data_2019936 _cell_angle_alpha 91.083 _cell_angle_beta 110.514 _cell_angle_gamma 99.713 _cell_length_a 11.2934 _cell_length_b 13.0083 _cell_length_c 15.8655 _exptl_crystal_F_000 1024.80 _reflns_d_resolution_high 0.7441 _cod_data_source_file fa3366Isup2.hkl _cod_data_source_block I _shelx_title ' X83012_0m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 205.66 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 8813.50 12013.54 13.11 o 3 0 0 15590.24 15449.76 212.71 o 4 0 0 15011.82 14704.58 140.48 o 5 0 0 1486.57 1248.90 26.63 o 6 0 0 5928.21 5409.28 54.68 o 7 0 0 3678.25 3851.78 50.99 o 8 0 0 1398.85 1405.33 32.10 o 9 0 0 5377.21 5479.25 103.58 o 10 0 0 3003.91 2925.18 68.01 o 11 0 0 102.58 137.50 28.94 o 12 0 0 4.12 19.38 23.74 o 13 0 0 68.96 56.41 29.61 o -13 1 0 522.87 448.68 52.86 o -12 1 0 324.57 264.59 33.96 o -11 1 0 92.99 81.04 38.85 o -10 1 0 210.68 194.49 26.54 o -9 1 0 777.18 830.32 20.14 o -8 1 0 2836.61 2666.90 54.81 o -7 1 0 1854.39 1849.30 27.87 o -6 1 0 203.03 189.73 10.45 o -5 1 0 1221.31 1289.22 25.25 o -4 1 0 7375.62 7204.08 49.66 o -3 1 0 23871.33 25653.70 431.96 o -2 1 0 13108.23 14030.96 23.07 o -1 1 0 1738.35 746.25 205.91 o 1 1 0 312.29 185.15 10.27 o 2 1 0 7884.42 8095.79 32.81 o 3 1 0 116.41 96.47 8.31 o 4 1 0 636.65 550.25 5.33 o 5 1 0 568.84 579.11 22.40 o 6 1 0 466.53 508.78 32.81 o 7 1 0 2787.71 2833.96 24.72 o 8 1 0 1175.06 1189.77 40.50 o 9 1 0 31.98 27.38 14.49 o 10 1 0 16.50 15.03 17.20 o 11 1 0 403.29 358.12 90.91 o 12 1 0 246.56 238.76 59.17 o 13 1 0 295.50 415.02 46.72 o -14 2 0 309.81 364.21 43.03 o -13 2 0 9.67 38.32 31.07 o -12 2 0 27.68 43.03 17.69 o -11 2 0 409.46 448.59 30.10 o -10 2 0 2312.13 2279.88 71.13 o -9 2 0 3097.39 2985.86 41.30 o -8 2 0 796.95 769.19 30.50 o -7 2 0 1074.00 1027.43 34.50 o -6 2 0 1788.49 1657.08 19.56 o 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171.36 143.50 8.80 o 3 3 0 244.09 341.59 18.58 o 4 3 0 3150.64 3291.53 31.92 o 5 3 0 1095.17 960.61 21.96 o 6 3 0 368.93 416.49 11.02 o 7 3 0 235.56 235.39 17.34 o 8 3 0 61.29 91.98 14.00 o 9 3 0 66.92 59.66 11.87 o 10 3 0 540.88 560.30 33.56 o 11 3 0 1339.34 1411.07 53.57 o 12 3 0 273.29 253.74 41.79 o 13 3 0 49.66 31.38 32.94 o -14 4 0 195.07 181.68 64.46 o -13 4 0 919.00 1023.91 80.46 o -12 4 0 300.05 310.96 69.35 o -11 4 0 546.21 