#------------------------------------------------------------------------------ #$Date: 2016-04-06 16:35:31 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181869 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/99/2019963.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2019963 _cell_angle_alpha 94.385 _cell_angle_beta 97.292 _cell_angle_gamma 101.074 _cell_length_a 12.3059 _cell_length_b 12.3943 _cell_length_c 20.4500 _exptl_crystal_F_000 1252.00 _reflns_d_resolution_high 0.7486 _cod_data_source_file bg2554mol-1sup2.hkl _cod_data_source_block mol-1 #BEGIN Tags that were not found in dictionaries: _shelx_title ' mol_1 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 283.27 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 970.46 685.22 19.81 o 2 0 0 569.52 512.72 15.37 o 3 0 0 1100.21 1283.17 64.02 o 4 0 0 10882.41 10506.25 152.76 o 5 0 0 183.12 255.65 20.15 o 6 0 0 595.81 613.60 18.71 o 7 0 0 109.31 117.05 9.76 o 8 0 0 1479.05 1510.06 29.52 o 9 0 0 181.55 151.07 12.05 o 10 0 0 823.25 779.65 22.36 o 11 0 0 0.24 -10.53 10.53 o 12 0 0 12.45 -11.45 11.45 o 13 0 0 182.26 164.48 18.99 o 14 0 0 17.70 1.62 24.02 o 15 0 0 110.33 74.71 20.97 o -16 1 0 17.33 35.46 21.08 o -15 1 0 37.46 42.16 19.71 o -14 1 0 111.42 132.79 19.89 o -13 1 0 111.62 97.36 13.92 o -12 1 0 38.27 39.17 12.45 o -11 1 0 93.90 62.87 11.67 o -10 1 0 37.82 40.88 10.19 o -9 1 0 9.40 6.55 8.61 o -8 1 0 50.48 55.49 8.84 o -7 1 0 1237.47 1326.64 25.76 o -6 1 0 181.77 183.64 21.98 o -5 1 0 661.66 724.38 15.95 o -4 1 0 1409.39 1389.84 26.31 o -3 1 0 3781.85 3841.44 108.08 o -2 1 0 1294.39 1180.86 53.17 o -1 1 0 211.43 214.70 9.66 o 0 1 0 434.44 302.34 8.59 o 1 1 0 10051.79 9600.57 156.40 o 2 1 0 2.05 11.67 3.79 o 3 1 0 9587.71 9610.11 193.58 o 4 1 0 597.17 531.41 33.66 o 5 1 0 266.75 403.96 12.05 o 6 1 0 1825.22 1973.00 34.44 o 7 1 0 2238.41 2421.56 41.75 o 8 1 0 82.07 78.86 9.83 o 9 1 0 1296.76 1305.33 28.15 o 10 1 0 274.82 253.77 17.00 o 11 1 0 477.73 447.69 18.24 o 12 1 0 134.93 147.88 14.40 o 13 1 0 287.44 323.94 24.81 o 14 1 0 62.49 80.00 20.24 o 15 1 0 2.87 -18.75 19.33 o -16 2 0 790.48 943.33 39.84 o -15 2 0 37.13 33.15 33.27 o -14 2 0 10.46 -5.16 14.70 o -13 2 0 290.37 268.72 18.57 o -12 2 0 0.71 -8.74 14.34 o -11 2 0 136.63 103.58 11.98 