data_2019987 _cell_angle_alpha 90.000 _cell_angle_beta 99.806 _cell_angle_gamma 90.000 _cell_length_a 11.7178 _cell_length_b 8.2765 _cell_length_c 37.4040 _exptl_crystal_F_000 1795.65 _reflns_d_resolution_high 0.7685 _cod_data_source_file yf3088zl9sup2.hkl _cod_data_source_block zl9 _shelx_title ' zl9 in P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 326.14 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1894.00 1624.32 30.83 o 3 0 0 41001.79 37894.71 739.52 o 4 0 0 634.03 636.63 13.98 o 5 0 0 19727.34 21420.53 315.07 o 6 0 0 92.48 151.35 7.72 o 7 0 0 16.69 22.57 5.58 o 8 0 0 1108.41 1278.58 28.51 o 9 0 0 426.43 418.11 15.78 o 10 0 0 974.42 1022.55 33.73 o 11 0 0 3153.02 3370.49 144.11 o 12 0 0 6.26 24.43 20.15 o 13 0 0 402.54 370.95 55.98 o 14 0 0 2.76 5.45 34.39 o 15 0 0 371.73 377.38 75.68 o 1 1 0 3.70 -1.73 1.73 o 2 1 0 53628.82 50761.99 524.62 o 3 1 0 12336.01 12443.02 175.02 o 4 1 0 135.18 124.93 4.72 o 5 1 0 3.06 20.92 3.13 o 6 1 0 9398.54 9873.52 123.11 o 7 1 0 925.59 911.50 14.25 o 8 1 0 536.75 584.91 11.80 o 9 1 0 2694.92 2697.91 54.80 o 10 1 0 1.35 0.94 8.01 o 11 1 0 283.98 314.14 18.30 o 12 1 0 960.03 1050.59 50.38 o 13 1 0 192.53 223.05 21.25 o 14 1 0 92.07 129.05 36.74 o 0 2 0 479.98 609.09 13.29 o 1 2 0 218.31 211.41 9.08 o 2 2 0 15313.87 15921.80 189.79 o 3 2 0 46380.64 48082.27 541.82 o 4 2 0 3210.57 3241.31 38.59 o 5 2 0 696.25 697.53 11.77 o 6 2 0 659.98 547.32 10.16 o 7 2 0 409.81 481.26 13.15 o 8 2 0 6.41 15.72 5.17 o 9 2 0 191.56 201.97 12.11 o 10 2 0 68.30 79.13 10.76 o 11 2 0 94.48 84.12 15.21 o 12 2 0 1143.71 1145.87 42.27 o 13 2 0 176.06 181.14 22.80 o 14 2 0 4.57 44.40 37.30 o 1 3 0 929.14 958.01 14.70 o 2 3 0 8045.03 8730.72 93.80 o 3 3 0 4507.96 4547.22 51.11 o 4 3 0 2652.19 2243.48 27.64 o 5 3 0 7667.15 8504.25 92.33 o 6 3 0 5258.93 5321.00 60.13 o 7 3 0 908.27 943.18 15.86 o 8 3 0 320.84 296.74 10.83 o 9 3 0 1179.11 1264.11 25.41 o 10 3 0 114.87 94.55 14.06 o 11 3 0 11.51 36.42 15.60 o 12 3 0 456.33 486.02 26.54 o 13 3 0 88.45 114.56 22.07 o 14 3 0 66.98 67.23 34.33 o 0 4 0 71.09 81.50 9.08 o 1 4 0 522.60 510.07 11.33 o 2 4 0 172.53 161.63 6.60 o 3 4 0 7913.65 8245.31 91.40 o 4 4 0 1540.78 1795.05 24.38 o 5 4 0 28.37 55.34 5.01 o 6 4 0 0.14 8.10 6.79 o 7 4 0 446.57 410.56 11.98 o 8 4 0 155.15 164.94 11.02 o 9 4 0 218.24 