#------------------------------------------------------------------------------ #$Date: 2016-04-06 16:40:35 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181870 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/00/2020086.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2020086 _cell_angle_alpha 89.659 _cell_angle_beta 79.993 _cell_angle_gamma 76.920 _cell_length_a 8.9219 _cell_length_b 12.4145 _cell_length_c 15.5650 _exptl_crystal_F_000 700.00 _reflns_d_resolution_high 0.6715 _cod_data_source_file ky30861.2THFsup2.hkl _cod_data_source_block 1.2THF #BEGIN Tags that were not found in dictionaries: _shelx_title ' 4943 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 192.50 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 3670.61 4415.26 63.49 o 2 0 0 4009.87 4073.61 49.40 o 3 0 0 1788.23 1812.03 32.01 o 4 0 0 3984.33 4025.65 62.86 o 5 0 0 10.95 -5.24 5.49 o 6 0 0 1698.66 1618.66 37.73 o 7 0 0 472.44 452.24 23.48 o 8 0 0 80.34 79.93 14.67 o 9 0 0 395.88 386.89 32.44 o 10 0 0 942.15 985.90 80.95 o 11 0 0 625.05 560.28 51.59 o 12 0 0 84.79 65.32 81.60 o -12 1 0 115.54 124.53 48.46 o -11 1 0 840.08 806.09 60.94 o -10 1 0 37.57 45.36 21.16 o -9 1 0 353.97 312.82 39.32 o -8 1 0 1702.46 1817.66 50.84 o -7 1 0 568.58 522.65 25.31 o -6 1 0 76.19 89.29 11.39 o -5 1 0 8691.29 8836.07 116.54 o -4 1 0 2801.99 2594.55 41.26 o -3 1 0 2688.57 2967.95 40.05 o -2 1 0 1140.09 1052.04 15.68 o -1 1 0 27539.89 25518.45 419.35 o 1 1 0 1809.20 2062.69 35.72 o 2 1 0 611.83 503.75 12.57 o 3 1 0 5328.93 5416.67 77.04 o 4 1 0 22.05 27.04 6.37 o 5 1 0 3287.77 3214.14 56.12 o 6 1 0 255.13 219.11 15.42 o 7 1 0 22.72 27.26 9.20 o 8 1 0 187.92 208.75 20.23 o 9 1 0 386.68 361.95 27.89 o 10 1 0 214.72 212.70 31.13 o 11 1 0 187.53 207.16 34.61 o 12 1 0 19.98 18.75 24.46 o -12 2 0 189.49 213.70 46.74 o -11 2 0 24.98 16.55 26.87 o -10 2 0 313.72 379.83 40.16 o -9 2 0 1549.17 1606.16 79.51 o -8 2 0 478.60 454.08 31.74 o -7 2 0 183.21 176.89 15.69 o -6 2 0 5951.98 5928.15 93.79 o -5 2 0 2985.43 2950.88 48.27 o -4 2 0 191.64 206.85 13.38 o -3 2 0 6381.93 6867.32 81.67 o -2 2 0 534.32 524.86 14.81 o -1 2 0 49.23 51.35 2.47 o 0 2 0 22276.31 22231.48 303.40 o 1 2 0 9505.64 9482.66 104.16 o 2 2 0 1000.14 1398.86 24.25 o 3 2 0 8.96 18.83 5.68 o 