#------------------------------------------------------------------------------ #$Date: 2016-04-06 16:35:31 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181869 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/99/2019994.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2019994 _cell_angle_alpha 90.000 _cell_angle_beta 98.950 _cell_angle_gamma 90.000 _cell_length_a 21.7231 _cell_length_b 5.6603 _cell_length_c 32.0745 _exptl_crystal_F_000 1584.00 _reflns_d_resolution_high 0.8001 _cod_data_source_file sk3586Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title '_L_leu_mal_2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 395.26 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 -7 0 2.76 341.66 139.62 o 0 -6 0 71.11 93.27 535.08 o 2 -6 0 125.37 75.88 250.45 o 4 -6 0 35.95 -101.82 523.66 o 6 -6 0 59.29 294.73 274.30 o 8 -6 0 32.33 131.61 197.94 o 10 -6 0 32.67 293.48 214.64 o 12 -6 0 3.71 31.87 171.73 o 14 -6 0 0.62 640.14 341.55 o 1 -5 0 691.14 934.88 244.23 o 3 -5 0 811.78 985.90 222.67 o 5 -5 0 84.34 335.30 161.06 o 7 -5 0 721.62 524.60 318.92 o 9 -5 0 401.02 207.98 155.30 o 11 -5 0 521.21 651.10 257.56 o 13 -5 0 46.96 8.24 86.71 o 15 -5 0 1.40 136.74 211.57 o 17 -5 0 3.63 64.07 274.45 o 0 -4 0 205.49 167.98 70.67 o 2 -4 0 2265.64 2674.17 238.00 o 4 -4 0 854.52 958.58 172.04 o 6 -4 0 334.72 452.67 175.10 o 8 -4 0 118.25 255.78 122.57 o 10 -4 0 142.63 275.23 123.58 o 12 -4 0 165.84 115.39 77.90 o 14 -4 0 187.00 69.43 293.29 o 16 -4 0 129.97 116.24 145.44 o 18 -4 0 20.09 55.65 148.06 o 20 -4 0 29.54 153.21 312.46 o 22 -4 0 4.48 17.03 280.06 o 1 -3 0 1557.62 1584.29 154.25 o 3 -3 0 6459.80 6623.09 426.49 o 5 -3 0 1490.04 1271.90 213.00 o 7 -3 0 2043.07 2202.91 256.18 o 9 -3 0 649.33 739.15 142.49 o 11 -3 0 24.63 49.08 74.63 o 13 -3 0 47.01 89.36 62.41 o 15 -3 0 198.21 142.03 91.37 o 17 -3 0 41.04 17.70 104.08 o 19 -3 0 52.53 128.93 82.68 o 21 -3 0 20.24 -68.88 68.88 o 23 -3 0 6.89 0.17 365.77 o 0 -2 0 5897.48 5589.05 321.19 o 2 -2 0 522.44 497.67 77.12 o 4 -2 0 385.93 296.00 72.11 o 6 -2 0 562.72 622.39 102.77 o 8 -2 0 1995.94 1962.20 146.32 o 10 -2 0 6762.89 7210.44 331.99 o 12 -2 0 378.53 372.29 114.36 o 14 -2 0 156.45 145.29 68.17 o 16 -2 0 397.67 463.78 104.07 o 18 -2 0 493.89 509.74 122.33 o 20 -2 0 59.18 -48.73 64.64 o 22 -2 0 2.85 63.09 67.47 o 24 -2 0 34.65 48.02 291.28 o 1 -1 0 3440.78 3297.09 120.36 o 3 -1 0 5864.18 5480.34 229.07 o 5 -1 0 