243.93 16.22 o 10 4 0 14.34 -1.05 18.71 o 11 4 0 0.34 -6.26 13.76 o 12 4 0 58.99 59.94 26.52 o 13 4 0 107.08 110.17 23.11 o 1 5 0 1.21 0.22 4.97 o 2 5 0 79.75 85.01 6.28 o 3 5 0 200.52 207.97 8.99 o 4 5 0 2552.43 2481.13 33.16 o 5 5 0 7657.39 7738.39 99.75 o 6 5 0 597.57 561.56 13.62 o 7 5 0 299.07 284.93 12.30 o 8 5 0 38.77 58.55 24.00 o 9 5 0 848.88 725.98 27.14 o 10 5 0 721.76 690.97 26.87 o 11 5 0 96.77 76.19 18.51 o 12 5 0 5.50 -3.36 37.82 o 13 5 0 359.17 286.64 31.26 o 0 6 0 3.60 -0.41 8.96 o 1 6 0 1437.68 1474.84 23.63 o 2 6 0 387.28 382.90 14.89 o 3 6 0 8.80 15.75 6.69 o 4 6 0 1197.13 1117.87 20.38 o 5 6 0 122.31 150.36 9.50 o 6 6 0 3354.69 3262.21 55.78 o 7 6 0 1225.03 1232.54 32.60 o 8 6 0 286.46 237.13 27.68 o 9 6 0 106.16 107.65 15.45 o 10 6 0 54.17 77.04 21.60 o 11 6 0 276.27 290.04 22.97 o 12 6 0 284.14 304.88 47.94 o 1 7 0 749.31 734.59 24.06 o 2 7 0 31.17 45.09 8.73 o 3 7 0 273.32 284.01 13.08 o 4 7 0 2.47 17.40 8.20 o 5 7 0 86.94 84.91 10.39 o 6 7 0 5.72 3.48 9.88 o 7 7 0 298.04 307.43 24.83 o 8 7 0 1260.83 1136.21 36.96 o 9 7 0 180.90 172.22 18.57 o 10 7 0 20.74 56.24 28.73 o 11 7 0 67.61 109.34 37.28 o 0 8 0 112.47 109.06 16.33 o 1 8 0 1446.81 1492.00 39.09 o 2 8 0 1419.53 1367.98 29.62 o 3 8 0 639.86 633.84 20.95 o 4 8 0 336.09 354.67 19.90 o 5 8 0 25.88 44.33 11.82 o 6 8 0 9.58 9.10 16.16 o 7 8 0 0.07 -18.42 18.42 o 8 8 0 136.39 159.92 36.36 o 9 8 0 12.01 32.28 42.35 o 10 8 0 154.76 48.73 137.89 o 1 9 0 95.96 88.70 15.06 o 2 9 0 1.36 -8.00 19.60 o 3 9 0 4.02 -19.72 22.80 o 4 9 0 403.45 403.86 50.94 o 5 9 0 2.04 9.99 28.96 o 6 9 0 67.97 -34.42 34.42 o 7 9 0 191.67 120.27 32.98 o 8 9 0 147.04 187.75 60.90 o 0 10 0 14.73 43.54 101.60 o 1 10 0 1.58 -1.42 41.72 o 2 10 0 118.81 92.11 31.38 o 3 10 0 1.23 19.71 31.05 o 4 10 0 396.22 348.20 39.70 o 5 10 0 236.55 102.84 36.47 o -15 1 1 113.27 49.76 85.01 o -14 1 1 8.54 24.29 38.51 o -13 1 1 1462.65 1558.39 43.60 o -12 1 1 183.85 202.84 20.14 o -11 1 1 4.46 0.67 11.04 o -10 1 1 1394.68 1460.28 27.78 o -9 1 1 122.05 146.02 7.85 o -8 1 1 657.88 661.83 13.54 o -7 1 1 3263.29 3346.74 49.75 o -6 1 1 73.82 94.29 4.55 o -5 1 1 810.60 743.95 10.97 o -4 1 1 1045.48 891.31 12.82 o -3 1 1 29890.39 31325.25 468.08 o -2 1 1 235.78 180.09 3.99 o -1 1 1 19910.22 19830.98 348.53 o 0 1 1 9020.31 9345.24 120.72 o 1 1 1 