data_2019943 _cell_angle_alpha 110.037 _cell_angle_beta 104.524 _cell_angle_gamma 103.208 _cell_length_a 10.0579 _cell_length_b 16.3027 _cell_length_c 16.7074 _exptl_crystal_F_000 1012.00 _reflns_d_resolution_high 0.7157 _cod_data_source_file eg3184Isup2.hkl _cod_data_source_block I _shelx_title ' wa1983 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 318.27 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4370.98 3561.13 228.13 o 3 0 0 11151.60 10633.39 244.66 o 4 0 0 9424.91 8345.99 466.27 o 5 0 0 10555.98 9597.27 460.98 o 6 0 0 758.67 728.84 42.53 o 7 0 0 5098.78 4780.36 180.32 o 8 0 0 1460.83 1529.87 68.88 o 9 0 0 2271.00 2503.27 115.36 o 10 0 0 12.62 3.45 15.17 o 11 0 0 1328.37 1425.19 80.92 o 12 0 0 1402.71 1375.79 110.72 o -12 1 0 257.08 290.94 25.46 o -11 1 0 104.83 140.84 15.93 o 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37735.12 1109.76 o -1 2 0 793.05 771.66 25.40 o 0 2 0 1276.79 984.03 42.56 o 1 2 0 20878.02 20844.07 709.03 o 2 2 0 25120.00 24403.42 541.97 o 3 2 0 104.31 123.65 12.16 o 4 2 0 31.17 51.26 14.01 o 5 2 0 9010.21 8216.15 279.34 o 6 2 0 13611.51 13259.63 619.48 o 7 2 0 507.96 457.88 18.46 o 8 2 0 565.48 606.75 16.24 o 9 2 0 726.36 823.19 40.83 o 10 2 0 2049.66 2176.92 150.69 o 11 2 0 310.04 321.30 24.13 o 12 2 0 635.86 667.48 50.74 o -13 3 0 574.92 522.97 60.21 o -12 3 0 690.49 708.31 59.48 o -11 3 0 2448.84 2712.87 92.97 o -10 3 0 191.24 204.91 16.05 o -9 3 0 2596.55 2994.80 98.48 o -8 3 0 5654.74 6333.08 214.88 o -7 3 0 1949.21 2269.00 60.30 o -6 3 0 1972.24 1863.53 43.78 o -5 3 0 5543.65 5774.36 250.15 o -4 3 0 54892.69 56704.01 244.18 o -3 3 0 2160.32 1708.74 83.90 o -2 3 0 2908.13 2943.02 102.98 o -1 3 0 191.32 150.08 17.30 o 0 3 0 6865.86 6157.94 115.82 o 1 3 0 101297.41 117757.66 3241.38 o 2 3 0 3113.67 2612.57 91.43 o 3 3 0 6916.14 6049.73 172.39 o 4 3 0 4726.56 4503.24 194.06 o 5 3 0 5033.83 4328.31 195.34 o 6 3 0 853.93 753.56 51.37 o 7 3 0 2208.76 2015.25 105.84 o 8 3 0 2946.59 2759.41 150.57 o 9 3 0 724.68 780.23 80.51 o 10 3 0 135.57 168.99 32.50 o 11 3 0 487.91 487.11 30.45 o -13 4 0 1897.98 1702.64 198.63 o -12 4 0 706.69 709.52 46.66 o -11 4 0 16.47 43.27 15.60 o -10 4 0 1420.97 1562.27 103.12 o -9 4 0 8704.19 9157.08 486.42 o -8 4 0 1167.54 1318.38 55.18 o -7 4 0 577.94 660.33 46.41 o -6 4 0 427.90 377.16 18.53 o -5 4 0 17522.59 17149.52 1448.68 o -4 4 0 11789.70 11698.31 664.15 o -3 4 0 2698.57 2361.86 127.59 o -2 4 0 38014.06 42985.52 1771.45 o -1 4 0 2415.75 2206.77 99.41 o 0 4 0 1414.02 1377.71 31.38 o 1 4 0 2050.28 1736.97 56.50 o 2 4 0 18203.54 16461.90 493.73 o 3 4 0 6077.72 4963.84 177.02 o 4 4 0 240.73 198.37 12.75 o 5 4 0 10.34 25.07 13.64 o 6 4 0 2689.37 2594.24 133.50 o 7 4 0 11555.23 11449.45 509.62 o 8 4 0 1096.10 1087.98 