4 2 0 1012.69 914.95 22.72 o 5 2 0 1015.83 998.67 24.07 o 6 2 0 0.01 -0.83 8.18 o 7 2 0 7.78 26.32 10.54 o 8 2 0 29.76 38.35 12.52 o 9 2 0 41.61 51.61 16.22 o 10 2 0 23.66 35.12 25.27 o 11 2 0 24.41 16.78 21.22 o 12 2 0 0.63 2.29 21.88 o -12 3 0 9.12 -24.13 40.22 o -11 3 0 696.46 644.53 127.76 o -10 3 0 370.97 364.70 56.12 o -9 3 0 52.44 40.78 19.49 o -8 3 0 22.19 26.53 16.20 o -7 3 0 1197.55 1215.05 42.63 o -6 3 0 1442.89 1313.69 51.42 o -5 3 0 201.84 199.89 12.20 o -4 3 0 2230.60 2187.62 34.00 o -3 3 0 1503.99 1490.41 22.47 o -2 3 0 831.77 851.95 14.47 o -1 3 0 79.74 110.34 5.76 o 0 3 0 177.36 159.79 10.01 o 1 3 0 58.61 47.84 3.28 o 2 3 0 757.30 637.40 13.39 o 3 3 0 75.04 56.24 7.24 o 4 3 0 140.61 114.99 10.42 o 5 3 0 119.69 85.17 9.62 o 6 3 0 582.99 562.99 33.95 o 7 3 0 235.33 258.74 23.85 o 8 3 0 53.95 66.41 14.42 o 9 3 0 381.48 481.15 31.73 o 10 3 0 988.44 981.28 53.11 o 11 3 0 429.33 473.55 61.38 o 12 3 0 85.29 84.87 29.04 o 13 3 0 272.54 331.83 46.52 o -11 4 0 765.92 871.01 78.39 o -10 4 0 10.14 10.60 23.76 o -9 4 0 1.41 12.84 28.54 o -8 4 0 91.45 76.17 16.89 o -7 4 0 140.76 125.08 17.52 o -6 4 0 859.48 833.41 30.38 o -5 4 0 262.58 246.41 14.78 o -4 4 0 8.51 24.44 5.17 o -3 4 0 107.36 85.38 7.28 o -2 4 0 19.90 17.49 2.94 o -1 4 0 177.10 167.88 6.70 o 0 4 0 129.64 129.04 5.88 o 1 4 0 201.65 185.63 5.20 o 2 4 0 5.16 0.17 3.47 o 3 4 0 32.63 20.87 5.25 o 4 4 0 41.01 86.42 9.65 o 5 4 0 700.91 599.87 26.73 o 6 4 0 129.33 136.48 13.23 o 7 4 0 0.10 -3.05 10.07 o 8 4 0 718.69 759.20 37.47 o 9 4 0 2694.34 2743.04 70.02 o 10 4 0 206.76 227.17 25.62 o 11 4 0 124.75 157.41 24.79 o 12 4 0 9.22 -7.21 21.57 o 13 4 0 231.62 237.49 41.27 o -11 5 0 80.71 88.44 36.57 o -10 5 0 20.03 -0.08 25.86 o -9 5 0 4.85 13.80 20.43 o -8 5 0 31.52 59.75 19.00 o -7 5 0 142.13 172.89 23.21 o -6 5 0 40.09 42.32 15.76 o -5 5 0 373.16 399.03 16.87 o -4 5 0 23.55 16.97 4.42 o -3 5 0 19.09 15.62 3.86 o -2 5 0 537.56 410.87 8.54 o -1 5 0 91.50 192.38 15.78 o 0 5 0 3376.32 3421.58 51.66 o 1 5 0 2107.98 1860.77 27.79 o 2 5 0 640.51 689.95 24.76 o 3 5 0 10.16 5.55 4.76 o 4 5 0 3289.23 3204.97 53.46 o 5 5 0 2261.94 2363.84 50.60 o 6 5 0 691.94 794.76 29.88 o 7 5 0 831.76 824.15 36.12 o 8 5 0 2363.56 2444.82 62.30 o 9 5 0 73.78 109.87 34.28 o 10 5 0 1713.60 