o -10 2 0 7.10 8.30 10.58 o -9 2 0 3.31 -8.33 8.33 o -8 2 0 286.56 300.34 13.11 o -7 2 0 3.08 6.53 8.65 o -6 2 0 47.99 47.90 6.89 o -5 2 0 6697.41 6651.27 98.74 o -4 2 0 281.85 255.07 12.34 o -3 2 0 13.51 24.02 18.20 o -2 2 0 0.36 0.80 7.41 o -1 2 0 11785.97 12719.27 188.77 o 0 2 0 2848.92 2845.08 64.05 o 1 2 0 2594.86 2706.54 40.94 o 2 2 0 53822.07 54560.54 808.95 o 3 2 0 970.37 1105.05 19.94 o 4 2 0 12535.60 13356.92 196.81 o 5 2 0 5578.75 5821.62 89.05 o 6 2 0 692.28 641.38 17.72 o 7 2 0 31.92 43.29 8.32 o 8 2 0 36.42 43.49 8.90 o 9 2 0 575.80 615.48 19.37 o 10 2 0 142.22 133.31 12.16 o 11 2 0 63.13 47.10 11.86 o 12 2 0 3.29 4.46 15.20 o 13 2 0 0.93 -16.53 16.53 o 14 2 0 2.96 0.41 18.97 o 15 2 0 80.00 68.30 31.31 o -16 3 0 39.25 40.60 30.53 o -15 3 0 328.13 360.07 22.76 o -14 3 0 319.11 306.11 19.71 o -13 3 0 242.54 220.53 28.50 o -12 3 0 0.26 -11.66 14.11 o -11 3 0 48.73 43.53 10.96 o -10 3 0 37.36 50.17 12.23 o -9 3 0 278.97 277.82 14.35 o -8 3 0 2.42 1.37 8.59 o -7 3 0 125.63 108.70 9.25 o -6 3 0 81.27 74.86 7.74 o -5 3 0 506.46 475.35 22.38 o -4 3 0 1097.33 1253.48 21.89 o -3 3 0 41.63 64.17 10.17 o -2 3 0 983.50 956.15 34.87 o -1 3 0 112.02 111.17 5.81 o 0 3 0 75.82 73.66 5.77 o 1 3 0 1492.88 1589.42 26.00 o 2 3 0 7562.01 7374.24 108.27 o 3 3 0 4194.78 4412.42 67.04 o 4 3 0 3852.28 4280.92 66.03 o 5 3 0 2790.89 2894.60 47.15 o 6 3 0 1272.51 1217.47 24.35 o 7 3 0 322.23 324.67 14.97 o 8 3 0 162.46 155.42 15.68 o 9 3 0 91.81 99.93 11.00 o 10 3 0 22.69 34.68 10.39 o 11 3 0 444.18 410.47 25.21 o 12 3 0 5.31 15.18 17.29 o 13 3 0 5.07 8.29 16.78 o 14 3 0 472.70 550.31 33.84 o 15 3 0 5.23 36.88 25.13 o -16 4 0 202.95 216.63 27.37 o -15 4 0 1.31 -30.72 38.06 o -14 4 0 10.51 -6.07 13.47 o -13 4 0 30.64 32.49 21.37 o -12 4 0 459.69 419.91 19.18 o -11 4 0 393.39 420.77 17.59 o -10 4 0 78.89 81.27 10.33 o -9 4 0 161.75 139.24 22.46 o -8 4 0 88.71 131.86 11.00 o -7 4 0 15.34 26.78 6.94 o -6 4 0 836.88 871.24 18.58 o -5 4 0 0.21 14.42 8.37 o -4 4 0 310.01 351.32 20.30 o -3 4 0 4708.80 4953.36 95.26 o -2 4 0 3156.94 3326.42 50.74 o -1 4 0 3192.96 3319.80 50.62 o 0 4 0 3109.17 3107.96 47.86 o 1 4 0 94.86 93.17 7.09 o 2 4 0 7003.86 6852.93 101.64 o 3 4 0 1316.34 1259.49 29.00 o 4 4 0 875.56 1044.95 23.31 o 5 4 0 416.80 420.39 14.94 