#------------------------------------------------------------------------------ #$Date: 2016-04-06 16:41:11 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181871 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/01/2020100.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2020100 _cell_angle_alpha 90 _cell_angle_beta 109.2930(16) _cell_angle_gamma 90 _cell_length_a 14.2245(2) _cell_length_b 14.2802(3) _cell_length_c 14.8887(3) _exptl_crystal_F_000 1104 _reflns_d_resolution_high 0.8367 _cod_data_source_file fa3370IIsup3.hkl _cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 249.01 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x+1/2, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 202.85 232.90 6.17 o 4 0 0 6638.46 6641.52 52.08 o 6 0 0 1832.91 1819.06 33.47 o 8 0 0 704.88 663.54 16.87 o 10 0 0 487.37 452.21 11.22 o 12 0 0 75.25 73.76 6.13 o 14 0 0 3.24 12.16 3.93 o 16 0 0 14.76 25.84 6.53 o 1 1 0 2379.19 2460.28 12.45 o 2 1 0 2961.72 2987.44 24.87 o 3 1 0 1239.69 1137.56 13.17 o 4 1 0 1226.06 1223.60 15.82 o 5 1 0 18.71 12.57 3.60 o 6 1 0 256.87 317.86 9.51 o 7 1 0 4492.14 4388.24 37.32 o 8 1 0 1373.87 1325.01 14.94 o 9 1 0 896.78 782.85 10.18 o 10 1 0 42.03 39.47 3.13 o 11 1 0 3831.55 3869.15 26.16 o 12 1 0 29.30 24.82 3.22 o 13 1 0 20.86 16.44 3.13 o 14 1 0 32.68 38.18 3.69 o 15 1 0 22.41 25.03 3.24 o 16 1 0 27.06 35.72 7.56 o 0 2 0 7215.34 7177.40 68.45 o 1 2 0 4188.49 4003.06 30.50 o 2 2 0 6135.06 6707.41 27.70 o 3 2 0 2453.03 2466.91 17.55 o 4 2 0 1063.89 1093.65 11.42 o 5 2 0 74.57 64.14 3.50 o 6 2 0 259.83 220.68 6.83 o 7 2 0 0.25 3.09 2.81 < 8 2 0 2299.37 2487.60 16.76 o 9 2 0 2.36 6.48 2.12 o 10 2 0 6150.40 6213.74 31.65 o 11 2 0 107.19 88.11 4.15 o 12 2 0 72.16 68.43 3.88 o 13 2 0 67.51 72.66 4.51 o 14 2 0 1401.19 1482.44 19.66 o 15 2 0 46.68 43.65 3.69 o 1 3 0 4204.95 4169.28 30.71 o 2 3 0 371.62 445.39 7.87 o 3 3 0 11670.10 11346.70 44.84 o 4 3 0 730.42 713.66 12.30 o 5 3 0 637.96 653.84 9.28 o 6 3 0 1180.05 1239.64 15.55 o 7 3 0 22.67 24.02 3.42 o 8 3 0 538.07 552.34 7.78 o 9 3 0 22.46 9.17 2.41 o 10 3 0 914.58 952.26 12.61 o 11 3 0 1330.97 1363.16 16.52 o 12 3 0 2161.65 2258.01 18.81 o 13 3 0 42.52 40.03 3.78 o 14 3 0 4.94 4.48 2.87 < 15 3 0 0.76 0.03 2.45 < 0 4 0 18656.50 19080.30 106.68 o 1 4 0 536.81 521.11 12.84 o 2 4 0 1268.77 1263.72 15.71 o 3 4 0 723.42 803.57 11.87 o 4 4 0 508.03 513.12 9.95 o 5 4 0 3219.58 3250.78 23.87 o 6 4 