data_2020059 _cell_angle_alpha 90.000 _cell_angle_beta 93.277 _cell_angle_gamma 90.000 _cell_length_a 10.3340 _cell_length_b 15.9714 _cell_length_c 25.3074 _exptl_crystal_F_000 1984.00 _reflns_d_resolution_high 0.8000 _cod_data_source_file yo3011Isup2.hkl _cod_data_source_block I _shelx_title ' mo_ti47_0m in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 398.26 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 45.29 565.19 33.08 o 4 0 0 22383.11 20296.56 487.33 o 6 0 0 599.18 639.28 76.94 o 8 0 0 52199.94 51625.71 770.45 o 10 0 0 1803.93 1396.70 116.27 o 12 0 0 11367.80 11981.70 286.20 o 1 1 0 81642.89 74576.50 762.91 o 2 1 0 2328.60 1577.65 22.77 o 3 1 0 17028.15 20310.20 165.28 o 4 1 0 410.79 823.84 26.62 o 5 1 0 14055.47 15334.99 165.73 o 6 1 0 4626.14 4108.37 76.61 o 7 1 0 3401.51 3773.01 78.01 o 8 1 0 1843.76 1341.11 49.34 o 9 1 0 7717.36 8547.34 152.74 o 10 1 0 3264.88 3235.16 100.78 o 11 1 0 16872.60 17355.88 258.84 o 12 1 0 218.50 357.56 57.07 o 0 2 0 61720.83 52292.49 633.11 o 1 2 0 32310.09 14025.82 115.13 o 2 2 0 84876.67 101967.93 663.10 o 3 2 0 315.93 128.24 14.14 o 4 2 0 5850.18 6543.74 99.40 o 5 2 0 291.38 392.58 25.83 o 6 2 0 43674.95 43781.29 470.46 o 7 2 0 363.83 684.19 47.09 o 8 2 0 29.34 32.73 36.34 o 9 2 0 3881.02 2948.92 92.88 o 10 2 0 10614.54 10431.06 178.81 o 11 2 0 732.51 691.86 62.74 o 12 2 0 1031.29 1008.18 80.77 o 1 3 0 90307.23 108177.97 854.50 o 2 3 0 244.20 6115.70 60.55 o 3 3 0 1217.51 2512.57 32.56 o 4 3 0 4113.33 3925.21 78.45 o 5 3 0 10261.68 10000.29 143.40 o 6 3 0 198.23 254.06 42.50 o 7 3 0 22997.94 22705.09 333.68 o 8 3 0 1385.91 887.50 49.94 o 9 3 0 11048.68 10405.31 175.35 o 10 3 0 538.84 618.49 59.61 o 11 3 0 10705.92 11053.95 215.09 o 12 3 0 555.22 513.59 62.62 o 0 4 0 2080.75 192.04 26.56 o 1 4 0 5619.27 8614.33 86.79 o 2 4 0 43473.71 51377.09 341.01 o 3 4 0 13558.76 9474.26 96.86 o 4 4 0 124032.75 130517.29 1109.92 o 5 4 0 989.85 764.92 39.09 o 6 4 0 2.43 51.00 25.55 o 7 4 0 2636.90 2529.87 66.68 o 8 4 0 3749.80 3880.31 86.83 o 9 4 0 2168.39 2116.56 73.10 o 10 4 0 4321.51 5115.34 156.00 o 11 4 0 1516.72 1204.02 73.31 o 12 4 0 6537.55 6145.27 176.29 o 1 5 0 34291.46 46631.97 510.81 o 2 5 0 11526.21 7358.49 79.95 o 3 5 0 5845.69 6845.54 82.50 o 4 5 0 285.19 5.85 18.53 o 5 5 0 33380.22 35157.09 463.96 o 6 