6719.34 6401.19 205.95 o 7 -1 0 4040.79 3798.98 164.67 o 9 -1 0 4130.25 4178.68 195.81 o 11 -1 0 658.36 542.51 94.02 o 13 -1 0 1438.51 1685.36 183.96 o 15 -1 0 475.26 470.36 100.98 o 17 -1 0 9.20 145.39 85.72 o 19 -1 0 357.49 423.23 131.35 o 21 -1 0 47.84 -23.77 119.90 o 23 -1 0 8.80 185.92 246.14 o 25 -1 0 39.44 232.39 529.63 o 2 0 0 2586.82 2418.43 132.58 o 4 0 0 4974.74 5165.73 234.10 o 6 0 0 30811.38 30294.00 1363.29 o 8 0 0 6858.99 6347.67 326.34 o 10 0 0 1091.71 1015.80 126.09 o 12 0 0 11885.49 10919.99 433.86 o 14 0 0 2100.45 1967.20 198.88 o 16 0 0 374.00 367.93 92.93 o 18 0 0 658.36 1015.80 278.50 o 20 0 0 221.05 302.09 190.31 o 22 0 0 4.44 -10.80 118.88 o 24 0 0 28.96 434.92 221.57 o 26 0 0 45.01 105.23 234.20 o 1 1 0 3433.06 3199.45 99.94 o 3 1 0 5860.67 5737.20 182.86 o 5 1 0 6714.04 6899.97 276.53 o 7 1 0 4042.83 4071.42 360.52 o 9 1 0 4131.73 3753.70 265.73 o 11 1 0 659.69 544.13 160.25 o 13 1 0 1439.11 1822.47 210.18 o 15 1 0 475.68 590.39 103.70 o 17 1 0 9.27 -93.87 118.67 o 19 1 0 357.50 326.05 189.36 o 21 1 0 48.00 72.23 234.84 o 23 1 0 8.84 180.04 137.86 o 25 1 0 39.42 404.71 245.35 o 0 2 0 5896.85 5808.08 321.29 o 2 2 0 523.05 642.76 76.02 o 4 2 0 385.81 422.63 83.70 o 6 2 0 562.69 427.24 165.82 o 8 2 0 1996.11 1872.52 169.22 o 10 2 0 6764.38 7419.79 626.11 o 12 2 0 378.65 428.38 164.20 o 14 2 0 156.15 221.05 126.61 o 16 2 0 398.08 716.39 252.35 o 18 2 0 492.55 335.41 194.42 o 20 2 0 59.17 84.96 132.75 o 22 2 0 2.84 -76.52 231.49 o 24 2 0 34.66 47.62 195.34 o 1 3 0 1556.52 1684.91 121.12 o 3 3 0 6461.96 7020.97 285.40 o 5 3 0 1488.43 1314.58 162.72 o 7 3 0 2041.70 2312.21 203.20 o 9 3 0 649.80 728.82 214.97 o 11 3 0 24.62 40.91 105.81 o 13 3 0 46.90 60.34 86.79 o 15 3 0 198.30 241.29 110.98 o 17 3 0 40.89 83.28 283.71 o 19 3 0 52.45 95.40 127.62 o 21 3 0 20.20 -32.87 61.43 o 23 3 0 6.90 56.31 130.56 o 0 4 0 205.95 228.83 61.60 o 2 4 0 2266.31 2743.63 164.11 o 4 4 0 855.26 1059.16 120.75 o 6 4 0 334.31 284.59 89.59 o 8 4 0 118.86 -20.76 94.60 o 10 4 0 142.51 321.98 141.30 o 12 4 0 165.78 360.59 132.84 o 14 4 0 187.08 303.83 158.36 o 16 4 0 129.86 86.04 176.72 o 18 4 0 20.17 -7.18 147.27 o 20 4 0 29.52 88.27 104.18 o 22 4 0 4.47 168.35 199.61 o 1 5 0 692.15 692.23 154.88 o 3 5 0 811.03 829.57 157.64 o 5 5 0 84.68 93.30 102.10 o 7 5 0 722.04 891.72 226.05 o 9 5 0 401.09 326.94 214.25 o 11 5 0 521.18 416.61 295.23 o 13 5 0 46.97 8.10 91.28 o 15 5 0 1.38 108.27 