659.82 595.71 8.63 o 2 1 1 57987.86 51935.94 569.96 o 3 1 1 3357.77 3751.90 49.46 o 4 1 1 3146.90 3009.26 37.14 o 5 1 1 13599.76 14908.82 155.64 o 6 1 1 4198.97 4052.03 45.68 o 7 1 1 464.66 432.27 9.51 o 8 1 1 3319.38 3307.45 45.23 o 9 1 1 96.82 84.59 7.77 o 10 1 1 81.85 82.80 11.40 o 11 1 1 799.94 758.57 27.25 o 12 1 1 196.42 253.20 19.27 o 13 1 1 135.40 173.20 20.93 o 14 1 1 47.66 84.84 27.28 o -14 2 1 73.22 134.78 25.35 o -13 2 1 92.94 89.05 18.93 o -12 2 1 62.77 62.82 19.47 o -11 2 1 336.70 364.76 25.41 o -10 2 1 34.61 34.29 9.83 o -9 2 1 2721.54 2766.42 40.76 o -8 2 1 18.19 16.85 4.96 o -7 2 1 5.66 13.11 4.48 o -6 2 1 356.95 345.09 8.44 o -5 2 1 10212.63 11103.14 117.69 o -4 2 1 4955.01 4608.60 50.69 o -2 2 1 12471.88 13609.96 155.54 o -1 2 1 101681.76 92767.51 1437.75 o 0 2 1 5139.05 5640.92 62.89 o 1 2 1 214.04 294.84 5.96 o 2 2 1 106367.41 100000.06 1182.32 o 3 2 1 3256.96 3376.16 43.27 o 4 2 1 1350.70 1212.67 16.95 o 5 2 1 114.82 129.13 5.31 o 6 2 1 4286.13 4164.16 47.54 o 7 2 1 1080.92 1169.50 18.30 o 8 2 1 2058.29 2045.72 40.51 o 9 2 1 380.53 339.48 12.94 o 10 2 1 68.03 54.99 17.66 o 11 2 1 630.91 632.86 27.62 o 12 2 1 38.35 97.02 15.11 o 13 2 1 41.27 64.52 21.56 o 14 2 1 188.34 193.31 26.99 o -14 3 1 124.87 121.31 30.48 o -13 3 1 37.21 69.22 22.11 o -12 3 1 48.02 69.04 16.46 o -11 3 1 568.43 500.71 28.47 o -10 3 1 0.21 19.92 11.46 o -9 3 1 217.46 219.24 11.22 o -8 3 1 1047.61 958.38 19.41 o -7 3 1 497.82 495.84 16.56 o -6 3 1 1467.00 1405.35 20.91 o -5 3 1 15.62 15.93 3.28 o -4 3 1 2697.30 2849.05 33.75 o -3 3 1 10103.19 10368.98 110.58 o -2 3 1 311.37 419.78 8.37 o -1 3 1 3695.29 3714.76 42.28 o 0 3 1 1.85 0.07 2.67 o 1 3 1 1745.27 1518.71 22.03 o 2 3 1 3349.69 3194.18 37.14 o 3 3 1 1949.16 1782.49 24.01 o 4 3 1 5716.00 5855.05 68.15 o 5 3 1 648.97 517.42 14.09 o 6 3 1 829.91 852.12 14.93 o 7 3 1 214.97 168.75 7.16 o 8 3 1 545.97 531.13 13.57 o 9 3 1 238.78 232.42 14.22 o 10 3 1 114.10 81.37 13.73 o 11 3 1 7.01 -2.35 19.08 o 12 3 1 306.97 319.76 22.15 o 13 3 1 201.52 202.90 31.19 o 14 3 1 130.33 107.72 37.23 o -14 4 1 20.42 -115.08 115.08 o -13 4 1 368.56 391.39 34.67 o -12 4 1 15.87 40.74 24.96 o -11 4 1 494.07 582.86 29.27 o -10 4 1 109.67 115.39 16.46 o -9 4 1 255.30 236.57 14.86 o -8 4 1 1303.22 1263.57 26.23 o -7 4 1 5283.28 5245.43 83.71 o -6 4 