1761.79 58.98 o 11 5 0 395.19 406.20 41.30 o 12 5 0 28.89 -6.95 19.10 o 13 5 0 39.52 20.22 61.49 o -11 6 0 57.87 40.22 45.97 o -10 6 0 12.87 24.51 30.26 o -9 6 0 96.72 109.09 30.45 o -8 6 0 15.41 28.24 17.18 o -7 6 0 859.83 826.13 47.15 o -6 6 0 392.89 355.98 29.04 o -5 6 0 0.48 -1.78 7.23 o -4 6 0 7.72 11.77 6.37 o -3 6 0 625.47 565.41 13.95 o -2 6 0 263.21 272.87 9.25 o -1 6 0 2479.97 2325.50 38.91 o 0 6 0 5358.18 5496.87 73.92 o 1 6 0 1560.64 1779.61 30.54 o 2 6 0 462.23 443.10 11.58 o 3 6 0 2739.21 2691.81 44.27 o 4 6 0 4766.11 4855.64 74.69 o 5 6 0 1087.87 1224.99 40.10 o 6 6 0 1028.46 1015.10 31.00 o 7 6 0 351.38 394.40 22.94 o 8 6 0 66.86 62.24 14.61 o 9 6 0 959.52 939.19 45.03 o 10 6 0 1770.59 1715.60 59.46 o 11 6 0 18.99 3.54 16.14 o 12 6 0 3.81 -20.51 20.51 o 13 6 0 651.02 617.55 109.18 o -10 7 0 18.26 34.70 27.80 o -9 7 0 14.72 0.79 24.55 o -8 7 0 956.57 1015.71 57.12 o -7 7 0 819.80 860.45 48.64 o -6 7 0 64.20 60.90 15.74 o -5 7 0 1327.78 1351.70 62.15 o -4 7 0 488.69 481.37 21.01 o -3 7 0 1.59 6.70 4.57 o -2 7 0 1987.05 1790.55 30.11 o -1 7 0 4472.75 4315.28 66.88 o 0 7 0 121.54 124.31 6.59 o 1 7 0 2828.44 2870.92 42.41 o 2 7 0 4868.96 4688.82 57.44 o 3 7 0 2714.76 2620.60 43.66 o 4 7 0 467.26 387.35 29.15 o 5 7 0 3131.81 3101.69 56.10 o 6 7 0 373.99 366.02 22.59 o 7 7 0 25.64 18.56 9.28 o 8 7 0 803.07 849.08 39.92 o 9 7 0 962.62 1013.89 47.22 o 10 7 0 45.86 27.10 15.62 o 11 7 0 807.97 916.96 56.79 o 12 7 0 752.11 816.85 57.10 o -10 8 0 40.96 -16.86 39.08 o -9 8 0 175.68 207.66 30.62 o -8 8 0 128.49 136.54 24.21 o -7 8 0 724.68 671.58 49.84 o -6 8 0 2270.75 2238.91 68.99 o -5 8 0 842.71 926.25 33.14 o -4 8 0 476.72 466.48 23.71 o -3 8 0 2132.97 2076.42 63.53 o -2 8 0 4612.29 4325.37 57.83 o -1 8 0 212.33 196.14 10.32 o 0 8 0 1456.68 1390.34 26.25 o 1 8 0 2455.00 2312.32 33.20 o 2 8 0 1187.33 1198.68 24.08 o 3 8 0 809.42 809.91 20.15 o 4 8 0 2763.14 2815.39 49.55 o 5 8 0 235.50 232.31 15.26 o 6 8 0 7.76 11.12 10.73 o 7 8 0 1161.41 1098.54 50.60 o 8 8 0 208.48 218.17 21.33 o 9 8 0 75.97 72.35 19.52 o 10 8 0 415.49 404.43 37.36 o 11 8 0 205.75 188.39 29.08 o 12 8 0 81.44 75.13 25.78 o -9 9 0 4.16 4.87 20.40 o -8 9 0 447.54 393.68 37.81 o -7 9 0 791.53 752.41 46.91 o -6 9 0 490.82 492.71 35.60 o -5 9 0 519.94 591.37 