data_2019956 _cell_angle_alpha 90.000 _cell_angle_beta 110.268 _cell_angle_gamma 90.000 _cell_length_a 15.1241 _cell_length_b 6.0111 _cell_length_c 14.3212 _exptl_crystal_F_000 504.00 _reflns_d_resolution_high 0.8537 _cod_data_source_file is5385Isup2.hkl _cod_data_source_block I _shelx_title ' mm_chandra_p7 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 188.73 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 990.53 605.06 36.38 o 2 0 0 4560.10 4957.02 152.44 o 3 0 0 1695.53 1797.91 55.23 o 4 0 0 9203.11 9898.30 345.60 o 5 0 0 1672.13 1820.32 56.08 o 6 0 0 138.17 130.23 12.03 o 7 0 0 3522.87 3358.20 314.49 o 8 0 0 15.84 15.02 1.70 o 9 0 0 480.22 450.44 16.97 o 10 0 0 362.96 313.13 15.87 o 11 0 0 376.57 385.47 13.74 o 12 0 0 1.45 1.58 0.80 o 13 0 0 353.43 336.49 12.20 o 15 0 0 47.65 47.68 5.10 o 16 0 0 9.61 6.79 1.36 o 1 1 0 112.59 132.93 3.15 o 2 1 0 1611.61 1676.34 36.45 o 3 1 0 3485.87 3579.65 77.55 o 4 1 0 1170.09 1153.16 27.06 o 5 1 0 164.55 182.88 4.75 o 6 1 0 60.84 54.05 2.33 o 8 1 0 20.34 20.53 0.93 o 9 1 0 74.62 90.06 2.26 o 10 1 0 127.12 126.07 3.07 o 11 1 0 59.07 54.89 1.92 o 12 1 0 124.75 128.35 4.06 o 13 1 0 13.34 15.51 1.16 o 14 1 0 10.64 10.94 0.84 o 15 1 0 1.26 1.38 0.43 o 16 1 0 45.07 42.81 2.94 o 0 2 0 165.37 158.38 10.45 o 1 2 0 816.95 788.43 21.74 o 2 2 0 90.45 104.28 2.76 o 3 2 0 437.14 446.41 9.98 o 4 2 0 845.34 761.59 14.21 o 5 2 0 47.88 52.36 2.49 o 6 2 0 7.27 9.98 0.55 o 7 2 0 65.98 61.10 1.38 o 8 2 0 438.21 421.67 8.25 o 9 2 0 177.15 176.57 3.75 o 10 2 0 70.69 66.90 1.67 o 11 2 0 400.09 416.74 10.40 o 12 2 0 2.18 5.00 0.57 o 13 2 0 0.17 0.47 0.50 o 14 2 0 1.31 1.78 0.59 o 15 2 0 42.37 40.49 1.65 o 1 3 0 227.40 186.88 15.45 o 2 3 0 3101.96 2929.70 94.39 o 3 3 0 26.44 23.19 0.80 o 4 3 0 5.73 6.44 0.88 o 5 3 0 1219.54 1111.84 18.79 o 6 3 0 566.03 550.93 8.91 o 7 3 0 234.32 233.06 4.23 o 8 3 0 678.09 664.36 11.42 o 9 3 0 213.25 229.13 4.39 o 10 3 0 2.76 4.39 0.65 o 11 3 0 136.30 138.28 3.26 o 12 3 0 399.07 408.92 12.47 o 13 3 0 129.73 130.40 3.19 o 14 3 0 0.17 -0.23 0.42 o 15 3 0 120.24 110.43 5.90 o 0 4 0 106.65 118.95 2.98 o 1 4 0 193.99 194.90 4.02 o 2 4 0 152.70 171.90 3.31 o 3 4 0 21.95 28.70 0.87 o 4 4 0 45.86 44.48 1.14 o 5 4 0 212.52 199.97 3.73 o 6 4 0 38.02 42.04 1.24 o 7 4 0 839.72 875.44 15.96 o 8 4 0 8.81 9.32 0.60 o 9 