were not found in dictionaries: _shelx_title ' yzq1 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 143.41 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1882.55 1857.85 40.37 o 2 0 0 1087.72 1158.06 25.62 o 3 0 0 689.83 679.45 15.26 o 4 0 0 10148.73 11442.96 336.48 o 5 0 0 291.46 293.98 13.03 o 6 0 0 275.63 260.66 12.32 o 7 0 0 507.92 502.21 21.76 o 1 1 0 7486.16 9310.13 180.09 o 2 1 0 1800.77 2354.68 44.21 o 3 1 0 413.95 402.83 7.27 o 4 1 0 41.80 41.09 1.07 o 5 1 0 1898.33 1940.32 51.27 o 6 1 0 17.90 21.56 1.65 o 7 1 0 58.60 61.97 3.36 o 0 2 0 20565.76 26135.17 1003.33 o 1 2 0 608.11 668.54 18.34 o 2 2 0 302.92 319.51 7.73 o 3 2 0 382.52 378.99 7.81 o 4 2 0 4922.05 5208.56 97.69 o 5 2 0 150.53 153.51 4.61 o 6 2 0 157.43 160.04 6.28 o 7 2 0 309.54 316.75 10.97 o 1 3 0 1239.18 1318.03 35.88 o 2 3 0 149.70 191.90 6.25 o 3 3 0 147.05 150.47 5.14 o 4 3 0 34.02 37.53 2.25 o 5 3 0 665.63 689.50 21.55 o 6 3 0 8.92 20.72 2.42 o 0 4 0 2349.67 2607.54 99.53 o 1 4 0 124.16 125.97 4.89 o 2 4 0 23.45 20.61 1.47 o 3 4 0 109.88 103.73 4.28 o 4 4 0 997.34 998.70 40.12 o -7 1 1 0.51 2.91 0.57 o -6 1 1 13.65 16.01 1.38 o -5 1 1 2.26 3.24 0.39 o -4 1 1 0.12 0.42 0.09 o -3 1 1 7.35 8.35 0.37 o -2 1 1 167.40 157.04 3.35 o -1 1 1 0.46 -0.52 0.52 o 0 1 1 5.81 2.07 0.22 o 1 1 1 1.96 2.40 0.26 o 2 1 1 111.58 108.37 2.67 o 3 1 1 2.42 2.93 0.24 o 4 1 1 0.31 0.30 0.12 o 5 1 1 0.03 1.58 0.60 o 6 1 1 15.55 14.57 1.28 o 7 1 1 0.02 0.86 0.37 o -7 2 1 6.85 9.03 1.28 o -6 2 1 3.16 3.86 0.46 o -5 2 1 30.34 29.89 1.45 o -4 2 1 56.19 66.35 1.75 o -3 2 1 13.05 10.37 0.73 o -2 2 1 1.26 1.04 0.37 o -1 2 1 111.49 94.30 3.24 o 0 2 1 205.17 247.96 7.31 o 1 2 1 7.70 6.15 0.48 o 2 2 1 2.34 1.60 0.25 o 3 2 1 28.32 23.57 0.89 o 4 2 1 55.92 58.73 1.89 o 5 2 1 1.67 3.26 0.48 o 6 2 1 2.14 2.30 0.54 o 7 2 1 8.43 7.25 1.55 o -6 3 1 44.58 54.95 3.80 o -5 3 1 5.50 7.43 0.86 o -4 3 1 0.06 0.35 0.52 o -3 3 1 11.34 10.11 0.85 o -2 3 1 267.66 310.84 9.45 o -1 3 1 0.25 1.59 0.54 o 0 3 1 11.25 14.90 1.90 o 1 3 1 4.95 4.62 1.38 o 2 3 1 210.26 230.55 7.29 o 3 3 1 5.36 6.84 1.12 o 4 3 1 2.01 3.60 0.54 o 5 3 1 0.09 0.69 0.43 o 6 3 1 51.96 66.88 4.84 o -4 4 1 37.54 32.83 