o 6 4 0 90.01 118.36 9.19 o 7 4 0 1246.21 1230.91 26.00 o 8 4 0 83.33 114.85 10.80 o 9 4 0 86.50 75.70 20.22 o 10 4 0 51.55 56.65 15.21 o 11 4 0 88.64 77.25 18.49 o 12 4 0 357.45 383.13 27.50 o 13 4 0 6.50 -18.06 19.06 o 14 4 0 142.04 136.81 24.34 o -16 5 0 32.18 6.17 21.96 o -15 5 0 477.40 502.79 33.61 o -14 5 0 52.05 49.86 44.89 o -13 5 0 379.02 340.26 26.16 o -12 5 0 58.39 69.54 11.81 o -11 5 0 1.97 8.47 9.54 o -10 5 0 1137.32 1021.65 33.02 o -9 5 0 341.64 368.50 14.67 o -8 5 0 557.02 545.43 15.85 o -7 5 0 323.74 294.47 44.28 o -6 5 0 357.85 278.97 14.25 o -5 5 0 33.61 33.36 4.29 o -4 5 0 238.65 294.04 21.85 o -3 5 0 279.32 228.35 12.98 o -2 5 0 1005.76 831.83 20.82 o -1 5 0 196.62 169.33 8.10 o 0 5 0 983.34 1004.28 19.36 o 1 5 0 1993.12 1982.14 33.34 o 2 5 0 3646.87 3925.38 60.98 o 3 5 0 4239.49 4486.72 83.71 o 4 5 0 3900.81 3889.00 61.83 o 5 5 0 2391.46 2576.92 44.01 o 6 5 0 145.39 137.29 13.88 o 7 5 0 19.76 5.98 7.45 o 8 5 0 38.78 57.14 12.72 o 9 5 0 102.80 86.21 24.39 o 10 5 0 11.97 -5.09 16.08 o 11 5 0 73.77 53.40 22.75 o 12 5 0 0.40 -17.80 18.18 o 13 5 0 1175.22 1246.23 45.08 o 14 5 0 193.48 186.28 28.89 o -16 6 0 108.46 58.40 26.68 o -15 6 0 11.49 17.05 20.98 o -14 6 0 61.32 112.22 22.18 o -13 6 0 89.51 81.53 20.19 o -12 6 0 22.42 9.36 30.12 o -11 6 0 546.24 555.19 19.68 o -10 6 0 1314.07 1269.54 28.31 o -9 6 0 479.93 462.14 19.70 o -8 6 0 1205.12 1199.02 25.23 o -7 6 0 122.29 135.92 8.48 o -6 6 0 2.62 0.93 10.38 o -5 6 0 55.99 40.43 13.01 o -4 6 0 2084.64 2219.29 49.73 o -3 6 0 275.66 257.08 7.84 o -2 6 0 2909.63 3067.59 48.45 o -1 6 0 458.48 373.40 11.26 o 0 6 0 8709.36 8857.18 130.90 o 1 6 0 2447.34 2710.89 44.54 o 2 6 0 5711.61 5851.06 89.13 o 3 6 0 907.71 806.06 18.72 o 4 6 0 352.07 363.65 12.92 o 5 6 0 25.21 16.13 7.47 o 6 6 0 305.16 346.95 16.11 o 7 6 0 102.28 104.44 10.46 o 8 6 0 1128.84 990.04 33.79 o 9 6 0 0.13 4.77 26.85 o 10 6 0 276.77 269.05 25.32 o 11 6 0 745.84 753.79 35.01 o 12 6 0 569.62 575.49 33.13 o 13 6 0 186.93 185.71 25.29 o -15 7 0 20.65 25.02 20.48 o -14 7 0 104.06 79.09 21.38 o -13 7 0 124.13 105.98 19.96 o -12 7 0 311.73 305.47 30.90 o -11 7 0 5.87 10.53 15.08 o -10 7 0 260.82 255.32 21.97 o -9 7 0 1555.70 1536.94 43.74 o -8 7 0 532.89 488.48 25.03 o -7 7 0 739.52 619.18 25.94 o -6 7 0 