541.23 48.50 o -10 4 0 1446.27 1445.30 103.09 o -9 4 0 1631.94 1687.48 32.67 o -8 4 0 1019.60 1088.15 72.06 o -7 4 0 83.81 78.28 12.27 o -6 4 0 557.03 637.96 38.59 o -5 4 0 1679.97 1541.54 58.41 o -4 4 0 4677.89 4541.80 102.07 o -3 4 0 7788.08 7985.76 120.87 o -2 4 0 6255.46 5673.70 96.69 o -1 4 0 5649.96 4877.74 64.15 o 0 4 0 29.30 108.02 6.45 o 1 4 0 2171.90 1985.68 30.36 o 2 4 0 2410.72 2089.39 12.80 o 3 4 0 2482.10 2285.88 50.41 o 4 4 0 1353.20 1500.38 13.03 o 5 4 0 936.46 962.35 12.94 o 6 4 0 1338.24 1457.83 44.32 o 7 4 0 118.47 135.19 8.80 o 8 4 0 637.85 626.72 27.12 o 9 4 0 209.37 213.34 16.85 o 10 4 0 22.69 10.05 15.60 o 11 4 0 213.97 206.22 27.52 o 12 4 0 279.37 338.30 45.92 o -14 5 0 1.07 0.40 38.32 o -13 5 0 6.55 10.09 37.96 o -12 5 0 155.51 217.11 49.66 o -11 5 0 603.10 737.94 70.42 o -10 5 0 177.46 227.74 28.27 o -9 5 0 211.75 246.23 40.59 o -8 5 0 80.02 103.04 12.67 o -7 5 0 48.29 40.41 8.89 o -6 5 0 2085.90 2110.91 46.90 o -5 5 0 9475.40 9323.75 266.15 o -4 5 0 3916.12 3825.02 71.13 o -3 5 0 436.77 564.48 17.43 o -2 5 0 2776.38 2851.38 65.39 o -1 5 0 77.73 40.85 5.82 o 0 5 0 5146.54 5476.10 123.94 o 1 5 0 4176.14 3982.39 22.45 o 2 5 0 1605.30 1536.43 39.92 o 3 5 0 0.26 0.04 8.62 o 4 5 0 2660.35 2580.97 29.12 o 5 5 0 4816.88 4750.03 59.26 o 6 5 0 912.79 931.18 20.32 o 7 5 0 1404.63 1444.99 30.72 o 8 5 0 18.41 16.63 13.29 o 9 5 0 87.62 108.38 26.94 o 10 5 0 1959.83 1997.55 46.72 o 11 5 0 2313.58 2473.21 118.43 o 12 5 0 286.23 304.24 46.23 o -13 6 0 2275.24 2257.74 175.82 o -12 6 0 653.87 613.16 61.17 o -11 6 0 33.15 48.99 32.81 o -10 6 0 612.88 662.99 44.59 o -9 6 0 523.27 610.31 54.77 o -8 6 0 1875.31 1884.06 63.17 o -7 6 0 5067.12 4983.94 99.71 o -6 6 0 2285.15 2407.42 50.81 o -5 6 0 1.44 4.45 16.89 o -4 6 0 9985.22 10232.52 257.35 o -3 6 0 14832.09 15366.81 179.91 o -2 6 0 442.51 599.69 17.43 o -1 6 0 94.79 234.54 12.63 o 0 6 0 351.98 390.80 16.40 o 1 6 0 921.19 937.90 20.27 o 2 6 0 3606.45 3317.40 31.03 o 3 6 0 10180.20 10356.64 137.05 o 4 6 0 2370.68 2465.48 23.38 o 5 6 0 2270.21 2312.42 25.56 o 6 6 0 626.29 642.68 25.43 o 7 6 0 955.07 1007.38 22.14 o 8 6 0 234.90 258.86 35.07 o 9 6 0 428.18 442.41 25.96 o 10 6 0 234.64 202.89 26.94 o 11 6 0 22.13 0.04 19.74 o 12 6 0 56.17 97.84 30.41 o -13 7 0 181.14 132.56 69.22 o -12 7 0 6.57 3.82 36.19 o -11 