58.08 o 9 4 0 5.71 22.05 15.04 o 10 4 0 701.54 700.06 39.26 o 11 4 0 1372.71 1240.44 69.25 o -13 5 0 59.74 56.23 21.37 o -12 5 0 447.77 461.41 27.17 o -11 5 0 1181.80 1217.36 29.97 o -10 5 0 3521.66 3776.56 296.34 o -9 5 0 4362.88 4515.92 97.85 o -8 5 0 2746.43 2931.17 76.64 o -7 5 0 7691.67 7320.32 703.68 o -6 5 0 636.17 628.28 25.13 o -5 5 0 5238.80 4567.44 232.42 o -4 5 0 2550.49 2535.78 136.69 o -3 5 0 32931.89 34986.75 1621.81 o -2 5 0 12924.20 13051.35 516.43 o -1 5 0 225.21 269.04 12.19 o 0 5 0 143.31 123.92 12.49 o 1 5 0 22954.79 24459.61 628.93 o 2 5 0 15687.11 14736.71 359.47 o 3 5 0 3812.75 3696.82 72.88 o 4 5 0 3412.91 3104.97 100.06 o 5 5 0 2759.95 2526.41 58.85 o 6 5 0 5957.61 5742.07 198.35 o 7 5 0 495.47 478.33 24.58 o 8 5 0 663.38 746.03 55.25 o 9 5 0 1034.81 1098.05 104.88 o 10 5 0 706.02 687.86 59.36 o 11 5 0 464.46 402.40 30.72 o -13 6 0 828.59 785.11 85.25 o -12 6 0 2011.65 2186.82 178.56 o -11 6 0 973.79 1020.79 71.04 o -10 6 0 663.33 711.71 29.86 o -9 6 0 697.64 762.12 19.48 o -8 6 0 9818.62 11413.72 241.42 o -7 6 0 5219.50 5346.04 91.44 o -6 6 0 9.53 33.13 14.73 o -5 6 0 62.84 67.40 13.83 o -4 6 0 6381.75 5291.84 381.91 o -3 6 0 16038.00 16549.92 770.97 o -2 6 0 367.36 325.35 12.92 o -1 6 0 5718.32 5295.39 201.97 o 0 6 0 4255.40 3909.28 147.62 o 1 6 0 17143.29 16979.91 418.02 o 2 6 0 6114.79 6379.52 131.67 o 3 6 0 6733.13 6258.70 110.77 o 4 6 0 4501.46 4431.28 167.16 o 5 6 0 1012.63 1013.23 37.34 o 6 6 0 634.21 561.91 17.25 o 7 6 0 1279.61 1261.20 57.27 o 8 6 0 3030.06 2967.87 230.48 o 9 6 0 956.57 971.07 96.98 o 10 6 0 7.55 27.13 17.32 o -13 7 0 2104.67 1901.70 197.68 o -12 7 0 740.70 843.68 51.33 o -11 7 0 101.39 118.84 17.69 o -10 7 0 886.79 908.95 48.92 o -9 7 0 4373.57 4701.26 76.82 o -8 7 0 8250.25 8373.89 338.98 o -7 7 0 347.05 314.20 21.16 o -6 7 0 3022.94 2800.00 93.96 o -5 7 0 2060.48 1743.31 153.82 o -4 7 0 16199.13 17299.16 885.85 o -3 7 0 166.26 123.15 14.28 o -2 7 0 16151.17 17167.69 875.21 o -1 7 0 12810.20 12711.28 560.88 o 0 7 0 1829.72 1806.40 64.46 o 1 7 0 309.49 222.11 13.04 o 2 7 0 2526.36 2437.16 53.82 o 3 7 0 17002.42 17023.76 808.35 o 4 7 0 931.41 885.94 32.21 o 5 7 0 211.07 204.56 14.29 o 6 7 0 937.94 906.59 60.34 o 7 7 0 3227.63 3195.35 165.80 o 8 7 0 1945.55 1906.79 130.73 o 9 7 0 106.19 114.31 16.91 o 10 7 0 544.47 513.78 51.63 o -13 8 0 639.72 584.19 51.70 o -12 8 0 501.05 580.54 34.75 o -11 8 0 2151.56 2281.41 160.98 o -10 8 0 1940.50 1920.02 119.93 o -9 8 0 1715.81 1812.34 45.98 o -8 8 0 241.93 277.18 20.93 o -7 8 0 11976.98 12464.76 1021.46 o -6 8 0 9072.13 9869.19 428.71 o -5 8 0 1834.70 1807.35 80.26 o -4 8 0 81.96 86.10 13.86 o -3 8 0 7671.46 7192.07 469.26 o -2 8 0 20422.79 20272.88 1202.80 o -1 8 0 440.31 351.51 17.32 o 0 8 0 