5 0 760.70 559.95 30.72 o 7 5 0 8641.69 8221.08 121.62 o 8 5 0 614.36 1134.86 52.28 o 9 5 0 14966.67 13109.10 205.28 o 10 5 0 44.80 -9.77 90.55 o 11 5 0 523.22 290.72 55.00 o 12 5 0 1241.18 1287.50 101.20 o 0 6 0 2778.63 2276.86 61.09 o 1 6 0 8163.65 13919.30 169.29 o 2 6 0 82918.30 77873.24 675.85 o 3 6 0 7678.22 5730.74 65.76 o 4 6 0 2705.74 3960.41 68.12 o 5 6 0 23330.88 18206.94 199.81 o 6 6 0 25030.31 24485.58 326.87 o 7 6 0 8540.67 7522.51 119.05 o 8 6 0 148.76 299.00 46.30 o 9 6 0 31.39 69.33 44.55 o 10 6 0 3411.49 3728.69 151.17 o 11 6 0 493.73 478.08 58.21 o 12 6 0 239.34 250.18 70.52 o 1 7 0 5649.64 6155.31 58.75 o 2 7 0 15918.39 12295.09 125.42 o 3 7 0 66935.55 71615.69 559.75 o 4 7 0 3213.40 3003.58 63.28 o 5 7 0 7389.63 7283.65 95.89 o 6 7 0 720.53 584.77 54.24 o 7 7 0 12948.67 12964.30 196.44 o 8 7 0 462.19 700.51 55.91 o 9 7 0 6005.75 6586.11 137.56 o 10 7 0 166.50 144.43 47.76 o 11 7 0 11459.03 11038.90 211.36 o 12 7 0 120.93 0.68 77.05 o 0 8 0 73050.91 77260.66 922.83 o 1 8 0 6897.48 7016.46 70.17 o 2 8 0 23212.04 25589.18 219.26 o 3 8 0 21954.86 25951.84 252.14 o 4 8 0 2008.04 1765.20 67.38 o 5 8 0 1859.31 1763.92 52.37 o 6 8 0 12432.74 13940.59 179.57 o 7 8 0 2837.46 3237.10 92.85 o 8 8 0 10075.80 10177.00 157.11 o 9 8 0 2903.58 2621.29 126.00 o 10 8 0 1192.29 939.56 66.77 o 11 8 0 787.01 1051.10 96.62 o 1 9 0 8942.82 8107.17 86.79 o 2 9 0 1835.63 1349.92 42.71 o 3 9 0 20101.53 22295.79 224.87 o 4 9 0 1435.02 1097.82 36.01 o 5 9 0 15013.24 15435.37 187.57 o 6 9 0 1.06 -2.99 34.14 o 7 9 0 2016.02 2035.59 99.40 o 8 9 0 168.55 117.58 46.84 o 9 9 0 10201.60 11094.20 188.77 o 10 9 0 204.27 419.62 78.97 o 11 9 0 6141.48 6642.96 191.51 o 0 10 0 25821.23 28716.43 386.41 o 1 10 0 9686.33 7381.86 105.54 o 2 10 0 14127.92 15668.77 151.03 o 3 10 0 252.96 550.15 35.19 o 4 10 0 23490.87 23362.68 221.08 o 5 10 0 612.96 1371.54 57.07 o 6 10 0 1674.94 1715.82 100.10 o 7 10 0 769.40 859.48 61.36 o 8 10 0 7217.90 6802.47 140.42 o 9 10 0 4324.66 4197.46 114.19 o 10 10 0 3005.85 2702.70 130.32 o 11 10 0 2352.63 1985.54 121.76 o 1 11 0 10476.17 9452.45 120.88 o 2 11 0 3010.99 2274.36 95.52 o 3 11 0 3046.47 2976.45 62.37 o 4 11 0 1660.29 1609.76 48.44 o 5 11 0 880.53 1084.48 55.99 o 6 11 0 418.01 387.72 47.83 o 7 11 0 11003.49 11176.11 185.91 o 8 11 0 502.04 387.62 