data_2019991 _cell_angle_alpha 90.000 _cell_angle_beta 94.576 _cell_angle_gamma 90.000 _cell_length_a 10.0405 _cell_length_b 29.5004 _cell_length_c 10.9664 _exptl_crystal_F_000 1736.00 _reflns_d_resolution_high 0.7700 _cod_data_source_file yo3008Isup2.hkl _cod_data_source_block I _shelx_title ' 1 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 370.59 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 137333.31 133213.86 3522.26 o 3 0 0 1374.48 1571.39 132.99 o 4 0 0 16782.51 16607.66 542.17 o 5 0 0 17310.49 17500.97 962.41 o 6 0 0 610.43 563.22 164.28 o 7 0 0 10925.48 10394.27 751.04 o 8 0 0 3561.11 3038.52 343.97 o 9 0 0 5794.57 6593.74 539.09 o 10 0 0 5.47 3.78 295.33 o 11 0 0 1626.88 1683.51 405.14 o 12 0 0 118.61 -12.71 361.00 o 2 1 0 30049.20 29896.51 799.16 o 3 1 0 1680.45 1600.99 153.00 o 4 1 0 18295.65 18387.39 413.98 o 5 1 0 40227.13 38761.55 916.89 o 6 1 0 5582.45 5178.40 251.40 o 7 1 0 4819.16 4848.20 251.81 o 8 1 0 270.77 325.25 131.37 o 9 1 0 3308.59 2998.91 277.22 o 10 1 0 107.41 936.75 419.53 o 11 1 0 0.33 153.64 168.12 o 12 1 0 1266.46 1249.26 723.96 o 2 2 0 18.63 44.05 37.51 o 3 2 0 211.56 421.94 85.12 o 4 2 0 106.02 92.93 57.63 o 5 2 0 18681.56 19004.75 509.19 o 6 2 0 17846.82 17232.03 537.43 o 7 2 0 938.79 1202.48 158.44 o 8 2 0 6727.31 6374.31 362.02 o 9 2 0 172.10 486.43 164.58 o 10 2 0 3576.93 3714.62 335.64 o 11 2 0 842.86 1071.01 331.89 o 12 2 0 14.57 921.02 950.00 o 2 3 0 5828.54 5726.45 181.91 o 3 3 0 9937.10 9354.43 237.11 o 4 3 0 42259.47 43331.04 907.87 o 5 3 0 24596.06 25986.01 646.43 o 6 3 0 42574.06 43377.70 1142.16 o 7 3 0 323.64 114.87 123.21 o 8 3 0 2484.18 2406.37 230.58 o 9 3 0 61.07 171.86 162.78 o 10 3 0 1163.73 1555.55 339.83 o 11 3 0 766.95 1225.32 292.67 o 12 3 0 1.52 203.02 361.97 o 1 4 0 12989.41 12635.80 292.86 o 2 4 0 7253.35 7500.76 168.34 o 3 4 0 207.60 319.55 55.42 o 4 4 0 11945.90 12020.94 309.45 o 5 4 0 1244.36 1711.53 140.17 o 6 4 0 611.71 1001.60 153.13 o 7 4 0 7418.02 7401.48 356.83 o 8 4 0 2.48 -2.93 147.41 o 9 4 0 4293.67 4914.38 343.75 o 10 4 0 56.99 210.04 181.34 o 11 4 0 495.38 567.97 211.66 o 12 4 0 231.88 1322.90 640.75 o 1 5 0 18839.26 18330.63 470.87 o 2 5 0 17510.93 18233.85 328.48 o 3 5 0 6442.15 5823.08 167.04 o 4 5 0 383.65 422.65 75.06 o 5 5 0 16731.85 16844.97 469.86 o 6 5 0 1089.83 1549.25 226.23 o 7 5 0 10123.16 10015.01 430.58 o 8 5 0 524.80 701.97 175.52 o 9 5 0 1043.50 1442.21 219.73 o 10 5 0 209.90 434.63 339.45 o 11 5 0 405.30 452.94 186.64 o 12 5 0 2054.00 2532.94 448.36 o 0 6 0 9887.04 10268.80 248.92 o 1 6 0 121572.40 123749.28 