0 491.40 589.25 11.99 o 7 4 0 30.06 33.46 2.61 o 8 4 0 10.77 5.38 1.81 < 9 4 0 96.39 89.01 4.15 o 10 4 0 2246.50 2214.46 21.86 o 11 4 0 253.54 249.69 7.85 o 12 4 0 47.20 48.22 4.36 o 13 4 0 8.79 10.22 2.63 o 14 4 0 82.05 74.71 4.63 o 15 4 0 89.70 102.00 5.28 o 1 5 0 2179.69 2038.68 25.50 o 2 5 0 10.38 15.24 3.40 o 3 5 0 541.15 506.08 9.88 o 4 5 0 1380.81 1364.83 17.79 o 5 5 0 368.18 262.30 9.14 o 6 5 0 176.20 209.79 6.42 o 7 5 0 4088.70 4136.34 23.02 o 8 5 0 485.08 485.35 8.40 o 9 5 0 1623.90 1564.64 15.91 o 10 5 0 0.11 -8.37 3.62 < 11 5 0 1840.78 1945.74 22.29 o 12 5 0 225.90 224.86 7.85 o 13 5 0 981.74 1051.58 13.01 o 14 5 0 2.91 3.43 2.34 < 15 5 0 1.31 3.18 2.28 < 0 6 0 1210.52 997.89 26.18 o 1 6 0 6662.16 7144.01 52.85 o 2 6 0 394.59 469.46 12.05 o 3 6 0 237.52 250.93 9.26 o 4 6 0 66.89 56.45 5.01 o 5 6 0 1874.44 1778.66 24.35 o 6 6 0 1366.45 1356.82 13.73 o 7 6 0 340.91 355.16 7.60 o 8 6 0 2.98 4.42 2.45 < 9 6 0 1243.60 1204.74 16.14 o 10 6 0 519.62 497.77 11.81 o 11 6 0 179.64 169.50 7.38 o 12 6 0 900.42 885.16 15.02 o 13 6 0 6.56 7.87 2.58 o 14 6 0 245.19 224.40 6.10 o 15 6 0 66.17 86.42 9.84 o 1 7 0 6147.55 6208.32 45.49 o 2 7 0 2710.86 2935.79 35.57 o 3 7 0 2301.61 2117.67 27.59 o 4 7 0 393.28 519.97 12.17 o 5 7 0 175.40 188.44 5.34 o 6 7 0 138.20 163.75 5.18 o 7 7 0 679.25 705.33 10.98 o 8 7 0 904.91 865.28 13.39 o 9 7 0 0.04 5.38 3.37 < 10 7 0 108.69 121.98 6.16 o 11 7 0 61.91 67.49 5.22 o 12 7 0 74.72 84.88 5.24 o 13 7 0 13.31 19.72 2.70 o 14 7 0 24.77 20.72 2.33 o 0 8 0 4710.55 4988.57 58.60 o 1 8 0 1022.56 907.74 21.16 o 2 8 0 233.41 292.80 8.08 o 3 8 0 491.98 505.68 8.74 o 4 8 0 104.30 188.94 6.06 o 5 8 0 614.01 704.30 11.21 o 6 8 0 229.47 203.25 6.38 o 7 8 0 597.44 594.58 11.04 o 8 8 0 6.53 1.77 2.61 < 9 8 0 988.03 1011.85 14.40 o 10 8 0 3139.99 3142.02 26.62 o 11 8 0 13.66 11.57 3.33 o 12 8 0 151.64 145.77 6.33 o 13 8 0 185.98 178.98 6.55 o 14 8 0 4.36 -2.20 3.32 < 1 9 0 378.14 409.11 9.73 o 2 9 0 3.65 11.11 2.43 o 3 9 0 317.11 408.08 8.43 o 4 9 0 1156.53 1179.91 15.64 o 5 9 0 1122.64 1108.26 15.85 o 6 9 0 439.71 426.87 10.00 o 7 9 0 2562.89 2757.83 24.45 o 8 9 0 916.82 989.82 15.23 o 9 9 0 3455.68 3544.59 27.44 o 10 9 0 4.32 3.50 3.07 < 11 9 0 139.28 135.77 6.31 o 12 9 0 456.75 474.41 11.68 o 13 9 0 1633.46 1658.08 17.27 o 0 10 0 1800.62 1724.71 31.77 o 1 10 0 13.93 11.48 3.15 o 2 10 0 422.52 440.96 9.45 o 3 10 0 51.16 51.31 3.93 o 4 10 0 1690.76 1677.91 18.98 