173.63 o 17 5 0 3.65 401.32 178.20 o 0 6 0 71.19 571.28 380.13 o 2 6 0 125.20 90.09 102.89 o 4 6 0 35.86 -74.96 376.53 o 6 6 0 59.32 66.47 197.33 o 8 6 0 32.36 -15.83 142.41 o 10 6 0 32.72 -43.43 89.43 o 12 6 0 3.70 -96.32 96.32 o 14 6 0 0.59 90.69 166.77 o 1 7 0 5.17 25.91 338.98 o 3 7 0 2.77 -1.30 306.10 o 1 -7 1 24.27 324.17 528.39 o 3 -7 1 12.03 10.85 159.74 o -14 -6 1 1.83 363.01 469.81 o -12 -6 1 47.29 28.57 501.96 o -10 -6 1 59.79 129.40 311.18 o -8 -6 1 92.14 59.68 112.33 o -6 -6 1 41.24 -126.27 204.20 o -4 -6 1 2.28 3.49 286.28 o -2 -6 1 30.63 53.88 145.70 o 0 -6 1 58.24 179.66 172.23 o 2 -6 1 83.65 -192.93 198.81 o 4 -6 1 3.67 172.73 257.14 o 6 -6 1 20.14 15.43 263.39 o 8 -6 1 149.70 181.64 156.48 o 10 -6 1 19.48 698.82 344.13 o 12 -6 1 37.86 -162.94 317.55 o 14 -6 1 16.09 202.61 250.42 o -19 -5 1 2.84 -49.55 323.82 o -17 -5 1 0.71 -7.36 423.24 o -15 -5 1 8.80 345.02 153.40 o -13 -5 1 201.22 55.92 215.24 o -11 -5 1 124.77 39.72 194.32 o -9 -5 1 338.86 593.31 199.68 o -7 -5 1 203.57 60.60 67.50 o -5 -5 1 71.98 121.84 138.07 o -3 -5 1 364.41 332.48 106.50 o -1 -5 1 342.77 281.29 102.10 o 1 -5 1 399.76 210.47 111.72 o 3 -5 1 172.97 57.27 128.46 o 5 -5 1 58.52 223.97 143.81 o 7 -5 1 136.27 190.23 123.63 o 9 -5 1 77.21 409.59 258.85 o 11 -5 1 27.90 -16.24 175.52 o 13 -5 1 6.10 107.34 163.63 o 15 -5 1 7.15 11.85 96.01 o 17 -5 1 2.43 17.61 104.03 o -22 -4 1 10.52 296.01 270.79 o -20 -4 1 37.29 178.91 179.82 o -18 -4 1 11.53 86.19 143.83 o -16 -4 1 0.37 298.03 157.40 o -14 -4 1 1.48 34.86 111.69 o -12 -4 1 305.39 547.80 169.21 o -10 -4 1 695.34 634.82 178.08 o -8 -4 1 1005.71 1075.03 247.60 o -6 -4 1 649.76 792.43 228.40 o -4 -4 1 258.95 117.09 94.56 o -2 -4 1 295.11 529.28 111.01 o 0 -4 1 1761.00 1728.49 188.48 o 2 -4 1 2831.13 3246.15 264.34 o 4 -4 1 51.57 107.35 86.25 o 6 -4 1 172.64 101.95 124.54 o 8 -4 1 533.51 343.79 184.42 o 10 -4 1 56.09 122.03 113.59 o 12 -4 1 9.59 65.53 82.88 o 14 -4 1 232.36 55.15 101.46 o 16 -4 1 32.18 -91.74 121.35 o 18 -4 1 13.28 -105.67 135.18 o 20 -4 1 27.01 94.09 102.03 o 22 -4 1 10.89 -115.65 188.33 o -23 -3 1 21.74 -42.78 107.60 o -21 -3 1 81.42 -63.75 153.45 o -19 -3 1 3.36 217.11 115.54 o -17 -3 1 3.49 69.18 105.50 o -15 -3 1 225.05 291.96 105.45 o -13 -3 1 139.44 98.90 66.52 o -11 -3 1 525.54 547.35 125.36 o -9 -3 1 248.90 195.31 82.16 o -7 -3 1 968.82 1100.62 182.66 o -5 -3 1 1096.72 1108.47 194.52 o -3 -3 1 82.17 141.58 56.23 o -1 -3 