4 0 1.29 2.21 0.60 o 10 4 0 3.92 5.06 0.52 o 11 4 0 18.22 16.01 0.72 o 12 4 0 40.05 36.67 1.10 o 13 4 0 26.28 24.58 1.79 o 1 5 0 48.78 46.95 1.34 o 2 5 0 132.73 131.38 2.92 o 3 5 0 0.22 0.20 0.35 o 4 5 0 35.58 37.55 1.16 o 5 5 0 239.45 263.11 5.61 o 6 5 0 90.58 99.75 2.76 o 7 5 0 86.42 88.94 2.64 o 8 5 0 0.25 0.18 0.46 o 9 5 0 31.31 32.78 1.42 o 10 5 0 99.92 98.07 2.71 o 11 5 0 32.72 31.99 1.59 o 0 6 0 105.19 105.61 7.48 o 1 6 0 13.03 13.21 1.02 o 2 6 0 30.18 28.82 1.21 o 3 6 0 18.45 20.43 1.10 o 4 6 0 1.96 3.00 0.66 o 5 6 0 30.39 30.72 1.54 o 6 6 0 7.39 7.42 0.72 o 7 6 0 141.75 149.93 8.94 o 8 6 0 31.36 31.14 1.60 o -16 1 1 1.63 0.74 0.60 o -15 1 1 6.30 8.32 0.78 o -14 1 1 100.28 104.02 3.08 o -13 1 1 190.37 194.16 5.21 o -12 1 1 4.57 4.86 0.57 o -11 1 1 56.39 55.23 1.89 o -10 1 1 468.64 413.56 9.63 o -9 1 1 414.59 411.03 8.98 o -8 1 1 1172.63 1058.56 24.87 o -7 1 1 1967.92 1877.85 61.91 o -6 1 1 2858.73 2753.04 53.36 o -5 1 1 9.37 7.84 0.38 o -4 1 1 4017.71 3991.90 82.00 o -3 1 1 2811.58 2882.84 56.11 o -2 1 1 19999.52 19134.76 372.65 o -1 1 1 33.17 30.84 0.78 o 0 1 1 3704.06 3879.46 86.11 o 1 1 1 364.63 411.61 8.99 o 2 1 1 2559.23 2749.08 59.64 o 3 1 1 7.96 12.95 0.52 o 4 1 1 8.38 9.56 0.43 o 5 1 1 1217.98 1293.04 38.76 o 6 1 1 67.56 65.94 3.00 o 7 1 1 1852.90 1673.45 39.16 o 8 1 1 192.33 171.13 3.57 o 9 1 1 12.89 12.59 0.68 o 10 1 1 527.48 520.19 11.34 o 11 1 1 568.27 569.38 14.18 o 12 1 1 39.02 44.84 1.99 o 13 1 1 22.49 24.77 2.03 o 14 1 1 17.68 16.88 0.98 o 15 1 1 63.47 66.43 2.75 o 16 1 1 70.31 52.80 3.63 o -16 2 1 59.39 57.91 6.80 o -15 2 1 198.46 203.77 10.53 o -14 2 1 159.33 164.72 5.14 o -13 2 1 24.69 26.49 2.26 o -12 2 1 135.43 144.86 3.54 o -11 2 1 0.93 1.05 0.44 o -10 2 1 10.43 12.55 0.59 o -9 2 1 72.13 66.99 1.44 o -8 2 1 1.19 2.03 0.43 o -7 2 1 183.79 189.55 3.45 o -6 2 1 726.49 663.35 14.50 o -5 2 1 846.54 796.14 22.50 o -4 2 1 608.61 562.37 11.65 o -3 2 1 535.42 540.80 12.05 o -2 2 1 2171.81 2114.79 52.81 o -1 2 1 753.31 709.71 17.76 o 0 2 1 2022.32 2023.95 54.71 o 1 2 1 267.06 273.43 6.51 o 2 2 1 1754.56 1610.91 35.12 o 3 2 1 4.17 5.21 0.26 o 4 2 1 138.13 125.19 2.99 o 5 2 1 805.69 741.32 22.80 o 6 2 1 308.99 267.56 4.75 o 7 2 1 576.56 600.36 11.61 o 8 2 1 20.01 16.76 0.68 o 9 2 1 40.12 34.06 1.02 o 10 2 1 514.95 539.16 11.56 o 11 2 1 0.25 1.33 