o 5 10 0 127.59 128.45 5.56 o 6 10 0 0.92 4.22 3.07 < 7 10 0 35.74 29.06 3.73 o 8 10 0 112.74 124.16 6.95 o 9 10 0 101.96 106.83 5.93 o 10 10 0 817.83 789.64 14.01 o 11 10 0 1021.10 1085.61 15.24 o 12 10 0 191.92 178.12 7.02 o 1 11 0 254.60 239.04 8.64 o 2 11 0 1457.94 1434.79 19.74 o 3 11 0 351.55 332.61 9.41 o 4 11 0 2080.93 2139.78 22.83 o 5 11 0 184.93 173.63 6.85 o 6 11 0 858.96 913.72 15.55 o 7 11 0 7.07 5.32 2.94 < 8 11 0 123.83 132.00 6.93 o 9 11 0 9.76 16.07 3.31 o 10 11 0 0.18 4.37 2.36 < 11 11 0 126.15 121.96 5.59 o 12 11 0 149.40 147.15 5.70 o 0 12 0 224.23 247.40 12.58 o 1 12 0 236.20 227.40 8.75 o 2 12 0 26.00 34.07 5.14 o 3 12 0 134.31 156.92 6.98 o 4 12 0 0.24 1.94 3.35 < 5 12 0 302.63 305.26 9.79 o 6 12 0 532.77 545.46 12.52 o 7 12 0 924.72 947.84 15.16 o 8 12 0 6.15 8.53 2.76 o 9 12 0 270.72 286.16 8.22 o 10 12 0 774.11 779.05 11.79 o 11 12 0 74.19 77.11 5.01 o 1 13 0 481.01 499.89 14.38 o 2 13 0 0.63 2.75 3.49 < 3 13 0 481.76 467.25 11.52 o 4 13 0 47.65 46.54 4.46 o 5 13 0 160.59 172.15 7.95 o 6 13 0 64.21 56.86 4.73 o 7 13 0 628.65 685.65 11.67 o 8 13 0 1877.13 1953.02 21.61 o 9 13 0 241.62 251.53 7.46 o 10 13 0 1.07 1.16 3.12 < 0 14 0 3508.20 3742.94 81.07 o 1 14 0 880.88 824.29 20.75 o 2 14 0 477.30 504.52 14.62 o 3 14 0 59.87 58.25 6.17 o 4 14 0 1916.38 1966.17 27.84 o 5 14 0 2.11 0.34 3.22 < 6 14 0 57.15 56.80 3.84 o 7 14 0 190.73 181.56 7.20 o 8 14 0 502.51 501.35 10.70 o 1 15 0 634.75 630.87 22.42 o 2 15 0 473.12 506.58 12.43 o 3 15 0 142.74 160.20 6.70 o 4 15 0 291.20 260.47 8.77 o 5 15 0 2.70 -0.21 3.17 < 6 15 0 372.99 390.34 10.60 o 7 15 0 522.51 521.90 16.52 o 0 16 0 555.87 610.29 28.11 o 1 16 0 0.13 -2.59 4.06 < 2 16 0 193.48 165.51 10.54 o 3 16 0 13.76 9.63 4.35 < 4 16 0 2.14 2.28 3.75 < 1 17 0 902.07 965.97 29.81 o -15 0 1 70.49 64.91 6.55 o -13 0 1 77.80 76.16 6.09 o -11 0 1 3.05 -8.28 3.73 < -9 0 1 795.31 834.50 15.38 o -7 0 1 6989.40 7352.46 70.05 o -5 0 1 4167.42 4053.30 46.78 o -3 0 1 30590.50 31400.20 115.91 o -1 0 1 33805.90 34629.50 76.28 o 1 0 1 14279.80 15043.50 66.59 o 3 0 1 1649.51 2018.09 26.68 o 5 0 1 327.76 392.13 12.61 o 7 0 1 42.84 67.61 9.09 o 9 0 1 1007.47 930.48 14.62 o 11 0 1 470.42 535.38 14.51 o 13 0 1 339.31 345.25 12.71 o 15 0 1 104.95 104.04 5.85 o -16 1 1 19.48 22.36 3.48 o -15 1 1 144.06 147.06 6.94 o -14 1 1 301.18 315.12 8.24 o -13 1 1 964.94 993.89 13.14 o -12 1 1 78.07 81.86 4.28 o -11 1 1 275.66 259.34 6.85 o -10 1 1 595.53 569.79 10.60 o -9 1 1 152.73 175.26 4.91 o -8 1 1 64.68 45.63 3.93 o -7 1 1 1150.83 1166.25 18.88 o -6 1 1 43.94 61.89 4.48 o -5 1 1 1531.30 1582.70 19.59 o -4 1 1 1642.76 1583.32 18.66 o -3 1 1 11504.00 11569.10 38.66 o -2 1 1 3417.02 3350.82 16.71 o -1 1 1 4075.48 3880.48 18.65 o 0 1 1 257.98 243.59 3.80 o 1 1 1 3274.84 3199.44 20.27 o 2 1 1 9.56 16.56 3.44 o 3 1 1 266.66 277.06 10.19 o 4 1 1 68.85 81.09 5.42 o 5 1 1 2.40 6.53 2.95 < 6 1 1 5828.65 5919.82 38.27 o 7 1 1 1024.35 1100.05 15.85 o 8 1 1 2562.75 2574.37 19.58 o 9 1 1 0.13 2.22 2.30 < 10 1 1 515.35 530.60 9.53 o 11 1 1 530.19 577.44 10.39 o 12 1 1 3334.25 3386.09 25.79 o 13 1 1 289.72 289.54 8.24 o 14 1 1 109.31 107.04 4.66 o 15 1 1 42.77 37.41 3.25 o -16 2 1 173.78 190.16 8.40 o -15 2 1 719.61 740.07 12.94 o -14 2 1 51.59 45.27 3.93 o -13 2 1 659.62 643.23 10.62 o -12 2 1 268.91 292.98 7.56 o -11 2 1 5805.54 5897.80 31.70 o -10 2 1 109.28 123.52 4.70 o -9 2 1 82.59 100.13 4.10 o -8 2 1 267.06 267.67 6.50 o -7 2 1 527.49 444.98 11.63 o -6 2 1 2.44 2.35 2.32 < -5 2 1 3412.27 3726.34 21.79 o -4 2 1 62.61 44.43 3.36 o -3 2 1 2317.62 2470.05 18.23 o -2 2 1 1943.22 1836.08 18.03 o -1 2 1 401.82 453.00 7.03 o 0 2 1 387.39 389.33 6.98 o 1 2 1 65083.20 62005.00 153.80 o 2 2 1 155.62 125.92 4.17 o 3 2 1 382.41 411.93 8.52 o 4 2 1 677.20 670.15 10.52 o 5 2 1 8.97 23.81 2.96 o 6 2 1 1050.19 1064.42 15.26 o 7 2 1 1704.28 1853.97 23.12 o 8 2 1 71.22 75.28 3.56 o 9 2 1 7173.19 7065.61 33.57 o 10 2 1 22.12 13.78 2.78 o 11 2 1 859.30 824.25 12.08 o 12 2 1 0.19 0.68 2.72 < 13 2 1 310.54 317.06 7.96 o 14 2 1 130.52 128.08 5.18 o 15 2 1 100.48 96.57 4.65 o -16 3 1 6.04 5.05 2.87 < -15 3 1 119.02 113.22 4.95 o -14 3 1 59.95 62.87 4.68 o -13 3 1 409.92 397.64 9.03 o -12 3 1 856.51 880.50 12.49 o -11 3 1 29.04 33.85 3.38 o -10 3 1 12.96 19.55 2.90 o -9 3 1 597.10 612.25 9.75 o -8 3 1 1574.80 1856.94 15.39 o -7 3 1 27.34 39.98 3.81 o -6 3 1 366.36 444.21 8.85 o -5 3 1 52.33 71.38 4.07 o -4 3 1 3065.49 3115.78 22.32 o -3 3 1 3843.06 3943.44 24.87 o -2 3 1 2345.54 2307.88 20.97 o -1 3 1 647.76 669.55 10.80 o 0 3 1 4296.94 4711.60 37.71 o 1 3 1 4988.13 5325.38 30.62 o 2 3 1 474.71 430.82 8.87 o 3 3 1 5065.73 5392.53 25.96 o 4 3 1 1040.37 1021.00 13.99 o 5 3 1 5170.33 5636.41 31.22 o 6 3 1 48.42 65.87 4.64 o 7 3 1 1684.50 1733.12 17.71 o 8 3 1 494.21 502.69 8.07 o 9 3 1 280.50 310.05 7.43 o 10 3 1 48.91 48.91 4.02 o 11 3 1 13.02 