1 2.22 10.39 42.33 o 1 -3 1 530.07 404.58 80.80 o 3 -3 1 3207.43 3399.04 302.31 o 5 -3 1 949.43 998.59 252.29 o 7 -3 1 518.48 659.63 137.13 o 9 -3 1 718.67 898.52 149.31 o 11 -3 1 109.79 116.83 72.06 o 13 -3 1 298.25 471.92 127.88 o 15 -3 1 52.78 88.55 56.25 o 17 -3 1 313.14 265.24 205.77 o 19 -3 1 68.29 142.26 56.34 o 21 -3 1 48.26 163.62 159.95 o 23 -3 1 6.53 -110.22 133.26 o -24 -2 1 8.50 -13.42 132.30 o -22 -2 1 76.07 217.40 147.76 o -20 -2 1 53.25 89.46 75.65 o -18 -2 1 182.78 153.39 100.28 o -16 -2 1 2.25 16.28 69.42 o -14 -2 1 30.02 8.00 37.86 o -12 -2 1 1489.84 1739.13 181.74 o -10 -2 1 1662.53 1720.36 169.64 o -8 -2 1 1414.13 1501.61 133.12 o -6 -2 1 416.16 295.31 89.46 o -4 -2 1 1433.04 1564.68 147.30 o -2 -2 1 240.60 245.84 49.23 o 0 -2 1 2875.91 2773.66 158.57 o 2 -2 1 1793.90 1784.88 152.72 o 4 -2 1 759.84 690.98 127.92 o 6 -2 1 1747.67 1574.20 115.66 o 8 -2 1 1382.01 1434.69 90.55 o 10 -2 1 267.87 282.00 69.78 o 12 -2 1 503.08 499.75 98.98 o 14 -2 1 17.66 103.73 74.61 o 16 -2 1 151.73 372.60 97.86 o 18 -2 1 27.39 95.11 148.88 o 20 -2 1 21.50 9.74 79.66 o 22 -2 1 76.74 132.91 136.41 o 24 -2 1 10.95 -239.11 690.34 o -25 -1 1 20.46 136.20 155.24 o -23 -1 1 11.63 -83.37 255.11 o -21 -1 1 207.70 317.47 150.13 o -19 -1 1 34.21 70.24 74.09 o -17 -1 1 48.31 136.36 56.17 o -15 -1 1 500.38 425.12 96.15 o -13 -1 1 359.74 304.65 74.96 o -11 -1 1 483.29 449.94 95.73 o -9 -1 1 328.57 306.09 52.26 o -7 -1 1 6120.51 5630.15 198.25 o -5 -1 1 3276.06 3272.02 150.02 o -3 -1 1 2617.99 2378.68 113.93 o -1 -1 1 10485.84 10020.78 252.68 o 1 -1 1 26524.85 27614.17 333.21 o 3 -1 1 40830.51 39494.04 977.70 o 5 -1 1 1799.20 1838.86 94.79 o 7 -1 1 2425.47 2428.65 127.70 o 9 -1 1 1104.92 1287.91 136.07 o 11 -1 1 986.25 1121.02 140.53 o 13 -1 1 394.33 427.48 87.03 o 15 -1 1 397.47 212.61 72.10 o 17 -1 1 488.47 474.47 137.50 o 19 -1 1 495.03 442.65 155.56 o 21 -1 1 222.18 242.21 139.06 o 23 -1 1 2.73 -111.78 111.78 o 25 -1 1 8.54 51.85 445.92 o -26 0 1 0.78 189.68 239.76 o -24 0 1 20.32 56.88 155.61 o -22 0 1 160.70 426.01 174.11 o -20 0 1 310.63 626.99 149.44 o -18 0 1 53.34 283.71 160.16 o -16 0 1 0.17 94.05 69.45 o -14 0 1 2562.55 2802.39 223.52 o -12 0 1 2400.17 2305.03 193.46 o -10 0 1 441.30 467.31 79.05 o -8 0 1 2660.16 2173.18 152.40 o -6 0 1 0.09 -15.55 36.38 o -4 0 1 20891.85 20932.74 468.50 o -2 0 1 71849.20 69494.77 1378.79 o 2 0 1 2396.38 2366.71 102.11 o 4 0 1 1123.28 1087.89 93.02 