0.50 o 12 2 1 80.75 84.21 2.50 o 13 2 1 126.52 131.06 4.27 o 14 2 1 31.49 31.87 1.35 o 15 2 1 17.47 16.38 1.19 o -15 3 1 63.29 55.73 3.40 o -14 3 1 33.32 35.48 1.24 o -13 3 1 72.29 71.79 1.98 o -12 3 1 5.97 9.01 1.02 o -11 3 1 686.03 712.89 13.87 o -10 3 1 25.04 28.69 0.96 o -9 3 1 8.18 8.63 0.51 o -8 3 1 14.90 12.45 0.53 o -7 3 1 290.07 279.74 4.69 o -6 3 1 40.38 34.67 0.85 o -5 3 1 2.25 6.08 0.37 o -4 3 1 117.89 107.42 2.98 o -3 3 1 3.06 2.67 0.39 o -2 3 1 56.66 55.26 3.14 o -1 3 1 312.86 331.15 18.41 o 0 3 1 823.10 846.36 37.79 o 1 3 1 0.12 0.50 0.28 o 2 3 1 55.82 60.13 2.37 o 3 3 1 141.43 136.89 2.84 o 4 3 1 430.51 400.43 7.16 o 5 3 1 49.94 43.39 1.06 o 6 3 1 4.59 5.49 0.35 o 7 3 1 138.03 143.11 2.73 o 8 3 1 100.29 104.22 2.22 o 9 3 1 299.93 318.03 5.94 o 10 3 1 18.64 18.73 0.79 o 11 3 1 8.40 9.62 0.61 o 12 3 1 42.35 41.01 1.26 o 13 3 1 32.21 29.83 1.12 o 14 3 1 15.89 10.48 0.87 o -13 4 1 13.24 17.07 0.88 o -12 4 1 122.74 131.21 2.88 o -11 4 1 29.64 31.63 1.08 o -10 4 1 6.74 7.94 0.61 o -9 4 1 57.48 62.76 1.60 o -8 4 1 531.01 567.45 10.52 o -7 4 1 461.30 490.65 9.17 o -6 4 1 430.37 447.19 7.83 o -5 4 1 220.56 231.10 4.24 o -4 4 1 339.38 359.39 6.34 o -3 4 1 9.45 11.38 0.54 o -2 4 1 433.25 418.17 7.05 o -1 4 1 268.75 243.41 4.57 o 0 4 1 165.68 177.91 3.01 o 1 4 1 293.75 258.41 4.79 o 2 4 1 223.75 211.53 4.01 o 3 4 1 838.92 825.90 16.38 o 4 4 1 25.74 33.81 1.10 o 5 4 1 1441.67 1452.66 26.24 o 6 4 1 325.57 347.12 6.61 o 7 4 1 78.23 85.58 2.01 o 8 4 1 86.42 87.23 2.23 o 9 4 1 407.87 419.33 9.12 o 10 4 1 86.64 91.46 2.37 o 11 4 1 7.28 7.65 0.57 o 12 4 1 91.07 84.66 3.28 o 13 4 1 55.79 48.93 2.95 o -11 5 1 14.62 12.65 0.91 o -10 5 1 88.18 87.89 2.72 o -9 5 1 21.68 20.66 1.13 o -8 5 1 28.95 32.31 1.19 o -7 5 1 31.39 32.03 1.16 o -6 5 1 20.05 20.25 1.19 o -5 5 1 10.31 11.42 0.66 o -4 5 1 50.16 52.32 1.44 o -3 5 1 80.41 91.42 2.36 o -2 5 1 2.19 3.08 0.47 o -1 5 1 14.14 13.79 0.68 o 0 5 1 11.87 11.94 0.65 o 1 5 1 15.19 15.32 0.80 o 2 5 1 1.77 1.79 0.46 o 3 5 1 36.94 40.59 1.94 o 4 5 1 8.98 10.34 0.71 o 5 5 1 359.23 382.97 8.66 o 6 5 1 5.13 6.57 0.71 o 7 5 1 2.69 3.61 0.56 o 8 5 1 79.66 91.01 2.68 o 9 5 1 106.01 95.48 2.70 o 10 5 1 44.89 44.38 1.49 o -8 6 1 19.43 17.19 1.06 o -7 6 1 9.39 11.11 0.71 o -6 6 1 35.84 38.20 1.69 o -5 6 1 54.75 55.02 2.13 o -4 6 1 0.11 0.47 