2.76 o -3 4 1 7.29 12.09 1.38 o -2 4 1 0.25 2.17 0.69 o -1 4 1 51.81 86.71 3.79 o 0 4 1 99.33 83.54 3.61 o 1 4 1 2.90 6.69 1.12 o 2 4 1 0.93 6.22 0.98 o 3 4 1 22.32 30.40 2.59 o 4 4 1 47.42 38.30 2.31 o -7 0 2 217.68 205.18 10.57 o -6 0 2 877.28 905.30 35.63 o -5 0 2 45.76 46.63 2.26 o -4 0 2 2480.22 2609.80 68.73 o -3 0 2 298.57 299.24 8.82 o -2 0 2 8620.13 9015.68 396.29 o -1 0 2 3184.36 3200.20 224.88 o 1 0 2 1217.09 1025.07 40.75 o 2 0 2 1980.06 1914.85 41.79 o 3 0 2 828.53 844.02 25.22 o 4 0 2 916.40 919.04 25.49 o 5 0 2 430.25 417.81 17.59 o 6 0 2 809.20 815.70 32.74 o 7 0 2 10.15 13.82 2.59 o -7 1 2 2033.47 2129.74 56.97 o -6 1 2 91.08 84.46 5.45 o -5 1 2 63.51 56.43 1.87 o -4 1 2 553.87 534.57 8.74 o -3 1 2 8514.96 9226.80 174.67 o -2 1 2 28.53 18.56 0.73 o -1 1 2 2582.96 2929.73 63.92 o 0 1 2 5369.78 6761.57 153.60 o 1 1 2 2741.04 2888.81 54.38 o 2 1 2 1318.89 1543.81 26.36 o 3 1 2 1914.99 1982.13 33.76 o 4 1 2 2253.91 2301.21 39.13 o 5 1 2 820.76 855.85 23.87 o 6 1 2 691.49 680.60 19.82 o 7 1 2 1058.73 1015.55 28.78 o -7 2 2 122.99 117.34 5.19 o -6 2 2 540.09 572.40 13.87 o -5 2 2 58.87 62.06 2.00 o -4 2 2 1129.29 1186.94 22.67 o -3 2 2 162.47 161.55 5.21 o -2 2 2 3433.09 3658.84 96.78 o -1 2 2 873.23 955.57 25.93 o 0 2 2 858.67 955.34 21.46 o 1 2 2 400.37 418.50 9.80 o 2 2 2 1314.80 1444.00 27.48 o 3 2 2 377.08 384.04 7.16 o 4 2 2 373.16 367.40 8.11 o 5 2 2 227.57 227.64 7.96 o 6 2 2 484.67 464.05 14.63 o 7 2 2 10.47 9.50 2.25 o -6 3 2 61.47 56.17 3.98 o -5 3 2 17.40 19.17 1.90 o -4 3 2 177.33 187.93 13.25 o -3 3 2 1844.39 1864.05 71.09 o -2 3 2 3.28 9.89 0.95 o -1 3 2 422.18 433.96 12.69 o 0 3 2 767.29 830.14 23.14 o 1 3 2 798.82 867.95 24.07 o 2 3 2 236.53 251.28 7.79 o 3 3 2 639.10 674.29 19.79 o 4 3 2 622.12 655.01 15.96 o -4 4 2 198.01 174.94 6.37 o -3 4 2 47.13 49.25 2.57 o -2 4 2 584.55 566.57 16.82 o -1 4 2 156.52 165.83 6.06 o 0 4 2 147.93 171.00 6.18 o 1 4 2 62.77 62.42 2.99 o 2 4 2 348.46 345.43 10.86 o 3 4 2 94.54 89.75 5.36 o 4 4 2 62.65 62.74 4.67 o -7 1 3 2.02 3.78 0.79 o -6 1 3 1.59 2.11 0.34 o -5 1 3 4.45 3.71 0.77 o -4 1 3 5.93 5.09 0.47 o -3 1 3 2.52 5.03 0.39 o -2 1 3 14.66 8.48 0.56 o -1 1 3 16.07 10.24 0.50 o 0 1 3 0.49 -0.45 0.45 o 1 1 3 2.19 0.76 0.20 o 2 1 3 0.84 0.37 0.10 o 3 1 3 0.11 0.89 0.27 o 4 1 3 0.48 0.83 0.20 o 5 1 3 0.01 0.24 0.52 o 6 1 3 0.96 1.04 0.37 o 7 1 3 0.13 0.69 0.69 o -7 2 3 1.18 3.01 0.66 o -6 2 3 0.08 0.73 0.27 o -5 2 3 28.03 24.70 1.09 o -4 2 3 11.17 12.26 0.98 o -3 2 3 0.22 0.89 0.16 o -2 2 3 5.05 2.30 0.54 o -1 2 3 18.52 16.59 0.98 o 0 2 3 0.83 1.32 0.64 o 1 2 3 8.44 4.63 0.41 o 2 2 3 5.68 4.57 0.51 o 3 2 3 4.57 5.07 0.57 o 4 2 3 0.18 0.63 0.19 o 5 2 3 21.04 18.49 1.49 o 6 2 3 5.60 5.31 1.21 o -6 3 3 5.93 8.81 1.04 o -5 3 3 14.39 14.86 1.10 o -4 3 3 18.98 23.52 1.52 o -3 3 3 6.47 5.70 0.85 o -2 3 3 22.97 25.79 1.52 o -1 3 3 12.67 18.22 1.22 o 0 3 3 9.70 11.92 0.98 o 1 3 3 2.52 2.20 0.41 o 2 3 3 4.07 5.94 0.63 o 3 3 3 0.43 0.97 0.31 o 4 3 3 1.73 5.61 0.70 o -4 4 3 7.69 10.56 1.47 o -3 4 3 0.18 4.79 0.95 o -2 4 3 0.32 7.60 1.08 o -1 4 3 11.24 15.81 1.22 o 0 4 3 0.79 0.55 0.29 o 1 4 3 10.10 18.01 1.28 o 2 4 3 1.95 7.94 1.04 o 3 4 3 1.37 2.38 0.41 o -8 0 4 671.14 653.71 27.73 o -7 0 4 1230.94 1289.19 50.22 o -6 0 4 1043.50 1111.85 30.69 o -5 0 4 88.98 84.95 3.49 o -4 0 4 6424.65 7229.08 272.69 o -3 0 4 11290.61 12541.33 339.58 o -2 0 4 1960.19 1830.32 141.93 o -1 0 4 746.91 687.04 24.07 o 0 0 4 12308.81 6697.54 260.44 o 1 0 4 4728.36 3751.47 146.96 o 2 0 4 983.08 1035.43 42.25 o 3 0 4 97.41 82.01 7.62 o 4 0 4 4828.31 4856.05 129.12 o 5 0 4 317.47 306.74 13.72 o 6 0 4 162.81 159.28 8.66 o -8 1 4 311.67 295.77 14.22 o -7 1 4 55.11 49.08 2.21 o -6 1 4 53.34 48.43 1.83 o -5 1 4 567.30 577.99 13.55 o -4 1 4 1177.90 1097.26 49.69 o -3 1 4 103.29 101.26 2.55 o -2 1 4 156.72 134.32 3.37 o -1 1 4 626.72 467.70 10.71 o 0 1 4 23.96 14.01 0.68 o 1 1 4 809.59 860.83 14.81 o 2 1 4 126.16 100.58 2.48 o 3 1 4 2006.50 2003.21 38.46 o 4 1 4 29.79 27.07 2.94 o 5 1 4 1487.46 1522.36 40.98 o 6 1 4 199.99 181.88 6.80 o -7 2 4 792.25 796.72 18.99 o -6 2 4 634.90 639.03 13.26 o -5 2 4 28.99 28.88 1.40 o -4 2 4 3013.68 3209.44 69.09 o -3 2 4 4170.19 4329.60 92.39 o -2 2 4 992.13 917.55 28.61 o -1 2 4 188.70 183.75 4.74 o 0 2 4 5111.15 5991.68 131.95 o 1 2 4 1827.44 1839.81 85.60 o 2 2 4 392.28 381.75 