13.68 2.75 o 12 3 1 837.79 886.13 11.02 o 13 3 1 1420.77 1444.52 15.12 o 14 3 1 302.11 278.89 8.46 o 15 3 1 261.58 255.69 7.67 o -15 4 1 81.26 82.14 4.26 o -14 4 1 0.51 -2.58 2.67 < -13 4 1 240.15 250.77 7.32 o -12 4 1 54.14 56.30 4.20 o -11 4 1 3199.79 3263.00 27.49 o -10 4 1 115.44 107.96 5.63 o -9 4 1 251.50 224.71 6.39 o -8 4 1 191.32 230.54 5.16 o -7 4 1 9.81 16.23 2.69 o -6 4 1 488.22 499.58 11.22 o -5 4 1 3397.70 3430.34 26.18 o -4 4 1 371.09 383.93 9.06 o -3 4 1 85.25 103.14 4.74 o -2 4 1 1945.06 1992.02 21.91 o -1 4 1 13294.90 13015.70 53.67 o 0 4 1 62.20 68.67 4.95 o 1 4 1 75.93 68.11 4.09 o 2 4 1 407.32 437.44 9.39 o 3 4 1 1282.66 1240.27 13.15 o 4 4 1 290.42 281.20 7.87 o 5 4 1 390.00 541.76 11.03 o 6 4 1 307.13 389.08 10.16 o 7 4 1 116.72 115.72 3.71 o 8 4 1 245.30 228.40 5.91 o 9 4 1 350.59 352.55 7.76 o 10 4 1 0.75 5.80 2.80 < 11 4 1 214.36 194.76 6.50 o 12 4 1 36.06 40.57 3.22 o 13 4 1 16.33 16.60 2.98 o 14 4 1 1257.21 1278.31 18.85 o 15 4 1 71.96 68.01 4.24 o -15 5 1 8.11 9.36 2.43 o -14 5 1 1183.74 1194.63 13.68 o -13 5 1 124.29 111.83 5.17 o -12 5 1 312.14 310.55 8.69 o -11 5 1 227.83 206.01 7.21 o -10 5 1 3403.09 3327.93 26.90 o -9 5 1 48.67 51.13 3.32 o -8 5 1 672.53 658.02 9.10 o -7 5 1 127.43 104.38 3.96 o -6 5 1 59.57 68.11 6.20 o -5 5 1 1077.18 1264.40 17.62 o -4 5 1 341.59 415.41 8.70 o -3 5 1 1224.71 1442.82 18.81 o -2 5 1 30.63 30.69 4.03 o -1 5 1 3417.43 3505.24 28.33 o 0 5 1 1541.10 1509.50 20.27 o 1 5 1 714.39 666.31 13.32 o 2 5 1 182.85 156.03 6.28 o 3 5 1 245.96 243.69 7.19 o 4 5 1 449.51 400.62 10.11 o 5 5 1 510.11 467.12 10.08 o 6 5 1 4042.58 4151.12 23.07 o 7 5 1 416.11 414.43 7.36 o 8 5 1 54.13 45.65 3.36 o 9 5 1 30.08 26.90 3.08 o 10 5 1 856.96 853.86 14.28 o 11 5 1 266.64 245.68 8.02 o 12 5 1 1175.80 1212.04 14.47 o 13 5 1 48.39 45.99 3.59 o 14 5 1 216.41 207.47 6.85 o 15 5 1 4.16 4.78 4.56 < -15 6 1 352.78 389.88 9.01 o -14 6 1 91.96 91.74 4.70 o -13 6 1 0.35 2.96 2.67 < -12 6 1 700.45 737.69 12.88 o -11 6 1 1345.44 1316.15 17.31 o -10 6 1 313.25 333.53 8.77 o -9 6 1 435.10 443.84 8.49 o -8 6 1 1522.86 1602.66 15.20 o -7 6 1 1981.36 2015.95 15.51 o -6 6 1 2213.98 2227.73 18.35 o -5 6 1 4978.38 5456.89 46.27 o -4 6 1 1250.58 1321.12 17.65 o -3 6 1 997.31 1104.64 15.63 o -2 6 1 10653.30 10991.50 57.94 o -1 6 1 4686.89 4715.44 36.63 o 0 6 1 5073.78 5580.60 39.91 o 1 6 1 1149.50 1127.33 19.11 o 2 6 1 1.89 11.82 4.50 < 3 6 1 11.86 17.62 3.49 