o 6 0 1 51467.16 47483.59 1672.80 o 8 0 1 4345.99 3970.90 271.35 o 10 0 1 1151.93 1055.41 155.70 o 12 0 1 4184.87 4337.40 281.65 o 14 0 1 235.53 207.33 80.89 o 16 0 1 39.92 1.54 48.78 o 18 0 1 46.32 189.80 120.88 o 20 0 1 62.37 128.83 127.93 o 22 0 1 58.13 276.79 152.98 o 24 0 1 2.54 147.72 344.40 o 26 0 1 0.70 61.71 183.78 o -25 1 1 20.51 -86.12 243.92 o -23 1 1 11.68 68.87 119.81 o -21 1 1 207.78 378.52 138.10 o -19 1 1 34.02 247.82 165.92 o -17 1 1 48.38 84.42 85.04 o -15 1 1 500.62 476.18 110.91 o -13 1 1 360.11 349.83 94.07 o -11 1 1 484.23 438.18 96.74 o -9 1 1 328.91 386.23 81.24 o -7 1 1 6127.65 6421.05 284.79 o -5 1 1 3283.83 3110.29 174.87 o -3 1 1 2622.15 2499.68 115.66 o -1 1 1 10475.37 9589.26 208.80 o 1 1 1 26547.95 26467.29 318.81 o 3 1 1 40805.00 40240.44 515.88 o 5 1 1 1801.89 1788.71 111.18 o 7 1 1 2431.21 2556.75 208.76 o 9 1 1 1104.84 1053.72 157.86 o 11 1 1 986.39 857.96 148.33 o 13 1 1 395.20 388.79 94.53 o 15 1 1 397.61 421.44 140.30 o 17 1 1 487.60 627.19 230.65 o 19 1 1 495.43 492.22 241.56 o 21 1 1 222.51 246.25 349.97 o 23 1 1 2.73 151.14 192.74 o 25 1 1 8.51 83.25 166.32 o -24 2 1 8.51 33.30 58.55 o -22 2 1 75.95 32.19 60.73 o -20 2 1 53.21 219.61 199.22 o -18 2 1 182.80 229.66 168.06 o -16 2 1 2.19 -32.09 74.95 o -14 2 1 29.87 220.88 95.80 o -12 2 1 1490.93 1497.51 539.17 o -10 2 1 1663.50 1739.91 322.85 o -8 2 1 1413.15 1466.29 152.81 o -6 2 1 415.99 402.79 68.30 o -4 2 1 1434.40 1236.32 170.93 o -2 2 1 241.03 198.43 46.68 o 0 2 1 2879.72 2881.99 144.21 o 2 2 1 1795.61 1815.71 107.05 o 4 2 1 760.02 679.22 103.12 o 6 2 1 1750.85 1611.00 215.31 o 8 2 1 1381.72 1288.57 130.23 o 10 2 1 267.97 191.82 81.76 o 12 2 1 503.60 767.24 222.39 o 14 2 1 17.65 135.63 162.54 o 16 2 1 151.22 378.00 186.89 o 18 2 1 27.10 19.26 114.66 o 20 2 1 21.43 225.02 263.95 o 22 2 1 76.66 111.93 98.93 o 24 2 1 10.96 3.18 117.54 o -23 3 1 21.77 -16.42 75.67 o -21 3 1 81.44 -88.77 97.08 o -19 3 1 3.35 125.95 124.80 o -17 3 1 3.48 85.06 70.37 o -15 3 1 224.52 211.30 384.72 o -13 3 1 139.39 13.10 111.65 o -11 3 1 526.16 489.73 190.12 o -9 3 1 247.99 155.06 131.39 o -7 3 1 969.40 1035.39 144.77 o -5 3 1 1097.69 924.99 152.16 o -3 3 1 82.11 58.40 38.36 o -1 3 1 2.30 33.87 30.33 o 1 3 1 530.79 577.75 74.99 o 3 3 1 3206.54 3161.32 185.47 o 5 3 1 950.80 1022.17 135.74 o 7 3 1 519.21 389.96 93.34 o 9 3 1 719.16 679.95 268.56 o 11 3 1 110.57 51.66 78.94 o 13 3 1 298.32 482.24 233.82 o 