51.55 o 9 11 0 1243.30 1303.06 102.56 o 10 11 0 1.95 0.30 74.51 o 0 12 0 3868.72 3978.42 109.99 o 1 12 0 1377.27 1438.28 54.72 o 2 12 0 20580.24 19340.16 176.58 o 3 12 0 2368.27 2031.41 61.73 o 4 12 0 9926.00 11032.39 173.44 o 5 12 0 1189.74 1400.63 63.33 o 6 12 0 6914.90 6363.94 119.60 o 7 12 0 71.50 58.68 45.42 o 8 12 0 1493.85 1352.25 72.15 o 9 12 0 360.65 472.13 84.69 o 10 12 0 7917.01 7925.60 262.66 o 1 13 0 7508.72 8337.02 119.96 o 2 13 0 36.18 46.07 34.55 o 3 13 0 5054.95 4425.20 80.31 o 4 13 0 3.63 5.86 42.42 o 5 13 0 10785.73 10087.68 147.30 o 6 13 0 1928.83 1843.54 72.69 o 7 13 0 9190.67 9552.94 161.77 o 8 13 0 734.07 691.02 88.41 o 9 13 0 2419.48 2029.31 196.40 o 0 14 0 22621.06 20476.33 317.48 o 1 14 0 1629.15 1736.09 88.40 o 2 14 0 1533.13 1598.99 62.37 o 3 14 0 9.23 111.88 39.21 o 4 14 0 16685.12 16971.63 217.36 o 5 14 0 3194.20 3047.60 93.54 o 6 14 0 4136.38 4207.79 101.18 o 7 14 0 612.65 587.21 78.08 o 8 14 0 4385.51 4308.44 159.35 o 9 14 0 3.17 55.47 78.51 o 1 15 0 5476.11 5410.01 103.84 o 2 15 0 272.85 228.81 44.01 o 3 15 0 4334.48 4968.95 101.38 o 4 15 0 256.35 405.79 48.48 o 5 15 0 7226.89 6790.45 119.30 o 6 15 0 294.12 347.98 47.74 o 7 15 0 1714.58 1491.51 102.32 o 8 15 0 385.97 451.47 87.83 o 0 16 0 3908.64 4108.41 137.89 o 1 16 0 40.88 129.41 44.42 o 2 16 0 11412.59 10665.27 152.57 o 3 16 0 1.41 47.62 44.81 o 4 16 0 2153.70 1773.44 71.70 o 5 16 0 310.72 352.99 51.85 o 6 16 0 13304.42 13215.55 206.71 o 7 16 0 0.88 2.72 66.00 o 1 17 0 6922.49 6650.76 168.17 o 2 17 0 246.27 274.86 48.73 o 3 17 0 6104.55 6218.80 117.61 o 4 17 0 22.78 -55.98 55.98 o 5 17 0 5881.22 5991.19 141.86 o 6 17 0 1.14 -53.46 59.13 o 0 18 0 12831.38 13720.88 333.68 o 1 18 0 104.17 187.20 51.54 o 2 18 0 2031.58 2027.76 92.10 o 3 18 0 1348.51 1434.32 84.31 o 4 18 0 4355.78 4233.20 129.06 o 5 18 0 1133.92 851.42 78.90 o 1 19 0 4700.06 4661.61 152.30 o 2 19 0 10.43 171.67 61.06 o 3 19 0 2540.27 2306.81 127.11 o -11 0 1 1017.47 1427.40 184.87 o -9 0 1 145.55 513.78 70.34 o -7 0 1 7613.11 8004.47 129.55 o -5 0 1 8390.67 7365.95 218.49 o -3 0 1 12281.83 17700.04 287.55 o -1 0 1 13727.77 8563.92 219.17 o 1 0 1 7509.99 2657.06 42.50 o 3 0 1 6630.63 9486.35 124.85 o 5 0 1 1170.03 1096.50 65.58 o 7 0 1 3237.64 3960.47 216.63 o 9 0 1 1745.14 1397.70 98.10 o 11 0 1 3.72 -18.10 