1483.16 o 2 6 0 3093.03 3049.75 127.97 o 3 6 0 43.13 136.64 113.52 o 4 6 0 235.41 477.30 73.72 o 5 6 0 995.83 1138.62 132.16 o 6 6 0 30.38 102.23 86.07 o 7 6 0 2937.00 3360.14 235.46 o 8 6 0 2066.86 2506.46 262.84 o 9 6 0 722.62 725.84 171.85 o 10 6 0 1184.62 1165.62 201.93 o 11 6 0 67.64 -45.88 202.35 o 12 6 0 103.17 379.40 294.09 o 1 7 0 1783.22 1935.19 78.55 o 2 7 0 1383.71 1633.95 131.86 o 3 7 0 3498.84 3233.07 160.76 o 4 7 0 11246.46 11135.42 311.48 o 5 7 0 32.48 -3.56 77.22 o 6 7 0 7332.78 7442.03 535.37 o 7 7 0 509.21 777.67 152.04 o 8 7 0 9465.21 8654.29 412.95 o 9 7 0 3285.69 3320.68 289.14 o 10 7 0 2126.96 2154.47 258.86 o 11 7 0 1931.09 1867.65 368.72 o 12 7 0 251.57 817.01 350.98 o 0 8 0 3392.34 3247.07 308.50 o 1 8 0 16875.44 16016.95 300.12 o 2 8 0 1076.46 1149.28 70.91 o 3 8 0 26507.49 27143.69 566.71 o 4 8 0 2359.63 2250.88 138.30 o 5 8 0 5392.08 5331.60 249.57 o 6 8 0 1091.04 1245.93 186.13 o 7 8 0 200.02 232.87 146.84 o 8 8 0 1477.53 1969.71 261.05 o 9 8 0 485.29 773.73 302.15 o 10 8 0 1550.28 1969.89 257.60 o 11 8 0 46.84 185.69 223.40 o 12 8 0 663.64 651.50 353.91 o 1 9 0 6057.11 6141.47 161.84 o 2 9 0 11751.05 11565.15 256.54 o 3 9 0 28231.31 28139.58 602.53 o 4 9 0 2371.33 2576.76 171.91 o 5 9 0 16194.16 17290.95 522.62 o 6 9 0 4165.08 4107.03 279.44 o 7 9 0 4386.55 4745.15 347.27 o 8 9 0 220.56 571.88 151.64 o 9 9 0 1540.60 1608.12 210.26 o 10 9 0 531.20 930.15 219.21 o 11 9 0 67.00 153.06 212.47 o 12 9 0 103.94 55.22 252.27 o 0 10 0 18348.93 16804.60 464.88 o 1 10 0 747.90 727.98 65.43 o 2 10 0 50938.33 50095.84 935.96 o 3 10 0 408.31 494.45 77.00 o 4 10 0 8476.79 8798.31 286.84 o 5 10 0 6563.81 6862.09 270.45 o 6 10 0 1071.99 1040.79 146.88 o 7 10 0 3781.01 3901.95 276.49 o 8 10 0 1773.65 1933.92 205.25 o 9 10 0 1717.09 2039.82 228.04 o 10 10 0 463.04 738.28 217.38 o 11 10 0 1413.53 1342.05 332.22 o 12 10 0 229.88 287.58 298.77 o 1 11 0 4017.44 4031.56 138.26 o 2 11 0 2317.09 2296.59 114.11 o 3 11 0 5315.12 5157.55 394.80 o 4 11 0 25262.88 25408.66 660.14 o 5 11 0 47.63 281.42 129.85 o 6 11 0 6761.68 7092.92 324.23 o 7 11 0 4489.57 4172.77 268.35 o 8 11 0 2504.27 3243.74 446.28 o 9 11 0 34.29 86.95 198.42 o 10 11 0 21.57 417.62 270.98 o 11 11 0 24.06 386.03 280.10 o 12 11 0 29.46 225.98 273.06 o 0 12 0 22.75 43.65 62.13 o 1 12 0 60059.53 60288.52 1160.36 o 2 12 0 13.70 82.74 70.23 o 3 12 0 54504.21 53969.51 1455.00 o 4 12 0 2957.13 2944.67 161.39 o 5 12 0 3955.74 3960.74 214.94 o 6 12 0 6733.46 6956.59 556.30 o 7 12 0 1642.04 1817.56 278.00 o 8 12 0 7020.98 7450.88 733.64 o 9 12 0 604.40 413.92 