0.50 o -3 6 1 31.60 30.47 1.09 o -2 6 1 24.19 22.42 2.06 o -1 6 1 0.16 1.41 0.84 o 0 6 1 20.14 17.23 1.54 o 1 6 1 10.66 10.30 1.27 o 2 6 1 0.16 -0.11 0.42 o 3 6 1 47.15 48.96 1.80 o 4 6 1 2.13 3.10 0.60 o 5 6 1 37.74 39.01 1.67 o 6 6 1 10.44 9.06 0.88 o 7 6 1 1.05 0.64 0.44 o -17 0 2 21.25 23.55 2.04 o -16 0 2 46.06 53.00 3.85 o -15 0 2 19.09 15.49 1.06 o -14 0 2 244.86 245.74 16.00 o -13 0 2 55.92 56.98 2.87 o -12 0 2 55.36 60.16 2.87 o -11 0 2 23.19 26.15 1.68 o -10 0 2 1378.03 1316.99 44.95 o -9 0 2 498.51 463.94 16.19 o -8 0 2 77.76 60.06 4.99 o -7 0 2 2064.12 1933.76 61.32 o -6 0 2 196.26 189.26 5.09 o -5 0 2 88.76 109.78 3.03 o -4 0 2 35619.35 36670.79 915.01 o -3 0 2 3234.87 3375.04 84.64 o -2 0 2 7303.20 7722.45 193.15 o -1 0 2 2.62 1.03 0.29 o 0 0 2 1560.36 1748.65 53.82 o 1 0 2 395.91 434.93 13.91 o 2 0 2 449.40 472.95 14.73 o 3 0 2 363.02 360.94 13.06 o 4 0 2 1560.26 1640.94 63.16 o 5 0 2 1106.89 1145.48 55.58 o 6 0 2 19.92 18.81 1.60 o 7 0 2 1143.71 936.82 32.05 o 8 0 2 1278.02 1288.17 43.86 o 9 0 2 314.84 323.48 11.82 o 10 0 2 0.84 2.46 0.56 o 11 0 2 154.80 154.64 4.93 o 12 0 2 271.14 262.15 9.71 o 13 0 2 24.60 28.98 2.72 o 14 0 2 0.60 0.45 1.13 o 15 0 2 120.34 129.23 7.48 o -17 1 2 19.43 14.49 1.58 o -16 1 2 0.03 0.91 0.56 o -15 1 2 12.06 10.52 0.86 o -14 1 2 45.94 46.45 1.55 o -13 1 2 9.86 12.53 0.83 o -12 1 2 38.95 35.62 1.47 o -11 1 2 70.69 68.35 2.60 o -10 1 2 0.75 0.55 0.34 o -9 1 2 780.48 681.57 13.63 o -8 1 2 1385.67 1257.04 32.51 o -7 1 2 477.78 472.71 13.49 o -6 1 2 432.05 414.76 7.94 o -5 1 2 1198.28 1202.22 21.44 o -4 1 2 15976.24 16051.42 297.70 o -3 1 2 33.24 29.97 0.69 o -2 1 2 8936.88 8754.97 162.18 o -1 1 2 1365.69 1518.51 30.99 o 0 1 2 33.10 35.12 0.90 o 1 1 2 39.99 38.84 1.00 o 2 1 2 31.17 31.19 0.96 o 3 1 2 2028.99 2070.64 52.30 o 4 1 2 429.37 472.45 11.62 o 5 1 2 2272.40 2265.71 76.95 o 7 1 2 10.35 14.80 0.64 o 8 1 2 0.98 2.33 0.31 o 9 1 2 218.69 222.11 5.08 o 10 1 2 162.08 165.00 4.53 o 11 1 2 34.56 31.00 1.38 o 12 1 2 78.08 83.94 2.65 o 13 1 2 21.41 24.20 1.24 o 14 1 2 96.75 93.89 3.62 o 15 1 2 4.58 3.85 0.65 o -16 2 2 20.34 21.88 1.44 o -15 2 2 1.69 0.98 0.65 o -14 2 2 60.50 65.22 2.53 o -13 2 2 455.16 463.35 25.82 o -12 2 2 146.31 151.70 3.34 o -11 2 2 142.40 151.50 3.08 o -10 2 2 786.15 783.48 13.06 o -9 2 2 614.30 613.64 