71.70 o -12 1 1 687.10 865.63 123.19 o -11 1 1 1077.52 1046.67 85.35 o -10 1 1 380.43 509.84 53.22 o -9 1 1 285.63 324.15 47.21 o -8 1 1 4664.48 4972.08 80.84 o -7 1 1 6013.64 5126.09 105.41 o -6 1 1 85.08 92.90 24.83 o -5 1 1 169.86 97.96 17.57 o -4 1 1 35.17 210.14 17.72 o -3 1 1 8801.74 7960.65 81.06 o -2 1 1 8089.92 14338.00 120.34 o -1 1 1 12862.78 2690.81 25.04 o 1 1 1 1002.83 219.97 7.46 o 2 1 1 12070.68 15472.11 129.09 o 3 1 1 280.04 719.27 21.35 o 4 1 1 4.44 42.97 21.13 o 5 1 1 6416.50 6519.60 101.10 o 6 1 1 903.88 929.47 42.39 o 7 1 1 478.96 656.26 55.06 o 8 1 1 1306.60 1208.14 61.08 o 9 1 1 483.49 821.29 58.51 o 10 1 1 276.14 58.23 48.03 o 11 1 1 1282.07 1565.32 92.84 o 12 1 1 1932.34 2131.77 94.42 o -12 2 1 604.88 678.68 156.38 o -11 2 1 663.50 668.38 69.28 o -10 2 1 58.01 473.46 47.52 o -9 2 1 1275.79 1185.88 76.07 o -8 2 1 3203.18 3706.21 68.59 o -7 2 1 235.64 307.28 32.01 o -6 2 1 4118.50 3729.68 64.83 o -5 2 1 3556.33 3921.15 56.96 o -4 2 1 6164.59 4661.96 59.40 o -3 2 1 1736.01 2519.75 36.22 o -2 2 1 134.31 10.19 8.25 o -1 2 1 37855.18 29891.81 214.48 o 0 2 1 4256.30 415.52 8.81 o 1 2 1 5425.70 7026.57 58.76 o 2 2 1 10788.37 5455.73 50.13 o 3 2 1 4681.98 4175.68 47.44 o 4 2 1 12788.47 10770.95 148.65 o 5 2 1 10066.58 11368.69 171.31 o 6 2 1 889.25 572.64 40.16 o 7 2 1 76.24 66.02 33.76 o 8 2 1 1311.35 1686.20 70.88 o 9 2 1 305.83 414.18 50.61 o 10 2 1 2061.67 1865.19 83.60 o 11 2 1 390.89 320.30 58.25 o 12 2 1 272.00 276.30 61.01 o -12 3 1 898.88 1141.24 89.03 o -11 3 1 1655.69 1515.11 83.07 o -10 3 1 106.74 76.90 41.07 o -9 3 1 297.53 280.58 51.74 o -8 3 1 3130.30 3679.57 84.03 o -7 3 1 282.21 202.97 27.76 o -6 3 1 1582.40 1707.10 54.12 o -5 3 1 318.70 627.34 28.11 o -4 3 1 3489.49 3731.18 49.30 o -3 3 1 37563.34 35014.93 274.10 o -2 3 1 3743.55 8441.27 65.97 o -1 3 1 102032.67 86999.81 608.71 o 0 3 1 8685.24 3789.76 33.86 o 1 3 1 22655.80 39188.57 289.14 o 2 3 1 26446.14 26319.85 195.78 o 3 3 1 10296.08 18152.73 150.67 o 4 3 1 1593.01 1135.63 37.54 o 5 3 1 63.95 61.45 23.61 o 6 3 1 1254.35 931.90 53.10 o 7 3 1 2660.64 2399.48 75.80 o 8 3 1 120.97 140.80 40.71 o 9 3 1 3185.98 2746.50 92.91 o 10 3 1 1377.31 949.99 67.10 o 11 3 1 405.87 423.85 69.06 o 12 3 1 179.57 316.93 61.54 o -12 4 1 116.16 204.15 70.13 o -11 4 1 171.87 309.84 51.36 o -10 