118.56 118.15 16.61 o -5 7 0 304.46 254.56 16.97 o -4 7 0 20.31 1.11 9.63 o -3 7 0 1.57 -4.23 4.66 o -2 7 0 165.60 146.56 8.82 o -1 7 0 363.65 374.81 12.08 o 0 7 0 328.64 248.89 12.27 o 1 7 0 508.33 440.49 13.99 o 2 7 0 289.15 240.05 12.12 o 3 7 0 880.54 817.33 20.11 o 4 7 0 31.60 29.73 8.05 o 5 7 0 4.24 5.27 8.18 o 6 7 0 2254.70 2268.11 42.06 o 7 7 0 257.23 249.90 22.51 o 8 7 0 293.51 346.51 24.29 o 9 7 0 143.02 154.02 19.75 o 10 7 0 0.13 12.87 25.95 o 11 7 0 11.97 18.98 18.69 o 12 7 0 47.38 46.22 20.51 o 13 7 0 31.92 33.85 23.52 o -15 8 0 13.30 2.69 32.66 o -14 8 0 93.79 56.41 21.85 o -13 8 0 78.17 87.22 20.50 o -12 8 0 204.70 172.16 27.75 o -11 8 0 22.55 30.18 16.32 o -10 8 0 222.91 216.84 22.65 o -9 8 0 9.42 13.53 13.99 o -8 8 0 1700.90 1513.79 43.04 o -7 8 0 1.09 -12.24 12.29 o -6 8 0 0.58 0.38 12.73 o -5 8 0 47.54 30.68 18.09 o -4 8 0 91.15 79.23 12.76 o -3 8 0 105.22 127.38 8.20 o -2 8 0 1085.27 1033.37 24.97 o -1 8 0 2359.67 2539.70 43.09 o 0 8 0 160.92 125.21 9.81 o 1 8 0 410.10 326.64 13.31 o 2 8 0 133.18 150.76 15.88 o 3 8 0 155.54 136.08 11.47 o 4 8 0 3112.01 3067.46 96.15 o 5 8 0 299.07 319.72 15.78 o 6 8 0 5.48 16.89 13.86 o 7 8 0 520.09 521.07 27.79 o 8 8 0 1325.40 1290.61 41.72 o 9 8 0 0.09 -7.01 15.91 o 10 8 0 0.19 -12.96 34.70 o 11 8 0 96.43 82.90 21.33 o 12 8 0 257.73 315.59 31.14 o -15 9 0 353.56 414.30 71.49 o -14 9 0 153.92 154.54 24.03 o -13 9 0 39.04 18.21 18.64 o -12 9 0 163.83 198.85 23.55 o -11 9 0 7.33 -6.56 16.39 o -10 9 0 349.46 350.47 25.93 o -9 9 0 56.13 60.68 15.87 o -8 9 0 1284.22 1184.69 38.27 o -7 9 0 168.69 137.44 29.06 o -6 9 0 530.32 520.04 25.72 o -5 9 0 6.46 3.85 13.13 o -4 9 0 931.22 924.71 75.67 o -3 9 0 900.14 848.97 37.26 o -2 9 0 17.97 23.86 7.68 o -1 9 0 267.83 248.09 14.02 o 0 9 0 791.25 770.13 20.02 o 1 9 0 8.43 -3.43 8.07 o 2 9 0 0.67 9.46 8.72 o 3 9 0 215.10 236.16 14.57 o 4 9 0 452.67 455.52 20.75 o 5 9 0 5.36 10.59 10.12 o 6 9 0 205.51 206.59 23.00 o 7 9 0 417.85 405.17 52.91 o 8 9 0 39.51 57.28 19.06 o 9 9 0 56.13 67.63 24.92 o 10 9 0 55.32 28.83 20.24 o 11 9 0 121.14 113.33 25.13 o -14 10 0 61.61 45.67 30.37 o -13 10 0 419.40 511.05 33.14 o -12 10 0 714.70 670.97 34.96 o -11 10 0 427.99 425.53 28.52 o -10 10 0 70.47 39.11 16.65 o -9 10 0 194.60 190.76 22.06 o -8 10 0 