7.83 o 3 2 4 56.59 56.26 1.83 o 4 2 4 2423.94 2507.52 62.79 o 5 2 4 196.15 203.03 10.22 o 6 2 4 82.89 90.59 6.05 o -6 3 4 9.88 11.92 1.38 o -5 3 4 219.52 239.78 24.09 o -4 3 4 249.15 230.30 7.60 o -3 3 4 19.11 19.67 1.34 o -2 3 4 31.70 44.58 2.94 o -1 3 4 359.21 380.40 11.25 o 0 3 4 12.26 15.96 1.47 o 1 3 4 275.16 299.01 7.68 o 2 3 4 75.47 80.58 2.87 o 3 3 4 531.98 522.22 13.02 o 4 3 4 4.20 7.61 1.20 o -4 4 4 595.05 546.67 16.57 o -3 4 4 661.82 626.27 18.50 o -2 4 4 221.24 201.86 7.04 o -1 4 4 15.69 12.92 1.16 o 0 4 4 824.17 860.44 24.50 o 1 4 4 333.66 342.90 10.80 o 2 4 4 72.64 63.10 4.15 o 3 4 4 12.53 13.88 1.16 o -8 1 5 0.00 0.86 0.52 o -7 1 5 1.60 2.54 0.40 o -6 1 5 15.77 12.25 0.95 o -5 1 5 7.78 5.45 1.10 o -4 1 5 0.12 1.08 0.29 o -3 1 5 5.38 8.17 0.56 o -2 1 5 96.90 81.58 1.95 o -1 1 5 17.86 17.83 0.67 o 0 1 5 0.00 -0.30 0.30 o 1 1 5 22.78 23.93 0.82 o 2 1 5 64.17 49.25 3.19 o 3 1 5 8.24 7.13 0.83 o 4 1 5 3.41 2.12 0.44 o 5 1 5 1.93 4.12 0.79 o 6 1 5 4.22 4.99 0.91 o -7 2 5 0.01 1.33 0.41 o -6 2 5 0.27 0.64 0.38 o -5 2 5 26.01 21.97 1.16 o -4 2 5 30.42 38.45 1.59 o -3 2 5 4.56 7.42 0.83 o -2 2 5 2.45 2.11 0.32 o -1 2 5 94.83 77.46 2.32 o 0 2 5 108.81 118.95 4.94 o 1 2 5 5.53 8.86 0.53 o 2 2 5 1.66 1.94 0.42 o 3 2 5 71.04 62.17 3.89 o 4 2 5 11.04 15.52 1.28 o -6 3 5 53.65 53.20 2.81 o -5 3 5 19.04 25.95 1.65 o -4 3 5 0.41 1.38 0.37 o -3 3 5 11.85 10.63 1.04 o -2 3 5 192.19 195.61 6.43 o -1 3 5 28.46 29.56 1.65 o 0 3 5 0.02 0.40 0.20 o 1 3 5 38.05 36.11 3.30 o 2 3 5 137.19 145.37 6.13 o 3 3 5 19.14 20.86 1.21 o 4 3 5 7.24 8.41 0.79 o -4 4 5 27.75 14.34 1.73 o -3 4 5 2.48 1.50 0.86 o -2 4 5 1.28 2.68 0.60 o -1 4 5 57.43 67.17 3.11 o 0 4 5 57.13 43.98 2.26 o 1 4 5 3.99 0.35 0.52 o 2 4 5 0.12 0.55 0.29 o 3 4 5 57.71 80.71 4.84 o -8 0 6 947.78 957.87 38.71 o -7 0 6 238.29 233.64 8.09 o -6 0 6 387.56 407.40 12.48 o -5 0 6 265.39 296.31 13.46 o -4 0 6 7151.50 7956.22 416.62 o -3 0 6 161.73 163.53 9.55 o -2 0 6 3088.91 2873.29 133.31 o -1 0 6 249.44 306.86 13.96 o 0 0 6 10944.23 8099.37 326.66 o 1 0 6 1285.15 1344.61 54.86 o 2 0 6 3806.72 3895.99 153.15 o 3 0 6 31.34 31.10 2.76 o 4 0 6 540.64 537.77 15.95 o 5 0 6 2.85 