4 1 147.83 202.57 60.13 o -9 4 1 890.81 1149.55 56.83 o -8 4 1 362.84 402.98 40.06 o -7 4 1 1695.77 2097.00 54.52 o -6 4 1 855.44 1221.31 43.49 o -5 4 1 7857.75 6803.71 83.57 o -4 4 1 12625.87 15758.55 146.30 o -3 4 1 1048.41 533.56 23.19 o -2 4 1 6242.67 9495.05 96.90 o -1 4 1 639.00 2141.81 29.05 o 0 4 1 189.05 121.42 10.21 o 1 4 1 2835.20 971.86 25.81 o 2 4 1 20847.08 21424.86 161.11 o 3 4 1 1590.10 3025.39 40.34 o 4 4 1 6.06 276.04 28.02 o 5 4 1 6469.66 5131.75 75.72 o 6 4 1 79.23 14.36 24.15 o 7 4 1 1286.22 1089.54 63.39 o 8 4 1 3691.22 3800.88 86.14 o 9 4 1 24.09 7.67 37.41 o 10 4 1 835.07 820.62 66.32 o 11 4 1 635.25 765.46 70.71 o 12 4 1 52.20 22.00 56.73 o -12 5 1 0.65 45.45 73.28 o -11 5 1 0.71 -61.22 61.22 o -10 5 1 102.34 30.29 44.19 o -9 5 1 741.63 1057.89 61.32 o -8 5 1 703.40 1046.32 50.50 o -7 5 1 1338.91 952.11 39.41 o -6 5 1 7888.50 8173.90 104.32 o -5 5 1 1647.24 1805.68 41.25 o -4 5 1 14198.44 10595.76 123.88 o -3 5 1 4133.67 1707.48 33.86 o -2 5 1 21082.41 23798.64 216.54 o -1 5 1 225.81 285.69 14.99 o 0 5 1 3906.24 5678.28 48.95 o 1 5 1 11513.10 13190.54 131.30 o 2 5 1 1507.25 2989.32 41.96 o 3 5 1 68.25 403.48 25.12 o 4 5 1 1974.86 2408.10 49.64 o 5 5 1 176.31 300.31 31.08 o 6 5 1 8756.59 7375.11 142.05 o 7 5 1 568.98 287.48 32.33 o 8 5 1 1404.34 1604.05 59.06 o 9 5 1 594.64 517.11 55.01 o 10 5 1 1156.24 1239.30 74.94 o 11 5 1 175.05 134.98 59.08 o 12 5 1 930.82 612.00 79.86 o -12 6 1 696.98 893.56 191.65 o -11 6 1 74.83 -0.87 66.23 o -10 6 1 4896.11 4509.36 110.40 o -9 6 1 9.29 3.04 41.41 o -8 6 1 2006.46 1826.52 59.83 o -7 6 1 668.85 517.28 31.62 o -6 6 1 62.35 537.81 35.16 o -5 6 1 64.35 276.45 26.65 o -4 6 1 20.65 600.29 29.09 o -3 6 1 8153.69 6513.85 67.98 o -2 6 1 2018.76 3068.32 47.29 o -1 6 1 5238.68 6450.50 73.81 o 0 6 1 7878.74 4555.89 50.78 o 1 6 1 77.25 130.65 16.53 o 2 6 1 42416.52 39555.18 367.25 o 3 6 1 3596.52 1980.16 71.32 o 4 6 1 729.01 2059.79 51.45 o 5 6 1 250.67 426.65 31.77 o 6 6 1 722.68 523.83 42.48 o 7 6 1 880.54 900.13 55.40 o 8 6 1 3017.89 3508.91 99.53 o 9 6 1 97.53 130.72 48.47 o 10 6 1 359.33 348.32 55.85 o 11 6 1 1.42 -21.82 48.94 o 12 6 1 831.81 641.95 92.28 o -12 7 1 142.26 200.50 69.38 o -11 7 1 9.83 23.27 68.83 o -10 7 1 6.42 71.71 63.63 o -9 7 1 99.53 188.31 44.27 o -8 7 1 2933.59 3550.85 95.68 o -7 7 