409.17 o 10 12 0 786.75 350.23 237.04 o 11 12 0 458.63 346.78 234.51 o 12 12 0 202.05 305.28 281.07 o 1 13 0 0.65 532.67 344.59 o 2 13 0 35062.96 34663.13 765.98 o 3 13 0 12048.79 12345.95 435.63 o 4 13 0 6319.24 6319.39 277.51 o 5 13 0 5094.83 5189.18 382.82 o 6 13 0 8422.06 8713.01 375.64 o 7 13 0 2290.65 2648.14 229.54 o 8 13 0 736.02 706.83 229.53 o 9 13 0 359.82 52.90 211.22 o 10 13 0 89.99 2.89 285.40 o 11 13 0 439.43 828.54 422.88 o 12 13 0 70.48 184.49 284.06 o 0 14 0 36787.37 37708.84 1136.35 o 1 14 0 962.07 1043.23 89.66 o 2 14 0 64302.59 64290.91 1378.72 o 3 14 0 102.53 200.86 127.93 o 4 14 0 7241.62 7231.55 276.84 o 5 14 0 559.86 679.06 212.84 o 6 14 0 53.14 207.27 112.77 o 7 14 0 5382.07 5195.66 315.16 o 8 14 0 178.55 9.53 128.45 o 9 14 0 2172.42 1369.33 248.45 o 10 14 0 393.82 216.68 224.59 o 11 14 0 572.58 932.13 408.35 o 12 14 0 52.35 969.23 433.72 o 1 15 0 11110.67 11771.02 328.65 o 2 15 0 3549.69 3663.79 309.93 o 3 15 0 5961.91 6197.65 226.93 o 4 15 0 3114.07 3071.81 179.72 o 5 15 0 9099.11 8980.46 366.13 o 6 15 0 269.35 67.88 102.13 o 7 15 0 9539.51 9727.36 459.02 o 8 15 0 123.63 171.82 235.59 o 9 15 0 267.25 255.47 154.96 o 10 15 0 767.22 1309.57 348.43 o 11 15 0 384.61 278.95 243.41 o 0 16 0 1420.53 1473.51 150.14 o 1 16 0 5594.69 5275.86 198.71 o 2 16 0 274.09 356.87 133.52 o 3 16 0 8709.71 8617.76 307.88 o 4 16 0 136.20 0.95 108.83 o 5 16 0 12.64 333.90 294.20 o 6 16 0 3293.38 3087.90 422.43 o 7 16 0 14.91 45.39 104.29 o 8 16 0 2232.86 1912.71 320.84 o 9 16 0 280.29 501.08 271.14 o 10 16 0 971.64 692.00 411.74 o 11 16 0 353.99 168.77 254.67 o 1 17 0 2050.28 2121.90 135.28 o 2 17 0 9936.86 9548.96 307.95 o 3 17 0 1375.24 1417.20 192.96 o 4 17 0 3916.87 3847.08 282.59 o 5 17 0 0.42 181.44 234.77 o 6 17 0 8847.94 8685.33 415.62 o 7 17 0 239.66 419.41 144.78 o 8 17 0 1953.48 1676.65 210.47 o 9 17 0 757.36 1107.22 417.81 o 10 17 0 489.46 419.73 256.84 o 11 17 0 1041.35 2440.30 562.96 o 0 18 0 85.02 271.98 116.17 o 1 18 0 1908.49 1888.45 133.69 o 2 18 0 3198.02 3326.94 273.20 o 3 18 0 1204.68 1305.42 130.20 o 4 18 0 1576.40 1650.96 211.72 o 5 18 0 1.03 -108.90 110.35 o 6 18 0 35.55 82.02 112.29 o 7 18 0 2132.00 2010.19 343.42 o 8 18 0 85.97 258.30 139.70 o 9 18 0 72.78 108.85 276.50 o 10 18 0 485.56 296.14 264.50 o 11 18 0 133.53 520.16 456.62 o 1 19 0 5876.59 6008.09 252.66 o 2 19 0 866.58 931.81 178.14 o 3 19 0 3712.55 3635.81 201.32 o 4 19 0 343.50 552.21 119.68 o 5 19 0 5405.41 5592.31 396.31 o 6 19 0 18.00 337.16 129.98 o 7 19 0 2105.22 2250.17 233.99 o 8 19 0 110.78 -6.38 187.37 o 9 19 0 