33.53 o -4 9 0 1045.50 1064.86 61.05 o -3 9 0 2093.23 2001.16 45.89 o -2 9 0 34.20 50.10 7.62 o -1 9 0 1925.17 1912.32 35.03 o 0 9 0 1063.46 913.43 19.32 o 1 9 0 628.36 602.27 13.71 o 2 9 0 2314.97 2428.53 37.72 o 3 9 0 1914.95 1940.35 30.63 o 4 9 0 60.16 61.36 10.24 o 5 9 0 143.44 113.40 13.44 o 6 9 0 530.39 616.57 34.30 o 7 9 0 164.52 216.83 21.07 o 8 9 0 242.23 215.01 27.81 o 9 9 0 6.49 13.04 15.60 o 10 9 0 58.52 63.55 20.65 o 11 9 0 318.30 373.93 38.77 o 12 9 0 159.26 180.11 32.36 o -9 10 0 218.30 216.69 69.53 o -8 10 0 81.88 113.11 26.05 o -7 10 0 44.35 39.20 30.19 o -6 10 0 674.83 681.80 72.93 o -5 10 0 716.81 688.54 35.94 o -4 10 0 38.39 38.88 11.13 o -3 10 0 292.19 323.55 18.45 o -2 10 0 1562.01 1502.01 34.44 o -1 10 0 28.60 27.69 6.31 o 0 10 0 31.74 32.66 6.18 o 1 10 0 349.02 372.56 14.00 o 2 10 0 87.97 108.73 10.99 o 3 10 0 26.37 35.19 8.57 o 4 10 0 1.69 4.27 7.87 o 5 10 0 82.06 74.17 14.27 o 6 10 0 37.38 28.21 17.86 o 7 10 0 640.01 675.87 39.40 o 8 10 0 13.00 3.55 14.76 o 9 10 0 309.53 312.16 35.00 o 10 10 0 43.57 50.57 20.29 o 11 10 0 4.95 -18.76 25.38 o 12 10 0 3.61 17.91 27.02 o -8 11 0 0.27 9.36 41.37 o -7 11 0 19.07 6.96 20.29 o -6 11 0 273.99 257.58 34.35 o -5 11 0 31.29 32.99 25.28 o -4 11 0 2.60 6.33 11.53 o -3 11 0 325.47 307.61 18.36 o -2 11 0 807.70 806.45 23.83 o -1 11 0 1.29 5.76 7.02 o 0 11 0 39.56 50.15 7.50 o 1 11 0 43.71 51.67 8.38 o 2 11 0 1343.13 1311.18 34.29 o 3 11 0 77.33 95.49 13.99 o 4 11 0 893.69 946.06 32.97 o 5 11 0 110.76 61.53 18.28 o 6 11 0 0.44 -3.17 13.69 o 7 11 0 156.55 130.44 22.87 o 8 11 0 692.62 651.07 48.70 o 9 11 0 34.45 73.47 22.67 o 10 11 0 582.98 606.48 52.83 o 11 11 0 369.26 350.24 44.09 o 12 11 0 373.67 280.04 73.94 o -7 12 0 114.88 100.53 28.58 o -6 12 0 49.56 72.51 46.74 o -5 12 0 8.07 3.85 18.25 o -4 12 0 5.41 6.36 12.44 o -3 12 0 101.85 107.78 21.37 o -2 12 0 17.19 10.63 9.52 o -1 12 0 3.45 8.40 8.66 o 0 12 0 121.11 173.14 14.91 o 1 12 0 0.14 -0.53 6.06 o 2 12 0 433.22 414.40 21.15 o 3 12 0 1545.58 1503.20 48.12 o 4 12 0 134.28 117.62 15.49 o 5 12 0 71.87 63.33 16.91 o 6 12 0 1233.55 1201.19 51.41 o 7 12 0 948.68 974.21 54.90 o 8 12 0 34.60 28.63 20.97 o 9 12 0 775.06 871.36 66.33 o 10 12 0 172.93 152.19 45.58 o 11 12 0 85.81 48.31 29.34 o -6 13 0 3.71 25.34 22.02 