1 4999.39 4271.52 105.72 o -6 7 1 86.71 162.74 28.54 o -5 7 1 1.28 -18.07 24.94 o -4 7 1 930.41 1041.38 29.89 o -3 7 1 2471.59 3039.56 47.81 o -2 7 1 48.97 115.08 18.74 o -1 7 1 3938.93 2455.36 36.72 o 0 7 1 530.59 882.15 35.62 o 1 7 1 2195.21 1619.06 32.33 o 2 7 1 419.60 181.78 19.96 o 3 7 1 695.28 2892.79 57.17 o 4 7 1 8703.31 8170.26 105.72 o 5 7 1 3341.94 3750.44 81.00 o 6 7 1 7335.46 6497.91 121.90 o 7 7 1 4904.01 5122.40 101.90 o 8 7 1 15733.14 15870.07 212.48 o 9 7 1 175.84 187.84 45.60 o 10 7 1 389.83 433.79 59.67 o 11 7 1 1.92 140.59 55.49 o 12 7 1 650.77 619.31 92.89 o -11 8 1 2292.06 2676.03 169.23 o -10 8 1 2285.85 2648.79 109.92 o -9 8 1 234.97 425.93 49.09 o -8 8 1 6840.54 7181.95 124.67 o -7 8 1 315.37 424.85 56.04 o -6 8 1 1571.82 1569.95 49.07 o -5 8 1 266.60 430.63 31.44 o -4 8 1 1952.85 2334.16 46.69 o -3 8 1 2166.68 3523.24 56.05 o -2 8 1 1004.75 771.63 30.12 o -1 8 1 1663.08 1060.32 25.64 o 0 8 1 3311.21 4140.24 61.58 o 1 8 1 16895.56 18153.74 162.68 o 2 8 1 817.73 795.94 40.05 o 3 8 1 406.54 513.57 36.78 o 4 8 1 1151.14 1293.72 49.88 o 5 8 1 802.26 862.32 48.17 o 6 8 1 297.91 261.95 41.85 o 7 8 1 0.12 -37.75 37.75 o 8 8 1 183.46 209.22 48.21 o 9 8 1 987.79 1163.95 72.69 o 10 8 1 237.50 505.22 65.91 o 11 8 1 355.45 612.52 65.49 o -11 9 1 6.12 115.44 74.55 o -10 9 1 68.30 171.36 92.84 o -9 9 1 1577.46 1592.17 114.22 o -8 9 1 22.87 46.10 38.62 o -7 9 1 573.31 442.73 48.25 o -6 9 1 143.11 192.60 38.07 o -5 9 1 21.77 5.55 25.14 o -4 9 1 114.42 302.35 24.74 o -3 9 1 145.60 511.57 31.18 o -2 9 1 466.26 367.55 25.00 o -1 9 1 2840.01 2368.45 43.32 o 0 9 1 370.77 193.96 23.82 o 1 9 1 3224.83 3482.84 53.68 o 2 9 1 9882.49 11730.76 118.89 o 3 9 1 104.84 149.94 29.27 o 4 9 1 1404.99 1744.71 58.92 o 5 9 1 566.66 368.50 38.21 o 6 9 1 1346.69 1494.96 67.61 o 7 9 1 1741.23 1798.92 77.80 o 8 9 1 16.88 8.73 45.94 o 9 9 1 521.15 753.90 65.86 o 10 9 1 1990.38 1893.73 122.67 o 11 9 1 44.60 188.47 77.91 o -11 10 1 776.57 930.93 97.74 o -10 10 1 12.66 409.86 79.74 o -9 10 1 385.81 285.71 74.57 o -8 10 1 130.42 130.45 41.14 o -7 10 1 6608.35 6627.62 120.61 o -6 10 1 197.95 101.06 37.50 o -5 10 1 2356.02 1886.91 90.84 o -4 10 1 7443.55 5897.65 86.21 o -3 10 1 10381.73 11140.71 127.67 o -2 10 1 1858.19 1871.61 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