10.29 o -8 2 2 3.32 3.80 0.52 o -7 2 2 142.79 137.83 3.16 o -6 2 2 2205.56 2019.47 45.92 o -5 2 2 484.09 461.71 13.19 o -4 2 2 819.53 822.52 16.02 o -3 2 2 612.13 617.13 14.67 o -2 2 2 2242.61 2312.95 50.60 o -1 2 2 1014.36 1043.76 26.43 o 0 2 2 812.22 831.04 17.33 o 1 2 2 1403.76 1370.17 28.29 o 2 2 2 58.24 67.01 1.53 o 3 2 2 378.80 373.73 7.92 o 4 2 2 905.92 812.38 35.53 o 5 2 2 448.18 428.63 7.57 o 6 2 2 70.22 70.23 1.48 o 7 2 2 9.26 11.03 0.55 o 8 2 2 517.98 485.47 9.48 o 9 2 2 71.92 78.17 2.10 o 10 2 2 69.13 68.55 1.90 o 11 2 2 72.04 67.96 2.20 o 12 2 2 19.65 15.52 0.82 o 13 2 2 3.62 3.64 0.61 o 14 2 2 25.94 20.14 0.98 o -15 3 2 43.07 46.74 3.06 o -14 3 2 6.21 6.71 0.55 o -13 3 2 82.86 76.38 2.72 o -12 3 2 118.63 123.78 2.83 o -11 3 2 53.64 63.95 1.93 o -10 3 2 6.65 8.56 0.66 o -9 3 2 3.43 3.12 0.36 o -8 3 2 1154.07 1161.24 18.51 o -7 3 2 160.94 153.41 2.73 o -6 3 2 57.80 43.04 1.10 o -5 3 2 1227.42 1163.43 19.67 o -4 3 2 239.41 201.69 3.65 o -3 3 2 7.16 3.67 0.41 o -2 3 2 447.55 527.90 11.09 o -1 3 2 1227.49 1084.84 34.10 o 0 3 2 293.99 289.05 10.89 o 1 3 2 78.54 77.58 2.72 o 2 3 2 171.54 117.89 2.56 o 3 3 2 185.19 165.46 3.04 o 4 3 2 229.89 207.85 3.73 o 5 3 2 157.39 147.91 2.81 o 6 3 2 450.77 434.51 7.11 o 7 3 2 187.60 175.58 3.43 o 8 3 2 0.81 2.41 0.73 o 9 3 2 157.54 163.10 3.25 o 10 3 2 19.44 22.77 0.90 o 11 3 2 12.93 12.76 0.68 o 12 3 2 12.53 13.97 0.89 o 13 3 2 116.11 110.91 3.41 o 14 3 2 10.99 8.60 1.13 o -14 4 2 11.73 10.64 1.13 o -13 4 2 0.13 -0.26 0.47 o -12 4 2 86.30 83.12 2.03 o -11 4 2 126.40 142.43 3.14 o -10 4 2 54.60 55.08 1.56 o -9 4 2 79.51 83.23 1.86 o -8 4 2 5.53 5.95 0.50 o -7 4 2 0.36 1.01 0.53 o -6 4 2 145.74 173.91 3.56 o -5 4 2 112.21 126.72 2.51 o -4 4 2 76.03 86.88 1.80 o -3 4 2 18.81 20.16 0.70 o -2 4 2 7.41 11.49 0.47 o -1 4 2 0.58 1.08 0.50 o 0 4 2 3.99 4.22 0.34 o 1 4 2 87.32 72.82 1.41 o 2 4 2 58.29 59.83 1.40 o 3 4 2 1135.99 1116.25 20.97 o 4 4 2 40.03 38.84 1.18 o 5 4 2 19.78 18.96 0.86 o 6 4 2 82.88 83.77 2.16 o 7 4 2 303.40 324.51 6.52 o 8 4 2 44.35 48.13 1.42 o 9 4 2 8.76 8.89 0.60 o 10 4 2 16.41 15.57 0.76 o 11 4 2 40.00 33.09 1.09 o 12 4 2 9.66 7.55 0.59 o -11 5 2 58.39 66.95 1.82 o -10 5 2 2.89 2.25 0.43 o -9 5 2 37.73 40.16 1.55 o -8 5 2 88.09 90.71 2.30 o -7 5 2 1.26 1.99 0.48 o -6 5 2 0.48 2.30 0.47 o -5 5 2 48.94 52.71 