o 4 6 1 945.02 921.64 17.62 o 5 6 1 741.10 689.47 11.35 o 6 6 1 19.60 26.50 2.40 o 7 6 1 109.07 100.52 4.17 o 8 6 1 396.58 422.23 7.97 o 9 6 1 2314.55 2380.64 22.92 o 10 6 1 29.25 30.01 3.98 o 11 6 1 1503.04 1447.17 20.51 o 12 6 1 175.00 163.73 6.41 o 13 6 1 731.72 767.45 10.68 o 14 6 1 13.50 15.87 2.66 o -14 7 1 280.34 260.83 6.84 o -13 7 1 146.39 131.20 5.91 o -12 7 1 1275.21 1306.15 18.10 o -11 7 1 124.19 123.85 6.58 o -10 7 1 142.00 143.83 5.69 o -9 7 1 0.60 4.37 2.54 < -8 7 1 14.61 11.63 2.87 o -7 7 1 26.09 28.25 2.84 o -6 7 1 1702.36 1721.85 14.78 o -5 7 1 240.00 334.15 7.80 o -4 7 1 9656.57 9580.16 61.40 o -3 7 1 92.64 50.78 4.68 o -2 7 1 1383.01 1196.88 18.29 o -1 7 1 0.89 4.72 3.72 < 0 7 1 935.81 712.98 17.18 o 1 7 1 3143.63 3427.46 35.77 o 2 7 1 4796.01 4409.35 40.89 o 3 7 1 990.58 941.39 18.82 o 4 7 1 1372.01 1450.22 17.46 o 5 7 1 412.13 420.45 7.69 o 6 7 1 15.83 16.10 2.46 o 7 7 1 1.89 10.06 2.43 o 8 7 1 0.48 4.65 2.70 < 9 7 1 115.92 113.02 5.47 o 10 7 1 68.72 59.41 4.76 o 11 7 1 176.72 191.14 7.36 o 12 7 1 55.54 57.06 4.38 o 13 7 1 28.60 22.00 2.58 o 14 7 1 13.35 8.15 3.36 < -14 8 1 0.98 1.63 1.92 < -13 8 1 184.46 217.05 7.27 o -12 8 1 1230.94 1150.36 16.43 o -11 8 1 3725.22 3676.71 30.05 o -10 8 1 412.44 392.24 9.21 o -9 8 1 9.23 2.78 2.83 < -8 8 1 1.52 7.24 2.78 < -7 8 1 1.63 2.67 2.60 < -6 8 1 777.91 710.39 11.17 o -5 8 1 13.62 13.74 2.56 o -4 8 1 82.72 86.74 3.98 o -3 8 1 2065.94 2451.00 21.95 o -2 8 1 2895.98 2980.70 23.43 o -1 8 1 5490.95 6097.67 45.88 o 0 8 1 23.55 6.13 3.39 < 1 8 1 578.40 603.55 11.59 o 2 8 1 755.69 854.99 13.63 o 3 8 1 728.69 829.72 11.10 o 4 8 1 18.28 35.43 3.26 o 5 8 1 980.05 999.31 12.40 o 6 8 1 2.97 0.49 2.53 < 7 8 1 132.21 128.27 5.25 o 8 8 1 50.28 38.44 3.55 o 9 8 1 2226.63 2341.86 21.75 o 10 8 1 4.39 5.46 3.27 < 11 8 1 184.99 170.29 6.42 o 12 8 1 41.45 44.56 4.35 o 13 8 1 46.20 46.29 3.41 o -13 9 1 485.69 464.40 10.58 o -12 9 1 554.95 622.92 12.71 o -11 9 1 0.72 -4.92 2.89 < -10 9 1 2782.29 2760.86 23.26 o -9 9 1 898.14 924.31 14.49 o -8 9 1 1058.83 1041.14 15.52 o -7 9 1 52.86 48.82 4.29 o -6 9 1 182.82 169.80 6.30 o -5 9 1 28.90 22.10 3.00 o -4 9 1 866.38 885.62 13.68 o -3 9 1 671.79 636.59 10.48 o -2 9 1 6.15 4.68 2.39 < -1 9 1 1804.96 2161.98 20.70 o 0 9 1 299.35 267.32 7.13 o 1 9 1 29.82 32.35 2.83 o 2 9 1 65.90 85.86 3.66 o 3 9 1 54.28 57.70 3.53 o 4 9 1 32.35 35.05 2.90 o 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