1 3212.22 2999.87 37.22 o -5 4 1 5864.48 5746.84 65.05 o -4 4 1 18641.67 19502.75 205.79 o -3 4 1 4415.13 4605.54 51.36 o -2 4 1 8416.02 8529.71 103.15 o -1 4 1 874.18 918.73 15.87 o 0 4 1 2535.99 2545.61 33.13 o 1 4 1 5631.98 5721.83 67.40 o 2 4 1 1909.28 1951.80 27.00 o 3 4 1 396.84 417.62 13.35 o 4 4 1 5498.79 5718.36 68.17 o 5 4 1 6295.79 6385.85 79.32 o 6 4 1 685.65 668.06 13.28 o 7 4 1 72.66 87.98 7.46 o 8 4 1 361.64 358.67 16.29 o 9 4 1 340.79 351.54 18.83 o 10 4 1 1940.35 1876.00 53.55 o 11 4 1 673.17 730.14 28.23 o 12 4 1 111.96 151.57 20.78 o 13 4 1 88.19 64.05 23.93 o -13 5 1 15.47 31.87 29.52 o -12 5 1 1.60 12.01 29.50 o -11 5 1 7.09 -1.64 16.98 o -10 5 1 72.39 118.76 16.00 o -9 5 1 21.58 28.29 9.33 o -8 5 1 42.88 47.90 13.83 o -7 5 1 660.70 674.95 15.95 o -6 5 1 0.96 4.16 5.95 o -5 5 1 108.32 150.90 8.39 o -4 5 1 1287.42 1280.64 21.72 o -3 5 1 1.46 9.57 5.02 o -2 5 1 58.22 49.45 5.84 o -1 5 1 321.75 312.30 10.46 o 0 5 1 67.21 72.03 6.22 o 1 5 1 3598.29 3641.83 44.40 o 2 5 1 2928.35 2966.21 37.58 o 3 5 1 3407.83 3402.93 42.03 o 4 5 1 298.66 286.76 11.15 o 5 5 1 1638.04 1693.65 24.70 o 6 5 1 2.23 1.75 11.30 o 7 5 1 3396.53 3324.52 50.68 o 8 5 1 67.03 23.00 19.68 o 9 5 1 83.77 87.50 11.74 o 10 5 1 137.01 126.16 14.69 o 11 5 1 52.42 79.47 18.00 o 12 5 1 4.49 34.53 33.13 o 13 5 1 0.51 20.22 35.92 o -12 6 1 44.99 69.55 21.95 o -11 6 1 49.62 53.25 31.45 o -10 6 1 9.17 47.66 15.95 o -9 6 1 82.04 130.55 16.37 o -8 6 1 59.49 78.75 22.29 o -7 6 1 833.17 815.01 27.34 o -6 6 1 194.98 217.20 9.43 o -5 6 1 219.42 228.21 11.84 o -4 6 1 246.17 250.83 11.99 o -3 6 1 1292.38 1329.91 21.43 o -2 6 1 4184.74 4035.61 49.96 o -1 6 1 209.93 217.81 9.93 o 0 6 1 2699.87 2669.36 34.91 o 1 6 1 2159.83 2208.06 31.27 o 2 6 1 292.57 318.16 12.63 o 3 6 1 280.28 270.80 11.19 o 4 6 1 379.99 402.84 15.18 o 5 6 1 2455.76 2397.03 39.05 o 6 6 1 2030.81 1951.01 33.89 o 7 6 1 1393.55 1407.71 30.80 o 8 6 1 13.30 10.97 8.54 o 9 6 1 52.74 59.00 15.56 o 10 6 1 37.64 67.51 22.38 o 11 6 1 2.99 9.52 28.70 o 12 6 1 11.90 50.52 35.91 o -11 7 1 325.58 202.36 39.51 o -10 7 1 23.56 38.67 17.81 o -9 7 1 54.37 112.18 36.00 o -8 7 1 236.37 235.40 30.90 o -7 7 1 614.27 586.54 27.84 o -6 7 1 59.23 79.98 13.73 o -5 7 1 379.01 402.05 16.46 o -4 7 1 87.50 89.41 12.61 o -3 7 1 273.74 288.16 13.12 o -2 7 1 547.22 