3.45 1.04 o 6 0 6 526.36 459.90 20.02 o -8 1 6 3.54 2.94 0.69 o -7 1 6 1565.41 1597.64 30.93 o -6 1 6 275.74 259.71 6.42 o -5 1 6 99.67 95.88 3.92 o -4 1 6 524.99 543.04 15.32 o -3 1 6 9650.06 10760.72 185.36 o -2 1 6 590.17 720.80 12.51 o -1 1 6 969.73 1156.27 22.51 o 0 1 6 517.54 498.38 10.02 o 1 1 6 11582.97 11814.12 201.37 o 2 1 6 67.21 63.52 1.97 o 3 1 6 2060.62 2006.67 146.60 o 4 1 6 763.70 752.56 18.04 o 5 1 6 1405.99 1335.59 36.23 o 6 1 6 33.66 29.72 2.94 o -7 2 6 140.76 137.40 7.96 o -6 2 6 245.59 239.98 10.66 o -5 2 6 169.99 168.11 6.18 o -4 2 6 3389.90 3529.37 94.16 o -3 2 6 96.76 100.53 3.79 o -2 2 6 1412.71 1421.14 31.67 o -1 2 6 16.87 25.72 1.46 o 0 2 6 4253.27 4527.86 100.43 o 1 2 6 396.30 404.05 8.45 o 2 2 6 1746.44 1747.57 49.53 o 3 2 6 25.82 26.66 1.90 o 4 2 6 323.57 331.03 11.17 o -6 3 6 97.96 93.91 5.88 o -5 3 6 26.81 22.84 1.70 o -4 3 6 120.24 103.74 4.22 o -3 3 6 2212.38 2201.43 59.42 o -2 3 6 43.60 61.71 8.30 o -1 3 6 194.01 222.69 13.68 o 0 3 6 207.57 202.85 5.53 o 1 3 6 2546.48 2666.72 60.19 o 2 3 6 16.88 29.75 1.52 o 3 3 6 569.01 580.98 18.42 o 4 3 6 310.64 307.09 10.98 o -4 4 6 676.44 568.55 24.42 o -3 4 6 31.52 36.83 2.76 o -2 4 6 247.85 232.98 7.91 o -1 4 6 14.37 40.43 3.80 o 0 4 6 651.86 609.92 17.82 o 1 4 6 46.22 45.54 2.56 o 2 4 6 291.99 259.30 8.98 o -8 1 7 4.07 3.32 0.61 o -7 1 7 3.36 7.26 0.72 o -6 1 7 2.64 2.03 0.30 o -5 1 7 1.40 0.86 0.23 o -4 1 7 22.24 18.36 3.02 o -3 1 7 31.52 31.22 0.93 o -2 1 7 7.97 7.08 0.47 o -1 1 7 5.62 7.14 0.45 o 0 1 7 17.66 13.25 0.94 o 1 1 7 14.59 18.83 2.28 o 2 1 7 2.27 2.90 0.80 o 3 1 7 1.40 3.14 0.77 o 4 1 7 1.62 2.22 0.44 o 5 1 7 3.49 4.60 1.21 o 6 1 7 0.36 1.21 0.52 o -7 2 7 1.42 2.11 0.57 o -6 2 7 3.63 5.68 2.42 o -5 2 7 79.64 67.91 3.29 o -4 2 7 8.10 8.92 0.99 o -3 2 7 8.30 9.07 0.85 o -2 2 7 13.76 16.59 0.90 o -1 2 7 140.92 122.85 3.06 o 0 2 7 6.18 7.44 0.60 o 1 2 7 40.69 28.79 1.36 o 2 2 7 0.34 0.85 0.41 o 3 2 7 42.35 34.28 2.26 o 4 2 7 4.76 8.12 1.73 o -6 3 7 7.95 9.35 0.85 o -5 3 7 3.22 5.19 0.86 o -4 3 7 57.77 65.22 3.98 o -3 3 7 54.95 50.66 2.50 o -2 3 7 17.76 18.22 1.22 o -1 3 7 9.48 11.64 0.83 o 0 3 7 42.15 47.63 1.68 o 1 3 7 31.95 27.35 1.81 