6149.57 6627.45 217.09 o 1 8 0 1714.65 1682.65 83.46 o 2 8 0 11502.80 11166.73 328.76 o 3 8 0 2736.44 2512.44 55.01 o 4 8 0 247.93 272.88 14.80 o 5 8 0 4033.21 3982.94 183.01 o 6 8 0 2240.93 2260.38 155.15 o 7 8 0 1329.83 1295.33 123.26 o 8 8 0 98.45 134.74 17.47 o 9 8 0 1522.65 1255.53 115.57 o 10 8 0 439.30 260.68 23.93 o -13 9 0 74.67 78.20 16.86 o -12 9 0 2777.32 2974.65 127.24 o -11 9 0 1950.14 1977.43 122.11 o -10 9 0 17.82 36.77 23.98 o -9 9 0 484.40 555.67 18.35 o -8 9 0 5281.38 6253.12 192.32 o -7 9 0 6325.19 6859.48 165.97 o -6 9 0 53.38 60.71 14.41 o -5 9 0 2657.25 2638.60 150.87 o -4 9 0 2580.66 2531.13 170.11 o -3 9 0 10391.94 9840.69 429.74 o -2 9 0 4497.88 4491.45 242.71 o -1 9 0 5400.44 5158.43 156.43 o 0 9 0 4273.88 4170.67 160.70 o 1 9 0 1884.15 1827.20 60.94 o 2 9 0 3285.00 3432.15 72.42 o 3 9 0 1931.55 1889.44 48.69 o 4 9 0 5644.00 5719.37 113.37 o 5 9 0 1237.04 1208.00 58.28 o 6 9 0 29.17 24.86 15.02 o 7 9 0 22.63 24.84 16.20 o 8 9 0 1281.81 1180.14 98.31 o 9 9 0 957.89 850.10 102.19 o -13 10 0 1172.24 1089.80 64.37 o -12 10 0 2148.81 2218.37 114.51 o -11 10 0 5.75 31.98 16.05 o -10 10 0 1283.45 1410.67 33.03 o -9 10 0 2811.89 2926.75 51.21 o -8 10 0 4195.06 3962.35 369.22 o -7 10 0 154.65 120.98 16.73 o -6 10 0 4352.25 4641.23 234.18 o -5 10 0 5755.49 6068.45 249.34 o -4 10 0 3108.35 3234.53 158.57 o -3 10 0 1883.99 2090.35 143.48 o -2 10 0 2278.60 1986.59 98.70 o -1 10 0 10805.37 10668.53 363.69 o 0 10 0 1946.04 1940.90 73.88 o 1 10 0 15.36 34.41 12.40 o 2 10 0 634.44 689.75 17.63 o 3 10 0 3431.81 3686.59 101.94 o 4 10 0 3564.93 3798.43 97.93 o 5 10 0 210.58 209.55 15.47 o 6 10 0 940.69 869.65 47.10 o 7 10 0 953.87 883.42 71.89 o 8 10 0 1306.57 1187.03 81.23 o 9 10 0 39.98 57.12 19.06 o -13 11 0 1074.13 1004.08 101.07 o -12 11 0 2.44 45.61 24.24 o -11 11 0 2570.53 2760.15 150.98 o -10 11 0 2194.23 2426.18 80.03 o -9 11 0 1611.85 1749.04 27.63 o -8 11 0 241.73 224.60 17.37 o -7 11 0 1879.47 1867.83 97.22 o -6 11 0 11239.78 11867.09 623.95 o -5 11 0 376.27 363.24 29.65 o -4 11 0 1308.05 1412.60 79.84 o -3 11 0 1940.45 1935.05 165.12 o -2 11 0 12748.58 13130.19 784.83 o -1 11 0 4671.54 4623.99 180.41 o 0 11 0 2237.77 2173.37 78.50 o 1 11 0 3625.14 3791.68 61.35 o 2 11 0 1797.79 1852.02 52.19 o 3 11 0 1858.99 1898.33 64.97 o 4 11 0 0.99 8.82 15.54 o 5 11 0 2083.89 2239.11 71.78 o 6 11 0 1247.18 1288.96 76.27 o 7 11 0 345.85 382.24 41.62 o 8 11 0 5.20 11.69 18.57 o -13 12 0 6.10 4.67 15.87 o -12 12 0 1382.69 1493.63 106.97 o -11 12 0 2381.89 2599.91 51.01 o -10 12 0 225.79 240.90 16.19 o -9 12 0 489.50 538.60 23.97 o -8 12 0 2177.64 2110.44 129.61 o -7 12 0 6679.54 6862.47 245.85 o -6 12 0 1502.96 1464.13 122.94 o -5 12 0 1609.17 1675.77 84.62 o -4 12 0 2358.11 2618.24 157.18 