7 0 202.32 79.66 24.27 o -10 7 0 517.98 450.63 53.57 o -9 7 0 1666.54 1586.93 42.19 o -8 7 0 1292.10 1279.53 57.48 o -7 7 0 389.10 418.09 11.65 o -6 7 0 1067.80 1031.78 18.98 o -5 7 0 905.58 935.76 31.96 o -4 7 0 1083.81 1170.88 30.05 o -3 7 0 1176.76 1167.99 18.58 o -2 7 0 26.90 24.14 13.16 o -1 7 0 15.30 6.71 9.56 o 0 7 0 3360.40 3515.04 59.52 o 1 7 0 9555.35 9947.04 146.30 o 2 7 0 3814.87 3788.21 37.07 o 3 7 0 535.51 502.87 26.09 o 4 7 0 0.86 0.44 7.78 o 5 7 0 130.35 139.10 9.38 o 6 7 0 3422.26 3466.63 54.19 o 7 7 0 2043.26 2047.12 57.83 o 8 7 0 2992.50 2977.59 70.95 o 9 7 0 1.31 4.22 19.16 o 10 7 0 1850.41 1981.77 62.19 o 11 7 0 419.46 462.24 58.32 o -13 8 0 622.52 709.09 100.82 o -12 8 0 1018.14 1131.76 105.53 o -11 8 0 453.10 424.80 50.37 o -10 8 0 489.36 508.96 46.81 o -9 8 0 48.66 28.94 14.80 o -8 8 0 1416.34 1334.69 43.79 o -7 8 0 4139.14 4253.38 102.78 o -6 8 0 2554.12 2685.39 33.12 o -5 8 0 344.84 360.17 37.92 o -4 8 0 908.14 766.35 56.19 o -3 8 0 4925.89 5143.22 40.50 o -2 8 0 6635.00 6644.53 219.92 o -1 8 0 3744.04 3798.53 38.32 o 0 8 0 818.03 793.64 70.15 o 1 8 0 384.41 451.34 9.51 o 2 8 0 208.60 181.24 7.11 o 3 8 0 1727.08 1754.48 29.78 o 4 8 0 1103.25 1183.91 27.07 o 5 8 0 542.72 542.34 18.94 o 6 8 0 358.55 345.32 33.34 o 7 8 0 2.60 2.44 10.98 o 8 8 0 960.44 961.55 35.87 o 9 8 0 412.42 431.03 34.76 o 10 8 0 220.69 178.44 39.16 o 11 8 0 39.06 52.14 33.79 o -13 9 0 565.14 758.83 101.53 o -12 9 0 211.61 181.15 48.77 o -11 9 0 1.53 0.00 35.34 o -10 9 0 1018.10 1058.32 59.70 o -9 9 0 1978.86 2052.32 56.95 o -8 9 0 3897.31 3773.37 106.78 o -7 9 0 52.38 44.72 28.98 o -6 9 0 538.95 535.36 12.71 o -5 9 0 337.65 392.31 25.69 o -4 9 0 4858.79 5046.80 81.31 o -3 9 0 4235.41 4280.72 88.42 o -2 9 0 7652.50 7853.07 199.29 o -1 9 0 965.53 1006.84 30.90 o 0 9 0 3837.18 4158.96 65.35 o 1 9 0 2727.03 2837.34 104.07 o 2 9 0 1918.72 2036.00 25.87 o 3 9 0 1266.53 1335.81 43.48 o 4 9 0 79.42 94.95 9.69 o 5 9 0 217.17 218.45 12.85 o 6 9 0 1714.52 1735.00 76.11 o 7 9 0 837.43 881.04 56.28 o 8 9 0 1095.26 1115.13 67.08 o 9 9 0 32.55 63.13 50.90 o 10 9 0 47.04 26.27 30.67 o -12 10 0 704.23 670.99 91.53 o -11 10 0 466.64 447.12 56.90 o -10 10 0 211.47 282.95 53.66 o -9 10 0 30.23 1.82 23.56 o -8 10 0 925.55 889.62 41.12 o 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