555.79 20.42 o -1 7 1 548.81 552.39 16.68 o 0 7 1 546.56 539.72 16.58 o 1 7 1 820.39 860.64 23.18 o 2 7 1 240.83 269.33 12.39 o 3 7 1 3.12 -8.00 8.00 o 4 7 1 522.35 514.97 21.75 o 5 7 1 443.62 483.89 25.43 o 6 7 1 1303.41 1220.94 52.62 o 7 7 1 780.32 760.20 22.68 o 8 7 1 525.71 481.33 26.38 o 9 7 1 201.46 273.58 25.47 o 10 7 1 0.91 -13.03 25.49 o 11 7 1 0.47 8.84 38.02 o -10 8 1 29.45 76.82 84.45 o -9 8 1 28.05 44.03 30.23 o -8 8 1 152.70 98.22 26.48 o -7 8 1 13.06 4.49 19.49 o -6 8 1 149.73 137.15 24.09 o -5 8 1 457.38 477.49 23.88 o -4 8 1 55.50 64.68 16.23 o -3 8 1 177.79 171.60 16.85 o -2 8 1 10.24 10.54 10.76 o -1 8 1 6.87 9.71 9.86 o 0 8 1 3.40 -7.54 12.77 o 1 8 1 131.57 109.72 11.42 o 2 8 1 177.02 144.09 12.49 o 3 8 1 8.15 16.57 15.06 o 4 8 1 264.26 267.21 15.74 o 5 8 1 1.58 13.61 11.37 o 6 8 1 64.50 49.51 18.71 o 7 8 1 37.66 33.34 24.45 o 8 8 1 404.65 332.11 52.52 o 9 8 1 54.12 23.64 29.68 o -8 9 1 136.83 54.95 33.11 o -7 9 1 9.51 24.51 34.42 o -6 9 1 11.28 -25.59 32.68 o -5 9 1 11.78 46.11 33.12 o -4 9 1 100.97 98.27 33.36 o -3 9 1 83.94 56.56 15.36 o -2 9 1 90.82 82.01 14.67 o -1 9 1 15.46 28.87 14.96 o 0 9 1 147.82 127.44 17.74 o 1 9 1 202.70 194.80 16.62 o 2 9 1 33.26 60.13 18.86 o 3 9 1 53.77 70.77 15.61 o 4 9 1 80.08 99.44 43.70 o 5 9 1 245.52 227.14 58.91 o 6 9 1 238.74 160.17 31.56 o 7 9 1 163.77 86.07 32.62 o 8 9 1 2.21 2.02 62.86 o -5 10 1 105.62 78.88 47.74 o -4 10 1 20.93 -23.05 55.66 o -3 10 1 48.59 16.14 57.16 o -2 10 1 19.19 13.43 29.82 o -1 10 1 39.87 9.21 26.03 o 0 10 1 37.30 70.45 27.83 o 1 10 1 28.48 17.09 21.99 o 2 10 1 42.29 52.27 46.08 o 3 10 1 32.42 -5.66 32.31 o 4 10 1 7.00 -33.33 33.33 o 5 10 1 0.71 -30.65 37.52 o -15 0 2 23.47 34.28 36.75 o -14 0 2 5.81 54.15 28.83 o -13 0 2 1400.39 1532.02 76.71 o -12 0 2 400.08 422.45 31.57 o -11 0 2 113.65 133.84 30.58 o -10 0 2 2508.77 2461.58 56.86 o -9 0 2 304.06 317.59 16.15 o -8 0 2 551.04 451.40 14.49 o -7 0 2 14439.41 15849.56 235.81 o -6 0 2 31129.88 36759.30 537.80 o -5 0 2 10989.30 10682.94 158.98 o -4 0 2 11817.04 11015.24 163.01 o -3 0 2 31259.93 30793.67 717.18 o -2 0 2 77658.85 66952.91 1338.58 o -1 0 2 1644.29 1401.64 31.30 o 1 0 2 2222.42 1743.25 37.65 o 2 0 2 6190.90 5902.06 87.13 o 3 0 2 11584.34 11935.59 213.03 o 4 0 2 823.12 647.87 15.39 o 5 0 2 24946.30 26173.21 383.57 o 