o -3 12 0 3537.63 3785.73 235.09 o -2 12 0 3889.83 3862.89 238.47 o -1 12 0 134.24 141.81 11.96 o 0 12 0 7178.58 7583.37 162.73 o 1 12 0 2696.62 2909.33 44.10 o 2 12 0 475.04 527.21 17.31 o 3 12 0 14.87 31.31 14.53 o 4 12 0 1959.49 2033.49 50.03 o 5 12 0 1499.24 1509.02 69.02 o 6 12 0 7.99 21.28 18.92 o 7 12 0 239.78 243.38 20.50 o -12 13 0 1193.20 1174.49 64.97 o -11 13 0 112.33 154.20 29.94 o -10 13 0 2010.46 2194.62 35.55 o -9 13 0 2476.68 2527.13 32.83 o -8 13 0 1391.95 1433.53 45.18 o -7 13 0 1419.94 1512.61 90.01 o -6 13 0 393.88 407.58 15.74 o -5 13 0 4300.43 4462.67 236.54 o -4 13 0 1057.18 1100.95 66.38 o -3 13 0 299.20 310.35 19.30 o -2 13 0 26.49 49.42 19.27 o -1 13 0 5700.65 6367.47 195.98 o 0 13 0 4444.37 4888.76 97.51 o 1 13 0 3.35 31.00 15.47 o 2 13 0 965.67 1040.05 35.70 o 3 13 0 1196.36 1287.10 28.82 o 4 13 0 2421.37 2593.51 101.42 o 5 13 0 228.78 263.98 22.25 o 6 13 0 649.33 627.85 23.57 o 7 13 0 646.99 497.69 44.25 o -12 14 0 156.53 175.65 18.04 o -11 14 0 952.85 965.80 41.53 o -10 14 0 3392.37 3707.43 95.87 o -9 14 0 485.49 537.28 22.62 o -8 14 0 134.48 150.77 18.55 o -7 14 0 858.56 888.69 22.97 o -6 14 0 6929.93 7258.20 448.87 o -5 14 0 2791.44 2969.06 211.78 o -4 14 0 1632.35 1691.34 100.71 o -3 14 0 1439.52 1507.13 132.07 o -2 14 0 1298.08 1291.42 118.40 o -1 14 0 3490.60 3677.28 112.91 o 0 14 0 158.39 173.57 17.06 o 1 14 0 2052.35 2261.49 49.66 o 2 14 0 1521.53 1662.80 22.77 o 3 14 0 828.10 940.65 20.69 o 4 14 0 152.16 181.67 19.07 o 5 14 0 312.25 315.88 24.31 o 6 14 0 1046.18 887.28 92.57 o -12 15 0 294.78 240.64 17.14 o -11 15 0 1876.47 1973.88 69.71 o -10 15 0 973.10 1030.83 47.96 o 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393.52 32.08 o -2 19 0 252.70 246.85 20.41 o -1 19 0 870.63 843.93 30.59 o 0 19 0 807.19 822.16 45.58 o 1 19 0 316.63 335.32 24.50 o -8 20 0 48.16 78.54 26.52 o -7 20 0 653.33 531.91 19.77 o -6 20 0 585.30 571.60 20.39 o -5 20 0 536.29 497.97 42.51 o -4 20 0 241.99 251.50 24.83 o -3 20 0 301.46 294.56 19.79 o -2 20 0 1042.89 915.00 85.93 o -1 20 0 274.14 265.60 21.90 o 0 20 0 14.39 39.20 25.93 o -6 21 0 167.87 165.75 17.31 o -5 21 0 0.11 31.02 17.55 o -4 21 0 138.52 132.38 17.86 o -3 21 0 1054.27 936.41 25.63 o 2 -21 1 330.58 275.45 29.75 o 3 -21 1 130.98 145.13 18.29 o 4 -21 1 655.43 664.84 53.01 o 5 -21 1 486.63 420.76 45.66 o 6 -21 1 373.51 339.72 20.89 o 7 -21 1 41.32 41.63 18.01 o 0 -20 1 275.00 257.34 20.54 o 1 -20 1 118.78 100.69 20.53 o 2 -20 1 125.76 136.87 19.62 o 3 -20 1 1254.69 1259.11 111.40 o 4 -20 1 700.45 645.64 39.38 o 5 -20 1 23.30 24.64 17.39 o 6 -20 1 26.87 44.89 18.89 o 7 -20 1 1284.85 1147.20 23.21 o 8 -20 1 1596.87 1372.77 46.82 o 9 -20 1 72.01 82.63 17.07 o -2 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