673.91 1415.10 423.19 o 10 19 0 1112.67 1518.04 498.22 o 11 19 0 504.69 1125.22 698.39 o 0 20 0 7471.84 7447.33 502.01 o 1 20 0 457.47 715.22 195.06 o 2 20 0 5473.44 5216.46 233.78 o 3 20 0 6.00 7.58 95.93 o 4 20 0 5190.88 5525.39 273.98 o 5 20 0 2718.38 2896.20 403.06 o 6 20 0 368.84 753.60 161.19 o 7 20 0 845.93 607.98 165.10 o 8 20 0 104.87 -2.41 123.27 o 9 20 0 1148.39 1289.49 294.23 o 10 20 0 63.46 1379.03 408.99 o 11 20 0 269.19 582.31 442.05 o 1 21 0 694.02 857.93 168.85 o 2 21 0 2923.82 2809.09 234.26 o 3 21 0 1459.66 1202.82 146.13 o 4 21 0 987.05 1358.20 213.92 o 5 21 0 534.72 667.18 134.31 o 6 21 0 2126.88 4062.79 1100.90 o 7 21 0 15.88 24.77 139.89 o 8 21 0 566.54 699.26 195.46 o 9 21 0 67.58 827.00 544.98 o 10 21 0 151.47 167.81 304.30 o 0 22 0 1070.33 1542.46 208.43 o 1 22 0 9491.29 9405.26 375.21 o 2 22 0 13.82 130.80 90.80 o 3 22 0 12040.17 11670.59 448.46 o 4 22 0 723.21 856.43 288.39 o 5 22 0 1206.10 1376.54 184.71 o 6 22 0 172.09 -27.82 112.91 o 7 22 0 1.47 104.76 126.96 o 8 22 0 903.83 989.95 210.33 o 9 22 0 8.81 -76.37 278.24 o 10 22 0 695.59 1696.79 1277.11 o 1 23 0 1129.75 1490.26 158.04 o 2 23 0 2502.20 2223.22 216.20 o 3 23 0 3665.36 3770.78 413.13 o 4 23 0 2167.15 2380.41 201.89 o 5 23 0 2546.02 2547.74 303.07 o 6 23 0 469.12 1004.60 176.88 o 7 23 0 999.54 723.40 234.56 o 8 23 0 281.95 492.30 342.15 o 9 23 0 130.00 516.84 427.72 o 10 23 0 6.48 -37.23 266.64 o 0 24 0 4708.39 4902.48 368.81 o 1 24 0 35.98 117.34 116.61 o 2 24 0 9019.02 9439.71 413.11 o 3 24 0 1095.93 777.99 172.47 o 4 24 0 2140.89 1980.90 188.20 o 5 24 0 1583.49 1885.01 198.94 o 6 24 0 6.72 -55.13 133.27 o 7 24 0 744.61 818.41 314.27 o 8 24 0 31.02 -19.76 206.60 o 9 24 0 1042.00 1344.20 398.70 o 10 24 0 10.55 142.97 365.47 o 1 25 0 48.35 300.24 121.46 o 2 25 0 76.64 465.03 249.74 o 3 25 0 1990.60 2213.82 202.56 o 4 25 0 769.77 1331.25 216.28 o 5 25 0 970.29 1360.87 179.38 o 6 25 0 667.20 737.63 213.49 o 7 25 0 303.39 373.21 198.66 o 8 25 0 73.65 138.60 295.40 o 9 25 0 116.93 1169.33 708.98 o 0 26 0 81.61 -83.74 149.79 o 1 26 0 6407.48 6140.75 325.03 o 2 26 0 1.30 174.91 146.84 o 3 26 0 6605.71 6188.82 419.64 o 4 26 0 331.46 1063.26 404.82 o 5 26 0 533.38 1123.84 373.73 o 6 26 0 91.09 57.38 179.27 o 7 26 0 179.27 205.40 205.65 o 8 26 0 1135.86 1085.71 415.92 o 9 26 0 0.24 -34.27 269.48 o 1 27 0 9.70 -20.35 130.81 o 2 27 0 1.62 -9.75 101.83 o 3 27 0 63.38 87.23 115.40 o 4 27 0 2068.11 2209.37 300.04 o 5 27 0 161.74 -92.50 265.91 o 6 27 0 261.42 1233.04 516.15 o 7 27 0 61.75 58.04 214.20 o 8 27 0 814.36 467.83 336.71 o 9 27 0 