15 3 1 52.75 159.56 128.20 o 17 3 1 313.62 337.41 182.46 o 19 3 1 68.39 268.12 239.65 o 21 3 1 48.10 -194.95 245.31 o 23 3 1 6.52 136.81 168.87 o -22 4 1 10.51 111.73 121.24 o -20 4 1 37.27 138.48 176.14 o -18 4 1 11.56 86.68 97.04 o -16 4 1 0.37 12.21 132.00 o -14 4 1 1.49 237.84 144.97 o -12 4 1 305.44 442.75 166.82 o -10 4 1 695.40 1165.25 240.69 o -8 4 1 1005.39 954.18 182.00 o -6 4 1 650.45 592.47 105.37 o -4 4 1 257.77 291.16 85.05 o -2 4 1 295.76 294.58 79.17 o 0 4 1 1761.96 1859.83 138.79 o 2 4 1 2827.79 3079.19 171.82 o 4 4 1 51.55 86.72 47.99 o 6 4 1 172.31 327.20 98.09 o 8 4 1 533.43 586.65 165.91 o 10 4 1 56.44 199.80 120.10 o 12 4 1 9.59 -30.45 195.94 o 14 4 1 232.54 461.32 274.71 o 16 4 1 32.18 -80.62 138.47 o 18 4 1 13.26 -62.16 104.24 o 20 4 1 27.01 -35.13 155.28 o 22 4 1 10.91 -37.16 238.68 o -19 5 1 2.85 47.71 242.76 o -17 5 1 0.70 54.20 118.04 o -15 5 1 8.79 -186.12 186.12 o -13 5 1 201.44 267.63 184.07 o -11 5 1 124.79 177.77 187.30 o -9 5 1 338.98 439.28 242.57 o -7 5 1 203.38 247.56 132.76 o -5 5 1 71.98 187.33 92.57 o -3 5 1 364.63 326.03 115.71 o -1 5 1 342.47 400.01 123.00 o 1 5 1 399.48 276.85 188.96 o 3 5 1 173.26 122.26 100.57 o 5 5 1 58.64 71.93 74.94 o 7 5 1 136.29 184.06 192.36 o 9 5 1 77.03 113.93 90.41 o 11 5 1 27.91 -50.20 61.71 o 13 5 1 6.10 -228.70 228.70 o 15 5 1 7.11 100.46 132.17 o 17 5 1 2.40 103.16 94.84 o -14 6 1 1.83 63.11 143.20 o -12 6 1 47.20 -206.43 206.43 o -10 6 1 59.84 -47.14 105.90 o -8 6 1 91.91 231.19 308.53 o -6 6 1 41.04 61.19 118.49 o -4 6 1 2.26 55.84 131.58 o -2 6 1 30.51 -8.89 89.66 o 0 6 1 58.01 20.17 131.87 o 2 6 1 83.71 59.62 126.54 o 4 6 1 3.63 110.00 102.69 o 6 6 1 20.30 190.41 174.88 o 8 6 1 149.73 85.15 80.16 o 10 6 1 19.37 -48.45 232.37 o 12 6 1 37.86 186.23 236.94 o 14 6 1 16.09 132.16 86.43 o -3 7 1 5.63 420.15 316.54 o -1 7 1 2.33 40.16 228.36 o 1 7 1 24.35 415.23 269.47 o 3 7 1 12.07 -359.78 359.78 o -1 -7 2 32.03 455.74 392.46 o 1 -7 2 15.64 96.21 426.36 o 3 -7 2 18.55 61.00 176.35 o -14 -6 2 16.92 -105.68 334.62 o -12 -6 2 13.28 -98.01 450.11 o -10 -6 2 58.03 -152.14 320.98 o -8 -6 2 20.50 -130.49 353.51 o -6 -6 2 22.73 65.56 397.75 o -4 -6 2 41.22 -119.55 138.91 o -2 -6 2 43.82 -76.83 176.43 o 0 -6 2 144.06 373.34 670.80 o 2 -6 2 35.18 -44.19 196.12 o 4 -6 2 16.32 -123.70 123.70 o 6 -6 2 40.81 86.05 253.99 o 8 -6 2 101.68 290.00 251.66 o 10 -6 2 1.05 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