595.40 561.98 29.50 o -7 10 0 691.64 656.34 28.86 o -6 10 0 942.54 831.92 42.48 o -5 10 0 3.24 -12.49 12.49 o -4 10 0 6.43 18.05 12.86 o -3 10 0 0.06 4.09 9.01 o -2 10 0 160.65 156.69 11.58 o -1 10 0 19.22 15.53 9.06 o 0 10 0 94.55 88.59 10.50 o 1 10 0 97.23 110.70 11.38 o 2 10 0 1277.92 1388.47 30.69 o 3 10 0 11.79 13.62 9.75 o 4 10 0 53.93 50.94 11.88 o 5 10 0 405.20 356.11 50.79 o 6 10 0 136.69 149.36 47.35 o 7 10 0 38.36 67.37 23.94 o 8 10 0 550.58 537.61 31.96 o 9 10 0 208.09 217.60 31.10 o 10 10 0 609.97 591.55 35.44 o -14 11 0 45.86 21.17 33.68 o -13 11 0 42.71 15.73 21.65 o -12 11 0 93.85 104.38 22.93 o -11 11 0 61.65 68.27 21.12 o -10 11 0 244.85 265.42 26.56 o -9 11 0 324.98 254.52 25.50 o -8 11 0 10.64 24.82 38.63 o -7 11 0 7.26 48.57 16.91 o -6 11 0 14.79 29.14 22.92 o -5 11 0 37.68 36.27 15.64 o -4 11 0 488.44 460.51 73.87 o -3 11 0 4.07 8.00 13.10 o -2 11 0 87.77 81.75 10.38 o -1 11 0 31.84 28.81 10.86 o 0 11 0 90.45 98.68 11.21 o 1 11 0 1366.08 1319.11 29.81 o 2 11 0 1730.68 1759.04 36.57 o 3 11 0 45.68 64.27 15.01 o 4 11 0 165.98 171.33 19.90 o 5 11 0 897.53 876.99 45.30 o 6 11 0 670.77 677.18 32.41 o 7 11 0 12.26 16.98 20.13 o 8 11 0 37.68 19.80 20.94 o 9 11 0 814.83 868.58 107.96 o -13 12 0 6.00 17.29 22.42 o -12 12 0 32.20 38.11 21.43 o -11 12 0 2.03 10.96 20.30 o -10 12 0 747.89 704.45 35.83 o -9 12 0 5.98 2.58 16.81 o -8 12 0 7.00 13.80 16.03 o -7 12 0 1541.15 1434.17 45.81 o -6 12 0 556.37 565.65 30.06 o -5 12 0 78.13 78.69 17.30 o -4 12 0 111.48 84.35 17.33 o -3 12 0 11.14 10.56 14.68 o -2 12 0 31.26 18.42 15.35 o -1 12 0 163.43 173.91 14.75 o 0 12 0 62.97 66.41 15.90 o 1 12 0 140.82 183.47 15.85 o 2 12 0 877.69 866.40 25.09 o 3 12 0 37.09 58.06 18.60 o 4 12 0 14.21 39.80 22.26 o 5 12 0 71.80 85.18 19.81 o 6 12 0 70.24 91.13 20.87 o 7 12 0 20.04 24.29 25.45 o 8 12 0 25.52 21.61 22.51 o -12 13 0 21.62 44.45 22.30 o -11 13 0 871.21 985.78 44.50 o -10 13 0 68.77 44.74 39.94 o -9 13 0 511.38 497.35 35.93 o -8 13 0 71.81 84.14 21.12 o -7 13 0 48.43 61.59 19.07 o -6 13 0 9.45 8.71 16.33 o -5 13 0 584.17 606.63 50.25 o -4 13 0 263.92 203.67 22.63 o -3 13 0 33.30 16.34 16.11 o -2 13 0 129.17 122.61 19.42 o -1 13 0 3.59 17.29 18.50 o 0 13 0 315.04 316.12 30.35 o 1 13 0 50.60 49.51 23.54 o 2 13 0 380.46 418.39 