241.58 405.67 344.28 o 0 28 0 253.81 348.13 164.28 o 1 28 0 2.16 -54.57 136.27 o 2 28 0 1292.68 1577.99 207.77 o 3 28 0 528.08 839.26 162.34 o 4 28 0 4.87 -44.61 166.85 o 5 28 0 34.95 205.43 185.03 o 6 28 0 96.61 317.63 209.73 o 7 28 0 56.05 -50.06 264.10 o 8 28 0 2.51 34.62 233.72 o 1 29 0 162.05 201.79 123.92 o 2 29 0 90.10 415.93 176.89 o 3 29 0 1431.61 2333.42 380.20 o 4 29 0 65.76 -62.08 142.03 o 5 29 0 500.36 1348.25 630.04 o 6 29 0 10.32 99.29 208.55 o 7 29 0 499.55 1586.28 729.11 o 8 29 0 173.56 342.24 389.90 o 0 30 0 705.79 825.41 530.15 o 1 30 0 294.96 11.86 102.11 o 2 30 0 75.10 -48.95 148.32 o 3 30 0 20.26 134.08 169.04 o 4 30 0 327.23 135.64 286.77 o 5 30 0 63.73 271.36 192.94 o 6 30 0 61.37 628.14 284.71 o 7 30 0 2.76 354.37 340.12 o 8 30 0 241.28 467.66 336.60 o 1 31 0 32.92 125.13 122.92 o 2 31 0 25.40 -140.44 170.05 o 3 31 0 31.61 -211.17 211.17 o 4 31 0 1301.79 827.74 262.31 o 5 31 0 73.09 -94.06 171.30 o 6 31 0 291.68 470.20 339.36 o 7 31 0 43.44 -216.36 535.29 o 0 32 0 60.02 191.22 213.21 o 1 32 0 704.23 1599.51 289.43 o 2 32 0 7.90 125.02 180.79 o 3 32 0 520.22 1057.41 294.10 o 4 32 0 1.98 99.19 192.06 o 5 32 0 224.37 230.87 266.53 o 6 32 0 61.30 577.89 326.94 o 7 32 0 3.28 101.57 259.45 o 1 33 0 9.16 -42.36 153.37 o 2 33 0 5.19 10.00 197.28 o 3 33 0 126.81 582.64 687.58 o 4 33 0 24.77 -123.81 206.34 o 5 33 0 210.04 215.93 230.52 o 6 33 0 284.32 462.37 368.26 o 0 34 0 2436.33 2133.30 653.00 o 1 34 0 68.20 87.57 236.90 o 2 34 0 794.27 1229.98 1136.10 o 3 34 0 295.80 784.29 389.07 o 4 34 0 509.14 873.94 282.50 o 5 34 0 56.84 374.80 442.09 o 1 35 0 76.71 -125.15 253.74 o 2 35 0 109.39 75.54 273.70 o 3 35 0 54.53 -56.90 278.69 o 4 35 0 74.41 264.56 358.85 o 5 35 0 326.59 -42.67 402.76 o 0 36 0 184.80 -134.05 449.05 o 1 36 0 1220.36 1225.87 461.46 o 2 36 0 50.94 109.67 337.16 o 3 36 0 132.11 522.03 415.92 o 4 36 0 151.82 580.38 531.96 o 1 37 0 76.68 68.58 298.20 o 2 37 0 6.99 716.94 399.69 o 3 37 0 87.83 1061.92 493.50 o 0 38 0 304.53 106.82 489.90 o 1 38 0 85.09 781.45 1079.51 o -13 1 1 369.74 410.73 439.81 o -12 1 1 780.68 357.77 260.35 o -11 1 1 624.64 887.81 455.25 o -10 1 1 756.75 764.56 233.72 o -9 1 1 1106.37 947.43 355.85 o -8 1 1 3416.49 2968.60 302.72 o -7 1 1 2400.37 2324.47 208.69 o -6 1 1 13812.00 14172.93 464.14 o -5 1 1 4012.60 3948.46 212.00 o -4 1 1 1899.94 1822.30 150.86 o -3 1 1 1449.47 1660.14 100.06 o -2 1 1 7973.80 7715.56 214.75 o 2 1 1 14369.64 14172.66 371.02 o 3 1 1 14264.14 14275.96 309.05 o 4 1 1 8458.30 8512.60 219.33 o 5 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