o -5 13 0 3.23 1.83 18.91 o -4 13 0 414.70 441.30 39.68 o -3 13 0 19.73 26.74 18.58 o -2 13 0 366.81 369.16 26.87 o -1 13 0 12.05 18.86 13.25 o 0 13 0 247.46 252.81 27.26 o 1 13 0 379.04 383.73 40.48 o 2 13 0 1130.31 1075.29 32.31 o 3 13 0 274.63 347.00 23.30 o 4 13 0 755.42 748.12 34.47 o 5 13 0 2143.15 2202.40 69.52 o 6 13 0 323.68 318.17 42.57 o 7 13 0 90.22 84.75 21.40 o 8 13 0 491.68 483.93 44.29 o 9 13 0 157.61 175.77 41.61 o 10 13 0 11.19 24.08 22.62 o 11 13 0 233.83 256.89 51.56 o -6 14 0 169.87 108.86 33.52 o -5 14 0 64.71 55.44 24.10 o -4 14 0 128.70 105.88 24.90 o -3 14 0 1134.54 1106.00 42.82 o -2 14 0 293.84 326.48 39.98 o -1 14 0 65.38 69.12 13.69 o 0 14 0 1680.82 1715.82 49.87 o 1 14 0 493.89 533.85 32.01 o 2 14 0 217.92 191.79 20.41 o 3 14 0 1105.39 1115.95 36.14 o 4 14 0 1298.47 1250.49 47.68 o 5 14 0 495.53 495.19 36.03 o 6 14 0 22.15 14.87 16.50 o 7 14 0 787.66 839.83 53.20 o 8 14 0 881.54 889.81 58.67 o 9 14 0 19.57 22.29 21.38 o 10 14 0 178.66 156.35 33.76 o -4 15 0 654.19 663.90 75.47 o -3 15 0 109.60 195.38 39.84 o -2 15 0 76.04 71.17 27.74 o -1 15 0 667.87 792.70 40.74 o 0 15 0 796.80 844.11 31.28 o 1 15 0 259.27 271.31 23.36 o 2 15 0 463.97 490.20 62.34 o 3 15 0 535.58 530.35 42.63 o 4 15 0 5.25 16.30 17.70 o 5 15 0 307.27 344.73 52.00 o 6 15 0 554.62 547.15 55.78 o 7 15 0 681.16 694.39 42.73 o 8 15 0 24.36 2.45 19.57 o 9 15 0 87.97 80.96 26.94 o -3 16 0 500.66 495.72 62.83 o -2 16 0 421.57 378.50 50.19 o -1 16 0 501.24 532.55 49.99 o 0 16 0 14.50 -4.18 15.54 o 1 16 0 205.76 204.11 22.30 o 2 16 0 457.53 450.87 39.49 o 3 16 0 22.48 29.17 18.54 o 4 16 0 344.18 363.25 46.35 o 5 16 0 993.22 1127.98 99.99 o 6 16 0 82.79 84.96 21.53 o 7 16 0 179.40 212.64 26.88 o 8 16 0 314.17 303.32 38.31 o -2 17 0 130.24 195.38 40.99 o -1 17 0 61.38 60.15 27.20 o 0 17 0 394.56 366.24 49.04 o 1 17 0 241.27 198.06 39.08 o 2 17 0 6.93 9.67 21.45 o 3 17 0 16.29 -6.39 17.08 o 4 17 0 90.65 90.48 25.19 o 5 17 0 87.63 101.78 26.40 o 6 17 0 132.20 171.51 45.21 o 7 17 0 0.41 1.12 20.16 o 1 18 0 67.42 36.39 29.88 o 2 18 0 0.58 -12.64 20.69 o 3 18 0 23.20 11.30 24.90 o 4 18 0 48.60 24.50 23.40 o 5 18 0 218.17 124.71 31.25 o -5 -18 1 292.28 345.35 35.04 o -4 -18 1 565.27 538.46 39.32 o -3 -18 1 358.75 323.71 50.57 o -2 -18 1 5.14 -8.81 23.37 o -1 -18 1 357.15 327.55 47.50 o -7 -17 1 77.81 80.90 24.37 o -6 -17 1 258.59 258.42 32.78 o -5 -17 1 217.69 178.05 27.00 o -4 -17 1 8.22 16.09 27.58 o -3 -17 1 18.33 13.23 18.32 o -2 -17 1 223.43 249.39 42.14 o -1 -17 1 2.85 7.15 27.77 o 0 -17 1 32.63 49.23 19.23 o 1 -17 1 30.52 27.35 14.66 o 2 -17 1 0.83 2.30 22.99 o -8 -16 1 3.67 -1.43 18.69 o -7 -16 1 1.30 7.34 16.00 o -6 -16 1 87.93 125.23 24.04 o -5 -16 1 20.68 26.80 21.80 o -4 -16 1 30.22 14.92 18.91 o -3 -16 1 137.00 144.50 52.68 o -2 -16 1 79.15 103.05 22.75 o -1 -16 1 20.63 49.39 36.39 o 0 -16 1 10.68 8.95 14.07 o 1 -16 1 9.32 7.91 14.17 o 2 -16 1 2.40 -10.05 13.90 o 3 -16 1 113.98 104.97 33.71 o -9 -15 1 0.09 -11.33 19.67 o -8 -15 1 4.71 -8.84 18.29 o -7 -15 1 398.59 405.71 44.07 o -6 -15 1 12.29 9.15 14.16 o -5 -15 1 32.39 21.41 15.73 o -4 -15 1 206.18 197.83 29.11 o -3 -15 1 256.75 236.42 23.76 o -2 -15 1 87.06 99.48 27.57 o -1 -15 1 185.29 178.23 25.44 o 0 -15 1 229.64 225.00 17.21 o 1 -15 1 20.83 33.18 21.45 o 2 -15 1 23.00 6.87 13.90 o 3 -15 1 117.20 147.44 23.92 o 4 -15 1 280.86 359.34 53.63 o 5 -15 1 97.13 145.19 40.61 o -10 -14 1 122.84 115.01 31.85 o -9 -14 1 13.60 5.93 21.90 o -8 -14 1 292.68 274.38 38.00 o -7 -14 1 14.11 5.82 14.57 o -6 -14 1 35.16 60.86 27.62 o -5 -14 1 233.52 201.60 24.23 o -4 -14 1 731.05 695.81 38.41 o -3 -14 1 230.28 263.22 23.89 o -2 -14 1 232.13 238.07 20.86 o -1 -14 1 303.39 306.76 21.83 o 0 -14 1 160.48 163.62 28.27 o 1 -14 1 467.61 471.13 31.80 o 2 -14 1 75.34 57.32 12.92 o 3 -14 1 371.79 417.01 36.88 o 4 -14 1 207.81 243.46 24.15 o 5 -14 1 364.43 353.87 67.42 o 6 -14 1 163.74 126.23 29.66 o -11 -13 1 7.76 2.68 47.12 o -10 -13 1 200.64 242.39 36.50 o -9 -13 1 100.00 85.13 36.95 o -8 -13 1 62.17 68.05 22.65 o -7 -13 1 580.07 566.87 37.70 o -6 -13 1 639.91 646.57 42.83 o -5 -13 1 502.44 462.42 45.24 o -4 -13 1 132.32 203.09 18.90 o -3 -13 1 552.59 515.91 25.45 o -2 -13 1 1184.01 1121.66 37.50 o -1 -13 1 270.41 240.06 17.89 o 0 -13 1 741.24 786.67 27.39 o 1 -13 1 1185.78 1147.78 34.21 o 2 -13 1 130.38 130.57 14.53 o 3 -13 1 332.65 370.02 46.49 o 4 -13 1 503.46 463.40 30.69 o 5 -13 1 106.01 113.55 24.26 o 6 -13 1 3.08 37.51 28.54 o 7 -13 1 408.74 340.57 60.91 o -11 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