o 2 3 7 6.64 7.90 0.77 o 3 3 7 5.55 3.97 0.73 o 4 3 7 5.46 7.98 0.91 o -3 4 7 6.63 12.10 1.10 o -2 4 7 7.37 4.34 0.73 o -1 4 7 83.42 103.83 4.27 o 0 4 7 6.90 7.62 1.03 o 1 4 7 33.35 46.99 2.24 o 2 4 7 0.28 4.49 0.69 o -8 0 8 1.75 2.92 0.95 o -7 0 8 1144.33 1144.96 31.97 o -6 0 8 4522.16 4963.93 130.39 o -5 0 8 14.62 12.21 1.08 o -4 0 8 668.09 697.50 26.85 o -3 0 8 1814.79 1746.34 47.98 o -2 0 8 6541.22 5872.92 239.49 o 0 0 8 1200.89 1241.06 55.30 o 1 0 8 2241.52 1748.59 71.02 o 2 0 8 1031.57 1058.50 44.18 o 3 0 8 613.30 611.92 26.92 o 4 0 8 401.30 402.89 12.62 o 5 0 8 182.34 183.65 9.26 o -8 1 8 64.85 59.90 2.79 o -7 1 8 1175.42 1171.31 23.27 o -6 1 8 43.79 40.35 1.95 o -5 1 8 967.37 514.92 23.41 o -4 1 8 2.62 3.79 0.54 o -3 1 8 915.28 874.80 33.57 o -2 1 8 205.41 198.94 4.51 o -1 1 8 2843.80 2901.54 55.59 o 0 1 8 583.80 575.35 12.51 o 1 1 8 140.17 135.54 3.59 o 2 1 8 1458.25 1329.67 30.55 o 3 1 8 1443.84 1433.22 33.05 o 4 1 8 61.93 67.75 2.80 o 5 1 8 8.82 9.92 1.40 o -7 2 8 711.57 635.43 41.45 o -6 2 8 2548.31 2378.03 260.68 o -5 2 8 1.02 2.92 0.66 o -4 2 8 308.73 307.75 15.20 o -3 2 8 932.80 906.45 20.77 o -2 2 8 3118.05 3264.27 62.61 o -1 2 8 0.46 5.18 0.49 o 0 2 8 591.16 606.09 12.38 o 1 2 8 975.37 954.47 22.28 o 2 2 8 588.32 544.52 17.27 o 3 2 8 289.23 278.37 10.05 o 4 2 8 257.03 245.96 9.26 o -6 3 8 13.13 12.42 1.37 o -5 3 8 308.49 290.63 10.32 o -4 3 8 7.03 14.56 1.22 o -3 3 8 226.36 205.90 6.98 o -2 3 8 101.58 100.80 3.28 o -1 3 8 857.04 860.02 17.49 o 0 3 8 120.36 113.79 3.78 o 1 3 8 26.15 26.69 1.44 o 2 3 8 440.74 406.09 13.75 o 3 3 8 579.66 555.96 18.16 o 4 3 8 33.94 38.01 4.15 o -3 4 8 227.80 199.49 7.23 o -2 4 8 619.89 540.52 22.92 o -1 4 8 0.14 7.60 0.66 o 0 4 8 102.96 92.23 8.39 o 1 4 8 171.52 153.55 7.96 o -8 1 9 6.06 5.07 0.79 o -7 1 9 0.12 0.28 0.24 o -6 1 9 3.22 2.30 0.50 o -5 1 9 5.80 3.94 0.98 o -4 1 9 13.38 12.37 1.29 o -3 1 9 0.22 0.84 0.22 o -2 1 9 5.96 4.77 0.47 o -1 1 9 11.32 8.87 0.52 o 0 1 9 8.20 7.43 0.52 o 1 1 9 0.31 0.24 0.35 o 2 1 9 4.27 4.61 1.64 o 3 1 9 0.29 0.35 0.69 o 4 1 9 0.06 0.17 0.37 o 5 1 9 0.00 0.35 0.37 o -7 2 9 0.05 1.12 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