6 0 2 6930.00 6660.22 102.17 o 7 0 2 745.33 975.59 20.90 o 8 0 2 4048.61 3802.06 63.02 o 9 0 2 1716.83 1763.84 51.29 o 10 0 2 1006.41 1078.04 65.75 o 11 0 2 104.25 181.43 36.29 o 12 0 2 8.47 2.16 27.11 o 13 0 2 404.64 363.72 44.55 o 14 0 2 21.58 19.61 34.72 o -15 1 2 174.99 148.02 41.55 o -14 1 2 339.45 355.93 27.66 o -13 1 2 154.30 191.59 21.95 o -12 1 2 51.88 16.30 17.31 o -11 1 2 2185.74 2196.33 46.81 o -10 1 2 158.62 138.36 10.17 o -9 1 2 382.06 345.13 10.74 o -8 1 2 14.48 43.64 6.32 o -7 1 2 543.18 536.67 10.43 o -6 1 2 421.93 468.90 8.81 o -5 1 2 73.57 54.76 3.41 o -4 1 2 1643.63 2128.91 26.69 o -3 1 2 1676.52 1534.60 20.57 o -2 1 2 2765.35 2406.69 26.35 o -1 1 2 13580.50 14697.95 178.20 o 0 1 2 207.20 135.40 4.03 o 1 1 2 1850.58 2014.37 23.51 o 2 1 2 2848.30 3459.85 45.32 o 3 1 2 10336.50 10674.28 122.50 o 4 1 2 2431.92 2420.68 30.59 o 5 1 2 259.48 390.57 7.62 o 6 1 2 1051.57 992.45 14.46 o 7 1 2 1087.19 1096.40 16.26 o 8 1 2 91.39 92.78 6.02 o 9 1 2 17.15 13.60 7.11 o 10 1 2 15.12 -5.98 9.97 o 11 1 2 277.70 306.58 29.58 o 12 1 2 185.84 232.89 21.78 o 13 1 2 533.91 584.91 33.70 o 14 1 2 566.88 645.90 74.02 o -14 2 2 3.02 49.53 23.01 o -13 2 2 228.73 252.56 21.33 o -12 2 2 39.66 47.43 17.93 o -11 2 2 586.68 564.10 25.22 o -10 2 2 295.03 297.64 14.69 o -9 2 2 2654.53 2485.68 56.63 o -8 2 2 1868.69 1720.83 26.70 o -7 2 2 6319.02 6332.68 73.19 o -6 2 2 163.04 118.51 5.35 o -5 2 2 4338.78 4481.28 49.90 o -4 2 2 6353.78 6639.99 71.49 o -3 2 2 4637.69 4868.46 57.50 o -2 2 2 73909.27 73370.64 1255.90 o -1 2 2 10824.53 11318.59 124.56 o 0 2 2 10138.23 11015.76 110.75 o 1 2 2 15507.62 16485.22 198.07 o 2 2 2 6281.05 6802.64 79.43 o 3 2 2 5485.64 5861.98 76.92 o 4 2 2 576.77 589.14 10.08 o 5 2 2 3169.62 3304.28 42.00 o 6 2 2 32.52 89.43 4.93 o 7 2 2 216.67 196.74 7.31 o 8 2 2 1313.70 1208.04 23.50 o 9 2 2 2211.56 2105.28 42.14 o 10 2 2 1287.05 1301.63 32.57 o 11 2 2 1116.46 1111.43 49.55 o 12 2 2 531.60 531.61 42.92 o 13 2 2 30.50 53.40 19.49 o 14 2 2 0.25 -10.79 25.56 o -14 3 2 288.99 322.45 33.90 o -13 3 2 18.94 51.79 25.50 o -12 3 2 40.58 88.07 16.35 o -11 3 2 115.68 156.56 18.34 o -10 3 2 105.63 85.31 11.77 o -9 3 2 36.88 27.23 7.63 o -8 3 2 1786.02 1756.12 37.66 o -7 3 2 206.28 217.76 8.31 o -6 3 2 52.78 65.84 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