34.18 o 3 13 0 855.86 959.37 36.24 o 4 13 0 79.22 66.39 22.47 o 5 13 0 105.53 161.34 23.49 o 6 13 0 0.21 32.92 21.75 o 7 13 0 100.20 62.03 23.60 o -11 14 0 134.18 144.98 26.09 o -10 14 0 138.64 155.62 25.24 o -9 14 0 33.69 51.81 20.31 o -8 14 0 0.03 -1.76 17.84 o -7 14 0 1.80 -8.44 26.80 o -6 14 0 264.83 274.97 27.57 o -5 14 0 296.16 257.20 25.36 o -4 14 0 221.16 212.03 25.21 o -3 14 0 95.75 102.65 19.85 o -2 14 0 273.30 368.45 28.29 o -1 14 0 451.22 506.42 30.06 o 0 14 0 18.36 40.80 18.37 o 1 14 0 114.80 115.08 19.82 o 2 14 0 25.20 20.62 17.79 o 3 14 0 86.09 68.07 32.66 o 4 14 0 1265.68 1345.76 48.00 o 5 14 0 439.69 466.07 33.83 o -9 15 0 6.59 13.00 20.89 o -8 15 0 260.09 340.65 31.84 o -7 15 0 246.93 297.45 44.20 o -6 15 0 0.52 10.54 19.07 o -5 15 0 280.74 269.60 28.31 o -4 15 0 208.28 161.16 23.19 o -3 15 0 51.89 47.96 19.60 o -2 15 0 214.05 242.56 34.95 o -1 15 0 10.35 12.85 27.58 o 0 15 0 32.53 93.87 22.30 o 1 15 0 0.18 -9.74 30.28 o 2 15 0 47.84 33.64 33.23 o 3 15 0 12.93 17.84 37.57 o -7 16 0 113.81 139.19 25.06 o -6 16 0 56.44 81.31 23.08 o -5 16 0 56.13 85.30 22.67 o -4 16 0 22.23 44.76 20.58 o -3 16 0 68.01 101.92 32.53 o -2 16 0 35.52 77.78 22.65 o -1 16 0 53.23 76.16 22.45 o 0 16 0 0.81 -16.78 29.30 o 0 -16 1 18.59 30.31 31.06 o 1 -16 1 27.71 69.87 22.37 o 2 -16 1 23.92 53.11 21.67 o 3 -16 1 65.59 119.78 23.48 o 4 -16 1 4.49 9.49 20.23 o 5 -16 1 30.59 3.58 21.44 o 6 -16 1 281.97 365.59 35.44 o 7 -16 1 18.88 22.23 20.38 o -3 -15 1 87.57 86.43 37.32 o -2 -15 1 124.69 156.41 37.73 o -1 -15 1 24.62 64.39 20.10 o 0 -15 1 13.64 19.73 20.87 o 1 -15 1 35.66 36.73 18.53 o 2 -15 1 344.80 391.66 30.08 o 3 -15 1 5.16 -3.99 17.91 o 4 -15 1 166.44 220.47 32.37 o 5 -15 1 59.33 69.67 30.45 o 6 -15 1 616.82 598.53 35.73 o 7 -15 1 8.62 30.40 19.78 o 8 -15 1 126.93 154.35 24.92 o 9 -15 1 4.24 24.79 22.67 o -5 -14 1 103.26 175.80 26.05 o -4 -14 1 248.71 347.08 52.55 o -3 -14 1 88.94 111.22 32.66 o -2 -14 1 646.23 610.70 50.54 o -1 -14 1 170.32 254.61 46.61 o 0 -14 1 5.00 33.22 18.25 o 1 -14 1 579.78 651.12 31.59 o 2 -14 1 24.99 47.20 31.51 o 3 -14 1 361.43 378.13 28.63 o 4 -14 1 46.22 48.41 18.25 o 5 -14 1 670.74 799.00 58.68 o 6 -14 1 1.41 26.61 18.34 o 7 -14 1 98.94 74.90 19.51 o 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