1.46 o -4 5 2 191.50 212.34 3.97 o -3 5 2 13.39 17.89 0.85 o -2 5 2 196.53 200.11 4.18 o -1 5 2 238.27 243.15 4.99 o 0 5 2 22.50 23.12 0.91 o 1 5 2 3.19 4.13 0.53 o 2 5 2 146.09 151.71 4.06 o 3 5 2 1341.19 1374.86 29.91 o 4 5 2 21.32 21.51 1.00 o 5 5 2 333.00 355.13 8.58 o 6 5 2 26.84 27.72 1.34 o 7 5 2 3.68 5.37 0.63 o 8 5 2 23.25 24.00 1.13 o 9 5 2 5.80 6.58 0.55 o 10 5 2 230.63 223.06 5.50 o -8 6 2 1.70 2.32 0.65 o -7 6 2 21.13 21.20 1.03 o -6 6 2 22.03 26.04 1.43 o -5 6 2 2.06 1.79 0.47 o -4 6 2 19.06 20.37 0.99 o -3 6 2 23.10 27.91 2.04 o -2 6 2 21.75 21.57 1.02 o -1 6 2 99.17 95.83 6.01 o 0 6 2 314.73 286.42 14.06 o 1 6 2 2.31 2.54 0.66 o 2 6 2 21.33 18.88 1.06 o 3 6 2 49.34 46.54 1.91 o 4 6 2 42.62 47.51 2.28 o 5 6 2 55.60 64.12 2.88 o 6 6 2 10.83 10.56 0.75 o 7 6 2 171.76 144.43 5.21 o -17 1 3 28.39 31.02 2.49 o -16 1 3 78.37 75.34 2.98 o -15 1 3 0.15 1.56 0.52 o -14 1 3 102.72 112.36 2.95 o -13 1 3 107.38 107.52 2.85 o -12 1 3 267.84 270.23 6.97 o -11 1 3 12.03 13.81 2.39 o -10 1 3 427.96 390.85 12.96 o -9 1 3 560.29 502.77 13.01 o -8 1 3 386.88 354.66 7.64 o -7 1 3 691.05 626.66 17.74 o -6 1 3 109.52 143.28 3.19 o -5 1 3 245.69 288.23 5.56 o -4 1 3 1613.00 1676.89 36.52 o -3 1 3 5614.72 5454.64 101.04 o -2 1 3 434.76 452.91 8.50 o -1 1 3 487.93 537.61 11.78 o 0 1 3 2405.08 2589.18 56.27 o 1 1 3 574.56 598.84 13.18 o 2 1 3 535.32 586.06 14.33 o 3 1 3 456.77 524.40 16.91 o 4 1 3 734.73 722.62 24.13 o 5 1 3 280.08 246.50 12.43 o 6 1 3 990.49 974.19 20.29 o 7 1 3 3.50 10.25 0.63 o 8 1 3 536.86 524.92 10.28 o 9 1 3 81.04 80.79 1.95 o 10 1 3 46.26 45.29 1.69 o 11 1 3 117.16 120.57 3.51 o 12 1 3 16.85 15.04 0.99 o 13 1 3 25.59 29.08 1.60 o 14 1 3 12.74 14.05 0.78 o -16 2 3 4.23 3.79 0.60 o -15 2 3 60.24 56.07 2.86 o -14 2 3 74.95 74.97 2.41 o -13 2 3 7.08 6.81 0.61 o -12 2 3 458.68 502.70 10.26 o -11 2 3 506.09 517.32 9.45 o -10 2 3 496.41 497.45 9.07 o -9 2 3 27.59 19.87 0.69 o -8 2 3 1235.78 1154.04 18.34 o -7 2 3 913.81 834.08 13.34 o -6 2 3 664.54 681.28 13.53 o -5 2 3 104.94 83.27 2.94 o -4 2 3 61.84 57.78 1.46 o -3 2 3 48.17 45.32 1.02 o -2 2 3 100.34 108.47 2.12 o -1 2 3 821.45 769.13 14.39 o 0 2 3 67.97 66.47 1.49 o 1 2 3 0.49 -0.24 0.24 o 2 2 3 754.41 724.28 15.12 o 3 2 3 4416.33 4331.77 197.90 o 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